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2015 2nd International Symposium on Physics and Technology of Sensors (ISPTS)最新文献

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Detection of acid phosphatase activity using ATP conferred protection of AgNPs against salt induced aggregation 使用ATP检测酸性磷酸酶活性可以保护AgNPs免受盐诱导的聚集
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220106
C. Tagad, S. Sabharwal, R. Aiyer
ATP conferred protection of silver nanoparticles (AgNPs) against salt induced aggregation has been used as a simple, sensitive and cost effective tool for detection of acid phosphatase (ACP) activity. In the absence of the enzymes, unreacted ATP protects AgNPs from salt-induced aggregation. Dephosphorylation of ATP in the presence of the enzyme reduces the protecting action of ATP and thus there is aggregation of AgNPs. Developed sensing tool for the detection of ACP were found to be suitable in the range of 0.6 to 7 units per ml.
ATP对银纳米粒子(AgNPs)抗盐诱导聚集的保护作用已被用作检测酸性磷酸酶(ACP)活性的一种简单、敏感和经济有效的工具。在没有酶的情况下,未反应的ATP保护AgNPs免受盐诱导的聚集。在酶的存在下ATP的去磷酸化降低了ATP的保护作用,因此存在AgNPs的聚集。开发的ACP检测传感工具适用于0.6 ~ 7单位/ ml的范围。
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引用次数: 0
Development of acid phosphate inhibition-based amperometric biosensor for determination of inorganic phosphate 酸性磷酸盐抑制型安培生物传感器测定无机磷酸盐的研制
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220083
Sudha J. Kulkarni, S. Tembe, M. Karve
The present study describes construction of amperometric biosensor for determination of inorganic phosphate (IP) using single enzyme acid phosphatase (ACP). A blend of biopolymers agarose and guar gum was used to immobilize ACP and estimation of inorganic phosphate was carried out electrochemically using substrate L-ascorbic acid-2-phosphate. Enzyme catalyzes substrate hydrolysis and ascorbic acid is formed as a product which shows oxidation peak at +0.08 V. This peak intensity decreases when enzyme electrode is dipped in inorganic phosphate solution prior to monitoring substrate hydrolysis. The response is linear in the range of 1 × 10-6 M to 4 × 10-5 M IP with a detection limit of 5 × 10-7 M. The enzyme sensor was stable over a period of three months with a marginal loss in enzyme activity when stored at 4° C under dry conditions. This single enzyme approach tries to overcome the drawbacks of multi-enzyme system for inorganic phosphate determination yet maintaining sensitivity and selectivity of enzymatic methods. Possible influence of other species coexisting with inorganic phosphate in water samples was investigated. The performance of this single enzyme based biosensor was in good agreement with earlier reports on biosensors for inorganic phosphate determination using multi-enzyme approach.
本研究利用单酶酸性磷酸酶(ACP)构建了测定无机磷酸盐(IP)的安培生物传感器。采用生物聚合物琼脂糖和瓜尔胶的混合物固定ACP,用底物l -抗坏血酸-2-磷酸电化学测定无机磷酸盐。酶催化底物水解,产物为抗坏血酸,在+0.08 V处出现氧化峰。当酶电极在监测底物水解之前浸入无机磷酸盐溶液时,该峰强度降低。在1 × 10-6 M ~ 4 × 10-5 M IP范围内,响应呈线性,检测限为5 × 10-7 M。在4°C干燥条件下,酶传感器在3个月的时间内保持稳定,酶活性略有下降。这种单酶法克服了多酶法测定无机磷酸盐的缺点,同时保持了酶法测定无机磷酸盐的灵敏度和选择性。考察了与无机磷酸盐共存的其他物种对水样的影响。这种基于单酶的生物传感器的性能与先前使用多酶法测定无机磷酸盐的生物传感器的报道很好地一致。
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引用次数: 0
Design simulation and fabrication of 3D electrode for dielectrophoretic chip 介电泳芯片三维电极的设计、仿真与制作
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220110
M. Singha, J. Nagaraju
This paper presents the design, simulation and fabrication of dielectrophoretic chip with integrated nickel 3D electrodes for bioparticle separation. Finite element analysis software COMSOL Multyphysics 4.3 is used to measure the electric field distribution and also the temperature profile inside the microfluidic channel. The temperature rise is found to be 0.5 K. Electric field distribution shows almost uniform electric field on XY plane at different Z axis. Fabrication of 3D nickel electrode is accomplished using electroplating process. 3D sidewall dielectrophoretic chip reduces the electrochemical effect and joule heating effect.
本文介绍了用于生物颗粒分离的集成镍三维电极介电泳芯片的设计、仿真和制作。利用有限元分析软件COMSOL multiphysics 4.3测量了微流控通道内的电场分布和温度分布。发现温升为0.5 K。在不同的Z轴上,电场分布在XY平面上几乎均匀。采用电镀工艺制备了三维镍电极。三维侧壁介电泳芯片降低了电化学效应和焦耳热效应。
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引用次数: 0
Influence of fuel to oxidizer ratio on gas sensing characteristics of ZnFe2O4 nanoparticles 燃料与氧化剂比对ZnFe2O4纳米颗粒气敏特性的影响
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220101
R. Godbole, V. Godbole, P. Rao, P. Alegaokar, S. Bhagwat
Highly porous zinc ferrite (ZnFe2O4) nano-size powders are synthesized by varying fuel to oxidizer ratio. The metal nitrates are used as oxidizers while glycine is used as a fuel. The synthesis of material is carried out using an auto-combustion method. It is observed that the enhancement of magnetization occur with the enhancement of `Fuel to Oxidizer' ratio i.e. Glycine to metal Nitrate (G/N) ratio. The structural, morphological, and magnetic features of samples are studied using XRD, SEM, EDAX, BET and VSM techniques. At the microscopic level, the materials exhibit a formation of spongelike structure containing nano-size particles. The XRD measurements confirm the formation of single phase spinel structure of zinc ferrite (ZnFe2O4). As a case study, the response of materials to ethanol gas is studied. It is observed that higher G/N ratio lead to lowering of gas sensitivity as well as operating temperature. The results are discussed in terms of reactions of surface oxygen with ethanol gas.
采用不同燃料与氧化剂比的方法合成了多孔铁酸锌(ZnFe2O4)纳米粉体。金属硝酸盐用作氧化剂,而甘氨酸用作燃料。材料的合成采用自燃烧法进行。观察到磁化强度随“燃料与氧化剂”比率即甘氨酸与金属硝酸盐(G/N)比率的提高而增强。采用XRD、SEM、EDAX、BET和VSM等技术研究了样品的结构、形貌和磁性特征。在微观水平上,材料表现出含有纳米级颗粒的海绵状结构的形成。XRD测定证实了锌铁氧体(ZnFe2O4)形成了单相尖晶石结构。以乙醇气体为例,研究了材料对乙醇气体的响应。结果表明,G/N比值越高,气敏性越低,工作温度越低。从表面氧与乙醇气体反应的角度对结果进行了讨论。
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引用次数: 0
Ferroelectric and piezoelectric properties of (Ba0.7Ca0.3)(Ti1−xSnx)O3 lead-free ceramics (Ba0.7Ca0.3)(Ti1−xSnx)O3无铅陶瓷的铁电和压电性能
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220071
Bharat G. Baraskar, S. P. Kharat, S. G. Kakade, R. Kambale, Y. D. Kolekar, S. Wada
The ferroelectric and piezoelectric properties of Sn4+ modified (Ba0.7Ca0.3)(Ti1-xSnx)O3, (with x = 0.000 to 0.100 in steps of 0.025) lead free electroceramics were investigated. With Sn4+ substitution, a structural phase transition from pure tetragonal to pseudo-cubic structure has been observed; which strongly influence the ferroelectric/ piezoelectric nature of the samples. At room temperature, all the samples exhibit typical polarization-electric field hysteresis as well as field induced strain butterfly loop which confirms the ferroelectric and piezoelectric nature. As Sn4+ content increases, the ferroelectric properties seems to be suppressed while the piezoelectric properties gets improved up to x = 0.075 and then decreased. Moderately high remanent polarization (Pr) and low coercive field (Ec) were observed for all compositions, which may be essential for storage and switching applications.
研究了Sn4+改性(Ba0.7Ca0.3)(Ti1-xSnx)O3(步骤为0.025,x = 0.000 ~ 0.100)无铅电陶瓷的铁电性能和压电性能。Sn4+取代后,结构相变由纯四方结构转变为伪立方结构;这强烈地影响了样品的铁电/压电性质。在室温下,所有样品都表现出典型的极化电场滞后和场致应变蝴蝶环,证实了铁电性和压电性。随着Sn4+含量的增加,铁电性能似乎受到抑制,而压电性能在x = 0.075范围内得到提高,然后下降。在所有成分中都观察到中等高的剩余极化(Pr)和低的矫顽力场(Ec),这可能是存储和开关应用所必需的。
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引用次数: 0
Development of optical fiber based chlorophyll and anthocyanin coated carbon dioxide biosensor 基于光纤的叶绿素和花青素涂层二氧化碳生物传感器的研制
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220078
Rohan Dhale, Vipul Dhongade, R. Aiyer, K. Kodam
The paper reports the development of low cost, portable and easily operable optical fiber based carbon dioxide biosensor (CO2). The chlorophyll and anthocyanin is used as active clads. Coriander and red leaf amaranth (amaranth) contain photosynthetic pigments viz. chlorophyll and anthocyanin. Developed sensors selectively show CO2 gas concentration dependent response from 1 to 500 ppm that is measured in terms of transmitted intensity through a plastic optical fiber. It is found that chlorophyll shows better response in terms of Sensitivity 1.571%/ppm than anthocyanin 0.667%./ppm. Thickness (Four layers) and clad length (7 mm) optimization is done for better sensitivity. Sensors show negligible response to humidity and methane gas. The sensor can be used when stored at room temperature (250C) up to a maximum of 25 days giving 85 to 90% retention of the response.
本文报道了一种低成本、便携、易操作的光纤二氧化碳生物传感器的研制。叶绿素和花青素被用作活性包层。香菜和红叶苋菜(苋菜)含有光合色素,即叶绿素和花青素。开发的传感器选择性地显示CO2气体浓度依赖于响应,从1到500 ppm,通过塑料光纤的传输强度来测量。叶绿素的敏感性为1.571%/ppm,而花青素的敏感性为0.667% /ppm。厚度(四层)和包层长度(7毫米)优化,以获得更好的灵敏度。传感器对湿度和甲烷气体的反应可以忽略不计。该传感器可在室温(250℃)下储存最多25天,保持85%至90%的响应。
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引用次数: 1
Synthesis and characterization of chemically deposited ZnO nanorods for NO2 gas sensing applications 二氧化氮气敏用化学沉积ZnO纳米棒的合成与表征
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220121
S. Vanalakar, S. Vhanalakar, V. Patil, N. Harale, B. Kale, P. Patil, J. H. Kim
Zinc oxide (ZnO) nanorod arrays were deposited on to the soda-lime glass substrates by wet chemical route using zinc acetate as precursor. The structural and surface morphological properties of the ZnO nanorod arrays (ZNAs) were investigated by X-ray diffraction (XRD), and scanning electron microscopy (SEM) respectively. The XRD pattern revealed wurtzite crystal structures of ZNAs, preferentially orienting in the (002) direction. Depending on the length of nanorod, the intensity of the (002) plane was found to be varied. SEM micrographs show the vertical alignment of ZNAs perpendicular to the substrate and increase in rod length with increase in deposition time. The Gas sensing device was prepared by using ZNAs and tested for NO2 gas at different temperatures, concentrations and size of nanorods. Response increased with gas concentration as well as temperature. It was revealed that ZNAs gas sensor operating at 150 0C temperature could detect NO2 at low concentration (100ppm) with very high sensitivity (90 %).
以醋酸锌为前驱体,采用湿法在钠石灰玻璃衬底上制备氧化锌纳米棒阵列。采用x射线衍射仪(XRD)和扫描电镜(SEM)研究了ZnO纳米棒阵列(ZNAs)的结构和表面形貌。XRD图谱显示ZNAs的纤锌矿晶体结构优先取向于(002)方向。根据纳米棒的长度,发现(002)平面的强度是不同的。SEM显微图显示了垂直于衬底的ZNAs的垂直排列,并且随着沉积时间的增加,棒的长度增加。利用ZNAs制备了气体传感装置,并对不同温度、浓度和纳米棒尺寸下的NO2气体进行了测试。响应随气体浓度和温度的增加而增加。结果表明,在150℃温度下工作的ZNAs气体传感器可以检测低浓度(100ppm)的NO2,灵敏度高达90%。
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引用次数: 0
Design, development and experimental study of novel configuration of retro reflective fiber optic sensor for measuring of surface roughness 表面粗糙度测量用反射式光纤传感器的设计、研制与实验研究
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220097
S. Patil, A. Shaligram
This paper reports a novel retro reflective fiber optic surface roughness sensor. The sensor probe consists of three parallel fibers and one inclined at an angle of 50. The reflector is placed at optimized distance in order to get maximum sensitivity for surface roughness measurement. Mathematical modeling of this fiber optic displacement sensor is reported based on ray tracing method. MS surfaces are sprayed with aluminum to get different surface roughness values which are measured on the standard instrument. Experiments are performed for measuring surface roughness values for these surfaces. Experimental results show good agreement with simulation results. These results are also compared and validated with standard instrument used to measure the surface roughness.
本文报道了一种新型的反射式光纤表面粗糙度传感器。传感器探头由三根平行光纤和一根倾斜成50度角的光纤组成。为了获得最大的表面粗糙度测量灵敏度,反射器被放置在最佳距离上。本文报道了基于光线追踪法的光纤位移传感器的数学建模。在质谱表面喷涂铝以获得不同的表面粗糙度值,这些值在标准仪器上测量。进行了测量这些表面粗糙度值的实验。实验结果与仿真结果吻合较好。这些结果还与用于测量表面粗糙度的标准仪器进行了比较和验证。
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引用次数: 1
Design and electro-thermal analysis of micro hotplates for chemical sensors using standard multi user MEMS process 基于标准多用户MEMS工艺的化学传感器微热板设计与电热分析
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220075
K. G. Girija, Damanjeet Kaur, Vinod Belwanshi, Jyoti Mehta, R. Vatsa, A. Topkar
Micro Hotplates are extensively used in chemical sensor, flow sensor and other micro systems. In this paper, we have presented the design, modeling and simulation results of serpentine, spiral and fan shape micro heaters based on standard Multi User MEMS Process for fabrication in a multi product wafer run. The heater structure was optimized to get good temperature homogeneity, low power consumption and better thermal isolation. Considering the power consumption and temperature homogeneity, spiral type heater with non-uniform width was observed to be the best choice among the three types of heater geometries.
微热板广泛应用于化学传感器、流量传感器和其他微系统。在本文中,我们介绍了基于标准多用户MEMS工艺的蛇形、螺旋形和扇形微加热器的设计、建模和仿真结果。对加热器结构进行了优化,获得了良好的温度均匀性、低功耗和良好的隔热性。考虑到功率消耗和温度均匀性,三种形状的加热器中,宽度不均匀的螺旋型加热器是最佳选择。
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引用次数: 8
Identification of hotspots on FPGA using Time to Digital Converter and distributed tiny sensors 基于时数转换器和分布式微型传感器的FPGA热点识别
Pub Date : 2015-03-07 DOI: 10.1109/ISPTS.2015.7220119
Mahantesh P. Mattada, Sachin Magadum, H. Guhilot
Fully digital time-domain temperature sensors are designed and placed at five different positions within FPGA. Five tiny pulse-generators are used as five temperature sensors. Using manual floor-planning four sensors are placed at four different corners and one at centre. Single 9-bit Time to Digital Converter is utilized for digital output coding. Vernier Time to Digital Converter with 6 picoseconds resolution is presented here. The overall design utilizes 184 logical elements of FPGA i.e. less than 1.5% of the total resources. Implemented temperature sensors give nearly 0.5°C resolution and maximum of ±1.5 LSB nonlinearity is observed over the range.
设计了全数字时域温度传感器,并将其放置在FPGA内的五个不同位置。五个微小的脉冲发生器被用作五个温度传感器。使用手动地板规划四个传感器放置在四个不同的角落和一个在中心。采用单9位时间-数字转换器进行数字输出编码。本文介绍了具有6皮秒分辨率的游标时间到数字转换器。整体设计利用FPGA的184个逻辑元件,即不到总资源的1.5%。实现的温度传感器提供近0.5°C的分辨率和最大±1.5 LSB的非线性在范围内观察到。
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引用次数: 7
期刊
2015 2nd International Symposium on Physics and Technology of Sensors (ISPTS)
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