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Seasonal Variability in Key Radiological Attributes in U-Processing Plant and Solid Waste Disposal Sites at Jaduguda, India 印度Jaduguda铀处理厂和固体废物处理场关键放射属性的季节变化
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-12-02 DOI: 10.1007/s12647-023-00708-z
Dibyendu Rana, V. N. Jha, R. L. Patnaik, M. K. Singh, S. K. Jha, M. S. Kulkarni

Like any other facilities, nuclear facilities are likewise connected with risks to the personnel and environment. The impact assessment of any facility is one of the essential prerequisites for its smooth running. Uranium ore is processed through different stages, such as size reduction, leaching, filtration, product recovery and waste deposition. Different stages of the ore processing can redistribute the activity of radio-nuclides and their measurement is essential for the impact analysis of the facility. Variation in radon and gamma levels is internationally investigated as a marker for seasonality in the natural radiation environment of an area. Accordingly, investigation for both plant and solid waste disposal sites has been carried out for radon (222Rn) and gamma levels to examine the influence on the workers and environment. The radon concentration in the workplace is observed to vary between 20 and 150 Bq m−3, which is within the reference threshold of 300 Bq m−3 suggested in the ICRP recommendation (ICRP 2014). The impacts of the facility on the surrounding environment are indistinguishable from those of the background. Findings suggest that the seasonality of change in radon level is considerable at either site and the gamma level change in the mill is ascribed to the nature and quantity of the source rather than the seasonal influences.

与任何其他设施一样,核设施同样与人员和环境的风险有关。任何设施的影响评估都是其顺利运行的必要先决条件之一。铀矿石经过不同的加工阶段,如粒度还原、浸出、过滤、产品回收和废物沉积。矿石加工的不同阶段可以重新分配放射性核素的活性,其测量对于设施的影响分析至关重要。氡和伽马水平的变化在国际上作为一个地区自然辐射环境季节性的标志进行了调查。因此,对工厂和固体废物处理场进行了氡(222Rn)和伽马水平调查,以检查对工人和环境的影响。观察到工作场所的氡浓度在20至150 Bq m - 3之间变化,这在ICRP建议(ICRP 2014)建议的300 Bq m - 3的参考阈值范围内。设施对周围环境的影响与背景的影响是无法区分的。研究结果表明,在任何一个地点,氡水平变化的季节性都相当可观,而工厂的伽马水平变化归因于源的性质和数量,而不是季节性影响。
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引用次数: 0
Development of Am-241 Activity Standards 制定Am-241活动标准
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-27 DOI: 10.1007/s12647-023-00698-y
Ritu Sharma, D. B. Kulkarni, R. Anuradha, V. Sathian, Probal Choudhury

The identification and monitoring of long-lived alpha-emitting radiotoxic radionuclide in nuclear waste management, environmental monitoring and internal dosimetry are crucial as far as the safety of individual, community and environment is concerned. This requires sample preparation techniques with thin, uniform and adherent deposition of actinides on the substrate for carrying accurate and high-resolution alpha-spectrometric measurements. Electrodeposition is one such technique. Standard sources prepared using this method can be used for calibration of detectors for alpha measurements. In this paper, we discuss the methodology adopted for electroplating Am-241 sources and subsequently carrying the standardization of electroplated sources with 2π-Proportional counter (PC). Efficiency of Am-241 electroplated source in 2πPC was determined to be 49%. The sources were further investigated for alpha-spectrometric measurements leading to the generation of high-resolution spectra exhibiting a full-width at half-maximum (FWHM) value of 38 keV. Scanning electron microscopy (SEM) for surface morphological studies yielded non-clustered deposition, indicating the even distribution of radionuclide and consequently, homogeneity. A tissue wipe test was performed to evaluate the adhesion of radionuclide on substrate. The present study reveals the absence of counts on wiped tissue indicating adherency in deposition.

就个人、社区和环境的安全而言,在核废料管理、环境监测和内部剂量测定中识别和监测长寿命α放射毒性放射性核素是至关重要的。这需要样品制备技术,在衬底上薄、均匀和粘附沉积锕系元素,以进行精确和高分辨率的α光谱测量。电沉积就是这样一种技术。用这种方法制备的标准光源可用于α测量的探测器的校准。本文讨论了用2π-比例计数器(PC)对Am-241源进行电镀及对电镀源进行标准化的方法。测定了Am-241电镀源在2πPC中的效率为49%。对这些源进行了进一步的α光谱测量,从而产生了高分辨率光谱,其半最大值全宽度(FWHM)值为38 keV。扫描电子显微镜(SEM)的表面形态学研究产生非簇状沉积,表明放射性核素均匀分布,因此,均匀性。用组织擦拭试验评价放射性核素在基质上的粘附性。目前的研究表明,没有计数擦拭组织表明附着在沉积。
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引用次数: 0
Estimation of Reference Gamma Radiation Field for Calibration of Radiation Monitors 辐射监测仪校准中参考辐射场的估计
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-25 DOI: 10.1007/s12647-023-00699-x
Sunil K. Singh, Liji Shaiju, Aashna Gupta, S. M. Tripathi, V. Sathian, Probal Chaudhury

Laboratories/facilities dealing with ionizing radiation encounter radiation field which are measured using suitable gamma radiation monitors, for area and personal monitoring. These radiation monitors are subjected to periodic calibrations to confirm that they are still fit for the purpose. In India, periodic calibration of these radiation monitors is carried out by NABL accredited calibration laboratories using source exposure devices containing radionuclide sources of 137Cs and/or 60Co. Calibration laboratories get the output from these source exposure devices standardized by RSSD, BARC, Mumbai. RSSD, BARC, provides a report on the measured output, in the form of air kerma rates at different distances, which is traceable to relevant national standards. The laboratory then uses the standardized radiation field in day-to-day calibration, by taking air kerma rate mostly at distance of 100 cm (fixed distance) as reference for estimating radiation fields at other distances by using inverse square law. The air kerma rate values obtained by the using inverse square law shows deviation from the measured values with an allowed deviation up to 5%. The impact of this deviation cannot be corrected thus is accounted in the form of uncertainty. This paper presents an average air kerma strength-based methodology which provides a simple and effective mechanism for estimating the conventional true value of air kerma rate at various distance which adds lower uncertainty to overall uncertainty, as compared to the method of using a fixed or reference distance (say 100 cm) based air kerma rate.

处理电离辐射的实验室/设施会遇到辐射场,使用合适的伽马辐射监测仪进行区域和个人监测。这些辐射监测仪定期进行校准,以确认它们仍然适合使用。在印度,这些辐射监测仪的定期校准是由NABL认可的校准实验室使用含有137Cs和/或60Co放射性核素源的源照射装置进行的。校准实验室获得由RSSD, BARC,孟买标准化的这些源暴露设备的输出。RSSD, BARC提供测量输出的报告,以不同距离的空气速率形式,可追溯到相关的国家标准。然后,实验室在日常校准中使用标准化辐射场,主要以100厘米(固定距离)的空气kerma率作为参考,利用平方反比定律估算其他距离的辐射场。利用平方反比定律得到的空气速率值显示出与实测值的偏差,允许偏差达5%。这种偏差的影响无法纠正,因此以不确定性的形式计算。本文提出了一种基于平均空气kerma强度的方法,该方法提供了一种简单有效的机制来估计不同距离下空气kerma速率的常规真实值,与使用固定或参考距离(例如100厘米)的方法相比,该方法在总体不确定性中增加了更低的不确定性。
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引用次数: 0
Development and Uncertainty Assessment of Low-Cost Portable EMG Acquisition Module 低成本便携式肌电信号采集模块的研制与不确定度评估
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-23 DOI: 10.1007/s12647-023-00706-1
Rohit Gupta, Inderjeet Singh Dhindsa, Ravinder Agarwal

Surface electromyography is an important and widely used biomedical measurement technique. In biomedical engineering, obtaining high-quality EMG data and processing it in real-time is challenging. Their calibration repeatability and reliability, on the other hand, remain in discussion. Furthermore, the metrological elements of EMG systems have not yet been studied. In this research work, a portable EMG acquisition module has been developed, and the uncertainty of two EMG characteristics for four everyday hand motions has been investigated. Furthermore, an inter-instrument comparison has been carried out in a controlled environment. For multiple trials, the result has been estimated for 10 people. While designing the experiment, two major uncertainty factors, muscle selection/electrode placement and subjective analysis, have been taken into consideration. The developed system's inter-instrument performance has been found to be similar to that of the existing system (p-value > 0.05). The total uncertainty of the developed system has been found to be in the range of 0.0106–0.0196% (p-value > 0.05) for RMS and 0.1001–0.2084% (p-value > 0.05) for MF. The existing commercial system, in contrast, exhibited uncertainty in the range of 0.0171–0.0359% (p-value > 0.05) for RMS and 0.1010–0.2088% (p-value > 0.05) for MF. The developed EMG acquisition system's performance and cost-effectiveness validate its utility and acceptability for low-cost product development.

表面肌电图是一种重要而广泛应用的生物医学测量技术。在生物医学工程中,获取高质量的肌电图数据并对其进行实时处理具有挑战性。另一方面,它们的校准可重复性和可靠性仍在讨论中。此外,肌电系统的计量要素尚未得到研究。在本研究中,开发了一种便携式肌电信号采集模块,并研究了四种日常手部运动的两种肌电信号特征的不确定性。此外,在受控环境下进行了仪器间比较。在多次试验中,对10个人的结果进行了估计。在设计实验时,考虑了两个主要的不确定性因素,肌肉选择/电极放置和主观分析。开发的系统的仪器间性能与现有系统相似(p值> 0.05)。开发的系统的总不确定度在RMS的0.0106-0.0196% (p值> 0.05)和MF的0.1001-0.2084% (p值> 0.05)之间。相比之下,现有商业系统的RMS不确定性为0.0171-0.0359% (p值> 0.05), MF不确定性为0.1010-0.2088% (p值> 0.05)。所开发的肌电信号采集系统的性能和成本效益验证了其在低成本产品开发中的实用性和可接受性。
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引用次数: 0
Performance Validation of the Acoustic Comparison Coupler for the Sound Level Meter Calibration 声级计校准用声学比较耦合器的性能验证
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-18 DOI: 10.1007/s12647-023-00696-0
Bondan Dwisetyo, Denny Hermawanto, Fajar Budi Utomo, Ninuk Ragil Prasasti, Chery Chaen Putri

An acoustic comparison coupler has been designed by the acoustic and vibration research group, National Research and Innovation Agency (BRIN). This research prototype is developed to be utilized by a private and industrial laboratory to comply with periodic tests of a sound level meter (SLM) for frequency weighting as the primary parameter. Further, the performance has been demonstrated in the previous paper. Nevertheless, the comparison test among the acoustic calibration systems associated with this mandatory parameter test has not been conducted yet. Therefore, the purpose of this work is to conduct the validation of this prototype as the SLM calibration system using the two established methods consists of the free field method by using free field facilities and insert voltage technique, and the second method by utilizing the multifunction acoustic calibrator in a pressure field condition. The measurement procedure is carried out following the standard IEC 61672–3. Therefore, the results are compared to the acceptance limit stated by this standard. This work also quantifies the uncertainty measurements that are provided by these methods. From the results, the measured frequency weighting is obtained using these methods. The deviation to the reference values and the expanded uncertainty measurement are also reported.

国家研究与创新署(BRIN)声学与振动研究小组设计了一种声学比较耦合器。这一研究原型的开发是为了供私人和工业实验室使用,以符合频率加权作为主要参数的声级计(SLM)的定期测试。此外,该性能在之前的论文中已经得到了验证。然而,与此强制性参数测试相关的声学校准系统之间的对比试验尚未进行。因此,本工作的目的是利用两种已建立的方法对该样机进行验证,其中一种方法是利用自由场设施和插入电压技术建立的自由场方法,另一种方法是利用压力场条件下的多功能声学校定器。测量程序按照标准IEC 61672-3进行。因此,将结果与本标准规定的可接受限度进行比较。这项工作还量化了这些方法提供的不确定度测量。根据测量结果,利用这些方法得到了测量频率的权重。本文还报道了与参考值的偏差和扩展不确定度测量。
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引用次数: 0
SRR and DGS-Based Highly Isolated Four-Port MIMO Antenna for Mid-5G Band and High-5G Band 基于SRR和dgs的中5g频段和高5g频段高隔离四端口MIMO天线
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-18 DOI: 10.1007/s12647-023-00704-3
Atanu Chowdhury, Prashant Ranjan

This manuscript proposed a compact four-port multiple input multiple output (MIMO) antenna based on four split-ring resonators (SRR) at the top and a defected ground structure (DGS) at the bottom of the substrate for 5G communication. SRRs are used to resonate at 4 GHz frequency in mid-5G band. A slot of “ + ” symbol is cut at the bottom (DGS) to enlarge the bandwidth. The proposed antenna also achieved a high-5G frequency band (26.8–29.8 GHz) (n257/n258 band) by four square-shaped ring slots at the ground plane. It further enhances the bandwidth in mid-5G band (2.9–6 GHz) (n74/n75/n76/n77/n78 band) and helps to achieve a high degree of isolation between each radiating element (over 40 dB) at both the 5G bands. The size of the proposed MIMO antenna is 60 mm × 60 mm × 1.6 mm. It achieves a maximum gain of 4.59 dB, 4.32 dB at the mid-5G and high-5G band, respectively. The maximum radiation efficiencies achieved are 89%, 81% at the mid-5G and high-5G band, respectively. The diversity functionality of the antenna is also outstanding as the value of ECC is 0.01–0.42, DG is 9.6–10 dB, and TARC is less than − 10 dB measured in both the bands. The entire performance of the proposed antenna is practically verified, discussed and presented.

本文提出了一种紧凑的四端口多输入多输出(MIMO)天线,该天线基于顶部的四个分环谐振器(SRR)和底部的缺陷接地结构(DGS),用于5G通信。srr用于在5g中期频段的4ghz频率上谐振。在底部(DGS)切割一个“+”符号槽以扩大带宽。该天线还通过在地平面上的四个方形环形槽实现了高5g频段(26.8-29.8 GHz) (n257/n258频段)。它进一步增强了5G中频段(2.9-6 GHz) (n74/n75/n76/n77/n78频段)的带宽,并有助于在两个5G频段实现每个辐射元件之间的高度隔离(超过40 dB)。MIMO天线的尺寸为60mm × 60mm × 1.6 mm。它在5g中频段和5g高频段的最大增益分别为4.59 dB和4.32 dB。在5g中频段和5g高频段实现的最大辐射效率分别为89%、81%。该天线的分集功能也很突出,在两个频段测量到的ECC值为0.01-0.42,DG值为9.6-10 dB, TARC值小于- 10 dB。对所提出的天线的整体性能进行了实际验证、讨论和介绍。
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引用次数: 0
Variations and Inter Relationship in Mid-tropospheric Carbon Dioxide, Temperature and Water Vapour Using AIRS Observations 对流层中二氧化碳、温度和水蒸气的变化及其相互关系
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-16 DOI: 10.1007/s12647-023-00689-z
Anju Gupta, S. K. Dhaka

In the present study, trends and variations in carbon dioxide (CO2), temperature and water vapour are analysed using 9 years (2003–2011) of mid-tropospheric (300–500 hPa) Atmospheric Infrared Sounder (AIRS) data. The focus of analysis remains on both a global as well as regional (India) scale along with improved understanding of their inter relationship. It was observed that the mid-tropospheric carbon dioxide increased from ~ 373 to ~ 393 ppm and ~ 373 to ~ 392 ppm, respectively, over the globe and the Indian region during 9 years. However, no substantial trends (increasing or decreasing) were observed in the temperature and water vapour observations for the same period of time. De-trended data of CO2, temperature and water vapour were further analysed to understand the inter relationship between these parameters and the influence of two greenhouse gases (CO2 and water vapour) on temperature. Analysis suggests a very high correlation (~ 0.90) between temperature and water vapour, however, no significant correlation was observed between temperature and carbon dioxide data, indicating that change in water vapour may have stronger influence on temperature compared to the change in CO2, this feature can play a more significant role as a greenhouse gas than CO2.

在本研究中,利用9年(2003-2011年)对流层中部(300-500 hPa)大气红外探测器(AIRS)数据分析了二氧化碳(CO2)、温度和水蒸气的趋势和变化。分析的重点仍然是全球和区域(印度)规模,以及对其相互关系的更好理解。结果表明,9年间,全球和印度地区对流层中层二氧化碳浓度分别从~ 373增加到~ 393 ppm和~ 373增加到~ 392 ppm。然而,在同一时期的温度和水汽观测中没有观测到实质性的趋势(增加或减少)。进一步分析了CO2、温度和水蒸气的非趋势数据,以了解这些参数与两种温室气体(CO2和水蒸气)对温度的影响之间的相互关系。分析表明,温度与水蒸气的相关性非常高(~ 0.90),但温度与二氧化碳的相关性不显著,这表明水蒸气的变化可能比CO2的变化对温度的影响更大,这一特征作为温室气体比CO2发挥更大的作用。
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引用次数: 0
Investigating DC Characteristics in Testing Precision Current Shunts for Steady State 在测试稳态精密电流分流器时研究直流特性
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-11-01 DOI: 10.1007/s12647-023-00697-z
Valentyn Isaiev, Svitlana Isaieva

This paper provides information on the performance study of precision current shunts in the context of their output voltage stability. Besides, it briefly focuses on the phenomena affecting the steady state of these measuring instruments. The authors present a methodology for testing current shunts to ensure a high-quality result of current measurement. The investigation highlights three characteristics of shunts (the dependence of resistance on temperature, the response of the output voltage to a fast increase of current, and the transition from a cold state to a warm one). The test equipment with precision shunts were considered during the experimental examination. The results of an investigation confirmed satisfactory operational properties and compliance with the needs of laboratories. Additionally, the authors emphasize using a precision shunt as a measuring standard when calibrating other instruments like high-precision digital ammeters. From this point of view, the simplified mathematical modeling of the change in the AC-DC transfer difference, depending on the resistance change caused by the warming current, was carried out.

本文介绍了精密电流分流器在输出电压稳定性方面的性能研究。此外,本文还简要介绍了影响这些测量仪器稳定状态的现象。作者提出了一种测试电流分流器的方法,以确保高质量的电流测量结果。调查强调了分流器的三个特性(电阻对温度的依赖性、输出电压对电流快速增加的响应以及从冷态到热态的过渡)。在实验检查过程中考虑了带有精密分流器的测试设备。调查结果表明,该设备的运行性能令人满意,符合实验室的需要。此外,作者还强调在校准其他仪器(如高精度数字电流表)时使用精密分流器作为测量标准。从这个角度出发,作者对交流-直流传输差的变化进行了简化数学建模,这种变化取决于升温电流引起的电阻变化。
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引用次数: 0
PM2.5 Observations of Outdoor and Indoor Environment at Dwarka, New Delhi, India 印度新德里 Dwarka 的室外和室内 PM2.5 观测数据
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-10-31 DOI: 10.1007/s12647-023-00694-2
Shristy Malik, A. S. Rao, Surendra K. Dhaka

Measurement of PM2.5 is carried out simultaneously outdoors as well as indoors using a Compact and Useful PM2.5 Instrument (CUPI) from Nov 2018 to Oct 2019. A high-time resolution data (~ 2 min interval) was recorded at Dwarka (West Delhi), New Delhi, to investigate the difference between outdoor and indoor ambient particulate matter. Year-long observations provide an opportunity to decipher that indoor PM2.5 concentration increases significantly from mid-November 2018 to mid-December 2018. During this high concentration occurrence of PM2.5, outdoor concentration was higher in the range of 100–200 µg/m3 than indoor. Indoor pollution was less by 30–50% in comparison to the outdoor environment. Analyses reveal that during a high pollution period, intermittently for a short period, outdoor PM2.5 was less, which coincides with clear weather days suggesting that indoor pollution did not disperse due to a closed environment. Diurnal variation of PM2.5 clearly shows high concentration stays until 12:00 noon in both indoor and outdoor environments, which reduces in the afternoon and again picks up in the evening. Diurnal variation of solar radiation showed a consistent increase from 9 am to 2 pm, while relative humidity declined considerably from 10 am to 4 pm (local time); these two factors correspond to less concentration in both indoor and outdoor environments. However, there is no significant difference between outdoor and indoor concentration during summer and monsoon season.

2018 年 11 月至 2019 年 10 月,使用紧凑实用 PM2.5 仪器(CUPI)在室外和室内同时进行 PM2.5 测量。在新德里 Dwarka(西德里)记录了高时间分辨率数据(约 2 分钟间隔),以研究室外和室内环境颗粒物之间的差异。长达一年的观测为破译室内 PM2.5 浓度在 2018 年 11 月中旬至 2018 年 12 月中旬显著增加提供了机会。在此次PM2.5高浓度发生期间,室外浓度在100-200微克/立方米范围内高于室内。与室外环境相比,室内污染减少了 30%-50%。分析表明,在高污染期间,间歇性的短时间内,室外 PM2.5 较少,这与晴朗的天气相吻合,表明由于环境封闭,室内污染没有扩散。PM2.5 的昼夜变化清楚地表明,室内和室外环境中的 PM2.5 浓度都很高,一直持续到中午 12:00,下午有所降低,傍晚又有所回升。太阳辐射的昼夜变化显示,从上午 9 点到下午 2 点,太阳辐射持续增加,而相对湿度则从上午 10 点到下午 4 点(当地时间)大幅下降;这两个因素导致室内和室外环境中的浓度降低。不过,在夏季和季风季节,室外和室内的浓度没有明显差异。
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引用次数: 0
Model Adequacy Checking in Homogeneity and Stability Studies 同质性和稳定性研究中的模型充分性检查
IF 1 4区 工程技术 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2023-10-26 DOI: 10.1007/s12647-023-00695-1
Luiz Henrique da Conceição Leal, Werickson Fortunato de Carvalho Rocha

The production of reference materials necessitates, among other factors, evaluations of homogeneity and stability. The aim of the homogeneity study is to ensure uniformity in property values across all samples. On the other hand, stability pertains to a sample’s ability to retain its property value over time. ISO Guide 35 dictates that homogeneity, between and within samples, is appraised using a one-way random effects analysis of variance, while stability is gauged by a univariate linear regression model. Both these statistical techniques presuppose the normality and homoscedasticity of the residuals. Notably, the ISO Guide 35 standard omits any reference to the assumption of homoscedasticity in its prescribed statistical methods. This communication introduces the Shapiro–Wilk and Koenker–Bassett tests as tools to verify the assumptions of normality and homoscedasticity, respectively. Moreover, it advances the feasible generalized least squares method as a remedy for instances where these assumptions are breached. Initial findings suggest that, in certain scenarios, breaches in statistical model assumptions might influence evaluations of homogeneity and/or stability.

除其他因素外,标准物质的生产还需要对均匀性和稳定性进行评估。均匀性研究的目的是确保所有样本的属性值一致。另一方面,稳定性与样品长期保持其属性值的能力有关。ISO 指南 35 规定,样本间和样本内的同质性采用单向随机效应方差分析进行评估,而稳定性则采用单变量线性回归模型进行衡量。这两种统计技术都以残差的正态性和同方差性为前提。值得注意的是,ISO 指南 35 标准在其规定的统计方法中没有提及同方差假设。本文介绍了 Shapiro-Wilk 检验和 Koenker-Bassett 检验,分别作为验证正态性和同方差假设的工具。此外,它还提出了可行的广义最小二乘法,作为对违反这些假设的情况的补救措施。初步研究结果表明,在某些情况下,统计模型假设的违背可能会影响对同质性和/或稳定性的评估。
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引用次数: 0
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