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Comparison of the Contributions of the Superplastic Deformation Mechanisms in Al-Mg-Fe-Ni-Zr-Sc Alloy with a Small Addition of Zn Processed by Rolling or Multidirectional Forging 通过轧制或多向锻造加工的少量添加锌的 Al-Mg-Fe-Ni-Zr-Sc 合金中超塑性变形机制的贡献比较
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601271
O. A. Yakovtseva, Z. S. Turaeva, A. A. Kishchik, A. V. Irzhak, V. V. Cheverikin, A. V. Mikhaylovskaya

Superplastic deformation is ensured by grain boundary sliding, which is accommodated by dislocation and diffusion creep. The contributions of these mechanisms depend on the microstructural parameters of alloys and temperature-strain rate conditions of deformation. In this work, the deformation behavior, grain structure parameters, and the contributions of the superplastic deformation mechanisms at the temperature 0.87Тm and constant strain rate 1 × 10–2 s–1 were compared between the rolled Al-5Mg-0.9Fe-0.83Ni-0.14Zr-0.08Sc-0.72Zn alloy with the initial nonrecrystallized grain structure and the recrystallized alloy treated by multidirectional isothermal forging (MDF). The strain rate sensitivity coefficient was ~0.5, and the elongation reached 400–520% under the specified conditions. Superplastic deformation of the rolled alloy resulted in dynamic recrystallization providing strain weakening. In the MDF-treated alloy, deformation was accompanied by strain hardening due to grain growth. Regardless of the treatment mode, at the steady flow stage, the alloy shows similar microstructural parameters and similar contributions of the deformation mechanisms, which were determined from microstructural evolution on the surface with markers. The contribution of grain boundary sliding was ~40%, and intragranular dislocation slip/creep provided was ~20%. The remaining strain localized near transverse grain boundaries with the formation of striated zones, which were associated with grain boundary sliding and diffusion creep mechanisms.

超塑性变形由晶界滑动保证,由位错和扩散蠕变调节。这些机制的作用取决于合金的显微组织参数和变形的温度-应变速率条件。本文比较了具有初始非再结晶组织的Al-5Mg-0.9Fe-0.83Ni-0.14Zr-0.08Sc-0.72Zn合金与经过多向等温锻造(MDF)处理的再结晶合金在0.87Тm温度和恒定应变速率1 × 10-2 s-1条件下的变形行为、晶粒组织参数以及超塑性变形机制的贡献。在规定的条件下,应变率敏感系数为~0.5,伸长率达到400 ~ 520%。轧制合金的超塑性变形导致动态再结晶,从而使应变减弱。在mdf处理的合金中,由于晶粒长大,变形伴随着应变硬化。无论采用何种处理方式,在稳定流动阶段,合金表现出相似的显微组织参数和变形机制的贡献,这是由标记表面的显微组织演变确定的。晶界滑移贡献约40%,晶内位错滑移/蠕变贡献约20%。剩余的应变局部分布在晶界附近,形成条纹带,与晶界滑动和扩散蠕变机制有关。
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引用次数: 0
Refinement of the Basic Equations of Phase Field Theory under Nonisothermal Conditions 非等温条件下相场理论基本方程的改进
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S102995992460126X
A. G. Knyazeva

The paper gives a brief review of thermodynamic theories that take into account the structure of materials and phase interfaces. Among them are classical thermodynamics, surface thermodynamics, thermodynamics with internal variables, and extended thermodynamics. It is shown that thermodynamic phase field theory has common features with both extended thermodynamics and thermodynamics with internal variables, but is not identical to them. Coupled phase field equations for binary systems under nonisothermal conditions are deduced based on classical thermodynamics of irreversible processes. Free energy is expanded in a series in temperature gradients, concentration, and phase variable. The obtained general relations are in agreement with the known ones. The new derivation method allowed refining the basic equations. It is shown that not only models of phase transitions with an infinitely narrow interface but also the theory of a two-phase region can be considered as a limiting variant of the theory. The effective transfer enthalpy and the enthalpy due to the evolution of the phase variable are explicitly given in the equations. It is shown that the general relations are equivalent when the basic equations are derived by any of the thermodynamic potentials. Phase field relations are deduced for a regular solution, and the physical meaning of different summands is clarified. The basic equations of phase field theory are derived with consideration for possible chemical interaction of the components.

本文简要回顾了考虑材料结构和相界面的热力学理论。其中有经典热力学、表面热力学、带内变量热力学和扩展热力学。结果表明,热力学相场理论具有扩展热力学和带内变量热力学的共同特点,但又不完全相同。基于经典不可逆过程热力学,推导了非等温条件下二元系统的耦合相场方程。自由能在温度梯度、浓度和相变量中展开。所得的一般关系与已知的一般关系是一致的。新的推导方法使基本方程得以改进。结果表明,无限窄界面相变模型和两相区域理论都可以看作是该理论的极限变体。方程中明确给出了有效传递焓和由相变量演化引起的焓。结果表明,当用任意热力学势导出基本方程时,一般关系是等价的。推导了正则解的相场关系,阐明了不同和的物理意义。考虑组分之间可能的化学相互作用,推导了相场理论的基本方程。
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引用次数: 0
Fundamental and Applied Aspects of Materials Science in Tribology 摩擦学中材料科学的基础和应用方面
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601908
A. V. Kolubaev, E. A. Kolubaev, A. I. Dmitriev, S. Yu. Tarasov, A. V. Chumaevskii

Dedicated to the 40th anniversary of the Institute of Strength Physics and Materials Science SB RAS. The paper reviews the current state of research in the field of sliding friction and wear and the related production technologies with an emphasis on the works of the Institute of Strength Physics and Materials Science SB RAS. These works gave fundamental results on structural and phase transformations of materials below the worn surface, which were later used as a basis for the development of wear-resistant materials, hard coatings, lubricants, and friction processing methods. The main mechanisms of deformation and metal flow in the subsurface layer during adhesive friction and friction stir welding are considered. The development of mathematical modeling of friction and wear processes for various materials is traced. Computer modeling of friction and wear processes allowed solving a number of theoretical and applied problems of plastic flow of materials in the sliding contact zone and the development of surface processing methods. The obtained results were used to explain material flow in friction stir welding. The evolution of industrial technologies based on unlubricated and adhesive friction is reviewed.

致力于SB RAS强度物理与材料科学研究所成立40周年。本文综述了滑动摩擦磨损及其生产技术的研究现状,重点介绍了SB RAS强度物理与材料科学研究所的工作。这些工作给出了磨损表面以下材料的结构和相变的基本结果,这些结果后来被用作耐磨材料、硬涂层、润滑剂和摩擦处理方法发展的基础。分析了粘接摩擦焊和搅拌摩擦焊中亚表层变形和金属流动的主要机理。对各种材料的摩擦和磨损过程的数学模型的发展进行了跟踪。摩擦和磨损过程的计算机建模允许解决滑动接触区材料塑性流动的许多理论和应用问题以及表面加工方法的发展。所得结果用于解释搅拌摩擦焊接中的物质流动。综述了基于无润滑和粘着摩擦的工业技术的发展。
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引用次数: 0
Nonlocal Transfer Mechanics in a Dynamically Deformed Medium. Wave Concept of the Mesoscale 动态变形介质中的非局部传递力学。中尺度的波浪概念
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601301
T. A. Khantuleva, Yu. I. Meshcheryakov, G. V. Konovalov, N. I. Zhigacheva, A. K. Divakov

Experimental results on the response of solids to shock loading obtained by the original method capable of real-time recording of mesoscopic characteristics contradict the conventional representation of elastic-plastic transition within the local equilibrium concepts of continuum mechanics. Nonlocal mathematical modeling of spatiotemporal correlations in a shock pulse based on nonequilibrium statistical mechanics allowed uniting the obtained experimental data within the new physical representation of shock wave phenomena where the mesoscopic carriers of deformation were interacting wave packets. Microstructural investigations of the studied materials reveal different scales of deformation in three ranges of shock velocities, which are responsible for macroscopic properties of materials.

通过能够实时记录细观特征的原始方法获得的固体对冲击载荷响应的实验结果与连续介质力学局部平衡概念中传统的弹塑性过渡表示相矛盾。基于非平衡统计力学的冲击脉冲时空相关性的非局部数学建模允许将获得的实验数据统一到冲击波现象的新物理表示中,其中变形的介观载体是相互作用的波包。对所研究材料的微观结构研究表明,在三个冲击速度范围内,材料的变形规模不同,这是材料宏观性能的原因。
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引用次数: 0
Free Vibration Analysis of a Functionally Graded Magneto-Piezo-Thermoelastic Ceramic-Metal Nanobeam Using Modified Nonlocal State-Space Strain Gradient Theory 利用修正的非局部状态-空间应变梯度理论分析功能分级磁-压电-热弹陶瓷-金属纳米梁的自由振动
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601258
R. Selvamani, L. Rubine, T. Prabhakaran, M. Yaylaci

This work studies how the variable nonlocal parameter is related to the material variations across a functionally graded (FG) nanobeam. Hamilton’s principle is used to derive the governing motion equations for a FG nanobeam within the refined higher-order state-space strain gradient theory. The presented formulation is tested numerically via Navier’s solution for a simply supported FG nanobeam. A comparison with the existing published findings is performed to show the precision of results. Furthermore, the effects of the nonlocal parameters of the ceramic and metal parts, as well as temperature, magnetic potential, and electric voltage on the free vibration response are investigated.

本文研究了非局部参数的变化与功能梯度纳米梁材料变化之间的关系。利用Hamilton原理推导了精细化高阶状态空间应变梯度理论中FG纳米梁的运动控制方程。所提出的公式通过Navier的解决方案进行了数值测试,用于简支FG纳米梁。并与已发表的研究结果进行了比较,以证明结果的准确性。此外,还研究了陶瓷和金属部件的非局部参数以及温度、磁势和电压对自由振动响应的影响。
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引用次数: 0
Damage Model of a Two-Layer TiB/Ti-Based Ceramic-Metal Composite under Three-Point Loading 三点加载下双层 TiB/Ti-B 基陶瓷-金属复合材料的损伤模型
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601283
K. A. Khvostunkov, P. M. Bazhin, M. V. Velikov, A. O. Zhidovich, M. S. Titov, M. S. Antipov

In this work, a model was developed for determining the critical load of a two-layer ceramic-metal composite under three-point loading based on the analysis of the local influence of distributed defects on the stress field. The stressed state is defined as the solution of a boundary value problem for a solid. The object of investigation was a two-layer TiB/Ti-based ceramic-metal composite obtained by free SHS (self-propagating high-temperature synthesis) compression. A method was developed for determining the statistical distribution of defects within a specimen based on metallographic cross-sectional analysis. The critical load was determined by the defect size probability density found from the experimental data. The cases of flat and sinusoidal interfaces between the composite layers were considered. A digital model of a two-layer beam deformed under three-point loading was built in Abaqus finite element software, which was used for numerical simulation of the stress field. Based on the numerical results, the stress field was corrected for the sinusoidal interface. The influence of the corrected stress field on the specimen strength was analyzed when the defect distribution pattern was similar to that in the composite with the flat interface. It was shown that the sinusoidal shape of the interface had no effect on the specimen strength, provided that the period and amplitude of deviation from the rectilinear shape were small relative to the linear size of the specimen.

本文在分析分布缺陷对应力场局部影响的基础上,建立了确定三点载荷下两层陶瓷-金属复合材料临界载荷的模型。应力状态被定义为固体边值问题的解。研究对象是通过自由SHS(自蔓延高温合成)压缩制备的双层TiB/ ti基陶瓷-金属复合材料。提出了一种基于金相截面分析的试样缺陷统计分布确定方法。根据实验数据得到的缺陷尺寸概率密度确定临界载荷。考虑了复合材料层间的平面界面和正弦界面的情况。在Abaqus有限元软件中建立了三点荷载作用下两层梁变形的数字模型,并对其应力场进行了数值模拟。根据数值结果,对正弦界面的应力场进行了修正。分析了当缺陷分布模式与平面界面相似时,修正后的应力场对试样强度的影响。结果表明,只要偏离直线形状的周期和幅度相对于试样的线性尺寸较小,则界面的正弦形状对试样的强度没有影响。
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引用次数: 0
Analysis of the Impact of the Viscoelastic Foundation on Bending and Vibration of FG Porous Nanoplates within Integral Higher-Order Shear Deformation Theory 在积分高阶剪切变形理论中分析粘弹性地基对 FG 多孔纳米板弯曲和振动的影响
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601313
I. Baghdali, A. Attia, F. Bourada, A. A. Bousahla, Abdeldjebbar Tounsi, H. Heireche, Abdelouahed Tounsi, M. Bourada, M. Yaylaci

This work examines the bending and vibration responses of a functionally graded (FG) 2D nanostructure resting on the viscoelastic foundation. The FG structure properties vary gradually in the thickness direction. In this investigation, three porosity patterns are examined. The nonlocal equilibrium equations are derived by Hamilton’s principle using Eringen’s nonlocal elasticity theory, which incorporates the integral plate theory with a reduced number of unknowns. The results computed for the studied simply supported FG nanoplates are compared with those published in the open literature. Several parametric studies are performed to illustrate various influences of the plate geometry, material inhomogeneity, elastic damping coefficient, and nonlocal effect on the stresses, frequency, and central deflection of FG nanoplates.

本文研究了基于粘弹性基础的功能梯度(FG)二维纳米结构的弯曲和振动响应。FG结构性能在厚度方向上逐渐变化。在本研究中,研究了三种孔隙模式。利用Eringen的非局部弹性理论,利用Hamilton原理推导了非局部平衡方程,该理论结合了积分板理论,减少了未知量。对所研究的简支FG纳米板的计算结果与公开发表的结果进行了比较。本文进行了几个参数研究,以说明板的几何形状、材料的不均匀性、弹性阻尼系数和非局部效应对FG纳米板的应力、频率和中心挠度的各种影响。
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引用次数: 0
Dependence of Magnetic Properties and Their Thermal Stability on the Phase Composition of Fe-Co-Cr-B-Si Alloy Ribbons Fe-Co-Cr-B-Si合金带的磁性能及其热稳定性与相组成的关系
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-04-09 DOI: 10.1134/S1029959924601295
E. N. Zanaeva, A. I. Bazlov

The work is devoted to magnetic materials based on (Fe62Cr24Co14)81+xB18–xSi1 (at %) alloys, where x = 0, 2, and 4. The materials were prepared in the form of metallic ribbons by melt spinning, i.e. rapid quenching from the melt onto a rotating copper disk in an inert atmosphere. In the as-spun state, ribbons had an amorphous structure. The structure and phase transformations in the alloys upon heating were analyzed using X-ray diffraction methods. The dependences of the magnetic moment and heat flow of the alloys heated at the same heating rate were found. Variation in the phase composition during crystallization of the amorphous structure and its influence on the magnetic properties of the alloys were studied. It was found that, for a highly coercive state to form, the alloy structure should present a mixture of the α and Fe3B phases, which is also characterized by high thermal stability and microhardness. The alloys demonstrate the coercive force 20.8–43.2 kA/m, saturation magnetization 0.70–1.15 T, residual magnetization 0.36–0.54 T, and microhardness 1350 ± 90 HV after crystallization heat treatment. The (Fe62Cr24Co14)81B18Si1 alloy has the best set of properties: high thermal stability, a decrease in the saturation magnetization (by 22%) and coercive force (by 13%) in the range from room temperature to 500°C.

这项工作致力于基于(Fe62Cr24Co14)81+ xB18-xSi1 (at %)合金的磁性材料,其中x = 0,2和4。该材料通过熔体纺丝以金属带的形式制备,即在惰性气氛中从熔体快速淬火到旋转的铜盘上。在纺丝状态下,带状具有无定形结构。利用x射线衍射分析了合金在加热过程中的组织和相变。发现了在相同加热速率下合金的磁矩和热流的依赖关系。研究了非晶组织结晶过程中相组成的变化及其对合金磁性能的影响。结果表明,为了形成高矫顽力态,合金组织应呈现α相和Fe3B相的混合,同时具有较高的热稳定性和显微硬度。晶化热处理后合金的矫顽力为20.8 ~ 43.2 kA/m,饱和磁化强度为0.70 ~ 1.15 T,残余磁化强度为0.36 ~ 0.54 T,显微硬度为1350±90 HV。在室温至500℃范围内,(Fe62Cr24Co14)81B18Si1合金具有较高的热稳定性,饱和磁化强度降低22%,矫顽力降低13%。
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引用次数: 0
Evolution of the Structure and Properties of Cu-56Au (at %) Alloy during L10-Type Atomic Ordering l10型原子有序过程中Cu-56Au (at %)合金结构与性能的演变
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-02-12 DOI: 10.1134/S102995992460109X
O. S. Novikova, E. G. Volkova, P. O. Podgorbunskaya, D. A. Zgibnev, A. A. Gavrilova, N. A. Kruglikov, A. Yu. Volkov

The ordered gold-copper alloy Cu–56 at % Au is widely used in instrument engineering as conductors of weak electrical signals in control devices. However, microstructural evolution and changes in the physicomechanical properties of the alloy during the disorder → order phase transformation (A1 → L10) are still poorly understood. In the present paper, we study the evolution of the microstructure and properties of the quenched Cu–56 at % Au alloy during the disorder → order phase transformation. The annealing time at 250°C ranged from 10 min to 4 months. Microstructural studies were performed using transmission electron microscopy, the ratio of volume fractions of the ordered and disordered phases was determined using X-ray diffraction analysis and resistometric measurement, and material properties were measured in mechanical tensile and microhardness tests. The fraction of the ordered phase, strength properties, and specific electrical resistivity were plotted as a function of the annealing time. It is found that the maximum strength properties correspond to the two-phase state (A1 + L10) of the alloy with an approximately equal phase ratio. It is shown that, with an increase in the fraction of the ordered phase, the tensile strain hardening coefficient almost doubles.

有序金铜合金Cu-56 at % Au在仪表工程中广泛用作控制装置中微弱电信号的导体。然而,在无序→有序相变(A1→L10)过程中,合金的显微组织演变和物理力学性能的变化仍然知之甚少。本文研究了Cu-56 at % Au淬火合金在无序→有序相变过程中组织和性能的演变。250℃下的退火时间从10分钟到4个月不等。通过透射电子显微镜进行微观结构研究,通过x射线衍射分析和电阻测量确定有序相和无序相的体积分数比,并通过机械拉伸和显微硬度测试测量材料性能。将有序相的分数、强度性能和比电阻率绘制为退火时间的函数。结果表明,在相比近似相等的情况下,合金的最大强度性能对应于两相状态(A1 + L10)。结果表明,随着有序相比例的增加,拉伸应变硬化系数几乎增加一倍。
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引用次数: 0
Influence of Structural Evolution and Load Level on the Properties of Creep and Recovery Curves Generated by a Nonlinear Model for Thixotropic Viscoelastoplastic Media 结构演化和荷载水平对触变粘弹塑性介质非线性模型生成的蠕变和恢复曲线特性的影响
IF 1.8 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2025-02-12 DOI: 10.1134/S1029959923600891
A. V. Khokhlov, V. V. Gulin

This paper continues the systematic analytical study of the properties of the previously constructed nonlinear shear deformation model of thixotropic viscoelastoplastic media, which takes into account the mutual influence of deformation and structural evolution. The ability of the model to describe the behavior of liquid and solid media (solidifying/solidified) is analyzed. The focus is on the response properties of the model to step loading, in particular, creep and recovery curves and curves of incremental cyclic loading. The aim is to find out what typical effects of viscoelastoplastic media the model can describe and what unusual effects/properties are generated by changes in the structuredness compared to typical creep and recovery curves of structurally stable materials. A system of two nonlinear differential equations is obtained to describe the response of the system to a given loading (not deformation) program, such as creep under constant load and arbitrary piecewise constant stress. A general solution to the Cauchy problem for this system is constructed in an explicit form for six arbitrary material parameters and an increasing material function governing the model, i.e. expressions are derived as quadratures for the shear strain and structuredness as functions of time, which depend on the initial conditions and all parameters of the model and loading program. An analytical study is performed for the basic properties of the family of creep and recovery curves and the structural evolution in these processes, their dependence on the time (monotonicity and convexity intervals, extrema, asymptotes, etc.), on the material parameters and function of the model, on the stress level and initial structuredness of the material, and on the initial stage of loading to a given stress before creep. It is proven that creep curves always increase with time, do not have inflection points, and have oblique asymptotes (although their initial arcs can differ considerably from straight lines). The structuredness at constant stress (at each incremental loading step, in particular, at zero stress) is always monotonic unlike other loading modes, but can decrease or increase depending on the relationship between the stress level and the initial structuredness at each incremental loading step. The model is shown to describe unusual effects observed in tests on some materials, e.g. the difference in the absolute values of strain jumps during loading and complete unloading and the opposite sign of residual strain with respect to the stress and strain signs at the creep stage. Several applicability indicators of the model are found, which can be conveniently verified using experimental data. Responses of the model to cyclic loading/unloading (creep/recovery), induced oscillations of the structuredness, and their effect on the rate of plastic strain accumulation are studied.

本文对先前建立的考虑变形与结构演化相互影响的触变粘弹塑性介质非线性剪切变形模型的特性进行了系统的分析研究。分析了该模型描述液体和固体介质(凝固/固化)行为的能力。重点研究了模型在阶跃加载下的响应特性,特别是蠕变和恢复曲线以及增量循环加载曲线。目的是找出模型可以描述的粘弹塑性介质的典型效应,以及与结构稳定材料的典型蠕变和恢复曲线相比,结构变化产生的异常效应/特性。得到了一个由两个非线性微分方程组成的系统来描述系统对给定加载(非变形)程序的响应,如恒载下的蠕变和任意分段恒应力下的蠕变。本文以显式形式建立了该系统Cauchy问题的通解,其中包含六个任意材料参数和一个控制模型的递增材料函数,即导出了剪切应变和结构度随时间的函数的正交表达式,它们取决于模型的初始条件和所有参数以及加载程序。分析研究了蠕变和恢复曲线族的基本特性和这些过程中的结构演变,以及它们对时间(单调性和凸性区间、极值、渐近线等)、模型的材料参数和函数、材料的应力水平和初始结构性以及蠕变前加载到给定应力的初始阶段的依赖关系。证明蠕变曲线总是随着时间的推移而增加,没有拐点,并且有倾斜的渐近线(尽管它们的初始弧可能与直线有很大的不同)。与其他加载模式不同,在恒应力下(特别是在零应力下)结构的结构性通常是单调的,但根据应力水平与初始结构性之间的关系,结构性可以减小或增大。该模型被证明可以描述在某些材料的试验中观察到的不寻常的影响,例如在加载和完全卸载期间应变跳变绝对值的差异以及相对于蠕变阶段的应力和应变符号的残余应变的相反符号。找到了模型的几个适用性指标,可以方便地利用实验数据进行验证。研究了模型对循环加载/卸载(蠕变/恢复)、结构性诱发振荡的响应及其对塑性应变积累速率的影响。
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引用次数: 0
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Physical Mesomechanics
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