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Oxidized Hastelloy Cloth Insulation for a Wind‐and‐React Processed Ag/Bi2Sr2CaCu2O8 Superconducting Magnet 氧化哈氏合金布绝缘的风和反应处理Ag/Bi2Sr2CaCu2O8超导磁体
Pub Date : 2006-04-21 DOI: 10.1063/1.2192413
K. Watanabe, G. Nishijima, S. Awaji, Y. Hikichi, T. Hasegawa
Practical multifilamentary Ag/Bi2Sr2CaCu2O8 round wires 1 mm in diameter exhibit critical current properties without anisotropy in fields up to 30 T and 4.2 K. We concentrate on the development of a Ag/Bi2Sr2CaCu2O8 insert coil by a wind‐and‐react method for a high field NMR superconducting magnet. Hastelloy cloth was used for the insulation for the wind‐and‐react process. A φ0.05 mm Hastelloy X (Hx) filament was knitted into a braid tube, and has a high mechanical strength and a good tolerance to oxidization at high temperature. We fabricated multifilamentary Ag/Bi2Sr2CaCu2O8 wires with Hx cloth, and heat‐treated them at around 890 °C in an oxygen atmosphere. It was found that the surface of Hx cloth is oxidized enough for a good electric insulation. Multifilamentary Ag/Bi2Sr2CaCu2O8 wires with oxidized Hx cloth insulation have the critical current of 720 A at 4.2 K in a self field.
实用的直径为1mm的多丝Ag/Bi2Sr2CaCu2O8圆线在高达30t和4.2 K的电场中表现出临界电流特性,无各向异性。我们专注于通过风-反应方法开发用于高场核磁共振超导磁体的Ag/Bi2Sr2CaCu2O8插入线圈。哈氏合金布用于风-反应过程的绝缘。将φ0.05 mm哈氏合金X (Hx)长丝编织成编织管,其机械强度高,高温耐氧化性好。我们用Hx布制备了多丝Ag/Bi2Sr2CaCu2O8丝,并在890℃左右的氧气环境中进行了热处理。结果发现,Hx布的表面氧化程度足以达到良好的电绝缘性。采用氧化Hx布绝缘的多丝Ag/Bi2Sr2CaCu2O8导线在自场4.2 K时的临界电流为720 A。
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引用次数: 1
Various Methods of Reducing AC Losses and Improving Stability of Internal‐Tin Nb3Sn Superconductors 减少交流损耗和提高内锡Nb3Sn超导体稳定性的各种方法
Pub Date : 2006-04-21 DOI: 10.1063/1.2192432
E. Gregory, B. Zeitlin, M. Tomsic, X. Wu, X. Peng, M. Sumption, E. Collings
In the past much of the emphasis in the development of Nb3Sn superconductors for High Energy Physics has been on improving the non‐Cu critical current density, (Jc), at 12 T. More recently the focus has shifted to improving the matrix residual resistivity ratio, (RRR), and decreasing the ac losses. In addition, the field of interest has risen to the 15–18 T range. Piece length and cost are also factors that are assumed not to deteriorate as the other properties are improved. In this paper we have emphasized reduction of losses by changing the conductor design. This has been explored both by the introduction of fins of various types and also by simply increasing the number of subelements using a tubular process, which has the potential of a low cost approach. The effect of these changes on the ease with which the multi‐subelementary material can be made is explored and discussed.
在过去,用于高能物理的Nb3Sn超导体的发展重点主要放在提高非Cu临界电流密度(Jc),在12 t,最近的重点已经转移到提高基体剩余电阻率(RRR)和减少交流损耗上。此外,感兴趣的领域已经上升到15-18 T区间。当其他性能得到改善时,工件长度和成本也被认为不会恶化。在本文中,我们强调通过改变导体设计来减少损耗。这已经通过引入各种类型的鳍片和使用管状工艺简单地增加子部件的数量进行了探索,这具有低成本方法的潜力。探讨了这些变化对制备多基元材料的难易程度的影响。
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引用次数: 4
The Superconducting Properties of High Density Bulk MgB2 Obtained by Reactive Liquid Mg Infiltration 反应性液态Mg浸润法制备高密度块状MgB2的超导性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192428
G. Giunchi
The reactive liquid Mg infiltration of Boron powders preforms is an easy technique to obtain high density and large superconducting bulk MgB2 manufacts, in which the supercurrents can percolate without obstacles by grains boundaries. The microstructure of these manufacts, as well their superconducting characteristics, can be tailored according to the Boron powders used and the particular arrangements of the reactants in a stainless steel container. A discussion of the superconducting characteristics of prototype manufacts of various shape will be given. The practical application of these manufacts, as permanent magnets for bearings or as current leads, will be discussed with reference to other superconducting bulk options. The expected temperature range for the use of this material will be between 15K and 30K and that calls for the development of reliable and cheap cryogenic systems.
硼粉预制件的反应液Mg渗透是制备高密度大体积超导MgB2的一种简便技术,其超电流可以不受晶界阻碍地渗透。这些产品的微观结构,以及它们的超导特性,可以根据所使用的硼粉和不锈钢容器中反应物的特殊排列来定制。讨论了不同形状的原型器件的超导特性。这些制造的实际应用,作为轴承的永磁体或电流引线,将参考其他超导体选项进行讨论。使用这种材料的预期温度范围将在15K到30K之间,这就要求开发可靠和廉价的低温系统。
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引用次数: 12
Thermal and Mechanical Properties of Poly‐Dicyclopentadiene (DCPD) at Cryogenic Temperatures 低温下聚双环戊二烯(DCPD)的热力学性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192354
V. Toplosky, R. Walsh
Poly‐diCylopentadiene (poly‐DCPD) resins are widely used because of their excellent physical and mechanical properties and their compatibility with various molding techniques. Poly‐DCPD’s ability to be rotationally molded has generated the potential for this crosslinked thermoset polymer to be used for cryogenic tanks. In turn, this has generated the need for cryogenic materials property data on these resins. In a collaborative research agreement between the National High Magnetic Field Laboratory (NHMFL) and Cymetech LLC, five different variations of poly‐DCPD have been thermally and mechanically characterized. Specifically, the tensile, compressive, shear and flexural properties have been measured at 77 K, as well as thermal contraction to 77 and 4 K. There are subtle differences in the properties between each formulation and larger discrepancies when compared to cryogenic data for other polymers. The thermal contraction to 77 K and elastic modulus are typical compared to other epoxies and polyester while the 77 K strength and elongation to failure are superior. The high strengths and elongations are good indicators that poly‐DCPD also has good toughness — an important property in many low temperature applications. This initial cryogenic properties database for poly‐DCPD allows it to be considered as a neat polymer in cryogenic applications, as well as an excellent matrix material for fiber reinforced composites in cryogenic applications.Poly‐diCylopentadiene (poly‐DCPD) resins are widely used because of their excellent physical and mechanical properties and their compatibility with various molding techniques. Poly‐DCPD’s ability to be rotationally molded has generated the potential for this crosslinked thermoset polymer to be used for cryogenic tanks. In turn, this has generated the need for cryogenic materials property data on these resins. In a collaborative research agreement between the National High Magnetic Field Laboratory (NHMFL) and Cymetech LLC, five different variations of poly‐DCPD have been thermally and mechanically characterized. Specifically, the tensile, compressive, shear and flexural properties have been measured at 77 K, as well as thermal contraction to 77 and 4 K. There are subtle differences in the properties between each formulation and larger discrepancies when compared to cryogenic data for other polymers. The thermal contraction to 77 K and elastic modulus are typical compared to other epoxies and polyester whi...
聚二氯戊二烯(Poly - DCPD)树脂由于其优异的物理和机械性能以及与各种成型技术的兼容性而被广泛应用。Poly - DCPD旋转成型的能力使这种交联热固性聚合物具有用于低温储罐的潜力。反过来,这又产生了对这些树脂的低温材料性能数据的需求。在国家高磁场实验室(NHMFL)和Cymetech LLC之间的合作研究协议中,五种不同的poly - DCPD变体进行了热特性和机械特性表征。具体来说,拉伸、压缩、剪切和弯曲性能已在77 K下测量,以及热收缩到77和4 K。与其他聚合物的低温数据相比,每种配方之间的性能存在细微差异,差异更大。与其他环氧树脂和聚酯相比,77k的热收缩和弹性模量是典型的,而77k的强度和断裂伸长率是优越的。高强度和高伸长率表明poly - DCPD也具有良好的韧性,这是许多低温应用的重要性能。聚- DCPD的初始低温性能数据库使其在低温应用中被认为是一种纯聚合物,以及在低温应用中纤维增强复合材料的优良基体材料。聚二氯戊二烯(Poly - DCPD)树脂由于其优异的物理和机械性能以及与各种成型技术的兼容性而被广泛应用。Poly - DCPD旋转成型的能力使这种交联热固性聚合物具有用于低温储罐的潜力。反过来,这又产生了对这些树脂的低温材料性能数据的需求。在国家高磁场实验室(NHMFL)和Cymetech LLC之间的合作研究协议中,五种不同的poly - DCPD变体进行了热特性和机械特性表征。具体来说,拉伸、压缩、剪切和弯曲性能已在77 K下测量,以及热收缩到77和4 K。与其他聚合物的低温数据相比,每种配方之间的性能存在细微差异,差异更大。与其他环氧树脂和聚酯相比,其热收缩率为77k,弹性模量为典型。
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引用次数: 15
Gas Evolution Measurements on Reactor Irradiated Advanced Fusion Magnet Insulation Systems 反应堆辐照先进聚变磁体绝缘系统的气体演化测量
Pub Date : 2006-04-21 DOI: 10.1063/1.2192369
K. Humer, E. Seidl, H. Weber, P. Fabian, S. Feucht, N. Munshi
Glass‐fiber reinforced plastics (GFRPs) are used as insulation materials for the superconducting magnet coils of the International Thermonuclear Experimental Reactor (ITER). The radiation environment present at the magnet location will lead to gas production, swelling and weight loss of the laminate, which may result in a pressure rise combined with undefined stresses on the magnet coil casing. Consequently, these effects are important parameters for the engineering and design criteria of superconducting magnet coil structures. In this study, newly developed epoxy and cyanate‐ester (CE) based S2‐glass fiber reinforced insulation systems were irradiated at ambient temperature in the TRIGA‐Mark II reactor (Vienna) to a fast neutron fluence of 1 and 5×1021 m−2 (E>0.1 MeV) prior to measurements of gas evolution, swelling and weight loss. The CE based laminates show increased radiation resistance, i.e. less gas evolution. The highest radiation hardness up to the highest dose was observed in a pure CE system. I...
玻璃纤维增强塑料(gfrp)被用作国际热核实验反应堆(ITER)超导磁体线圈的绝缘材料。磁铁位置的辐射环境会导致层压板产生气体、膨胀和失重,这可能会导致压力上升,并对磁铁线圈套管产生未定义的应力。因此,这些效应是超导磁体线圈结构工程和设计准则的重要参数。在这项研究中,新开发的基于环氧树脂和氰酸酯(CE)的S2 -玻璃纤维增强绝缘系统在TRIGA‐Mark II反应堆(维也纳)的环境温度下辐照到快中子流量为1和5×1021 m−2 (E>0.1 MeV),然后测量气体释放、膨胀和失重。CE基层压板显示出更高的抗辐射能力,即更少的气体逸出。在纯CE体系中观察到最高剂量下的最高辐射硬度。我…
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引用次数: 9
Deformation Behavior of AZ80 Wrought Magnesium Alloy at Cryogenic Temperatures AZ80变形镁合金在低温下的变形行为
Pub Date : 2006-04-21 DOI: 10.1063/1.2192349
W. Tang, Xiuyan Li, Enhou Han, Yong-bo Xu, Yiyi Li
The influence of temperature on the deformation and failure behavior of AZ80 wrought Mg alloy has been examined from 77K to 298K. It is found that the yield strength (YS) and ultimate strength (UTS) are increasing with the temperature decreasing, while the elongation is decreasing especial between 213K and 143K. Based on the mechanical tests, observation of environmental scanning electron microscope (ESEM) and transmission electron microscope (TEM), it is proposed that the alloy deforms mainly by slips and twins, but undergoes different mechanism of cleavage in the range of testing temperature. At T>213K, the alloy ductility is higher because the dislocations could pass through twins but pile up at precipitate phase: Mg17Al12, which causes the crack nucleate. At T<143K, the alloy ductility is lower because the dislocation slip are suppressed greatly and dislocations pile up at twins, and cause crack nucleate and expand along twins quickly. At 143K
在77K ~ 298K范围内,研究了温度对AZ80变形镁合金变形和失效行为的影响。结果表明,随着温度的降低,合金的屈服强度(YS)和极限强度(UTS)逐渐升高,而伸长率则逐渐降低,在213K ~ 143K之间表现得尤为明显。通过力学试验、环境扫描电镜(ESEM)和透射电镜(TEM)观察,认为合金变形主要以滑移和孪晶变形为主,但在试验温度范围内发生不同的解理机制。在tbbb213k时,由于位错可以穿过孪晶,但在Mg17Al12析出相堆积,导致裂纹形核,合金的塑性较高。在T<143K时,由于位错滑移受到极大抑制,位错在孪晶处堆积,导致裂纹迅速形核并沿孪晶扩展,合金塑性较低。在143 k
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引用次数: 4
Mechanical Properties of JK2LB at 4K JK2LB在4K时的力学性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192351
Jun Feng, J. Kim, R. Ballinger, J. Minervini
The jacket of the central solenoid (CS) for ITER is designed to support cyclic tension load generated by the electro‐magnetic hoop force during operation. Therefore, the CS jacket material requires high tensile strength, high ductility, and high resistance to fatigue. JK2LB was developed in Japan as a candidate material for CS jacket by using low carbon and boron additions in JK2. The preliminary data of mechanical property for JK2LB without cold work has shown improvement of ductility in comparison to JK2. As a routine multi‐party verification process, a series of new mechanical tests including tensile, fatigue crack growth and fracture toughness have been carried out at 4K in MIT for both the base metal and welds of JK2LB. The test materials provided by JAREI were subjected to various cold work and aging before testing. It is found that the cold work has significant impact on the properties. Large variation of the tensile properties is observed. It includes a few specimens with brittle‐like behavior. Th...
ITER中央螺线管(CS)的夹套设计用于支持运行期间由电磁环力产生的循环张力载荷。因此,CS护套材料要求高抗拉强度、高延展性和高抗疲劳性。JK2LB是日本通过在JK2中添加低碳和硼而开发的CS夹套候选材料。未经冷加工的JK2LB的力学性能初步数据表明,与JK2相比,JK2LB的延展性有所改善。作为一种常规的多方验证过程,在麻省理工学院的4K温度下对JK2LB的母材和焊缝进行了一系列新的力学测试,包括拉伸、疲劳裂纹扩展和断裂韧性。JAREI提供的试验材料在试验前经过各种冷加工和时效处理。研究发现,冷加工对材料的性能有显著影响。拉伸性能变化很大。它包括一些具有脆性行为的标本。Th……
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引用次数: 5
Development of 2T‐Class MgB2 Solenoid Coil 2T‐级MgB2电磁线圈的研制
Pub Date : 2006-04-21 DOI: 10.1063/1.2192408
K. Tanaka, H. Kitaguchi, H. Kumakura, H. Yamada, M. Hirakawa, M. Okada
This paper reports on the fabrication and testing of a MgB2 coil made using a wind & react method. We made a 130m‐long Fe/Cu‐composite sheathed, SiC‐doped MgB2‐superconducting round wire using an in‐situ PIT method. Using a 92m‐long wire, we fabricated a solenoid coil with 722 turns. In the coil test, we measured the Ic of the coil under various external fields and temperatures. The Ic of the coil reached 162 A (Je = 340 A/mm2) at 4.2 K and in the external field of 2 T. The coil generated 2.2 T (the center magnetic field, Bo); thus the total field reached 4.2 T. The Je exceeded 100 A/mm2 in the external fields of 4 T, 2.5 T, and 1 T at 15 K, 20 K, and 25 K, respectively. The Jc of the coil was almost equal to that of the short sample. This indicates that the 92m‐long wire has a very homogeneous Jc distribution.
本文报道了用风反应法制备的MgB2线圈的制作和试验。我们使用原位PIT方法制作了一根130米长的Fe/Cu复合护套、SiC掺杂的MgB2超导圆线。使用一根92米长的电线,我们制作了一个722圈的电磁线圈。在线圈测试中,我们测量了不同外场和温度下线圈的Ic。在4.2 K和2t的外场下,线圈的Ic达到162 A (Je = 340 A/mm2),线圈产生2.2 T(中心磁场Bo);总电场达到4.2 T,在15k、20k和25k条件下,4t、2.5 T和1t的外电场均超过100 A/mm2。线圈的Jc几乎等于短样品的Jc。这表明92米长的导线具有非常均匀的Jc分布。
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引用次数: 2
AC loss (50-200 Hz) in YBCO conductors with filaments and Cu stabilization 具有细丝和Cu稳定化的YBCO导体的交流损耗(50- 200hz)
Pub Date : 2006-04-21 DOI: 10.1063/1.2192437
M. Sumption, A. Contractor, S. Kawabata, E. Collings
AC loss measurements have been made on YBCO coated conductors in externally applied sinusoidal AC fields using the pick‐up coil method. Various arrangements of YBCO coated conductor have been measured at frequencies of 50 Hz, 75 Hz, 100 Hz, 150 Hz, and 200 Hz, with amplitudes ranging from 0 to 140 mT. Three different sets of IBAD‐based YBCO coated conductor were measured: (i) unfilamented conductors with Cu added either on one side only, or on both sides (as well as the edges), (ii) conductors with various numbers of filament, (iii) 4 mm wide conductors. All samples were 4 cm long and untwisted. The per cycle AC loss per unit length of conductor, displayed in the format Q/B (in J/T.m) vs. Bm. enabled separation of the eddy current and hysteretic components of the total loss, after which the results were analyzed and discussed. The resistivity of the interfilamentary connections were characterized and the results compared to expectation.
在外部正弦交流磁场中,用检波线圈法测量了YBCO涂层导体的交流损耗。在50hz, 75hz, 100hz, 150hz和200hz的频率范围内,测量了不同排列的YBCO涂层导体,幅度从0到140 mT。测量了三种不同的IBAD基YBCO涂层导体:(i)仅在一侧或两侧(以及边缘)添加Cu的无丝导体,(ii)具有不同数量的丝的导体,(iii) 4mm宽的导体。所有的样品都是4厘米长,没有扭曲。单位长度导体的每周期交流损耗,以Q/B (J/T.m) vs. Bm的格式显示。使总损耗的涡流和滞后分量分离,然后对结果进行分析和讨论。对纤维间连接的电阻率进行了表征,并与预期结果进行了比较。
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引用次数: 1
Effect of an Aging Heat Treatment on the 4 K Fracture and Fatigue Properties of 316LN and Haynes 242 时效热处理对316LN和Haynes 242合金4k断裂和疲劳性能的影响
Pub Date : 2006-04-21 DOI: 10.1063/1.2192340
R. Walsh, V. Toplosky, Ke Han, J. Miller
Since the introduction of the cable‐in‐conduit conductor (CICC) concept, a variety of alloys have been proposed for fabricating the jacket. The jacket provides primary containment of the liquid helium coolant and is typically also the primary structural component for the magnet coils. These functions create requirements for strength, toughness, fatigue crack resistance, and fabricability. When the CICC uses Nb3Sn superconductor, the conduit alloy must retain good mechanical properties after exposure to the superconductor’s reaction heat treatment. Here we present data from cryogenic fracture toughness and fatigue crack growth rate tests on 316LN and a Cr‐Mo‐Ni base super‐alloy (Haynes 242) at 4 K before and after the exposure to the heat treatment. These alloys are presently being considered as candidates for use in the next‐generation series connected hybrid magnet for the NHMFL. Both of the alloys are found to have adequate fatigue and fracture properties for the CICC application while the superalloy ha...
自引入电缆-导管导体(CICC)概念以来,已经提出了各种合金来制造护套。护套提供液氦冷却剂的主要容器,通常也是磁铁线圈的主要结构部件。这些功能产生了对强度、韧性、抗疲劳裂纹和可制造性的要求。采用Nb3Sn超导体时,管道合金经超导体反应热处理后,必须保持良好的力学性能。在这里,我们给出了316LN和Cr - Mo - Ni基超级合金(Haynes 242)在4 K热处理前后的低温断裂韧性和疲劳裂纹扩展速率测试数据。这些合金目前被认为是下一代串联混合磁体用于NHMFL的候选人。两种合金都具有足够的抗疲劳和断裂性能,而高温合金则具有较好的抗疲劳和断裂性能。
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引用次数: 12
期刊
Advances in cryogenic engineering
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