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The Superconducting Properties of High Density Bulk MgB2 Obtained by Reactive Liquid Mg Infiltration 反应性液态Mg浸润法制备高密度块状MgB2的超导性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192428
G. Giunchi
The reactive liquid Mg infiltration of Boron powders preforms is an easy technique to obtain high density and large superconducting bulk MgB2 manufacts, in which the supercurrents can percolate without obstacles by grains boundaries. The microstructure of these manufacts, as well their superconducting characteristics, can be tailored according to the Boron powders used and the particular arrangements of the reactants in a stainless steel container. A discussion of the superconducting characteristics of prototype manufacts of various shape will be given. The practical application of these manufacts, as permanent magnets for bearings or as current leads, will be discussed with reference to other superconducting bulk options. The expected temperature range for the use of this material will be between 15K and 30K and that calls for the development of reliable and cheap cryogenic systems.
硼粉预制件的反应液Mg渗透是制备高密度大体积超导MgB2的一种简便技术,其超电流可以不受晶界阻碍地渗透。这些产品的微观结构,以及它们的超导特性,可以根据所使用的硼粉和不锈钢容器中反应物的特殊排列来定制。讨论了不同形状的原型器件的超导特性。这些制造的实际应用,作为轴承的永磁体或电流引线,将参考其他超导体选项进行讨论。使用这种材料的预期温度范围将在15K到30K之间,这就要求开发可靠和廉价的低温系统。
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引用次数: 12
Effect of an Aging Heat Treatment on the 4 K Fracture and Fatigue Properties of 316LN and Haynes 242 时效热处理对316LN和Haynes 242合金4k断裂和疲劳性能的影响
Pub Date : 2006-04-21 DOI: 10.1063/1.2192340
R. Walsh, V. Toplosky, Ke Han, J. Miller
Since the introduction of the cable‐in‐conduit conductor (CICC) concept, a variety of alloys have been proposed for fabricating the jacket. The jacket provides primary containment of the liquid helium coolant and is typically also the primary structural component for the magnet coils. These functions create requirements for strength, toughness, fatigue crack resistance, and fabricability. When the CICC uses Nb3Sn superconductor, the conduit alloy must retain good mechanical properties after exposure to the superconductor’s reaction heat treatment. Here we present data from cryogenic fracture toughness and fatigue crack growth rate tests on 316LN and a Cr‐Mo‐Ni base super‐alloy (Haynes 242) at 4 K before and after the exposure to the heat treatment. These alloys are presently being considered as candidates for use in the next‐generation series connected hybrid magnet for the NHMFL. Both of the alloys are found to have adequate fatigue and fracture properties for the CICC application while the superalloy ha...
自引入电缆-导管导体(CICC)概念以来,已经提出了各种合金来制造护套。护套提供液氦冷却剂的主要容器,通常也是磁铁线圈的主要结构部件。这些功能产生了对强度、韧性、抗疲劳裂纹和可制造性的要求。采用Nb3Sn超导体时,管道合金经超导体反应热处理后,必须保持良好的力学性能。在这里,我们给出了316LN和Cr - Mo - Ni基超级合金(Haynes 242)在4 K热处理前后的低温断裂韧性和疲劳裂纹扩展速率测试数据。这些合金目前被认为是下一代串联混合磁体用于NHMFL的候选人。两种合金都具有足够的抗疲劳和断裂性能,而高温合金则具有较好的抗疲劳和断裂性能。
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引用次数: 12
Thermal and Mechanical Properties of Poly‐Dicyclopentadiene (DCPD) at Cryogenic Temperatures 低温下聚双环戊二烯(DCPD)的热力学性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192354
V. Toplosky, R. Walsh
Poly‐diCylopentadiene (poly‐DCPD) resins are widely used because of their excellent physical and mechanical properties and their compatibility with various molding techniques. Poly‐DCPD’s ability to be rotationally molded has generated the potential for this crosslinked thermoset polymer to be used for cryogenic tanks. In turn, this has generated the need for cryogenic materials property data on these resins. In a collaborative research agreement between the National High Magnetic Field Laboratory (NHMFL) and Cymetech LLC, five different variations of poly‐DCPD have been thermally and mechanically characterized. Specifically, the tensile, compressive, shear and flexural properties have been measured at 77 K, as well as thermal contraction to 77 and 4 K. There are subtle differences in the properties between each formulation and larger discrepancies when compared to cryogenic data for other polymers. The thermal contraction to 77 K and elastic modulus are typical compared to other epoxies and polyester while the 77 K strength and elongation to failure are superior. The high strengths and elongations are good indicators that poly‐DCPD also has good toughness — an important property in many low temperature applications. This initial cryogenic properties database for poly‐DCPD allows it to be considered as a neat polymer in cryogenic applications, as well as an excellent matrix material for fiber reinforced composites in cryogenic applications.Poly‐diCylopentadiene (poly‐DCPD) resins are widely used because of their excellent physical and mechanical properties and their compatibility with various molding techniques. Poly‐DCPD’s ability to be rotationally molded has generated the potential for this crosslinked thermoset polymer to be used for cryogenic tanks. In turn, this has generated the need for cryogenic materials property data on these resins. In a collaborative research agreement between the National High Magnetic Field Laboratory (NHMFL) and Cymetech LLC, five different variations of poly‐DCPD have been thermally and mechanically characterized. Specifically, the tensile, compressive, shear and flexural properties have been measured at 77 K, as well as thermal contraction to 77 and 4 K. There are subtle differences in the properties between each formulation and larger discrepancies when compared to cryogenic data for other polymers. The thermal contraction to 77 K and elastic modulus are typical compared to other epoxies and polyester whi...
聚二氯戊二烯(Poly - DCPD)树脂由于其优异的物理和机械性能以及与各种成型技术的兼容性而被广泛应用。Poly - DCPD旋转成型的能力使这种交联热固性聚合物具有用于低温储罐的潜力。反过来,这又产生了对这些树脂的低温材料性能数据的需求。在国家高磁场实验室(NHMFL)和Cymetech LLC之间的合作研究协议中,五种不同的poly - DCPD变体进行了热特性和机械特性表征。具体来说,拉伸、压缩、剪切和弯曲性能已在77 K下测量,以及热收缩到77和4 K。与其他聚合物的低温数据相比,每种配方之间的性能存在细微差异,差异更大。与其他环氧树脂和聚酯相比,77k的热收缩和弹性模量是典型的,而77k的强度和断裂伸长率是优越的。高强度和高伸长率表明poly - DCPD也具有良好的韧性,这是许多低温应用的重要性能。聚- DCPD的初始低温性能数据库使其在低温应用中被认为是一种纯聚合物,以及在低温应用中纤维增强复合材料的优良基体材料。聚二氯戊二烯(Poly - DCPD)树脂由于其优异的物理和机械性能以及与各种成型技术的兼容性而被广泛应用。Poly - DCPD旋转成型的能力使这种交联热固性聚合物具有用于低温储罐的潜力。反过来,这又产生了对这些树脂的低温材料性能数据的需求。在国家高磁场实验室(NHMFL)和Cymetech LLC之间的合作研究协议中,五种不同的poly - DCPD变体进行了热特性和机械特性表征。具体来说,拉伸、压缩、剪切和弯曲性能已在77 K下测量,以及热收缩到77和4 K。与其他聚合物的低温数据相比,每种配方之间的性能存在细微差异,差异更大。与其他环氧树脂和聚酯相比,其热收缩率为77k,弹性模量为典型。
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引用次数: 15
Deformation Behavior of AZ80 Wrought Magnesium Alloy at Cryogenic Temperatures AZ80变形镁合金在低温下的变形行为
Pub Date : 2006-04-21 DOI: 10.1063/1.2192349
W. Tang, Xiuyan Li, Enhou Han, Yong-bo Xu, Yiyi Li
The influence of temperature on the deformation and failure behavior of AZ80 wrought Mg alloy has been examined from 77K to 298K. It is found that the yield strength (YS) and ultimate strength (UTS) are increasing with the temperature decreasing, while the elongation is decreasing especial between 213K and 143K. Based on the mechanical tests, observation of environmental scanning electron microscope (ESEM) and transmission electron microscope (TEM), it is proposed that the alloy deforms mainly by slips and twins, but undergoes different mechanism of cleavage in the range of testing temperature. At T>213K, the alloy ductility is higher because the dislocations could pass through twins but pile up at precipitate phase: Mg17Al12, which causes the crack nucleate. At T<143K, the alloy ductility is lower because the dislocation slip are suppressed greatly and dislocations pile up at twins, and cause crack nucleate and expand along twins quickly. At 143K
在77K ~ 298K范围内,研究了温度对AZ80变形镁合金变形和失效行为的影响。结果表明,随着温度的降低,合金的屈服强度(YS)和极限强度(UTS)逐渐升高,而伸长率则逐渐降低,在213K ~ 143K之间表现得尤为明显。通过力学试验、环境扫描电镜(ESEM)和透射电镜(TEM)观察,认为合金变形主要以滑移和孪晶变形为主,但在试验温度范围内发生不同的解理机制。在tbbb213k时,由于位错可以穿过孪晶,但在Mg17Al12析出相堆积,导致裂纹形核,合金的塑性较高。在T<143K时,由于位错滑移受到极大抑制,位错在孪晶处堆积,导致裂纹迅速形核并沿孪晶扩展,合金塑性较低。在143 k
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引用次数: 4
Mechanical Properties of JK2LB at 4K JK2LB在4K时的力学性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192351
Jun Feng, J. Kim, R. Ballinger, J. Minervini
The jacket of the central solenoid (CS) for ITER is designed to support cyclic tension load generated by the electro‐magnetic hoop force during operation. Therefore, the CS jacket material requires high tensile strength, high ductility, and high resistance to fatigue. JK2LB was developed in Japan as a candidate material for CS jacket by using low carbon and boron additions in JK2. The preliminary data of mechanical property for JK2LB without cold work has shown improvement of ductility in comparison to JK2. As a routine multi‐party verification process, a series of new mechanical tests including tensile, fatigue crack growth and fracture toughness have been carried out at 4K in MIT for both the base metal and welds of JK2LB. The test materials provided by JAREI were subjected to various cold work and aging before testing. It is found that the cold work has significant impact on the properties. Large variation of the tensile properties is observed. It includes a few specimens with brittle‐like behavior. Th...
ITER中央螺线管(CS)的夹套设计用于支持运行期间由电磁环力产生的循环张力载荷。因此,CS护套材料要求高抗拉强度、高延展性和高抗疲劳性。JK2LB是日本通过在JK2中添加低碳和硼而开发的CS夹套候选材料。未经冷加工的JK2LB的力学性能初步数据表明,与JK2相比,JK2LB的延展性有所改善。作为一种常规的多方验证过程,在麻省理工学院的4K温度下对JK2LB的母材和焊缝进行了一系列新的力学测试,包括拉伸、疲劳裂纹扩展和断裂韧性。JAREI提供的试验材料在试验前经过各种冷加工和时效处理。研究发现,冷加工对材料的性能有显著影响。拉伸性能变化很大。它包括一些具有脆性行为的标本。Th……
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引用次数: 5
Gas Evolution Measurements on Reactor Irradiated Advanced Fusion Magnet Insulation Systems 反应堆辐照先进聚变磁体绝缘系统的气体演化测量
Pub Date : 2006-04-21 DOI: 10.1063/1.2192369
K. Humer, E. Seidl, H. Weber, P. Fabian, S. Feucht, N. Munshi
Glass‐fiber reinforced plastics (GFRPs) are used as insulation materials for the superconducting magnet coils of the International Thermonuclear Experimental Reactor (ITER). The radiation environment present at the magnet location will lead to gas production, swelling and weight loss of the laminate, which may result in a pressure rise combined with undefined stresses on the magnet coil casing. Consequently, these effects are important parameters for the engineering and design criteria of superconducting magnet coil structures. In this study, newly developed epoxy and cyanate‐ester (CE) based S2‐glass fiber reinforced insulation systems were irradiated at ambient temperature in the TRIGA‐Mark II reactor (Vienna) to a fast neutron fluence of 1 and 5×1021 m−2 (E>0.1 MeV) prior to measurements of gas evolution, swelling and weight loss. The CE based laminates show increased radiation resistance, i.e. less gas evolution. The highest radiation hardness up to the highest dose was observed in a pure CE system. I...
玻璃纤维增强塑料(gfrp)被用作国际热核实验反应堆(ITER)超导磁体线圈的绝缘材料。磁铁位置的辐射环境会导致层压板产生气体、膨胀和失重,这可能会导致压力上升,并对磁铁线圈套管产生未定义的应力。因此,这些效应是超导磁体线圈结构工程和设计准则的重要参数。在这项研究中,新开发的基于环氧树脂和氰酸酯(CE)的S2 -玻璃纤维增强绝缘系统在TRIGA‐Mark II反应堆(维也纳)的环境温度下辐照到快中子流量为1和5×1021 m−2 (E>0.1 MeV),然后测量气体释放、膨胀和失重。CE基层压板显示出更高的抗辐射能力,即更少的气体逸出。在纯CE体系中观察到最高剂量下的最高辐射硬度。我…
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引用次数: 9
Cryogenic Power Converter Module Performance 低温功率转换器模块性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192373
M. Hennessy, E. Mueller, O. Mueller, J. Park, R. R. Neal
Several cryogenic power converter modules were built and tested, including a low‐voltage, high‐power series based on Cryo‐MOSFETs and a high‐voltage, high‐power series based on Cryo‐IGBTs. Half‐bridge modules were manufactured and demonstrated in liquid nitrogen. The hardware is such that several half‐bridge modules can be interconnected to form a multiphase full bridge. Conduction losses in the MOSFET modules were reduced by more than an order of magnitude. Switching powers up to 340 kW were achieved in the MOSFET modules, and 720 kW was demonstrated in the IGBT series. These modules can be utilized in fully integrated, megawatt‐level cryogenic power systems.
研究人员构建并测试了几种低温功率转换器模块,包括基于Cryo - mosfet的低压高功率系列和基于Cryo - igbt的高压高功率系列。在液氮中制造并演示了半桥模块。硬件是这样的,几个半桥模块可以相互连接,形成一个多相全桥。MOSFET模块的传导损耗降低了一个数量级以上。在MOSFET模块中实现了高达340 kW的开关功率,在IGBT系列中演示了720 kW。这些模块可用于完全集成的兆瓦级低温电力系统。
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引用次数: 4
Superconducting Materials for Practical Applications 超导材料的实际应用
Pub Date : 2006-04-21 DOI: 10.1063/1.2192376
A. Campbell
Different applications of superconductors require different material properties. In this paper a short account is given of the relevant properties of the main materials of interest, BSCCO, MgB2 and YBCO. While BSCCO tapes are well established, the low irreversibility field limits their use at 77K while at 30K where they can stand reasonably high magnetic fields, the cheapness and ease of manufacture of MgB2 makes this new material a serious competitor. Bulk YBCO is also well developed and can produce high fields, but coated YBCO conductors have more applications if the cost can be brought down. AC losses are central to many applications. Since the loss/vol is proportional to Jc, but the volume of material required for a given magnet is inversely proportional to Jc the loss is independent of the material used and depends only on the width of the conductor. However using fine filaments requires that they be decoupled, and is in conflict with the need to avoid high angle grain boundaries across the current p...
超导体的不同应用需要不同的材料特性。本文简要介绍了主要感兴趣的材料BSCCO、MgB2和YBCO的相关性质。虽然BSCCO磁带已经很成熟,但低不可逆性场限制了它们在77K下的使用,而在30K下,它们可以承受相当高的磁场,MgB2的廉价和易于制造使这种新材料成为一个严重的竞争对手。块状YBCO也得到了很好的发展,可以产生高场,但如果能降低成本,涂层YBCO导体将有更多的应用。交流损耗是许多应用的核心。由于损耗/vol与Jc成正比,但给定磁铁所需的材料体积与Jc成反比,因此损耗与所用材料无关,仅取决于导体的宽度。然而,使用细丝要求它们去耦,并且与避免高角度晶界穿过电流的需求相冲突。
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引用次数: 0
The Effect on the Superconducting Properties of the Addition of Oxygen and Titanium to (Nb‐1Zr)3Sn Mono Element Internal Tin (MEIT) Conductors 氧和钛对(Nb‐1Zr)3Sn单元素内锡(MEIT)导体超导性能的影响
Pub Date : 2006-04-21 DOI: 10.1063/1.2192389
B. Zeitlin, E. Gregory, J. Marte, M. Benz, R. Scanlan, D. Dietderich
MEIT conductors fabricated with Nb‐1at%Zr filaments are evaluated as to the effect of the additions of Oxygen and Titanium introduced through the tin core. The effects as a function of time and temperature are evaluated through reaction area and grain size. Current density in the reaction layer is evaluated as a function of magnetic field and the reaction variables. In the temperature range of 850 °C to 900°C the addition of oxygen yielded the best results with layer current density of 1877 A/mm2 at 12 T. Fabrication experience with Nb‐1at%ZrOx filaments and solutions are also discussed.
用Nb‐1at%Zr长丝制备MEIT导体,评价了通过锡芯引入氧和钛的影响。通过反应面积和晶粒尺寸来评价其随时间和温度的影响。反应层中的电流密度是磁场和反应变量的函数。在850°C至900°C的温度范围内,氧的添加在12 t时产生的层电流密度为1877 A/mm2的最佳结果,并讨论了Nb - 1at%ZrOx长丝的制作经验和解决方案。
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引用次数: 4
Ic Enhancement Effect in Nb3Sn Coils Fabricated by the React‐and‐Wind Method 反应-风法制备Nb3Sn线圈中的Ic增强效应
Pub Date : 2006-04-21 DOI: 10.1063/1.2192392
K. Miyoshi, S. Awaji, H. Oguro, G. Nishijima, K. Watanabe
We found that critical current Ic, upper critical field Bc2 and critical temperature Tc are greatly enhanced by pre‐bending treatment for bronze route Nb3Sn superconductors, called the pre‐bending effect. The superconducting properties of Nb3Sn superconductor are sensitive to strain. However, a pre‐bending treatment of the Nb3Sn wire enhances the properties. This is because the treatment causes relaxation of the residual strain in the Nb3Sn layer in the wire.Interestingly, the pre‐bending effect also makes the Nb3Sn wire stronger against strain. By using this effect, the react‐and‐wind (R&W) method is expected to be applicable for the fabrication of the Nb3Sn superconducting coil. In this paper, the development of Nb3Sn coils made by the R&W method with the pre‐bending effect is described, and the efficiency of the cable assembled by the reacted Nb3Sn strands is discussed.
我们发现,预弯曲处理大大提高了铜路Nb3Sn超导体的临界电流Ic、上临界场Bc2和临界温度Tc,称为预弯曲效应。Nb3Sn超导体的超导性能对应变敏感。然而,对Nb3Sn线进行预弯曲处理可以提高其性能。这是因为处理引起了线材中Nb3Sn层残余应变的松弛。有趣的是,预弯曲效应也使Nb3Sn线抗应变更强。利用这一效应,R&W方法有望应用于Nb3Sn超导线圈的制备。本文介绍了用R&W法制备具有预弯曲效应的Nb3Sn线圈的研究进展,并讨论了反应后的Nb3Sn链组装电缆的效率。
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引用次数: 5
期刊
Advances in cryogenic engineering
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