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Notched Three‐Point Bend Testing of GFRP Woven Laminates at Cryogenic Temperatures and Analysis of Fracture and Damage Properties 低温下GFRP编织层压板的缺口三点弯曲试验及断裂和损伤性能分析
Pub Date : 2006-04-21 DOI: 10.1063/1.2192360
K. Sanada, Y. Shindo
The cryogenic damage and fracture properties of GFRP (glass fiber reinforced polymer) woven laminates has been investigated theoretically and experimentally. Three‐point bend tests were carried out with SENB (single‐edge‐notched bend) specimens at room temperature, liquid nitrogen temperature and liquid helium temperature. SENB specimens with different widths and thicknesses were prepared and tested. The results of SENB specimens were compared with those of CT (compact tension) specimens. A finite element analysis was also conducted to predict the response of the damaged SENB specimen. Effective elastic moduli were determined under the assumption of uniform strain inside the representative volume element. Hoffman failure criterion was selected as the criterion for fiber‐dominated failure, and matrix microcracking was detected by the maximum strain criterion. The virtual crack extension method was adopted to calculate strain energy release rate which leads to determination of stress intensity factor. In order to verify the model, correlations between experimental and analytical results were made, in terms of the load‐displacement response and the extent of damage growth. Reasonable agreements were found between the calculations and the experimental data.
对玻璃钢(GFRP)机织层合板的低温损伤和断裂性能进行了理论和实验研究。在室温、液氮温度和液氦温度下,用SENB(单刃缺口弯曲)试样进行三点弯曲试验。制备了不同宽度和厚度的SENB试样并进行了试验。将SENB试样的结果与CT(致密张力)试样的结果进行比较。通过有限元分析预测了受损SENB试件的响应。在假设具有代表性的体积单元内部应变均匀的情况下,确定了有效弹性模量。采用Hoffman破坏准则作为纤维主导破坏准则,采用最大应变准则检测基体微裂纹。采用虚拟裂纹扩展法计算应变能释放率,从而确定应力强度因子。为了验证该模型,在荷载-位移响应和损伤增长程度方面,将实验结果与分析结果进行了关联。计算结果与实验数据吻合较好。
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引用次数: 0
Static and Dynamic Performance of Newly Developed ITER Relevant Insulation Systems after Neutron Irradiation 新研制的ITER相关绝缘系统在中子辐照后的静态和动态性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192370
R. Prokopec, K. Humer, H. Fillunger, R. Maix, H. Weber
Fiber reinforced plastics will be used as insulation systems for the superconducting magnet coils of ITER. The fast neutron and gamma radiation environment present at the magnet location will lead to serious material degradation, particularly of the insulation. For this reason, advanced radiation‐hard resin systems are of special interest. In this study various R‐glass fiber / Kapton reinforced DGEBA epoxy and cyanate ester composites fabricated by the vacuum pressure impregnation method were investigated. All systems were irradiated at ambient temperature (340 K) in the TRIGA reactor (Vienna) to a fast neutron fluence of 1×1022 m−2 (E>0.1 MeV). Short‐beam shear and static tensile tests were carried out at 77 K prior to and after irradiation. In addition, tension‐tension fatigue measurements were used in order to assess the mechanical performance of the insulation systems under the pulsed operation conditions of ITER. For the cyanate ester based system the influence of interleaving Kapton layers on the st...
纤维增强塑料将用作ITER超导磁体线圈的绝缘系统。存在于磁体位置的快中子和伽马辐射环境将导致严重的材料退化,特别是绝缘。由于这个原因,先进的辐射硬树脂系统是特别感兴趣。采用真空加压浸渍法制备了各种R -玻璃纤维/卡普顿增强环氧树脂和氰酸酯复合材料。所有系统在TRIGA反应堆(维也纳)的环境温度(340 K)下辐照,快中子通量为1×1022 m−2 (E>0.1 MeV)。辐照前后分别在77k下进行短梁剪切和静拉伸试验。此外,为了评估绝缘系统在ITER脉冲运行条件下的力学性能,还使用了张力-张力疲劳测量。在氰酸酯基体系中,研究了卡普顿层的交错分布对反应性能的影响。
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引用次数: 4
Tantalum Sheet for Superconductor Diffusion Barrier Applications 超导体扩散势垒用钽片
Pub Date : 2006-04-21 DOI: 10.1063/1.2192399
S. Mathaudhu, K. Hartwig, R. E. Barber, T. Pyon
This report presents preliminary results of a project with the aim to fabricate fine‐grained tantalum sheet having a uniform microstructure that co‐deforms well with pure copper for superconductor diffusion barrier applications. Multi‐pass equal channel angular extrusion (ECAE) was used to refine the microstructure of 25 mm square cross‐section bars of Ta; rolling was used to convert the bars to 0.38 mm thick sheet. Cu‐Ta co‐deformation characteristics were evaluated by assembling and drawing experimental Cu‐Ta composite wires, containing the ECAE processed sheets, to 0.83 mm diameter and metallographically examining the thinned 2–4 micron Ta layer. The ECAE processed Ta sheet co‐deformed well with Cu, and was found to have a smaller recrystallized grain size, a narrower grain size distribution and a slightly higher hardness compared to commercial diffusion barrier grade Ta sheet. The favorable results encourage further work.
本报告介绍了一个项目的初步结果,该项目旨在制造具有均匀微观结构的细晶钽片,其与纯铜的共变形良好,用于超导扩散屏障应用。采用多道次等径角挤压法(ECAE)细化了25 mm方截面Ta棒材的微观结构;用轧制将棒材转化为0.38毫米厚的薄板。通过组装和拉伸含有ECAE加工板材的实验Cu - Ta复合丝至0.83 mm直径,并对薄的2-4微米的Ta层进行金相检查,评估了Cu - Ta共变形特性。ECAE可以很好地处理Ta片与Cu的共变形,并且发现与商业扩散屏障级Ta片相比,Ta片具有更小的再结晶晶粒尺寸,更窄的晶粒尺寸分布和稍高的硬度。良好的结果鼓励进一步的工作。
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引用次数: 3
Microstructure and Superconducting Properties of V-Based Laves Phase Compound Multifilamentary Wires Synthesized by a Rapidly Heating and Quenching Process to Hf-Zr/V Composite 快速加热淬火制备Hf-Zr/V复合材料V基laaves相复合多丝丝的组织与超导性能
Pub Date : 2006-04-21 DOI: 10.1063/1.2192401
Y. Hishinuma, A. Kikuchi, Y. Iijima, Y. Yoshida, T. Takeuchi, Kiyoshi Inoue, A. Nishimura
We have tried to study low activation superconducting materials of the many V‐based compound superconductors, and selected the V based Laves phase (V2(Hf,Zr)) compound because of its high upper critical field (Hc2) exceeding 20 T, its neutron irradiation resistance, and its low activation in the fusion reactor compared with those of Nb‐based A15 wires.The fabrication, microstructure and superconductivity of V2(Hf,Zr) multifilamentary wire synthesized by applying a rapidly‐heating/quenching (RHQ) and annealing process to the simple precursor using pure Hf and Zr mixture powder and pure V tube matrix were investigated. We found that a thick reaction layer was formed between the powder mixture filament and V matrix after the RHQ treatment and then it was increased with an increment of heating energy. Offset Tc values of samples were raised by increasing heating energy, and maximum Tc values occurred at 8.3 K. The maximum Jc value was obtained for a sample of post‐annealing at 600°C for 10 h. Jc dependence on...
我们尝试研究了许多V基化合物超导体的低活化超导材料,并选择了V基Laves相(V2(Hf,Zr))化合物,因为它的上临界场(Hc2)超过20 T,耐中子辐照,并且与Nb基A15导线相比,它在聚变反应堆中的活化率低。研究了以纯Hf和Zr混合粉末和纯V管为基体,采用快速加热/淬火(RHQ)和退火工艺合成的V2(Hf,Zr)多丝的制备工艺、微观结构和超导性。我们发现,经过RHQ处理后,粉末混合灯丝与V基之间形成了一层较厚的反应层,随着加热能量的增加,反应层逐渐增大。随着加热能量的增加,样品的偏移Tc值升高,在8.3 K时达到最大值。在600°C下退火10 h后获得了最大的Jc值。
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引用次数: 1
Magnetization Analysis of Magnesium Boride Wires 硼化镁丝的磁化分析
Pub Date : 2006-04-21 DOI: 10.1063/1.2192406
J. Cave, W. Zhu
Cycled applied field magnetization curves contain a wealth of information on critical current density and flux pinning that is not commonly exploited. Detailed magnetization data for magnesium boride wire cores have been analyzed for critical state model consistency. The iron‐sheathed silicon nitride doped magnesium boride wires were prepared from pure magnesium and boron powders with nano‐scale silicon nitride additions (MgB2−x(Si3N4)x/7 with x = 0 – 0.4). A subsequent short annealing heat treatment, 800 degrees C and of 1 hour duration in Argon, was applied to create the desired phase. Magnetization critical current densities were up to ∼340 kA/cm2 at 5K and 1T. Major and minor loop analysis will be described, for field sweeps up to 3 tesla at fixed temperatures and for temperature sweeps from 5K to 45K in fixed fields, with respect to parameters describing the critical state model.
循环外加磁场磁化曲线包含了大量关于临界电流密度和磁通钉接的信息,这些信息通常不被利用。对硼化镁铁芯的详细磁化数据进行了临界状态模型一致性分析。以纯镁和硼粉为原料,加入纳米级氮化硅(MgB2−x(Si3N4)x/7, x = 0 ~ 0.4),制备了铁包覆氮化硅掺杂硼化镁线。随后在氩气中进行800℃、持续1小时的短退火热处理,以产生所需的相。在5K和1T下,磁化临界电流密度高达~ 340 kA/cm2。根据描述临界状态模型的参数,将描述在固定温度下高达3特斯拉的场扫描和在固定场中从5K到45K的温度扫描的主回路和小回路分析。
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引用次数: 1
Long‐Length YBCO Coated Stainless Steel Tapes with High Critical Currents 具有高临界电流的长长度YBCO涂层不锈钢带
Pub Date : 2006-04-21 DOI: 10.1063/1.2192414
A. Usoskin, A. Rutt, J. Knoke, R. Dietrich
Progress in manufacturing 40m long YBCO coated stainless steel tapes by ion beam assisted deposition and by high‐rate pulsed laser deposition is reported. A critical current of 84.5A (77K, self field) was observed for end‐to‐end measurements of the 40m long tape based on a 1.05μm thick and 3.6mm wide YBCO film. This implies that a critical current of 235A per cm‐width is achieved by just a 1 μm thick YBCO layer. Analysis of the influence of local defects onto the integral U(I) curves allowed to formulate a general criterion for the homogeneity in terms of reduced number of tape parameters.A deterioration of tapes induced by mechanical torsion starts at a very high deformation degree: irreversibility threshold corresponds to 3000 angular degrees per meter for 4mm wide coated tape loaded with a 40N tensile axial force.
本文报道了离子束辅助沉积和高速率脉冲激光沉积制备40m长YBCO涂层不锈钢带的进展。在1.05μm厚、3.6mm宽的YBCO薄膜上,对40m长的胶带进行了端对端测量,发现临界电流为84.5A (77K,自场)。这意味着仅通过1 μm厚的YBCO层就可以实现每厘米宽235A的临界电流。通过分析局部缺陷对积分U(I)曲线的影响,可以根据减少的胶带参数数量制定均匀性的一般准则。机械扭转引起的胶带劣化始于非常高的变形程度:对于加载40N拉伸轴向力的4mm宽涂覆胶带,不可逆阈值对应于每米3000角度。
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引用次数: 10
Fabrication and Characterization of YBCO Coated Conductors by Inclined Substrate Deposition 斜基底沉积制备YBCO涂层导体及其表征
Pub Date : 2006-04-21 DOI: 10.1063/1.2192418
B. Ma, U. Balachandran, Yongli Xu, R. Bhattacharya
Inclined substrate deposition (ISD) is an effective method for rapid fabrication of high‐quality template layers for YBCO‐coated conductors. We have deposited biaxially textured ISD‐MgO films on flexible metallic tapes in a reel‐to‐reel system by electron‐beam evaporation at rapid deposition rates, 2–10 nm⋅s−1. Strontium ruthenium oxide (SRO) buffer and YBCO films were grown by pulsed laser deposition (PLD). Pole figure analysis of a meter‐long ISD‐MgO tape was carried out by X‐ray diffraction using a Bruker’s D8 DISCOVER equipped with GADDS (general area detection diffraction system). The c‐axis of the ISD‐MgO film was tilted away from substrate normal. A full‐width at half maximum (FWHM) of ≈10° was observed from the φ‐scan of the MgO (002) diffraction measured on samples deposited with 35° inclination angle. Surface morphology measured by atomic force microscopy revealed a roof‐tile shaped structure for the ISD‐MgO films. Through the use of the SRO buffer, biaxial alignment in the YBCO film deposited o...
倾斜衬底沉积(ISD)是快速制备高质量YBCO涂层导体模板层的有效方法。在卷筒对卷筒系统中,我们通过电子束蒸发在柔性金属带上以2-10 nm·s−1的快速沉积速率沉积了双轴纹理的ISD - MgO薄膜。采用脉冲激光沉积(PLD)法制备了锶钌氧化物(SRO)缓冲膜和YBCO薄膜。使用配备gadd(一般区域检测衍射系统)的布鲁克D8 DISCOVER,通过X射线衍射对一米长的ISD - MgO磁带进行了极图分析。ISD - MgO薄膜的c轴偏离衬底法线。在倾角为35°的样品上,通过对MgO(002)衍射进行φ扫描,观察到半峰全宽(FWHM)约为10°。原子力显微镜测量的表面形貌显示ISD - MgO薄膜呈屋顶瓦状结构。通过使用SRO缓冲液,在YBCO薄膜的双轴排列中沉积…
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引用次数: 2
The Force Relaxation in Levitating High Tc Superconductor 高Tc超导体悬浮中的力弛豫
Pub Date : 2006-04-21 DOI: 10.1063/1.2192429
E. Ito, Y. Komano, K. Sawa, M. Murakami, N. Sakai, I. Hirabayashi
In development of a flywheel energy storage system, electric power loss reduction is expected by using superconducting bearings. However, for realization of superconducting bearing strong levitation force, rotation loss reduction and axial descent reduction are required. It is known with axial descent reduction technology that a preload method is effective, whereas by this method, the levitation force becomes quite small compared with the normal levitation. We confirmed the performance of the preload method by experiment using a YBCO superconducting electromagnet. The preload method is improved and a method, which does not change the rate of the force relaxation and makes the levitation force larger than the existing preload method is proposed.
在飞轮储能系统的开发中,期望通过使用超导轴承来降低电力损耗。然而,要实现超导轴承的强悬浮力,需要减少旋转损失和轴向下降。轴向下降减少技术是已知的预加载方法是有效的,然而,通过这种方法,与正常的悬浮相比,悬浮力变得相当小。用YBCO超导电磁铁实验验证了预载方法的性能。对预紧力法进行了改进,提出了一种既不改变力松弛速率,又使悬浮力大于现有预紧力法的方法。
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引用次数: 0
A Low Hysteresis NiTiFe Shape Memory Alloy Based Thermal Conduction Switch 一种低迟滞氮铁形状记忆合金基热传导开关
Pub Date : 2006-04-21 DOI: 10.1063/1.2192327
J. Lemanski, V. Krishnan, R. Manjeri, W. Notardonato, R. Vaidyanathan
Shape memory alloys possess the ability to return to a preset shape by undergoing a solid state phase transformation at a particular temperature. This work reports on the development and testing of a low temperature thermal conduction switch that incorporates a NiTiFe shape memory element for actuation. The switch was developed to provide a variable conductive pathway between liquid methane and liquid oxygen dewars in order to passively regulate the temperature of methane. The shape memory element in the switch undergoes a rhombohedral or R‐phase transformation that is associated with a small hysteresis (typically 1–2 degrees C) and offers the advantage of precision control over a set temperature range. For the NiTiFe alloy used, its thermomechanical processing, subsequent characterization using dilatometry, differential scanning calorimetry and implementation in the conduction switch configuration are addressed.
形状记忆合金具有通过在特定温度下进行固态相变而恢复到预定形状的能力。这项工作报告了一种低温导热开关的开发和测试,该开关包含用于驱动的nitfe形状记忆元件。该开关是为了在液态甲烷和液态氧杜瓦之间提供一个可变的导电通路,以被动调节甲烷的温度。开关中的形状记忆元件经历了一个菱形或R相位的转变,这与一个小的滞后(通常为1-2摄氏度)有关,并提供了在设定温度范围内精确控制的优势。对于所使用的NiTiFe合金,其热机械加工,随后使用膨胀法,差示扫描量热法进行表征,并在传导开关配置中实现。
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引用次数: 22
Linear Thermal Expansion Measurements of Single Crystal Silicon for Validation of Interferometer Based Cryogenic Dilatometer 单晶硅线性热膨胀测量对干涉仪低温膨胀仪的验证
Pub Date : 2006-04-21 DOI: 10.1063/1.2192331
P. Karlmann, K. Klein, P. Halverson, R. Peters, M. Levine, D. Buren, M. Dudik
Linear thermal expansion measurements were performed for high‐purity P‐type single crystal silicon over a temperature range of 30K to 310K to validate the accuracy of JPL’s interferometer‐based Cryogenic Dilatometer Facility. This system was developed to better characterize thermophysical properties of precision engineering materials at cryogenic temperatures for space‐based optical systems. An accurate measurement of these properties is critical for the success of missions such as the James Webb Space Telescope and the Terrestrial Planet Finder Coronagraph where picometer‐level instabilities and thermal deformations impact performance. Results from these single crystal silicon measurements show a mean system repeatability of 4 ppb/K in the coefficient of thermal expansion (CTE) from 35K to 305K. Comparison with NIST/CODATA recommended values shows agreement of better than 2 ppb/K from 30K to 80K, better than 11 ppb/K from 80K to 165K, and better than 2 ppb/K from 165K to 305K.
在30K至310K的温度范围内对高纯度P型单晶硅进行了线性热膨胀测量,以验证JPL基于干涉仪的低温膨胀仪设备的准确性。该系统的开发是为了更好地表征空间光学系统中精密工程材料在低温下的热物理特性。这些特性的精确测量对于詹姆斯韦伯太空望远镜和类地行星探测日冕仪等任务的成功至关重要,其中皮米级的不稳定性和热变形会影响性能。这些单晶硅测量结果表明,在35K至305K的热膨胀系数(CTE)中,平均系统重复性为4 ppb/K。与NIST/CODATA推荐值的比较显示,从30K到80K的一致性优于2 ppb/K,从80K到165K的一致性优于11 ppb/K,从165K到305K的一致性优于2 ppb/K。
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引用次数: 12
期刊
Advances in cryogenic engineering
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