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Bulletin of the National Technical University "KhPI". Series: Chemistry, Chemical Technology and Ecology最新文献

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INVESTIGATION OF RECYCLING PROCESSES OF MIXED WASTE OF CONSUMPTION OF THERMOPLASTICS AND INTRODUCTION OF PRODUCTS ON THEIR BASIS IN INDUSTRY 热塑性塑料消费混合废弃物回收工艺的研究及在工业基础上的产品介绍
V. Avramenko, A. V. Blyznyuk, L. P. Pidhorna, Hanna Nikolaevna Cherkashina, O. M. Rassokha, Tamara Volodymirovna Kolomietz
Developed technologically compatible polymer composite materials with controlled properties on the basis of partially oxidized polyolefins and polystyrene, the level of properties which is not inferior, and in some cases 1.2-1.4 times higher than the level of properties of compositions on the basis of certified materials. Revealed that the secondary polyethylene and polystyrene plastics have smaller (in comparison with primary materials) the junction temperature in the highly elastic state and the interval of basketcount less resistance to deformation and, consequently, less ability to change modes of processing. Comparison of properties of primary plastics and plastics that were taken from the waste of consumption, shows that both polyethylene and polystyrene in the process of operation undergo significant property changes. To a greater extent these changes in the secondary materials compared to primary occur in the polyethylene (a gel-fraction, unsaturated the group consisting of oxygen, decreases the molecular weight and the melt flow rate). Studied the degree of aging and related natural changes of the chemical structure of recycled polyethylene and polystyrene plastics on the properties of composite materials. In addition to aging, a significant impact on the processes of thermo - and photo-oxidation has a supramolecular structure of polymers, which significantly influences the formation of a complex of operational properties of products. The dependence of viscosity of the mixture at different temperatures and the value of shear stress shows that there is a sharp decrease of melt viscosity that occurs in mixtures of polymers in a time close to the limit of compatibility. Reveals that the use of only partially oxidized polyethylene and polystyrene oxidized, or only one component (polyethylene or polystyrene) does not lead to a substantial increase in the strength characteristics.
在部分氧化聚烯烃和聚苯乙烯的基础上,开发了具有可控性能的技术相容高分子复合材料,其性能水平不低于,在某些情况下比认证材料基础上的组合物性能水平高1.2-1.4倍。结果表明,二次聚乙烯和聚苯乙烯塑料在高弹性状态下的结温较小(与初级材料相比),篮数间隔较小,抗变形能力较小,因此改变加工方式的能力较小。通过对原塑料和废旧塑料的性能比较,发现聚乙烯和聚苯乙烯在操作过程中都发生了明显的性能变化。与主要材料相比,次要材料中的这些变化在更大程度上发生在聚乙烯中(由氧组成的不饱和基团的凝胶分数降低了分子量和熔体流动速率)。研究了再生聚乙烯和聚苯乙烯塑料的老化程度及相关化学结构的自然变化对复合材料性能的影响。除老化外,显著影响热氧化和光氧化过程的还有聚合物的超分子结构,这显著影响产物操作性质络合物的形成。不同温度下混合物粘度与剪应力值的关系表明,聚合物混合物中熔体粘度在接近相容性极限的时间内急剧下降。揭示了仅使用部分氧化的聚乙烯和聚苯乙烯,或仅使用一种组分(聚乙烯或聚苯乙烯)不会导致强度特性的大幅增加。
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引用次数: 0
TREATMENT OF WASTEWATER OF POULTRY ABATTOIR BY COAGULATION 混凝法处理家禽屠宰场废水
Konstantyn Makhlay, M. Tseitlin, V. Raiko
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引用次数: 0
ADSORPTION OF ACETIC ACID AND THE PROMOTERS OF FORMATION OF PEROXO GROUPS ON PLATINUM AT HIGH ANODIC POTENTIALS 高阳极电位下铂对乙酸的吸附及过氧基形成促进剂的研究
Tetiana Andriyivna Bilous, Gennadiy Georgiyovych Tulsky, I. Chahine, Karina Nikolaevna Krotinova
{"title":"ADSORPTION OF ACETIC ACID AND THE PROMOTERS OF FORMATION OF PEROXO GROUPS ON PLATINUM AT HIGH ANODIC POTENTIALS","authors":"Tetiana Andriyivna Bilous, Gennadiy Georgiyovych Tulsky, I. Chahine, Karina Nikolaevna Krotinova","doi":"10.20998/0821.2019.01.01","DOIUrl":"https://doi.org/10.20998/0821.2019.01.01","url":null,"abstract":"","PeriodicalId":9407,"journal":{"name":"Bulletin of the National Technical University \"KhPI\". Series: Chemistry, Chemical Technology and Ecology","volume":"34 1","pages":""},"PeriodicalIF":0.0,"publicationDate":"2019-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"90918234","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
pH SENSOR WITH FREQUENCY OUTPUT FOR ECOLOGICAL CONTROL OF WATER pH传感器与频率输出,生态控制水
G. S. Popenko, Tatyana Borisivna Belikova, Vita Shumejko
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引用次数: 0
CONDITIONS OF FORMATION AND PHYSICO-CHEMICAL CHARACTERISTICS OF LITHIUM COORDINATION NITRATES OF LANTANOIDES LI3[LN2(NO3)9]∙3H2O (LN–LA–ND) 镧系化合物li3 [ln2 (no3)9]∙3h2o (ln - la - and)锂配位硝酸盐的形成条件及物理化学特性
O. Dryuchko, D. Storozhenko, N. Bunyakina, I. Ivanytska, V. Khaniukov, K. Kytaihora
Single-crystal samples were synthesized and a complex physicochemical characterization of the lithium coordination nitrates of the rare-earth elements of the cerium subgroup of the isostructural series Li 3 [Ln 2 (NO 3 ) 9 ]∙3H 2 O (Ln – La–Nd) was carried out in order to obtain reliable knowledge of the joint behavior of the constituent components and features of transformations in the systems of nitrate precursors during the formation with thermal activation (25–1000  o C) of multicomponent oxide REE-containing functional materials for various purposes with structure perovskite, garnet according to modern technologies with reproducible perfect stable properties. It has been revealed that the structure of this type of compounds is based on rare-earth oxygen polyhedra in one way or another connected in space. Ln 3+ ions play a dominant role in the complexation process, showing high coordination numbers of 12. The individuality of Ln-complexes in coordination nitrates is manifested: in a limited set of Ln-polyhedra; in the tendency of the complexing ion to create around itself a symmetrically organized coordination sphere; that the complexes with different composition and stoichiometry may correspond to the same, although significantly distorted coordination polyhedra. Li + cations in the structure formation of alkaline rare-earth nitrates can have a significant effect on the shape of Ln 3+ -polyhedra and on the spatial packing of their construction. The data obtained give a good reason to assume that the process of decomposition of crystalline alkaline rare-earth nitrates in technological objects during thermal activation begins with the breaking of alkaline metal-oxygen bonds. This fact is confirmed by the results of studies on the behavior of the above compounds in the range of 25–1000 °C by thermographic means. Thermograms of the samples are characterized by two, in addition to the initial state, temperature ranges of mass stabilization, corresponding to the formation of anhydrous complex nitrates and their thermolysis products at temperatures above 900 °C. The predominant phase of the final products is – LiLnO 2 .
合成了单晶样品,一个复杂的物理化学特征的锂协调硝酸盐稀土元素铈子群的同构的李系列3 (Ln 2(3号)9)∙3 h 2 O (Ln - La-Nd)是为了获得可靠的知识组成的联合行为组件和特性的转换系统中硝酸盐前体形成的热激活(25 - 1000 O C)多组分各种用途的含稀土氧化物功能材料具有钙钛矿、石榴石等结构,根据现代技术具有完美的可重复性和稳定性。这类化合物的结构是基于稀土氧多面体以这样或那样的方式在空间上连接。Ln 3+离子在络合过程中起主导作用,其配位数高达12。配合物在配位硝酸盐中的个性表现为:在有限的一组ln多面体中;络合离子倾向于在自身周围形成一个对称组织的配位球;不同组成和化学计量的配合物可能对应相同的配位多面体,但存在明显的畸变。碱性稀土硝酸盐结构形成中的Li +阳离子对l3+多面体的形状及其结构的空间排列有显著影响。所得数据有充分的理由认为,在热活化过程中,结晶型碱性稀土硝酸盐在工艺对象中的分解过程始于碱性金属-氧键的断裂。用热像仪对上述化合物在25-1000℃范围内的行为进行了研究,结果证实了这一事实。样品的热图特征除了初始状态外,还有两个质量稳定的温度范围,对应于在900℃以上的温度下无水络合硝酸盐及其热裂解产物的形成。最终产物的主要相是- LiLnO 2。
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引用次数: 1
ELECTROCHEMICAL SYNTHESIS OF POROUS CRYSTALLINE TANTAL OXIDE 多孔晶体氧化钽的电化学合成
S. Vodolazhchenko, L. V. Lyashok, S. Deribo, V. Gomozov
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引用次数: 0
THERMODYNAMICS, STATIC AND KINETICS OF SORBTION ON NATURAL SORBENTS 天然吸附剂吸附的热力学、静态和动力学
J. Gumnitsky, V. Sabadash
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引用次数: 0
DEVELOPMENT OF NEW FORMS OF CATALYTIC ELEMENTS IN AMMONIA OXIDATION REACTORS WITH A FIXED GRANULAR BED 固定颗粒床氨氧化反应器中催化元素新形态的研究
N. Masalitina, A. Savenkov, O. Bliznjuk, Olexandr Ogurtsov, Mikola Fedosovych Kleshchev
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引用次数: 0
ACTIVATION OF POROUS GRAPHITE ELECTRODES 多孔石墨电极的活化
K. Rutkovska, A. Tulskaya, I. Senkevich, A. Brovin, Aleksandr Yurievych Belozerov
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引用次数: 0
OBTAINING AND PROPERTIES OF CERAMIC PIGMENTS ON THE BASIS OF SPENT CATALYSTS 利用废催化剂制备陶瓷颜料及其性能研究
S. Avina, G. S. Pryvalova, O. Kobziev, Viktoria Dmytrivna Shtepa
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引用次数: 0
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Bulletin of the National Technical University "KhPI". Series: Chemistry, Chemical Technology and Ecology
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