Pub Date : 2024-06-05DOI: 10.1016/j.cryogenics.2024.103865
Pankaj Sagar , Kashif Akber
The work discusses on the behavior of dielectric properties of various commercially available insulators with respect to temperature (4.2 K to 300 K) and operating frequency range of 2.52 KHz to 500 KHz. A conventional parallel plate-based capacitor setup was designed and developed considering various conditions. The dielectric constant was found to be very dependent on the pre-breakdown partial discharges at low temperatures. At 4.2 K the discharges move far away from the electrodes and exert high electric stress on the sample under test, which results in the breakdown or the decrease in the dielectric strength. The relative permittivity () also decreased rapidly with the increase in frequency in most of the samples, this decrease is due to the reduction of space charge polarization effect. The correlation between the dielectric properties, operating frequencies and temperature have been studied in detailed.
该研究讨论了各种市售绝缘体在温度(4.2 K 至 300 K)和工作频率(2.52 KHz 至 500 KHz)范围内的介电特性。考虑到各种条件,我们设计并开发了一种基于平行板的传统电容器装置。在低温条件下,发现介电常数与击穿前的局部放电有很大关系。在 4.2 K 时,放电远离电极,对被测样品施加高电应力,导致击穿或介电强度下降。大多数样品的相对介电系数(ϵr)也随着频率的增加而迅速降低,这种降低是由于空间电荷极化效应的减弱。我们详细研究了介电特性、工作频率和温度之间的相关性。
{"title":"Studies on temperature dependent dielectric properties of some insulators down to liquid helium temperatures","authors":"Pankaj Sagar , Kashif Akber","doi":"10.1016/j.cryogenics.2024.103865","DOIUrl":"https://doi.org/10.1016/j.cryogenics.2024.103865","url":null,"abstract":"<div><p>The work discusses on the behavior of dielectric properties of various commercially available insulators with respect to temperature (4.2 K to 300 K) and operating frequency range of 2.52 KHz to 500 KHz. A conventional parallel plate-based capacitor setup was designed and developed considering various conditions. The dielectric constant was found to be very dependent on the pre-breakdown partial discharges at low temperatures. At 4.2 K the discharges move far away from the electrodes and exert high electric stress on the sample under test, which results in the breakdown or the decrease in the dielectric strength. The relative permittivity (<span><math><msub><mrow><mi>ϵ</mi></mrow><mrow><mi>r</mi></mrow></msub></math></span>) also decreased rapidly with the increase in frequency in most of the samples, this decrease is due to the reduction of space charge polarization effect. The correlation between the dielectric properties, operating frequencies and temperature have been studied in detailed.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"141 ","pages":"Article 103865"},"PeriodicalIF":2.1,"publicationDate":"2024-06-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141323225","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-06-01DOI: 10.1016/j.cryogenics.2024.103861
Zeyu Li, Weifeng Deng
The adsorption characteristics of the selected activated carbon have an important effect on the performance of the sub-Kelvin helium sorption cooler. In this paper, a test system for the adsorption amount of the carbons based on a G-M cooler was built, which has the advantages of being detachable and high gas seal performance. The adsorption isotherm of the three carbons (5.3 K-40 K, 0–0.6 MPa) for 4He were experimentally tested, and the data were fitted according to the Dubinin theory. In addition, the calculation methods of sorption cooler were summarized and a model of cooling power prediction was established. Based on the above theoretical model and experimental data, a carbon with high specific surface area and excellent adsorption properties was selected as filler, and a prototype of 4He sorption cooler was developed. The lowest temperature and holding time of the prototype are 923 mK and 8.47 h, respectively, in good agreement with the theoretical model. The model and the experimental method can provide reference for the design of sorption coolers at sub-Kelvin temperatures.
{"title":"Investigation on the adsorption characteristics of activated carbons in the sub-Kelvin 4He sorption cooler","authors":"Zeyu Li, Weifeng Deng","doi":"10.1016/j.cryogenics.2024.103861","DOIUrl":"10.1016/j.cryogenics.2024.103861","url":null,"abstract":"<div><p>The adsorption characteristics of the selected activated carbon have an important effect on the performance of the sub-Kelvin helium sorption cooler. In this paper, a test system for the adsorption amount of the carbons based on a G-M cooler was built, which has the advantages of being detachable and high gas seal performance. The adsorption isotherm of the three carbons (5.3 K-40 K, 0–0.6 MPa) for <sup>4</sup>He were experimentally tested, and the data were fitted according to the Dubinin theory. In addition, the calculation methods of sorption cooler were summarized and a model of cooling power prediction was established. Based on the above theoretical model and experimental data, a carbon with high specific surface area and excellent adsorption properties was selected as filler, and a prototype of <sup>4</sup>He sorption cooler was developed. The lowest temperature and holding time of the prototype are 923 mK and 8.47 h, respectively, in good agreement with the theoretical model. The model and the experimental method can provide reference for the design of sorption coolers at sub-Kelvin temperatures.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"140 ","pages":"Article 103861"},"PeriodicalIF":2.1,"publicationDate":"2024-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141132368","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-06-01DOI: 10.1016/j.cryogenics.2024.103856
Bo Liu , Wei Zhang , Feng Chen , Jie Cai , XunMing Wang , Yi Liu , JinLing Zhang , Qian Wang
The Multistage LNG cryogenic submersible pump is one of the crucial power equipment in LNG transport process. However, the high hydraulic losses and low efficiency of this pump make it necessary to optimize the structure of its impeller in order to reduce energy losses. In this study, an optimization strategy based on particle swarm optimization (PSO) and least squares support vector regression (LSSVR) machine is proposed to optimize the structure of impeller. The optimization of the impeller structure with the PSO-LSSVR method increased the head and efficiency of the LNG cryogenic submersible pump by 0.57% and 2.72%, respectively. Comparing the calculation results of PSO-LSSVR method with the CFD results, we found that the relative error between them don’t exceed 3%, which verified the calculation accuracy of the method. Then, an enstrophy dissipation theory is introduced to quantitatively analyze the pump energy loss. Comparing the impellers before and after optimization revealed that the maximum reduction in impeller energy loss was 18%.. The distribution and mechanism of vortex generation inside the impeller were analyzed with the Q-criterion and the relative vortex transport equation. The relative vortex transport equation revealed that the horseshoe vortex structure at the leading edge of the optimized impeller blade was suppressed, and the relative vortex stretching term and the Coriolis force term, which dominate the evolution of the vortex structure, were reduced. This study will provide related reference for the optimal design of Multistage LNG cryogenic submersible pumps.
{"title":"Performance prediction and optimization strategy for LNG multistage centrifugal pump based on PSO-LSSVR surrogate model","authors":"Bo Liu , Wei Zhang , Feng Chen , Jie Cai , XunMing Wang , Yi Liu , JinLing Zhang , Qian Wang","doi":"10.1016/j.cryogenics.2024.103856","DOIUrl":"10.1016/j.cryogenics.2024.103856","url":null,"abstract":"<div><p>The Multistage LNG cryogenic submersible pump is one of the crucial power equipment in LNG transport process. However, the high hydraulic losses and low efficiency of this pump make it necessary to optimize the structure of its impeller in order to reduce energy losses. In this study, an optimization strategy based on particle swarm optimization (PSO) and least squares support vector regression (LSSVR) machine is proposed to optimize the structure of impeller. The optimization of the impeller structure with the PSO-LSSVR method increased the head and efficiency of the LNG cryogenic submersible pump by 0.57% and 2.72%, respectively. Comparing the calculation results of PSO-LSSVR method with the CFD results, we found that the relative error between them don’t exceed 3%, which verified the calculation accuracy of the method. Then, an enstrophy dissipation theory is introduced to quantitatively analyze the pump energy loss. Comparing the impellers before and after optimization revealed that the maximum reduction in impeller energy loss was 18%.. The distribution and mechanism of vortex generation inside the impeller were analyzed with the Q-criterion and the relative vortex transport equation. The relative vortex transport equation revealed that the horseshoe vortex structure at the leading edge of the optimized impeller blade was suppressed, and the relative vortex stretching term and the Coriolis force term, which dominate the evolution of the vortex structure, were reduced. This study will provide related reference for the optimal design of Multistage LNG cryogenic submersible pumps.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"140 ","pages":"Article 103856"},"PeriodicalIF":2.1,"publicationDate":"2024-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.sciencedirect.com/science/article/pii/S0011227524000766/pdfft?md5=2152cc66659680421792bdbbee931fe8&pid=1-s2.0-S0011227524000766-main.pdf","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141039330","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-05-31DOI: 10.1016/j.cryogenics.2024.103863
Yunkai Tang , Donghui Liu , Shouhong Shan , Dongke Li , Xiaohui Lin , Shuiliang Zhen , Chao Zhang , Huadong Yong
Rare-earth (Re)Ba2Cu3O7−x (ReBCO) no-insulation (NI) coil is widely concerned due to its excellent electromagnetic and thermal properties. However, the presence of the turn-to-turn shunts in NI coils leads to that complexity of numerical simulation is increased. In this paper, a modified J model is proposed and the corresponding explicit–implicit hybrid algorithm is designed to calculate NI coils. The numerical results are in good agreement with the experimental data and the circuit model. The homogenization model is also proposed to simulate the large-scale NI coils in the background magnets. The modified J model has good accuracy and fast calculation speed, which can also be used to solve electromagnetic fields of insulation coils efficiently.
稀土(Re)Ba2Cu3O7-x(ReBCO)无绝缘(NI)线圈因其优异的电磁和热性能而受到广泛关注。然而,无绝缘线圈中匝间分流的存在导致数值模拟的复杂性增加。本文提出了一种改进的 J 模型,并设计了相应的显隐混合算法来计算 NI 线圈。数值结果与实验数据和电路模型十分吻合。同时还提出了同质化模型来模拟背景磁体中的大规模 NI 线圈。改进后的 J 模型具有良好的精度和快速的计算速度,也可用于高效求解绝缘线圈的电磁场。
{"title":"A modified J model for efficiently calculating the electromagnetic fields of ReBCO no-insulation pancake coils using an explicit–implicit hybrid algorithm","authors":"Yunkai Tang , Donghui Liu , Shouhong Shan , Dongke Li , Xiaohui Lin , Shuiliang Zhen , Chao Zhang , Huadong Yong","doi":"10.1016/j.cryogenics.2024.103863","DOIUrl":"https://doi.org/10.1016/j.cryogenics.2024.103863","url":null,"abstract":"<div><p>Rare-earth (Re)Ba<sub>2</sub>Cu<sub>3</sub>O<sub>7−x</sub> (ReBCO) no-insulation (NI) coil is widely concerned due to its excellent electromagnetic and thermal properties. However, the presence of the turn-to-turn shunts in NI coils leads to that complexity of numerical simulation is increased. In this paper, a modified J model is proposed and the corresponding explicit–implicit hybrid algorithm is designed to calculate NI coils. The numerical results are in good agreement with the experimental data and the circuit model. The homogenization model is also proposed to simulate the large-scale NI coils in the background magnets. The modified J model has good accuracy and fast calculation speed, which can also be used to solve electromagnetic fields of insulation coils efficiently.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"141 ","pages":"Article 103863"},"PeriodicalIF":2.1,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141243716","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-05-31DOI: 10.1016/j.cryogenics.2024.103864
Yu. Yu Puzina, A.P. Kryukov
The paper presents experimental data on the recovery heat flux during the boiling of superfluid helium (He II) on a flat heater located inside a U-shaped channel. The lower part of the channel is filled with monodisperse porous backfill. The paper includes information on the experimental cell, the data processing and synchronization technique, and the results of experiments conducted at different heater immersion depths and liquid temperatures. The paper presents also a mathematical description of heat transfer processes in superfluid helium for confined conditions. The calculated values are compared with experimental data. The effect of the porous backfill permeability on the recovery heat flux, including the case of a free channel is discussed. It is demonstrated that the increase in the heat flux in the channel initiates oscillations of the phase interface.
本文介绍了超流体氦(He II)在位于 U 形通道内的平面加热器上沸腾时的回收热通量的实验数据。通道下部填充了单分散多孔回填材料。论文包括有关实验单元、数据处理和同步技术的信息,以及在不同加热器浸入深度和液体温度下进行的实验结果。论文还对封闭条件下超流体氦的传热过程进行了数学描述。计算值与实验数据进行了比较。讨论了多孔回填渗透率对回收热通量的影响,包括自由通道的情况。研究表明,通道中热流的增加会引发相界面的振荡。
{"title":"Recovery heat flux at superfluid helium boiling in a U-shape channel with a porous backfill","authors":"Yu. Yu Puzina, A.P. Kryukov","doi":"10.1016/j.cryogenics.2024.103864","DOIUrl":"https://doi.org/10.1016/j.cryogenics.2024.103864","url":null,"abstract":"<div><p>The paper presents experimental data on the recovery heat flux during the boiling of superfluid helium (He II) on a flat heater located inside a U-shaped channel. The lower part of the channel is filled with monodisperse porous backfill. The paper includes information on the experimental cell, the data processing and synchronization technique, and the results of experiments conducted at different heater immersion depths and liquid temperatures. The paper presents also a mathematical description of heat transfer processes in superfluid helium for confined conditions. The calculated values are compared with experimental data. The effect of the porous backfill permeability on the recovery heat flux, including the case of a free channel is discussed. It is demonstrated that the increase in the heat flux in the channel initiates oscillations of the phase interface.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"141 ","pages":"Article 103864"},"PeriodicalIF":2.1,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141250899","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-05-31DOI: 10.1016/j.cryogenics.2024.103866
Yang Liu, Yuanwen Gao
A 3D finite element mechanical-electric numerical model was constructed to analyze the mechanical-electric performance of TSSC cables under torsional and radial loads at 77 K. The results indicate that when subjected to torsional load, the tapes in the outermost region within the slot of TSSC cable initially exhibit a decreasing trend, gradually expanding towards the inner region. The magnitude of this decrease progressively diminishes in the direction from outer to inner. Conversely, under radial loading, the normalized critical current density of the tapes in the innermost region within the slot initially decreases and expands outward along the radius. The tapes in the middle region remain mostly unaltered, while the outer region follows a pattern of increasing from inside out and reaches its peak at layers 28 and 29. Moreover, under torsional loads, TSSC cables display a higher normalized critical current density in the counterclockwise direction compared to the clockwise direction. To enhance the critical current density performance of TSSC cables under torsional loads, it is suggested to appropriately reduce the pitch, decrease the width of superconducting tape, increase the number of stacked tapes, enlarge the width of the slot and the diameter of the diversion trench, as well as increase the inner diameter while decreasing the outer diameter of the helical core. The choice of material for helical cores is not significantly impactful. On the other hand, under radial loads, factors such as tape width, number of stacked tapes, slot width, diversion trench diameter, and inner and outer diameters of the helical core have similar effects. Additionally, increasing the pitch length or adding more slots can enhance the critical current density performance of TSSC cables. Selecting different materials for the helical core also contributes positively to this improvement.
{"title":"Variations in critical current density of TSSC cable under torsional and radial loads","authors":"Yang Liu, Yuanwen Gao","doi":"10.1016/j.cryogenics.2024.103866","DOIUrl":"https://doi.org/10.1016/j.cryogenics.2024.103866","url":null,"abstract":"<div><p>A 3D finite element mechanical-electric numerical model was constructed to analyze the mechanical-electric performance of TSSC cables under torsional and radial loads at 77 K. The results indicate that when subjected to torsional load, the tapes in the outermost region within the slot of TSSC cable initially exhibit a decreasing trend, gradually expanding towards the inner region. The magnitude of this decrease progressively diminishes in the direction from outer to inner. Conversely, under radial loading, the normalized critical current density of the tapes in the innermost region within the slot initially decreases and expands outward along the radius. The tapes in the middle region remain mostly unaltered, while the outer region follows a pattern of increasing from inside out and reaches its peak at layers 28 and 29. Moreover, under torsional loads, TSSC cables display a higher normalized critical current density in the counterclockwise direction compared to the clockwise direction. To enhance the critical current density performance of TSSC cables under torsional loads, it is suggested to appropriately reduce the pitch, decrease the width of superconducting tape, increase the number of stacked tapes, enlarge the width of the slot and the diameter of the diversion trench, as well as increase the inner diameter while decreasing the outer diameter of the helical core. The choice of material for helical cores is not significantly impactful. On the other hand, under radial loads, factors such as tape width, number of stacked tapes, slot width, diversion trench diameter, and inner and outer diameters of the helical core have similar effects. Additionally, increasing the pitch length or adding more slots can enhance the critical current density performance of TSSC cables. Selecting different materials for the helical core also contributes positively to this improvement.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"141 ","pages":"Article 103866"},"PeriodicalIF":2.1,"publicationDate":"2024-05-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141243715","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-05-26DOI: 10.1016/j.cryogenics.2024.103862
Niannian Dai , Peng Jia , Qianxi Qu , Huan Chen , Liguo Wang , Yaran Shi , Rendong Guo , Dong Xu , Laifeng Li
To study the separation of helium isotopes by cryogenic adsorption, figuring out the adsorption characteristics of helium isotopes at low temperature is necessary. In this paper, a cryogenic adsorption measurement device has been established. It consists of a cryostat with a GM Cryocooler as cold source, a Setaram gas sorption instrument and a temperature controller. The helium-4 adsorption isotherms were studied under different temperatures and pressures (15–300 K, 0–1.5 MPa) by volumetric method. The results showed that a little helium was adsorbed by activated carbon at 300 K and 77 K. The amount of adsorbed helium increased with the temperature decreased from 20 K to 15 K. At pressures lower than 0.2 bar, the adsorption capacity increased rapidly as the pressure increased. Besides, the isosteric heats of adsorption were obtained, which was around 515 J/mol and changed little. Moreover, the cryogenic adsorption results were analyzed by Langmuir model and Toth model.
要研究低温吸附分离氦同位素,就必须弄清氦同位素在低温下的吸附特性。本文建立了一个低温吸附测量装置。它由一个以 GM Cryocooler 为冷源的低温恒温器、一个 Setaram 气体吸附仪和一个温度控制器组成。在不同温度和压力(15-300 K,0-1.5 MPa)下,采用体积法研究了氦-4 吸附等温线。结果表明,在 300 K 和 77 K 条件下,活性炭能吸附少量氦气;随着温度从 20 K 降至 15 K,氦气的吸附量增加。此外,还得到了等效吸附热,吸附热约为 515 J/mol,且变化不大。此外,还利用 Langmuir 模型和 Toth 模型对低温吸附结果进行了分析。
{"title":"The adsorption characteristics of helium under low temperature","authors":"Niannian Dai , Peng Jia , Qianxi Qu , Huan Chen , Liguo Wang , Yaran Shi , Rendong Guo , Dong Xu , Laifeng Li","doi":"10.1016/j.cryogenics.2024.103862","DOIUrl":"https://doi.org/10.1016/j.cryogenics.2024.103862","url":null,"abstract":"<div><p>To study the separation of helium isotopes by cryogenic adsorption, figuring out the adsorption characteristics of helium isotopes at low temperature is necessary. In this paper, a cryogenic adsorption measurement device has been established. It consists of a cryostat with a GM Cryocooler as cold source, a Setaram gas sorption instrument and a temperature controller. The helium-4 adsorption isotherms were studied under different temperatures and pressures (15–300 K, 0–1.5 MPa) by volumetric method. The results showed that a little helium was adsorbed by activated carbon at 300 K and 77 K. The amount of adsorbed helium increased with the temperature decreased from 20 K to 15 K. At pressures lower than 0.2 bar, the adsorption capacity increased rapidly as the pressure increased. Besides, the isosteric heats of adsorption were obtained, which was around 515 J/mol and changed little. Moreover, the cryogenic adsorption results were analyzed by Langmuir model and Toth model.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"141 ","pages":"Article 103862"},"PeriodicalIF":2.1,"publicationDate":"2024-05-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141308577","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Cryogenic distillation is a significant method for producing pure oxygen and nitrogen gas. In the past, due to the high cost and difficulty of conducting cryogenic experiments, the structured packings used in cryogenic distillation are mainly developed and designed by referring to the testing results of room-temperature fluids. The real flow characteristics of cryogenic fluids on structured packings, such as flow pattern and wettability which significantly determines the distillation performance, have seldom been revealed. In this study, with the help of a three-dimensional CFD model and a visual experimental setup, the liquid nitrogen (LN2) flow characteristics within the geometric unit of a 45° inclined packing element were revealed detailedly under different liquid loads and crimping angles. Comparison studies were also conducted to show the different film flow characteristics between water and LN2. Additionally, optimization of the crimping angles based on 250Y structured packing was explored. Both simulation and experiment show that the flow pattern and wetting mechanism of the hydraulic test on water are different from those of LN2 in the actual cryogenic distillation. The LN2 has much better film flow performance than water due to its different physical properties. In addition, it is found that the crimping angle has a significant effect on the wetting area ratio. For LN2, the crimping angle of 90° can basically result in a high enough wetting area ratio, while for water, the crimping angle as large as 120° is needed to achieve a high wetting area ratio. It shows that testing and designing the structured packing with water as the main working medium will bring apparent errors in real cryogenic distillation process.
{"title":"Numerical and experimental investigation of cryogenic fluid flow characteristics on corrugated packing surfaces","authors":"Xiaoqin Zhi, Yixuan Teng, Huabin Zhou, Gaoming Zhan, Limin Qiu","doi":"10.1016/j.cryogenics.2024.103860","DOIUrl":"https://doi.org/10.1016/j.cryogenics.2024.103860","url":null,"abstract":"<div><p>Cryogenic distillation is a significant method for producing pure oxygen and nitrogen gas. In the past, due to the high cost and difficulty of conducting cryogenic experiments, the structured packings used in cryogenic distillation are mainly developed and designed by referring to the testing results of room-temperature fluids. The real flow characteristics of cryogenic fluids on structured packings, such as flow pattern and wettability which significantly determines the distillation performance, have seldom been revealed. In this study, with the help of a three-dimensional CFD model and a visual experimental setup, the liquid nitrogen (LN<sub>2</sub>) flow characteristics within the geometric unit of a 45° inclined packing element were revealed detailedly under different liquid loads and crimping angles. Comparison studies were also conducted to show the different film flow characteristics between water and LN<sub>2</sub>. Additionally, optimization of the crimping angles based on 250Y structured packing was explored. Both simulation and experiment show that the flow pattern and wetting mechanism of the hydraulic test on water are different from those of LN<sub>2</sub> in the actual cryogenic distillation. The LN<sub>2</sub> has much better film flow performance than water due to its different physical properties. In addition, it is found that the crimping angle has a significant effect on the wetting area ratio. For LN<sub>2</sub>, the crimping angle of 90° can basically result in a high enough wetting area ratio, while for water, the crimping angle as large as 120° is needed to achieve a high wetting area ratio. It shows that testing and designing the structured packing with water as the main working medium will bring apparent errors in real cryogenic distillation process.</p></div>","PeriodicalId":10812,"journal":{"name":"Cryogenics","volume":"140 ","pages":"Article 103860"},"PeriodicalIF":2.1,"publicationDate":"2024-05-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"141084339","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"工程技术","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-05-11DOI: 10.1016/j.cryogenics.2024.103859
Yanan Li , Ping Liu , Peng Zhao , Ke Li , Wei Dai
The salt pill suspensions play a critical role in determining the performance of adiabatic demagnetization refrigerators (ADR). Kevlar suspensions are commonly used to hold the salt pill in place and to minimize the thermal leak. However, traditional solutions such as tensioning the Kevlar and fixing it on mechanical frame with the help of epoxy or running it around a pulley are quite challenging. This paper presents an innovative suspension using 3D printing technology and a polyether ether ketone (PEEK) multi-ring suspension has been designed and tested. Numerical analysis shows that a single piece of the suspension may contribute about 1.10 μW thermal leak between 4 K and 0.3 K. To test its performance, a two-stage ADR is built with Gadolinium Gallium Garnet (GGG) as the first stage and chromium potassium alum (CPA) salt pill as the second stage which is supported by the PEEK suspension. The GGG stage is mainly used to provide an initial temperature for CPA stage. Typically, starting from 1 K@4 T, a no-load lowest temperature of 66.1 mK is achieved at a demagnetization rate of 0.005 T/s in the experiments. The thermal leak of the PEEK suspension with and without 1 K heat sink has been analyzed and compared, with the former one showing a big reduction of the thermal leak. This paper confirms the feasibility of PEEK as an ADR suspension material and provides a potential 3D printing method for complex suspension designs.
盐丸悬浮液对绝热消磁制冷器(ADR)的性能起着至关重要的作用。通常使用凯夫拉悬浮液来固定盐丸,以减少热泄漏。然而,传统的解决方案,如拉紧凯夫拉纤维并借助环氧树脂将其固定在机械框架上,或使其围绕滑轮运行,都是相当具有挑战性的。本文介绍了一种使用 3D 打印技术的创新悬挂装置,并设计和测试了一种聚醚醚酮(PEEK)多环悬挂装置。数值分析表明,在 4 K 和 0.3 K 之间,单片悬浮液可产生约 1.10 μW 的热泄漏。为测试其性能,我们构建了一个两级 ADR,第一级为钆镓石榴石(GGG),第二级为铬钾明矾(CPA)盐丸,由 PEEK 悬浮液支撑。GGG 阶段主要用于为 CPA 阶段提供初始温度。通常情况下,从 1 K@4 T 开始,在实验中以 0.005 T/s 的退磁速率达到 66.1 mK 的空载最低温度。本文分析并比较了带 1 K 散热片和不带 1 K 散热片的 PEEK 悬浮液的热泄漏情况,前者大大减少了热泄漏。本文证实了 PEEK 作为 ADR 悬浮材料的可行性,并为复杂的悬浮设计提供了一种潜在的 3D 打印方法。
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