Pub Date : 2026-01-30eCollection Date: 2026-02-01DOI: 10.1016/j.fochx.2026.103620
Xinyi Huang, Yingmin Tian, Yufei Yang, Miaohua Zheng, Ling Wang, Shanshan Wang, Tao Zhang, Hongzhao Lu
To overcome the subjectivity of traditional bacon authentication, this study developed an objective discrimination framework integrating LC-MS/MS-based metabolomics with machine learning. Metabolomic profiling of bacon samples from pork belly (LRW) and pork rump (LRT) identified 100 differential metabolites common to both groups. The Kruskal-Wallis H test (p < 0.05) identified 75 significant features, which were further reduced to 22 key metabolites through random forest-based feature selection and low-variance filtering. Subsequently, a multidimensional evaluation of these 22 key metabolites (VIF < 75, label correlation >85%, and information gain = 1) highlighted four candidate discriminatory metabolites, including 6-hydroxyoctanoylcarnitine characterizing LRT, and dimethylethanolamine, xanthine, and ethyl hydrogen fumarate associated with LRW. Bidirectional validation using RF, KNN, SVM, and FNN models demonstrated robust discriminatory performance. This framework provides a basis for optimizing bacon production and offers a generalizable paradigm for data-driven biomarker discovery in meat products.
{"title":"LC-MS/MS-based metabolomics coupled with machine learning for screening candidate biomarkers in bacon.","authors":"Xinyi Huang, Yingmin Tian, Yufei Yang, Miaohua Zheng, Ling Wang, Shanshan Wang, Tao Zhang, Hongzhao Lu","doi":"10.1016/j.fochx.2026.103620","DOIUrl":"10.1016/j.fochx.2026.103620","url":null,"abstract":"<p><p>To overcome the subjectivity of traditional bacon authentication, this study developed an objective discrimination framework integrating LC-MS/MS-based metabolomics with machine learning. Metabolomic profiling of bacon samples from pork belly (LRW) and pork rump (LRT) identified 100 differential metabolites common to both groups. The Kruskal-Wallis H test (<i>p</i> < 0.05) identified 75 significant features, which were further reduced to 22 key metabolites through random forest-based feature selection and low-variance filtering. Subsequently, a multidimensional evaluation of these 22 key metabolites (VIF < 75, label correlation >85%, and information gain = 1) highlighted four candidate discriminatory metabolites, including 6-hydroxyoctanoylcarnitine characterizing LRT, and dimethylethanolamine, xanthine, and ethyl hydrogen fumarate associated with LRW. Bidirectional validation using RF, KNN, SVM, and FNN models demonstrated robust discriminatory performance. This framework provides a basis for optimizing bacon production and offers a generalizable paradigm for data-driven biomarker discovery in meat products.</p>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"103620"},"PeriodicalIF":8.2,"publicationDate":"2026-01-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12887885/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146164788","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Plant-based milk analogues are suitable substitutes for animal milk, more environmentally friendly, and sustainable. The microbiological stability, quality, anti-nutritional elements, and techno-functional properties of plant analogues and their proteins need to be considered. The type and concentration of reactive plasma species are influenced by parameters such as frequency, voltage, electrode spacing, treatment time, and gas composition. These factors regulate the efficacy of cold plasma in microbial disinfection and enzyme inactivation. The results indicate that cold plasma enhances the solubility, emulsifying properties, hydrophilicity, and foaming characteristics of plant-based analogues and proteins. In this study, the most potential sources of cold plasma and their impact on the functional characteristics of plant milk and proteins are thoroughly discussed. The work presents current insights into cold plasma for plant-based milk analogues and highlights their prospective applications, recent research, and developments in the field.
{"title":"Exploring the impact of atmospheric cold plasma technology on plant-based milk analogues and their proteins: A review.","authors":"Entesar Hanan, Shivangi Srivastava, Aamir Hussain Dar, Kshirod Kumar Dash, Vinay Kumar Pandey, Rafeeya Shams, Sharath Kumar, Ufaq Fayaz, Ayaz Mukarram Shaikh, Kovács Béla","doi":"10.1016/j.fochx.2026.103519","DOIUrl":"10.1016/j.fochx.2026.103519","url":null,"abstract":"<p><p>Plant-based milk analogues are suitable substitutes for animal milk, more environmentally friendly, and sustainable. The microbiological stability, quality, anti-nutritional elements, and techno-functional properties of plant analogues and their proteins need to be considered. The type and concentration of reactive plasma species are influenced by parameters such as frequency, voltage, electrode spacing, treatment time, and gas composition. These factors regulate the efficacy of cold plasma in microbial disinfection and enzyme inactivation. The results indicate that cold plasma enhances the solubility, emulsifying properties, hydrophilicity, and foaming characteristics of plant-based analogues and proteins. In this study, the most potential sources of cold plasma and their impact on the functional characteristics of plant milk and proteins are thoroughly discussed. The work presents current insights into cold plasma for plant-based milk analogues and highlights their prospective applications, recent research, and developments in the field.</p>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"103519"},"PeriodicalIF":8.2,"publicationDate":"2026-01-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12887886/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146164769","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-26eCollection Date: 2026-02-01DOI: 10.1016/j.fochx.2026.103592
Xiuhua He, Yanchi Zhou, Qiaozhu Wei, Weimin Zhang, Tian Li
As a high-value legume crop, the chemical basis underlying flavor and nutritional quality differences among cowpea (Vigna unguiculata L. Walp., Vu) varieties remains poorly understood, limiting targeted quality improvement. This study integrated headspace gas chromatography-ion mobility spectrometry with ultra-high-performance liquid chromatography-tandem mass spectrometry to comprehensively analyze metabolites in 14 Chinese cowpea varieties. A total of 174 volatile organic compounds were identified, with esters, heterocyclic compounds, and ketones accounting for 51.15% of the total. Principal component analysis and fingerprint clustering revealed variety-specific distribution patterns of volatile components, with the Vu-1 variety showing significant enrichment in β-pinene and 3-pentanol. Metabolomic analysis further identified 392 differentially expressed metabolites, revealing that amino acid metabolism and flavonoid metabolism are the core pathways determining varietal differences. This study systematically elucidates the chemical characteristics of cowpea varieties from a metabolomic perspective, providing important evidence for quality improvement and high-value utilization of legume crops.
作为一种高价值豆科作物,豇豆(Vigna unguiculata L. Walp)风味和营养品质差异的化学基础。(如Vu)品种仍然知之甚少,限制了有针对性的质量改进。本研究将顶空气相色谱-离子迁移谱法与超高效液相色谱-串联质谱法相结合,对14个豇豆品种的代谢产物进行了综合分析。共鉴定出174种挥发性有机化合物,其中酯类、杂环类和酮类化合物占51.15%。主成分分析和指纹聚类分析揭示了挥发性成分的分布规律,其中u-1品种显著富集β-蒎烯和3-戊醇。代谢组学分析进一步鉴定出392种差异表达代谢物,表明氨基酸代谢和类黄酮代谢是决定品种差异的核心途径。本研究从代谢组学角度系统阐明了豇豆品种的化学特性,为豆科作物的品质改良和高价值利用提供重要依据。
{"title":"Comprehensive volatile profiling and metabolomics analysis of cowpea.","authors":"Xiuhua He, Yanchi Zhou, Qiaozhu Wei, Weimin Zhang, Tian Li","doi":"10.1016/j.fochx.2026.103592","DOIUrl":"10.1016/j.fochx.2026.103592","url":null,"abstract":"<p><p>As a high-value legume crop, the chemical basis underlying flavor and nutritional quality differences among cowpea (<i>Vigna unguiculata</i> L. Walp., Vu) varieties remains poorly understood, limiting targeted quality improvement. This study integrated headspace gas chromatography-ion mobility spectrometry with ultra-high-performance liquid chromatography-tandem mass spectrometry to comprehensively analyze metabolites in 14 Chinese cowpea varieties. A total of 174 volatile organic compounds were identified, with esters, heterocyclic compounds, and ketones accounting for 51.15% of the total. Principal component analysis and fingerprint clustering revealed variety-specific distribution patterns of volatile components, with the Vu-1 variety showing significant enrichment in β-pinene and 3-pentanol. Metabolomic analysis further identified 392 differentially expressed metabolites, revealing that amino acid metabolism and flavonoid metabolism are the core pathways determining varietal differences. This study systematically elucidates the chemical characteristics of cowpea varieties from a metabolomic perspective, providing important evidence for quality improvement and high-value utilization of legume crops.</p>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"103592"},"PeriodicalIF":8.2,"publicationDate":"2026-01-26","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12887094/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146164808","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21DOI: 10.1016/j.fochx.2026.103568
Jiao Wang , Jiarong Hu , Boya Zhu , Xinyu Wang , Ao Zhang , Kai Liang , Wei Ding , Yu Zheng , Min Wang
Cereal vinegars constitute a distinctive category across different vinegar varieties in the world. Among them, Shanxi aged vinegar (SAV) is characterized by distinct flavor and sensory profiles. This study aimed to explore the main skeleton aroma-active compounds (AAC) and sensory profiles of SAV. Similar aroma profiles of most SAV samples exhibited by E-nose and GC–MS. A total of 196 volatile compounds were identified in SAV. Among these, 46 compounds were designated as key AACs (odor activity value (OAV) ≥ 1). 35 compounds were identified as main skeleton AACs by multiple statistical analysis. Aldehydes and sulfur-compounds dominated the key AACs, with high OAVs for 3-methyl-butanal and methionol. The sensory wheel and main skeleton AACs of SAV were first assessed using check-all-that-apply (CATA) and OAV. The correlation between key AACs and sensory properties was analyzed, revealing that most of these compounds exert a significant influence on the sensory attributes of the vinegar.
{"title":"The main skeleton aroma active compounds and sensory characteristics of Chinese geographical indication product: Shanxi aged vinegar","authors":"Jiao Wang , Jiarong Hu , Boya Zhu , Xinyu Wang , Ao Zhang , Kai Liang , Wei Ding , Yu Zheng , Min Wang","doi":"10.1016/j.fochx.2026.103568","DOIUrl":"10.1016/j.fochx.2026.103568","url":null,"abstract":"<div><div>Cereal vinegars constitute a distinctive category across different vinegar varieties in the world. Among them, Shanxi aged vinegar (SAV) is characterized by distinct flavor and sensory profiles. This study aimed to explore the main skeleton aroma-active compounds (AAC) and sensory profiles of SAV. Similar aroma profiles of most SAV samples exhibited by <em>E</em>-nose and GC–MS. A total of 196 volatile compounds were identified in SAV. Among these, 46 compounds were designated as key AACs (odor activity value (OAV) ≥ 1). 35 compounds were identified as main skeleton AACs by multiple statistical analysis. Aldehydes and sulfur-compounds dominated the key AACs, with high OAVs for 3-methyl-butanal and methionol. The sensory wheel and main skeleton AACs of SAV were first assessed using check-all-that-apply (CATA) and OAV. The correlation between key AACs and sensory properties was analyzed, revealing that most of these compounds exert a significant influence on the sensory attributes of the vinegar.</div></div>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"Article 103568"},"PeriodicalIF":8.2,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146037009","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Food waste poses global challenges to sustainability, human health, and the environment. Meat production significantly contributes to the byproducts generated during slaughter and processing. These by-products, which are rich in proteins and lipids, can be valorized via enzymatic hydrolysis or green extraction to produce bioactive peptides. These peptide activities and beneficial properties include antioxidant, antihypertensive, antimicrobial, and anti-inflammatory activities, and thus, have potential as functional foods and nutraceuticals. Notably, bioactive peptides can modulate gut microbiota by promoting beneficial species (e.g., Lactobacillus and Bifidobacterium) while suppressing pathogenic microbes. This interaction improves the integrity of the gut barrier, immune responses, and metabolic health. Integrating meat byproduct valorization within a circular economic framework does not reduce environmental pollution but also creates opportunities for sustainable food innovation. Despite advances in peptide extraction and application, key challenges remain, including large-scale production, taste optimization, and regulatory compliance. Future research should optimize production techniques, assess long-term health impacts, and explore industrial scalability.
{"title":"Harnessing meat byproducts for health: bioactive peptides to modulate gut microbiota and promote sustainability","authors":"Muhammad Waqar , Farhang Hameed Awlqadr , Qudrat Ullah , Amna Muneer , Nageen Mushtaq , Iqra Rafiq , Waqas Haider , Nimra Sajjad , Worawan Panpipat , Manat Chaijan , Temesgen Anjulo Ageru","doi":"10.1016/j.fochx.2026.103538","DOIUrl":"10.1016/j.fochx.2026.103538","url":null,"abstract":"<div><div>Food waste poses global challenges to sustainability, human health, and the environment. Meat production significantly contributes to the byproducts generated during slaughter and processing. These by-products, which are rich in proteins and lipids, can be valorized via enzymatic hydrolysis or green extraction to produce bioactive peptides. These peptide activities and beneficial properties include antioxidant, antihypertensive, antimicrobial, and anti-inflammatory activities, and thus, have potential as functional foods and nutraceuticals. Notably, bioactive peptides can modulate gut microbiota by promoting beneficial species (e.g., <em>Lactobacillus</em> and <em>Bifidobacterium</em>) while suppressing pathogenic microbes. This interaction improves the integrity of the gut barrier, immune responses, and metabolic health. Integrating meat byproduct valorization within a circular economic framework does not reduce environmental pollution but also creates opportunities for sustainable food innovation. Despite advances in peptide extraction and application, key challenges remain, including large-scale production, taste optimization, and regulatory compliance. Future research should optimize production techniques, assess long-term health impacts, and explore industrial scalability.</div></div>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"Article 103538"},"PeriodicalIF":8.2,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146036996","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-21eCollection Date: 2026-01-01DOI: 10.1016/j.fochx.2026.103546
Yuchen Deng, Shiyuan Chen, Jie Feng, Chuandong Fang, Jiancong Huo, Huimin Lin, Shucheng Liu, Soottawat Benjakul, Bin Zhang
[This corrects the article DOI: 10.1016/j.fochx.2025.103383.].
[这更正了文章DOI: 10.1016/j.fochx.2025.103383.]。
{"title":"Corrigendum to \"Multispectral study on the effects of capsaicin on myofibrillar proteins structure and functional characteristics in <i>Litopenaeus vannamei</i>\" [Food Chem.: X 32 (2025) 103383].","authors":"Yuchen Deng, Shiyuan Chen, Jie Feng, Chuandong Fang, Jiancong Huo, Huimin Lin, Shucheng Liu, Soottawat Benjakul, Bin Zhang","doi":"10.1016/j.fochx.2026.103546","DOIUrl":"https://doi.org/10.1016/j.fochx.2026.103546","url":null,"abstract":"<p><p>[This corrects the article DOI: 10.1016/j.fochx.2025.103383.].</p>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"33 ","pages":"103546"},"PeriodicalIF":8.2,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC12853039/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146104505","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Effects of peanut roasting conditioning before aqueous ethanol extraction of oil on the functional properties and structure of peanut protein isolate (PPI) and peanut protein concentrate (PPC) were investigated to facilitate value-added utilization of low-denatured meal from oil aqueous extraction. Except for solubility, the functional properties of PPI and PPC were maintained or improved after roasting. Specifically, the solubility (36.99%), foam stability (78.64%), emulsification activity index (27.37 m2/g) and emulsification stability index (23.18 min) of PPI were 1.54, 1.87, 1.17 and 1.26 times those of commercially available soy protein isolate (SPI), respectively. PPI exhibited reductions of 4.63% in α-helix and 6.03% in β-sheet, while PPC showed an increase of 0.67% in α-helix but a decrease of 7.04% in β-sheet. These results revealed that roasting induced structural disorders of peanut proteins, thereby improving their functionality, which provide a theoretical basis and new approach for improving protein properties and broadening their application.
{"title":"The improvement role of peanut roasting conditioning before oil extraction on protein functional properties","authors":"Qian Lu, Yubao Guo, Ruijie Zhao, Deyun Guo, Yihan Lei, Mengjiao Zeng","doi":"10.1016/j.fochx.2026.103570","DOIUrl":"10.1016/j.fochx.2026.103570","url":null,"abstract":"<div><div>Effects of peanut roasting conditioning before aqueous ethanol extraction of oil on the functional properties and structure of peanut protein isolate (PPI) and peanut protein concentrate (PPC) were investigated to facilitate value-added utilization of low-denatured meal from oil aqueous extraction. Except for solubility, the functional properties of PPI and PPC were maintained or improved after roasting. Specifically, the solubility (36.99%), foam stability (78.64%), emulsification activity index (27.37 m<sup>2</sup>/g) and emulsification stability index (23.18 min) of PPI were 1.54, 1.87, 1.17 and 1.26 times those of commercially available soy protein isolate (SPI), respectively. PPI exhibited reductions of 4.63% in α-helix and 6.03% in β-sheet, while PPC showed an increase of 0.67% in α-helix but a decrease of 7.04% in β-sheet. These results revealed that roasting induced structural disorders of peanut proteins, thereby improving their functionality, which provide a theoretical basis and new approach for improving protein properties and broadening their application.</div></div>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"Article 103570"},"PeriodicalIF":8.2,"publicationDate":"2026-01-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146037008","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-20DOI: 10.1016/j.fochx.2026.103573
Parham Joolaei Ahranjani, Giovanna Ferrentino
This study explores the oxidative stability of zein-derived based Pickering emulsions, focusing on the synergistic effects of interfacial particle concentration and phase-specific antioxidant delivery. Emulsions were prepared with varying ZNP concentrations (0.5–2.0%, w/v) in combination with xanthan gum as a co-stabilizer, to which l-ascorbic acid in aqueous phase and α-tocopherol in oil phase were added, individually or in combination. Emulsions with 0.5–1.0% ZNP remained physically stable during 10 days at 40 °C, while increasing ZNP to 2.0% significantly reduced droplet size (22.3 ± 0.55 μm to 16.1 ± 0.38 μm) and enhanced oxidative stability, increasing induction time from 4.07 ± 0.10 × 105 s to 5.15 ± 0.12 × 105 s. Antioxidants further improved the oxidative stability in a concentration-dependent manner, with α-tocopherol outperforming l-ascorbic acid. Notably, co-delivery of both antioxidants produced a synergistic effect, extending induction time to 6.06 ± 0.17 × 105 s and achieving an antioxidant efficiency of 25.04 ± 2.10 at 2.0% ZNP and 30 μM of each antioxidant. Synergism was confirmed by combination index (CI < 1) analysis. Isothermal calorimetry was used for continuous real-time observation of lipid oxidation and provided kinetic parameters including induction time (τ), inhibited and uninhibited oxidation rates (Rinh, Runi), oxidizability index (O.I.), and antioxidant efficiency (A.E.). These findings establish a novel approach to modulate oxidative stability through dual-phase antioxidant localization and interfacial nanoparticle design in emulsion-based food systems.
{"title":"Modulating oxidative stability of zein-stabilized Pickering emulsions via interfacial nanoparticle localization and dual-phase antioxidant synergism: a real-time kinetic assessment by isothermal calorimetry","authors":"Parham Joolaei Ahranjani, Giovanna Ferrentino","doi":"10.1016/j.fochx.2026.103573","DOIUrl":"10.1016/j.fochx.2026.103573","url":null,"abstract":"<div><div>This study explores the oxidative stability of zein-derived based Pickering emulsions, focusing on the synergistic effects of interfacial particle concentration and phase-specific antioxidant delivery. Emulsions were prepared with varying ZNP concentrations (0.5–2.0%, <em>w</em>/<em>v</em>) in combination with xanthan gum as a co-stabilizer, to which <span>l</span>-ascorbic acid in aqueous phase and α-tocopherol in oil phase were added, individually or in combination. Emulsions with 0.5–1.0% ZNP remained physically stable during 10 days at 40 °C, while increasing ZNP to 2.0% significantly reduced droplet size (22.3 ± 0.55 μm to 16.1 ± 0.38 μm) and enhanced oxidative stability, increasing induction time from 4.07 ± 0.10 × 10<sup>5</sup> s to 5.15 ± 0.12 × 10<sup>5</sup> s. Antioxidants further improved the oxidative stability in a concentration-dependent manner, with α-tocopherol outperforming <span>l</span>-ascorbic acid. Notably, co-delivery of both antioxidants produced a synergistic effect, extending induction time to 6.06 ± 0.17 × 10<sup>5</sup> s and achieving an antioxidant efficiency of 25.04 ± 2.10 at 2.0% ZNP and 30 μM of each antioxidant. Synergism was confirmed by combination index (CI < 1) analysis. Isothermal calorimetry was used for continuous real-time observation of lipid oxidation and provided kinetic parameters including induction time (τ), inhibited and uninhibited oxidation rates (R<sub>inh</sub>, R<sub>uni</sub>), oxidizability index (O.I.), and antioxidant efficiency (A.E.). These findings establish a novel approach to modulate oxidative stability through dual-phase antioxidant localization and interfacial nanoparticle design in emulsion-based food systems.</div></div>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"Article 103573"},"PeriodicalIF":8.2,"publicationDate":"2026-01-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146037007","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-20DOI: 10.1016/j.fochx.2026.103543
Ziyan Sun , Zhicong Song , Andong Zhou , Yongjian Lin , Jiahui Yao , Kevin H. Mayo , Yifa Zhou , Lin Sun
Polysaccharides, a primary component from Pleurotus eryngii (P. eryngii), have diverse biological activities. To systematically investigate structural features of these polysaccharides, we have developed a sequential extraction strategy with gradient-enhanced solvent-oriented purification that includes cold and hot water, enzymes assisted, dilute and concentrated alkali. Five polysaccharides CWP (0.19%), HWP (0.1%), EAP (0.14%), DAP (0.65%), CAP (0.34%) were obtained. The sequential extraction strategy developed here is practical, significantly improving the total extraction yield compared to single methods. After purification, we obtained eight homogeneous polysaccharides. Using several characterization techniques, we discovered that P. eryngii polysaccharides contained five structural types, including β-1,3-D-glucan, β-1,6-D-glucan, α-1,6-D-galactan, α-1,3-D-mannan, and a novel polysaccharide α-1,2-D-mannan, with ratios of 20:7:4.3:1.6:1. This study provides valuable insights into the structural diversity and relative abundance of polysaccharides in P. eryngii. Our findings provide a foundation for further investigation into their structure-activity relationships and potential applications.
{"title":"Polysaccharides from Pleurotus eryngii: sequential extraction and structural characterization","authors":"Ziyan Sun , Zhicong Song , Andong Zhou , Yongjian Lin , Jiahui Yao , Kevin H. Mayo , Yifa Zhou , Lin Sun","doi":"10.1016/j.fochx.2026.103543","DOIUrl":"10.1016/j.fochx.2026.103543","url":null,"abstract":"<div><div>Polysaccharides, a primary component from <em>Pleurotus eryngii</em> (<em>P. eryngii</em>), have diverse biological activities. To systematically investigate structural features of these polysaccharides, we have developed a sequential extraction strategy with gradient-enhanced solvent-oriented purification that includes cold and hot water, enzymes assisted, dilute and concentrated alkali. Five polysaccharides CWP (0.19%), HWP (0.1%), EAP (0.14%), DAP (0.65%), CAP (0.34%) were obtained. The sequential extraction strategy developed here is practical, significantly improving the total extraction yield compared to single methods. After purification, we obtained eight homogeneous polysaccharides. Using several characterization techniques, we discovered that <em>P. eryngii</em> polysaccharides contained five structural types, including β-1,3-D-glucan, β-1,6-D-glucan, α-1,6-D-galactan, α-1,3-D-mannan, and a novel polysaccharide α-1,2-D-mannan, with ratios of 20:7:4.3:1.6:1. This study provides valuable insights into the structural diversity and relative abundance of polysaccharides in <em>P. eryngii</em>. Our findings provide a foundation for further investigation into their structure-activity relationships and potential applications.</div></div>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"Article 103543"},"PeriodicalIF":8.2,"publicationDate":"2026-01-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146037003","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2026-01-20DOI: 10.1016/j.fochx.2026.103571
Feng Kong, Yue Li, Hongrun Lu, Yishuai Ding
Wheat bran, rich in fiber and bioactives, often impairs dough and final product quality upon incorporation. This study employed microwaving (MWB), steam explosion (SWB), and solid–state fermentation to modify wheat bran to improve its functionality in dough and noodles. All modifications reduced particle size (15.04%–29.77%) and increased bran surface area, improving dough water absorption. Notably, SWB drastically increased the content of phenolics (90.23%), flavonoids (2.65–fold), and water–extractable arabinoxylans (6.23–fold) while reducing bran crystallinity indices. The modifications differentially improved dough: MWB prolonged development and stability time, whereas SWB improved elasticity (increased G' and reduced tanδ) and disulfide bond content, indicating a strengthened gluten network. Consequently, noodles incorporating SWB achieved superior sensory scores, particularly in palatability and smoothness. Overall, steam explosion might be an effective bran modification strategy for balancing nutritional enrichment with enhanced dough rheology and noodle quality. These findings provide mechanistic and practical insights for cereal bran valorization.
{"title":"Comparative effects of wheat bran modifications by microwaving, steam explosion and solid-state fermentation on reconstituted dough properties and corresponding noodles qualities","authors":"Feng Kong, Yue Li, Hongrun Lu, Yishuai Ding","doi":"10.1016/j.fochx.2026.103571","DOIUrl":"10.1016/j.fochx.2026.103571","url":null,"abstract":"<div><div>Wheat bran, rich in fiber and bioactives, often impairs dough and final product quality upon incorporation. This study employed microwaving (MWB), steam explosion (SWB), and solid–state fermentation to modify wheat bran to improve its functionality in dough and noodles. All modifications reduced particle size (15.04%–29.77%) and increased bran surface area, improving dough water absorption. Notably, SWB drastically increased the content of phenolics (90.23%), flavonoids (2.65–fold), and water–extractable arabinoxylans (6.23–fold) while reducing bran crystallinity indices. The modifications differentially improved dough: MWB prolonged development and stability time, whereas SWB improved elasticity (increased G' and reduced tanδ) and disulfide bond content, indicating a strengthened gluten network. Consequently, noodles incorporating SWB achieved superior sensory scores, particularly in palatability and smoothness. Overall, steam explosion might be an effective bran modification strategy for balancing nutritional enrichment with enhanced dough rheology and noodle quality. These findings provide mechanistic and practical insights for cereal bran valorization.</div></div>","PeriodicalId":12334,"journal":{"name":"Food Chemistry: X","volume":"34 ","pages":"Article 103571"},"PeriodicalIF":8.2,"publicationDate":"2026-01-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146037002","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"农林科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}