We have successfully synthesized two new half-doped perovskites, MnV0.5Nb0.5O3 and MnV0.5Ta0.5O3, with unique small Mn2+ cations at the A site under high-temperature and high-pressure conditions (6...
{"title":"High-pressure synthesis of half-doped perovskites MnV0.5Nb0.5O3 and MnV0.5Ta0.5O3 with unusual A-site small Mn2+ cations","authors":"Xun Kang, Hiroaki Hayashi, Alexei A. Belik, Yoshihiro Tsujimoto, Kazunari Yamaura","doi":"10.1080/08957959.2023.2283543","DOIUrl":"https://doi.org/10.1080/08957959.2023.2283543","url":null,"abstract":"We have successfully synthesized two new half-doped perovskites, MnV0.5Nb0.5O3 and MnV0.5Ta0.5O3, with unique small Mn2+ cations at the A site under high-temperature and high-pressure conditions (6...","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-11-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138526768","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-02DOI: 10.1080/08957959.2023.2266555
Hamed Yaghooti, Abbas Pak
ABSTRACT In pressure sensors, pressure measurement is based on the movements of the elastic elements under different pressures. Since there is no elastic element able to move under low and high pressures, there is a serious limitation to measuring low and high pressures concurrently. This paper proposes an innovative mechanism for measuring high and low pressures concurrently. In the proposed mechanism, a variable-thickness diaphragm and a protective part were used to measure a broad range of pressures. The proposed mechanism was manufactured and the accurate pressure source was used to test the behavior of the mechanism under different pressures. Using this configuration raised the sensitivity and accuracy of high-range pressure sensors, and increased the turndown ratio to 1500 by employing a new elastic element. Employing this mechanism in pressure sensors leads to use one pressure sensor for measuring a broad range of pressure instead of using several distinct sensors.
{"title":"A novel mechanism for low- and high pressure measurement with variable-thickness diaphragm","authors":"Hamed Yaghooti, Abbas Pak","doi":"10.1080/08957959.2023.2266555","DOIUrl":"https://doi.org/10.1080/08957959.2023.2266555","url":null,"abstract":"ABSTRACT In pressure sensors, pressure measurement is based on the movements of the elastic elements under different pressures. Since there is no elastic element able to move under low and high pressures, there is a serious limitation to measuring low and high pressures concurrently. This paper proposes an innovative mechanism for measuring high and low pressures concurrently. In the proposed mechanism, a variable-thickness diaphragm and a protective part were used to measure a broad range of pressures. The proposed mechanism was manufactured and the accurate pressure source was used to test the behavior of the mechanism under different pressures. Using this configuration raised the sensitivity and accuracy of high-range pressure sensors, and increased the turndown ratio to 1500 by employing a new elastic element. Employing this mechanism in pressure sensors leads to use one pressure sensor for measuring a broad range of pressure instead of using several distinct sensors.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-10-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135901060","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-10-02DOI: 10.1080/08957959.2023.2267746
Zhiwei Liu, Caihua Yang, Song Guo, Feng Ding
ABSTRACTWe propose a novel structure of ultrahigh pressure die which consists of a split compression cylinder, a support ring, and steel wire winding, and the impacts of various steel wire winding methods on the ultimate cylinder pressure-bearing capacity are investigated. The investigations are conducted on the pre-stressing dies using the equal tensile stress (ETS), equal shear stress (ESS), and constant tangential stress (CTS) winding approaches. First, it is determined theoretically what the maximum cavity pressure and the necessary number of winding layers would be. The shear stresses of the cylinder and the support ring, the displacements of the cylinder, and the axial stresses of the steel wire layer are then examined using the finite element method. The results of the theoretical calculation and simulation are compared and discussed. The findings indicate that the ESS winding is a better option.KEYWORDS: Ultra-high pressuresteel wire windingfinite elementprestress Disclosure statementNo potential conflict of interest was reported by the author(s).Data availabilityThe data that support the findings of this study are available from the corresponding author upon reasonable request.Additional informationFundingThis research is supported by the National Science Foundation of China under grant number 51605007 and the National Science Foundation of Anhui Province under grant number1708085QE126, and we sincerely appreciate them.
{"title":"The study of steel wire winding split type ultrahigh pressure die based on different winding methods","authors":"Zhiwei Liu, Caihua Yang, Song Guo, Feng Ding","doi":"10.1080/08957959.2023.2267746","DOIUrl":"https://doi.org/10.1080/08957959.2023.2267746","url":null,"abstract":"ABSTRACTWe propose a novel structure of ultrahigh pressure die which consists of a split compression cylinder, a support ring, and steel wire winding, and the impacts of various steel wire winding methods on the ultimate cylinder pressure-bearing capacity are investigated. The investigations are conducted on the pre-stressing dies using the equal tensile stress (ETS), equal shear stress (ESS), and constant tangential stress (CTS) winding approaches. First, it is determined theoretically what the maximum cavity pressure and the necessary number of winding layers would be. The shear stresses of the cylinder and the support ring, the displacements of the cylinder, and the axial stresses of the steel wire layer are then examined using the finite element method. The results of the theoretical calculation and simulation are compared and discussed. The findings indicate that the ESS winding is a better option.KEYWORDS: Ultra-high pressuresteel wire windingfinite elementprestress Disclosure statementNo potential conflict of interest was reported by the author(s).Data availabilityThe data that support the findings of this study are available from the corresponding author upon reasonable request.Additional informationFundingThis research is supported by the National Science Foundation of China under grant number 51605007 and the National Science Foundation of Anhui Province under grant number1708085QE126, and we sincerely appreciate them.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":0.0,"publicationDate":"2023-10-02","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"135901708","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-23DOI: 10.1080/08957959.2023.2247542
S. Hunt
ABSTRACT In high pressure multi-anvil experiments X-radiography is used to ascertain strain in deforming samples because the tooling prevents optical or other direct observations of the sample. The processing of these X-radiographic images to determine bulk sample strain is one of the limiting factors to making measurements closer to the strains and strain-rates that occur during mantle convection or the passage of seismic waves. Typically, sample deformation in these experiments is tracked by the displacement of high-contrast marker foils in X-radiographs. X-radiographs are treated individually or pairwise in a multi-step process that tracks the displacement of marker foils during experiments. Here I develop a new algorithm, FoilTrack, that treats all the X-radiographic observations in a single-step process, resulting in improved accuracy and consistency of length changes determined from X-radiographic images, as well as providing more realistic parameter uncertainty. The improvements are demonstrated using data from small-strain sinusoidal deformation experiments.
{"title":"FoilTrack: a package to increase strain-resolution by improved X-radiographic image processing","authors":"S. Hunt","doi":"10.1080/08957959.2023.2247542","DOIUrl":"https://doi.org/10.1080/08957959.2023.2247542","url":null,"abstract":"ABSTRACT In high pressure multi-anvil experiments X-radiography is used to ascertain strain in deforming samples because the tooling prevents optical or other direct observations of the sample. The processing of these X-radiographic images to determine bulk sample strain is one of the limiting factors to making measurements closer to the strains and strain-rates that occur during mantle convection or the passage of seismic waves. Typically, sample deformation in these experiments is tracked by the displacement of high-contrast marker foils in X-radiographs. X-radiographs are treated individually or pairwise in a multi-step process that tracks the displacement of marker foils during experiments. Here I develop a new algorithm, FoilTrack, that treats all the X-radiographic observations in a single-step process, resulting in improved accuracy and consistency of length changes determined from X-radiographic images, as well as providing more realistic parameter uncertainty. The improvements are demonstrated using data from small-strain sinusoidal deformation experiments.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-08-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48734351","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-08-20DOI: 10.1080/08957959.2023.2248357
Y. Seryotkin, M. Ignatov
ABSTRACT The high pressure structural evolution of a natural fluorapophyllite-(K) K0.70(NH4)0.20 Ca3.97Na0.07[Al0.04Si7.96O20]F0.99·(H2O)8.05, Z = 2, a = 8.9757(2), c = 15.7920(2) Å, space group P4/mnc, from Nidym river, East Siberia, Russia, compressed in penetrating (ethanol:water 4:1 mixture) and non-penetrating (paraffin oil) media up to 4.7 GPa, was studied by single-crystal X-ray diffraction with a diamond anvil cell. The compressibility is identical in both media. At the initial stage the compression proceeds mainly within the plane (xy) and less along the z-axis; above 3 GPa the compression becomes almost isometric. Within the whole pressure range there are no signs of the symmetry lowering. The main pressure-induced effect on the tetrahedral layer consists in a cooperative rotation of the 4-fold rings, which provides the structure compression within the (xy) plane. The compression along the z-axis proceeds through the shortening of the interlayer distance, whereas the thickness of silicate layer remains almost unchanged.
{"title":"Structure evolution of fluorapophyllite-(K) under high pressure","authors":"Y. Seryotkin, M. Ignatov","doi":"10.1080/08957959.2023.2248357","DOIUrl":"https://doi.org/10.1080/08957959.2023.2248357","url":null,"abstract":"ABSTRACT The high pressure structural evolution of a natural fluorapophyllite-(K) K0.70(NH4)0.20 Ca3.97Na0.07[Al0.04Si7.96O20]F0.99·(H2O)8.05, Z = 2, a = 8.9757(2), c = 15.7920(2) Å, space group P4/mnc, from Nidym river, East Siberia, Russia, compressed in penetrating (ethanol:water 4:1 mixture) and non-penetrating (paraffin oil) media up to 4.7 GPa, was studied by single-crystal X-ray diffraction with a diamond anvil cell. The compressibility is identical in both media. At the initial stage the compression proceeds mainly within the plane (xy) and less along the z-axis; above 3 GPa the compression becomes almost isometric. Within the whole pressure range there are no signs of the symmetry lowering. The main pressure-induced effect on the tetrahedral layer consists in a cooperative rotation of the 4-fold rings, which provides the structure compression within the (xy) plane. The compression along the z-axis proceeds through the shortening of the interlayer distance, whereas the thickness of silicate layer remains almost unchanged.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-08-20","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"42677215","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-07-03DOI: 10.1080/08957959.2023.2233680
Robin Fréville, A. Dewaele, N. Guignot, G. Garbarino, M. Mezouar
ABSTRACT The equation of state of potassium iodide, KI, has been determined up to 156 GPa at 298 K by angular-dispersive X-ray diffraction in diamond-anvil-cell. Helium pressure transmitting medium was used to minimize non-hydrostatic stress on the sample. The B2 phase is stable at least between 2 and 156 GPa. Pressure–volume data were fitted using a Rydberg–Vinet equation of state. The volume, isothermal bulk modulus and its pressure derivative of B2-KI at ambient pressure are , GPa and . It allows using KI as a pressure calibrant in high pressure experiments.
{"title":"Equation of state of KI up to 150 GPa","authors":"Robin Fréville, A. Dewaele, N. Guignot, G. Garbarino, M. Mezouar","doi":"10.1080/08957959.2023.2233680","DOIUrl":"https://doi.org/10.1080/08957959.2023.2233680","url":null,"abstract":"ABSTRACT The equation of state of potassium iodide, KI, has been determined up to 156 GPa at 298 K by angular-dispersive X-ray diffraction in diamond-anvil-cell. Helium pressure transmitting medium was used to minimize non-hydrostatic stress on the sample. The B2 phase is stable at least between 2 and 156 GPa. Pressure–volume data were fitted using a Rydberg–Vinet equation of state. The volume, isothermal bulk modulus and its pressure derivative of B2-KI at ambient pressure are , GPa and . It allows using KI as a pressure calibrant in high pressure experiments.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-07-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"48921114","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-07-03DOI: 10.1080/08957959.2023.2230348
Logan J. Leinbach, Isaac R. Rhoden, K. Leinenweber, O. Andersson, A. Gordeeva, U. Häussermann
ABSTRACT A multianvil cell assembly with octahedral edge length 25 mm has been adapted for high pressure investigations involving water-rich environments up to 6.5 GPa and 400°C. Water-rich samples are confined in Teflon containers with a volume up to 300 mm3. Applicability tests were performed between 250 and 400°C by investigating the transformation of amorphous titania particles close to the rutile–TiO2-II (∼5 GPa) phase boundary, and the transformation of amorphous silica particles close to the quartz–coesite (∼2.5 GPa) and coesite–stishovite (∼7 GPa) phase boundaries. The performed experiments employed 25.4 mm tungsten carbide anvils with a truncation edge length of 15 mm. The sample pressure at loads approaching 820 t was estimated to be around 6.5 GPa. The large volume multianvil cell is expected to have broad and varied application areas, ranging from the simulation of geofluids to hydrothermal synthesis and conversion/crystal growth in aqueous environments at gigapascal pressures.
{"title":"Large volume multianvil cell assembly for hydrothermal synthesis and conversions up to 6.5 GPa and 400°C","authors":"Logan J. Leinbach, Isaac R. Rhoden, K. Leinenweber, O. Andersson, A. Gordeeva, U. Häussermann","doi":"10.1080/08957959.2023.2230348","DOIUrl":"https://doi.org/10.1080/08957959.2023.2230348","url":null,"abstract":"ABSTRACT A multianvil cell assembly with octahedral edge length 25 mm has been adapted for high pressure investigations involving water-rich environments up to 6.5 GPa and 400°C. Water-rich samples are confined in Teflon containers with a volume up to 300 mm3. Applicability tests were performed between 250 and 400°C by investigating the transformation of amorphous titania particles close to the rutile–TiO2-II (∼5 GPa) phase boundary, and the transformation of amorphous silica particles close to the quartz–coesite (∼2.5 GPa) and coesite–stishovite (∼7 GPa) phase boundaries. The performed experiments employed 25.4 mm tungsten carbide anvils with a truncation edge length of 15 mm. The sample pressure at loads approaching 820 t was estimated to be around 6.5 GPa. The large volume multianvil cell is expected to have broad and varied application areas, ranging from the simulation of geofluids to hydrothermal synthesis and conversion/crystal growth in aqueous environments at gigapascal pressures.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-07-03","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"49350821","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-06-24DOI: 10.1080/08957959.2023.2225702
Vili Grigorova, S. Shcheka, F. Salehi, K. Kamenev, S. Clark
ABSTRACT A 3D Finite Element Analysis model was developed to describe the temperature distribution inside a novel neutron transparent high-pressure sample assembly. The validity of the model was established by conducting experimental validation. The Finite Element Analysis model was utilised to evaluate the sample assembly’s temperature gradients and optimise its geometry and components. The results indicate that the discrepancy between the temperature recorded in the laboratory using thermocouples and the temperature calculated by the Finite Element Analysis model was only 4% under the assumption that the thermocouple was positioned in the middle of the sample assembly. The models further demonstrate that the Finite Element Analysis approach is a valuable tool for optimising the sample assembly by considering the impact of different materials and variations in the shape of its components.
{"title":"Use of finite element analysis for the thermal gradient determination of a neutron transparent high-pressure sample environment for neutron tomography","authors":"Vili Grigorova, S. Shcheka, F. Salehi, K. Kamenev, S. Clark","doi":"10.1080/08957959.2023.2225702","DOIUrl":"https://doi.org/10.1080/08957959.2023.2225702","url":null,"abstract":"ABSTRACT\u0000 A 3D Finite Element Analysis model was developed to describe the temperature distribution inside a novel neutron transparent high-pressure sample assembly. The validity of the model was established by conducting experimental validation. The Finite Element Analysis model was utilised to evaluate the sample assembly’s temperature gradients and optimise its geometry and components. The results indicate that the discrepancy between the temperature recorded in the laboratory using thermocouples and the temperature calculated by the Finite Element Analysis model was only 4% under the assumption that the thermocouple was positioned in the middle of the sample assembly. The models further demonstrate that the Finite Element Analysis approach is a valuable tool for optimising the sample assembly by considering the impact of different materials and variations in the shape of its components.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-06-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43377774","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-06-04DOI: 10.1080/08957959.2023.2218535
S. Rashchenko, M. Kolesnichenko, Anastasia O. Mikhno, A. Shatskiy
ABSTRACT Na-Ca double carbonates were found as the inclusions in ‘superdeep’ Juina diamonds and as the products of high pressure experiments and thus are regarded as the potential host of CO2 in the deep mantle. Recently, Na-rich carbonate (21.0% wt. of Na2O vs. 13.6% wt. of CaO) was reported as the product of experiment with carbonated eclogite treated at 21 GPa and 1200°C. Na/Ca ratio of this carbonate corresponds to Na4Ca(CO3)3 phase with cubic symmetry synthesized at 6 GPa. The stability of Na4Ca(CO3)3 at higher pressures has not been investigated yet. Herein, we report an in situ Raman study of Na4Ca(CO3)3 carbonate up to 11 GPa in order to reveal stability of its structure at mantle pressures. Obtained results strongly imply for reversible phase transition near 8 GPa associated with decrease of symmetry. The observed phase transition questions the stability of cubic Na4Ca(CO3)3 under conditions of mantle transition zone.
{"title":"High pressure Raman study of Na4Ca(CO3)3 from the ambient pressure to 11 GPa","authors":"S. Rashchenko, M. Kolesnichenko, Anastasia O. Mikhno, A. Shatskiy","doi":"10.1080/08957959.2023.2218535","DOIUrl":"https://doi.org/10.1080/08957959.2023.2218535","url":null,"abstract":"ABSTRACT Na-Ca double carbonates were found as the inclusions in ‘superdeep’ Juina diamonds and as the products of high pressure experiments and thus are regarded as the potential host of CO2 in the deep mantle. Recently, Na-rich carbonate (21.0% wt. of Na2O vs. 13.6% wt. of CaO) was reported as the product of experiment with carbonated eclogite treated at 21 GPa and 1200°C. Na/Ca ratio of this carbonate corresponds to Na4Ca(CO3)3 phase with cubic symmetry synthesized at 6 GPa. The stability of Na4Ca(CO3)3 at higher pressures has not been investigated yet. Herein, we report an in situ Raman study of Na4Ca(CO3)3 carbonate up to 11 GPa in order to reveal stability of its structure at mantle pressures. Obtained results strongly imply for reversible phase transition near 8 GPa associated with decrease of symmetry. The observed phase transition questions the stability of cubic Na4Ca(CO3)3 under conditions of mantle transition zone.","PeriodicalId":12864,"journal":{"name":"High Pressure Research","volume":null,"pages":null},"PeriodicalIF":2.0,"publicationDate":"2023-06-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"43882936","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
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