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Inhibitory effect of high hydrostatic pressure, nisin, and moderate heating on the inactivation of Paenibacillus sp. and Terribacillus aidingensis spores isolated from UHT milk 高静水压、乳酸链球菌肽和适度加热对超高温灭菌乳中分离的Paenibacillus sp.和Terrillus aidingensis孢子灭活的抑制作用
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1946054
S. Kmiha, C. Modugno, C. Aouadhi, H. Simonin, S. Méjri, J. Perrier-Cornet, A. Maaroufi
ABSTRACT The sensitivity of Paenibacillus sp. and Terribacillus aidingensis spores to combined action of HP, nisin and moderate heating were investigated for the first time. The results showed that the effect of HP on spores varies with pressure level, treatment temperature, spore species and presence of nisin. T. aidingensis spores were more resistant than Paenibacillus sp., whatever the treatment applied. The inactivation rates of both spore species did not exceed 2.7log (CFU/mL) after HP treatment at 600 MPa/50°C/10 min. However, a high synergistic effect of nisin and HP was observed after a treatment at 500 MPa/10 min/50°C with addition of nisin during HP and into the recovery medium, leading to 6log (CFU/mL) and 4log (CFU/mL) reduction for Paenibacillus and Terribacillus spores, respectively. Finally, the fraction of germinated spores by HP was measured and the results showed that germination induction is not the only underlying mechanisms of nisin sensitization by HP.
首次研究了Paenibacillus sp.和Terribacillus aidingensis孢子对HP、nisin和温和加热联合作用的敏感性。结果表明,HP对孢子的影响随压力水平、处理温度、孢子种类和nisin的存在而变化。无论施用何种处理,辅助芽孢杆菌孢子的抗性都强于芽孢杆菌。HP在600 MPa/50℃/10 min下处理后,两种孢子的失活率均不超过2.7log (CFU/mL)。然而,在500 MPa/10 min/50℃条件下,在HP和恢复培养基中添加nisin后,观察到nisin和HP的高度协同效应,导致Paenibacillus和Terribacillus孢子分别减少6log (CFU/mL)和4log (CFU/mL)。最后,我们测量了HP的萌发孢子的比例,结果表明萌发诱导并不是HP致敏nisin的唯一潜在机制。
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引用次数: 5
Refractive index of MgAl2O4 transparent ceramic under quasi-isentropic compression loading 准等熵压缩载荷下MgAl2O4透明陶瓷的折射率
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1940999
K. Bao, Xianfeng Zhang, Guiji Wang, T. Chong, Jia-jie Deng, D. Han, M. Tan
ABSTRACT The indirect method of obtaining in situ particle velocity of sample, under dynamic high-pressure loading experiments, generates an error due to the influence of rarefaction wave from the sample-window interface. Using the spinel as a window is an attractive method to reduce the error due to the total impedance matching of sample and window in the loading experiments of the spinel. To explore the possibility of the spinel as a window, ramp wave compression experiments were conducted to determine the refractive index of loading longitudinal stress range below 15.9 GPa. The result showed smooth particle velocity curve and linear relationship between refractive index and density. The effect of temperature on refractive index can be negligible, proved by analyzing the effect of temperature on polarizability. It is indicated that the spinel can be used as a window for loading experiments of the spinel and similar impedance materials.
摘要:在动态高压加载实验中,间接获取样品原位颗粒速度的方法由于样品-窗口界面的稀薄波的影响而产生误差。在尖晶石加载实验中,采用尖晶石作为窗口是一种很有吸引力的减小样品与窗口总阻抗匹配误差的方法。为了探索尖晶石作为窗口的可能性,进行了斜波压缩实验,确定了加载纵向应力范围在15.9 GPa以下的折射率。结果表明,粒子速度曲线平滑,折射率与密度呈线性关系。通过分析温度对偏振率的影响,证明了温度对折射率的影响可以忽略不计。结果表明,尖晶石可作为尖晶石及类似阻抗材料加载实验的窗口。
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引用次数: 1
High pressure stability of β-Zr: no evidence for isostructural phase transitions β-Zr的高压稳定性:没有证据表明存在同构相变
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1957863
E. O’Bannon, P. Söderlind, D. Sneed, M. Lipp, H. Cynn, J. S. Smith, C. Park, Z. Jenei
ABSTRACT Isostructural transitions have been reported to occur in several pure elements; however, most of these have been disproven. Zr is one of those elements which remains controversial with two reports of an isostructural bcc-to-bcc transition at ∼56–60 GPa at an ambient temperature and a more recent report proposing a second bcc-to-bcc transition at 110 GPa. Here, we report a detailed experimental and theoretical study of zirconium in the pressure region of the proposed isostructural transition(s). We conducted three room temperature static compression experiments using Ne as a pressure transmitting medium up to 80 GPa. We see no evidence for an isostructural transition finding a smooth compression curve for β-Zr. We determined the theoretical volume, elastic parameters, and Poisson’s ratio for β-Zr up to 717 GPa and no obvious anomalies are identified. Our new results join the growing body of evidence that does not find evidence of isostructural transitions in β-Zr.
据报道,在几种纯元素中发生了等结构跃迁;然而,这些观点大多已被推翻。Zr是那些仍然存在争议的元素之一,有两份报告称,在~56–60时发生了同构bcc到bcc的转变 环境温度下的GPa和最近的一份报告提出了110时的第二次bcc到bcc转变 GPa。在这里,我们报道了锆在所提出的同构转变的压力区的详细实验和理论研究。我们进行了三次室温静态压缩实验,使用Ne作为压力传递介质,压力高达80 GPa。我们没有发现任何证据表明β-Zr存在一条光滑的压缩曲线。我们确定了高达717的β-Zr的理论体积、弹性参数和泊松比 GPa,未发现明显异常。我们的新结果加入了越来越多的证据,这些证据没有发现β-Zr中同构转变的证据。
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引用次数: 2
Chilled storage stability of spice marinated and high pressure processed Indian white prawns (Fenneropenaeus indicus) 香料腌制和高压加工印度白对虾的冷藏稳定性
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1957864
G. Joseph, C. K. Kamalakanth, K. R. Remya Kumari, J. Bindu, K. K. Asha
ABSTRACT Chilled storage stability of marinated and high pressure treated peeled and undeveined Indian white prawns (Fenneropenaeus indicus) were studied. The prawns were marinated with condiments viz. chilli powder, salt and turmeric, and - vacuum packed in ethylene-vinyl alcohol copolymer pouches. Marinated unpressurized prawn samples were kept as control. The products were stored at 2 ± 1°C for evaluating - shelf life by analysing biochemical, microbiological and organoleptic parameters. Pressurization significantly altered the quality indices such as pH, total volatile basic nitrogen, free fatty acid, thiobarbituric acid, total plate count and overall acceptability of samples. The control and 200  MPa treated sample were rejected on 20th and 25th day of storage respectively, whereas 250 and 300  MPa treated samples achieved a shelf life of 35 days. Among the samples, the prawns treated at 250  MPa were found to be organoleptically superior with respect to its biochemical and microbiological quality parameters.
摘要对印度对虾(Fenneropenaeus indicus)腌制和高压处理后去皮和未去皮的冷藏稳定性进行了研究。虾用辣椒粉、盐和姜黄等调味料腌制,真空包装在乙烯-乙烯醇共聚物袋中。以未加压腌制的对虾为对照。产品在2±1℃下保存,通过分析生化、微生物和感官参数来评估保质期。加压显著改变了样品的pH、总挥发性碱氮、游离脂肪酸、硫代巴比妥酸、总板数和总体可接受度等质量指标。对照和200 MPa处理的样品分别在第20天和第25天被拒收,而250和300 MPa处理的样品的保质期为35天。结果表明,在250 MPa条件下处理的对虾在生化和微生物质量指标上具有较好的感官优势。
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引用次数: 1
Equations of state of new boron-rich selenides B6Se and B12Se 新型富硼硒化物B6Se和B12Se的状态方程
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-06-08 DOI: 10.1080/08957959.2021.1961765
K. Cherednichenko, Y. Le Godec, V. Solozhenko
ABSTRACT Two novels boron-rich selenides, orthorhombic B6Se and rhombohedral B12Se, have been recently synthesized at high pressures and high temperatures. Room-temperature compressibilities of these phases were studied in a diamond anvil cell using synchrotron powder X-ray diffraction. A fit of experimental p–V data by the third-order Birch–Murnaghan equation of state yielded the bulk moduli of 155(2) GPa for B12Se and 144(3) GPa for B6Se. No pressure-induced phase transitions have been observed in the studied pressure range, that is, up to 35 GPa.
近年来,在高压高温条件下合成了两种新型的富硼硒化物,正交B6Se和菱形B12Se。利用同步加速器粉末X射线衍射在金刚石砧座室中研究了这些相的室温压缩率。通过三阶Birch–Murnaghan状态方程对实验p–V数据进行拟合,得出体积模量为155(2) B12Se和144的GPa(3) B6Se的GPa。在所研究的压力范围内,即高达35,未观察到压力引起的相变 GPa。
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引用次数: 2
Reflective imaging, on-axis laser heating and radiospectrometry of samples in diamond anvil cells with a parabolic mirror 用抛物面镜对金刚石砧细胞样品进行反射成像、轴上激光加热和放射光谱分析
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-04-03 DOI: 10.1080/08957959.2021.1921173
G. Spiekermann, L. Libon, C. Albers, R. Sakrowski, S. Petitgirard, C. Sahle, M. Sundermann, H. Gretarsson, I. Sergueev, C. Sternemann, M. Wilke, M. Murakami
ABSTRACT We describe the use of a silver-coated 90 parabolic mirror of 33 mm focal length as objective for imaging, on-axis laser heating and radiospectrometric temperature measurements of a sample compressed in a diamond anvil cell in a laser heating system. There, spatial resolution and imaging quality of the parabolic mirror are similar to the one of a 10× objective. The temperature measurements between 500 and 900 nm are essentially free from chromatic aberration. The parabolic mirror was also perforated with a 220-μm hole, allowing for on-axis imaging, laser heating and incidence of X-rays simultaneously at synchrotron facilities. The parabolic mirror is thus a well-suited alternative to existing refractive and reflective objectives in laboratory and synchrotron laser heating systems.
摘要:我们描述了33的镀银90抛物面反射镜的使用 mm焦距作为成像目标,对在激光加热系统中的金刚石砧座单元中压缩的样品进行轴上激光加热和辐射光谱温度测量。在那里,抛物面镜的空间分辨率和成像质量类似于10×物镜。温度测量值介于500和900之间 nm基本上没有色差。抛物面镜上还开了一个220μm的孔,可以在同步加速器设备上同时进行轴上成像、激光加热和X射线入射。因此,抛物面镜是实验室和同步加速器激光加热系统中现有折射和反射物镜的一种非常合适的替代方案。
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引用次数: 2
New cooling system for a three-axis multi-anvil press with 6-6 geometry 6-6三轴多砧压力机新型冷却系统
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-04-03 DOI: 10.1080/08957959.2021.1910254
C. M. Howard, N. Walte
ABSTRACT A new custom-designed cooling system is described that was developed for the SAPHiR three-axis multi-anvil press with MA6-6 anvil geometry at the FRM II neutron source in Garching. The system was designed to remove heat from the secondary anvils by flowing a cryogen around custom-designed cooling rings or cooling jackets. Currently, this cryo-system is capable of achieving temperatures of 83 K without interfering with the anvil geometry and pressure transfer, thus not limiting the attainable maximum pressure or the capability of performing deformation experiments. In this study, pressures of up to ca. 8 GPa were attained at 83 K with sample volumes up to 130 mm3. The system is portable and can be implemented into any three-axis multi-anvil press with a MA6-6 anvil geometry, opening up new areas of high pressure cryo-research at synchrotron and neutron facilities, including investigating the interior of icy moons.
摘要介绍了一种新的定制冷却系统,该系统是为位于Garching的FRM II中子源的具有MA6-6砧座几何形状的SAPHiR三轴多砧压力机开发的。该系统旨在通过在定制设计的冷却环或冷却套周围流动冷冻剂来去除二次砧的热量。目前,这种低温系统能够达到83 K,而不干扰砧座几何形状和压力传递,从而不限制可获得的最大压力或进行变形实验的能力。在这项研究中,压力高达ca.8 GPa达到83 K,样品体积高达130mm3。该系统是便携式的,可以在任何具有MA6-6砧座几何形状的三轴多砧座压力机上实现,为同步加速器和中子设施的高压低温研究开辟了新的领域,包括研究结冰卫星的内部。
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引用次数: 0
Calibration of ruby (Cr3+:Al2O3) and Sm2+:SrFCl luminescence lines from the melting of mercury: constraints on the initial slopes 汞熔化红宝石(Cr3+:Al2O3)和Sm2+:SrFCl发光线的校准:初始斜率的限制
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-04-03 DOI: 10.1080/08957959.2021.1931168
Guoyin Shen, Jesse S. Smith, C. Kenney-Benson, S. Klotz
ABSTRACT We have measured the luminescence shifts of the ruby’s R1- and R2-lines and the line of 5D0→7F0 from Sm2+:SrFCl corresponding to the melting pressure of mercury that is recommended by the AIRAPT task force as an International Practical Pressure Scale (IPPS). The linear coefficients of the pressure dependence of the R1-, R2-lines, and the luminescence line of Sm2+:SrFCl are determined to be 0.3722 ± 0.002, 0.3796 ± 0.002, and 1.123 ± 0.002 nm/GPa, respectively. The results not only put tight constraints on the initial slopes of ruby and Sm2+:SrFCl gauges, but also link the luminescence-based pressure gauges to the more fundamental primary piston gauges.
我们测量了Sm2+:SrFCl中红宝石R1-和r2线以及5D0→7F0线的发光位移,对应于AIRAPT工作组推荐作为国际实用压力刻度(IPPS)的汞熔化压力。结果表明,Sm2+:SrFCl的R1-线、r2 -线和发光线的压力依赖性线性系数分别为0.3722±0.002、0.3796±0.002和1.123±0.002 nm/GPa。结果不仅严格限制了ruby和Sm2+:SrFCl压力表的初始斜率,而且还将基于发光的压力表与更基本的初级活塞压力表联系起来。
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引用次数: 2
Nonstoichiometric Fe–V–Al full Heusler alloys under high pressure: thermoelectric properties 高压下非化学计量Fe–V–Al全Heusler合金的热电性能
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-04-03 DOI: 10.1080/08957959.2021.1924702
I. Korobeynikov, A. Y. Usik, T. E. Govorkova, S. Emelyanova, V. Marchenkov
ABSTRACT The Heusler alloys are promising material for various applications, including thermoelectric power generators. There are several ways to improve their properties, among which the substitution of constituent elements, nanostructuring, temperature treatment, thin films engineering etc. This work is devoted to the experimental study of thermoelectric properties of Fe–V–Al-based Heusler alloys with different compositions under high pressure. The Seebeck coefficient and electrical resistance of several compounds were measured as a function of applied pressure up to 10 GPa at room temperature. The experimental results demonstrated a diversity of pressure responses of the thermoelectric properties that can be observed in chemically similar Heusler alloys under variation in their compositions. Moderate enhancing of the thermoelectric power factor, S 2/r (where S is the Seebeck coefficient and r is the electrical resistivity) was observed in Fe-rich Fe2.1V0.91Al0.99 compound at a pressure about ∼1 GPa. It was found that all alloys with weak deviation from stoichiometric composition had a feature in their S (P) pressure behavior at P∼2 GPa which could be related to semimetal-metal phase transition.
摘要赫斯勒合金是一种很有前途的材料,可用于各种应用,包括热电发电机。有几种方法可以改善它们的性能,其中包括成分的替代、纳米结构、温度处理、薄膜工程等。本工作致力于对不同成分的Fe–V–Al基Heusler合金在高压下的热电性能进行实验研究。测量了几种化合物的塞贝克系数和电阻,作为施加压力的函数,最高可达10 室温下的GPa。实验结果表明,在化学相似的赫斯勒合金中,在其成分变化的情况下,可以观察到热电性能的压力响应的多样性。在大约~1的压力下,在富含Fe的Fe2.1V0.91Al0.99化合物中观察到热电功率因数S2/r(其中S是塞贝克系数,r是电阻率)的适度增强 GPa。研究发现,所有与化学计量成分偏差较小的合金在P~2时都具有S(P)压力行为的特征 GPa可能与半金属-金属相变有关。
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引用次数: 1
Hydrostaticity in high pressure experiments: some general observations and guidelines for high pressure experimenters 高压实验中的静力学:高压实验人员的一般观察和指南
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-03-24 DOI: 10.1080/08957959.2021.1903457
K. Takemura
ABSTRACT The characteristics of hydrostatic stress conditions are discussed and compared with real experimental observations made under high pressure with a diamond-anvil cell. While fluid pressure-transmitting media give a well-defined single stress condition, solid pressure-transmitting media give a variety of stress conditions within the limit of their shear strength under high pressure. Owing to its low shear strength, solid helium would be the best choice for a pressure-transmitting medium to at least 100 GPa. However, helium is so compressible that care should be taken on minimizing irregular deformation of a gasket hole, which often causes complicated stress states. A review is given on the quasi-hydrostatic limits of solidified pressure-transmitting media, and some ways to reduce nonhydrostaticity are discussed including the case of low-temperature experiments.
讨论了静流体应力条件的特点,并与金刚石砧池高压下的实际实验结果进行了比较。流体传压介质具有明确的单一应力条件,而固体传压介质在高压作用下在其抗剪强度极限内具有多种应力条件。由于其较低的抗剪强度,在100 GPa以上的压力传递介质中,固体氦是最佳选择。然而,氦气是可压缩的,因此应注意尽量减少垫圈孔的不规则变形,这通常会导致复杂的应力状态。综述了固体传压介质的准静力极限,讨论了降低非静力性的方法,包括低温实验的情况。
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引用次数: 14
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High Pressure Research
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