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Influence of Rolling and Ageing On Mechanical Properties of AA2195 Based Metal Matrix Composites 轧制和时效对AA2195基金属基复合材料力学性能的影响
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.011
Srinivasa Rao. M, K. T. Balaram Padal
The modern Aluminium based composites have a great demand in the field of aerospace applications due to their lightweight, high strength, high stiffness, and superior mechanical properties. The main objective is to fabricate the AA2195 composites through Medium Frequency Induction Furnace (MFIF) with Taguchi L16 design of experiments, hot rolling process and heat treatment of composites is done and then compare the mechanical properties of hot rolled and heat treated AA2195 composite with casted composite. It is analyzed the effects of reinforcements like graphite and boron carbide on the mechanical behaviors and microstructure of both AA2195 composites. The microstructures revealed that reinforcements were distributed uniformly throughout the composites. It observed that the elemental investigation on SEM and XRD for both the composites showed that formed intermetallic compounds (IMCs) helped refine the microstructure and further increased the mechanical properties. The hot rolled and heat-treated AA2195 composite fabricated at 8% B4C and 6% Gr exhibits the more enhanced ultimate tensile strength, hardness, and reduction in density, % elongation compared to the casted composite. The rolling process is used to reduce the porosity of the composite. In contrast, heat treatment enhances the composite's mechanical properties like strength and hardness.
现代铝基复合材料以其轻量化、高强、高刚度和优异的机械性能在航空航天领域有着巨大的需求。主要目的是采用田口L16设计的中频感应炉(MFIF)制备AA2195复合材料,对复合材料进行热轧工艺和热处理,然后将热轧和热处理后的AA2195复合材料与铸造复合材料的力学性能进行比较。分析了石墨和碳化硼增强剂对两种AA2195复合材料力学行为和显微组织的影响。显微组织表明,增强材料在复合材料中分布均匀。通过SEM和XRD对复合材料进行元素分析,发现形成的金属间化合物(IMCs)有助于细化复合材料的微观结构,进一步提高了复合材料的力学性能。以8% B4C和6% Gr制备的热轧和热处理AA2195复合材料与铸造复合材料相比,具有更高的极限抗拉强度和硬度,并降低了密度和伸长率。轧制工艺用于降低复合材料的孔隙率。相反,热处理提高了复合材料的机械性能,如强度和硬度。
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引用次数: 0
Analysis of Automated Emergency Braking System to Investigate Forward Collision Condition Using Scenario-Based Virtual Assessment 基于场景虚拟评估的自动紧急制动系统前碰撞工况分析
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.029
Lee Kah Onn, Colin Rei, Vimal Rau Aparow, Cheok Jun Hong, Alex Au Yong Lup Wai, Zulhaidi Mohd Jawi
In the recent trend of automotive technologies, active safety systems for vehicles have become one of the key elements to reduce road traffic conditions. Automated vehicles are known as one of the active safety systems to minimize road traffic congestion and unwanted road hazardous situations. Generally, automated vehicles are designed using advanced driving assistance system (ADAS) technology to enhance the safety capability of the vehicles. Moreover, automated vehicles are designed to adopt multiple scenarios with different types of traffic situations. Generally, the performance of automated vehicles is evaluated to adapt with various road conditions and different type of traffic conditions, autonomously. Nonetheless, most of the safety testing was conducted in a controlled environment and with less traffic conditions. Moreover, this technology is tested in developed countries and mostly evaluated for highway driving scenarios, with less pedestrians and motorist’s road users. On the other hand, in developing countries such as Malaysia, most of the automotive researchers have initiated research related to automated vehicle based on controlled environment only. One of the primary focuses for the current automotive researchers is to reduce road accidents due to frontal collision. Thus, automated emergency braking systems have been heavily investigated by most developers to minimize road accidents. Most of the researchers analyze the system in terms of theoretical based simulation and tested using actual vehicle for physical testing. However, this type of testing is not sufficient to optimize the performance of automatedemergency braking systems for developing countries. Therefore, this study focuses on scenario-based virtual assessment to evaluate the capability of autonomous vehicles using automated emergency braking system without causing road casualties with the distance range is 4.5m to 0.5m depending on vehicle speed.
在最近的汽车技术发展趋势中,车辆主动安全系统已成为减少道路交通状况的关键因素之一。自动驾驶汽车被认为是一种主动安全系统,可以最大限度地减少道路交通拥堵和不必要的道路危险情况。自动驾驶汽车一般采用先进驾驶辅助系统(ADAS)技术来提高车辆的安全性能。此外,自动驾驶汽车的设计是为了适应多种不同类型的交通情况。一般来说,自动驾驶车辆的性能评估是为了能够自主地适应各种道路条件和不同类型的交通条件。尽管如此,大多数安全测试都是在受控环境中进行的,交通条件较少。此外,这项技术在发达国家进行了测试,主要针对行人和驾车者的道路使用者较少的高速公路驾驶场景进行评估。另一方面,在马来西亚等发展中国家,大多数汽车研究人员已经开始了仅基于受控环境的自动驾驶汽车相关研究。减少因正面碰撞引起的道路交通事故是当前汽车研究人员关注的主要问题之一。因此,大多数开发人员都对自动紧急制动系统进行了大量研究,以尽量减少道路事故。研究人员对该系统的分析大多是基于理论的仿真和实际车辆的物理测试。然而,这种类型的测试不足以优化发展中国家自动紧急制动系统的性能。因此,本研究侧重于基于场景的虚拟评估,评估自动驾驶汽车使用自动紧急制动系统而不造成道路伤亡的能力,距离范围为4.5m ~ 0.5m,具体取决于车速。
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引用次数: 0
A Review On Electrospun Short Fiber Production 电纺短纤维生产综述
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.004
Cheryl Rinai Raja, Marini Sawawi, Siti Kudnie Sahari, Magdalene Andrew, Chin Suk Fun
Nanotechnology has become the interest of researchers in recent years for their unique properties of submicron scale materials. Nanotechnology also consists of nanofibers made from natural or synthetic polymers which can be electrospun into ultra-thin continuous fibers. These nanofibers are versatile as it can be found in various applications such as in filtration, affinity membranes, tissue engineering, biosensors, scaffolds, drug delivery and fiber reinforcement. Over the years, many researchers have reported various methods used to produce short electrospun fiber by means of ultrasonication, mechanical cutting, UV cutting, precipitation method, microtome cutting, cryo-microcutting, cryogenic milling, ball milling, and razor blade cutting under liquid nitrogen. The aim of this paper is to provide a review on electrospun short fiber production which elaborates more on the scission methods of the continuous as-spun fibers. The literature shows that several methods have been proposed and utilized, with varying degrees of success. Overall, it can be concluded that further research is needed to fully understand the complexities of this area and to develop a more effective approach.
纳米技术以其亚微米尺度材料的独特性能,近年来成为研究人员的兴趣。纳米技术还包括由天然或合成聚合物制成的纳米纤维,这些聚合物可以被静电纺成超薄的连续纤维。这些纳米纤维用途广泛,可以用于过滤、亲和膜、组织工程、生物传感器、支架、药物输送和纤维增强等各种应用。多年来,许多研究者报道了在液氮条件下超声波、机械切割、紫外切割、沉淀法、显微切割、低温微切割、低温铣削、球磨、剃须刀片切割等生产短电纺纤维的各种方法。本文对电纺短纤维的生产进行了综述,重点介绍了连续纺短纤维的切割方法。文献表明,已经提出并利用了几种方法,取得了不同程度的成功。总的来说,可以得出结论,需要进一步的研究,以充分了解这一领域的复杂性,并制定更有效的方法。
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引用次数: 0
Mechanical Response of Applying Different Parameters On Negative Stiffness Honeycomb Structure 应用不同参数对负刚度蜂窝结构的力学响应
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.007
Abdalla Rabie Takrouny, Faris Tarlochan
It has become apparent that negative stiffness behavior may have potential applications in vibration isolation mechanisms, vibro-acoustic dampening materials, and mechanical switches. Unlike traditional honeycombs, due to these properties, a negative honeycomb can absorb substantial amounts of mechanical energy whilst maintaining a stable stress. The force threshold under displacement loading was investigated of three variables applied on different models of negative-stiffness honeycomb (NSH) structures. The three variables are material applied, honeycomb unit cell, and beam thickness of the negative honeycomb structure. Accordingly, nine models were developed, and the three varied materials were assigned repeatably to each model and then force threshold were studied after validating the model. The Finite element analysis (FEA) for formed model was validated and shows force value of 289 N with an error of 5% compared to the referenced model. In the 4- unit cell model, the highest force threshold of approximately 240 N was noticed during loading phase at the beam thickness of 19.05 mm for both nylon 11 and 12 material. Finally, the force threshold of 550 N during loading and unloading phases was observed for nylon 6/6 material at beam thickness of 19.05 mm. The results obtained confirm the negative stiffness behavior on the models and shows that the force threshold applied is reduced comparing to forces required in the conventional honeycombs models.
很明显,负刚度行为可能在隔振机制、振声阻尼材料和机械开关中有潜在的应用。与传统的蜂窝不同,由于这些特性,负蜂窝可以吸收大量的机械能,同时保持稳定的应力。研究了3个变量对不同模型负刚度蜂窝结构在位移荷载作用下的力阈值。这三个变量是应用的材料、蜂窝单元和负蜂窝结构的梁厚度。据此,建立了9个模型,并将3种不同的材料重复分配给每个模型,验证模型后对力阈值进行研究。对成形模型进行了有限元分析,得到的受力值为289 N,与参考模型的误差为5%。在4单元胞模型中,尼龙11和尼龙12材料在梁厚为19.05 mm时,加载阶段的最高力阈值约为240 N。最后,对尼龙6/6材料在梁厚为19.05 mm时,在加载和卸载阶段观察到550 N的力阈值。所得结果证实了模型的负刚度特性,并表明所施加的力阈值与传统蜂窝模型所需的力相比有所降低。
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引用次数: 0
Characterization of 3D Orthogonal Woven Carbon/Kevlar Composite Under Tensile Loading 拉伸载荷下三维正交编织碳/凯夫拉复合材料的表征
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.018
Ram Vishal G, Dalbir Singh, Srikanth H. V
In the present work, the tension response of polypropylene (PP) based composites reinforced with Carbon/Kevlar fabrics was investigated. The weft, wrap, and binder are considered in the direction (XYZ) and woven into a 3D fabric. Two homogeneous fabrics with Carbon (CCC), Kevlar (KKK), hybrid Carbon/Kevlar (CCK), and hybrid Kevlar/Carbon (KKC) fabrics were produced using a hand-made spoke frame. The architecture of the fabrics was three-dimensional orthogonal (3D-O). Four different composite laminates were manufactured using a vacuum bag-assisted moulding technique. The tensile loading was applied using a Nano-UTM set-up at travel of +6.25/-3.1 mm and software-automated generation of stress-strain data. The results indicated that the tensile properties of thermoplastic 3D-O composites are sensitive. In all the composites, the peak stress, strength, and modulus were increased when noticed with the 2D fabric. The experimental results show that the tensile strength of CCK and CCC with carbon fibres used in their weft and warp direction was greater than that of KKC and KKK with Kevlar fibres used in fibres weft and warp direction. The hybridization and 3D orthogonal weaving method also increased the tensile strength. The observation were characterized through scanning electron microscope.
本文研究了碳纤维/凯夫拉纤维增强聚丙烯基复合材料的拉伸响应。纬纱、包纱和粘合剂在方向(XYZ)上被考虑并编织成3D织物。两种均质织物分别为碳(CCC)、凯夫拉(KKK)、混合碳/凯夫拉(CCK)和混合凯夫拉/碳(KKC)织物。织物的结构是三维正交的(3D-O)。使用真空袋辅助成型技术制造了四种不同的复合层压板。拉伸载荷使用纳米utm装置施加,行程为+6.25/-3.1 mm,软件自动生成应力-应变数据。结果表明,热塑性3D-O复合材料的拉伸性能敏感。在所有复合材料中,峰值应力、强度和模量都随着二维织物的增加而增加。实验结果表明,经向和纬向使用碳纤维的CCK和CCC的抗拉强度大于经向和纬向使用凯夫拉纤维的KKC和KKK的抗拉强度。杂交法和三维正交编织法也提高了织物的抗拉强度。通过扫描电镜对观察结果进行了表征。
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引用次数: 0
Optimization of Co-Flow Jet Parameters for Ahmed Body Application 艾哈迈德体应用共流射流参数优化
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.025
Ikram Derghal, Mohd Saifuddin, Mohd Hafiz Mohd Noh, Ahmad Hussein Abdul Hamid
This study evaluates the drag reduction strategy of suction and blowing on idealize automotive vehicle, Ahmed Body. Optimization approach is adapted in order to analyse the effect of slot location, momentum coefficient and slot angle on the vehicle which experiencing drag. Despite all the efforts that have been done to reduce the Ahmed body drag using various active flow control system, most of the drag reduction were only less than 15%. A 25° Ahmed body with build in co-flow jet is modelled using a CAD software. The flow around the Ahmed body is simulated at Reynolds number based on length Re = 4.29 × 106. The governing equation were solve using an open source software package, which has been validated against experimental data. Pressure Implicit with Splitting of Operator (PISO) algorithm is applied to solve the equation. The outcome of the simulation are varies depending on the variables. Some show a decrease in drag while there are also that actually increase the drag of the system. This are caused by the suction and blowing slots that effect the surrounding air flow whether it is reducing or increasing the wake size downstream of the body. The result shows the momentum coefficient and location of both suction and blowing jet played an important role of manipulating the flow around the body and reducing the drag. The velocity contours indicated that the key to drag reduction is by using 40 m/s jet velocity, placement of suction and blowing away from each other.
本研究对理想汽车艾哈迈德车身的吸气和吹气减阻策略进行了评估。采用优化方法分析了槽位、动量系数和槽角对受阻力车辆的影响。尽管采用了各种主动气流控制系统来降低Ahmed车身阻力,但大多数减阻效果都不到15%。采用CAD软件对内置共流射流的25°艾哈迈德体进行了建模。在雷诺数为Re = 4.29 × 106的条件下,模拟了Ahmed体周围的流动。利用开源软件包求解了控制方程,并通过实验数据进行了验证。采用压力隐式分割算子(PISO)算法求解该方程。模拟的结果因变量的不同而不同。有些显示阻力减少,而有些实际上增加了系统的阻力。这是由于吸入和吹气槽对周围空气流动的影响造成的,无论是减少还是增加机体下游的尾迹尺寸。结果表明,吸、吹两种射流的动量系数和位置对控制绕流和减小阻力都有重要作用。速度曲线表明,采用40 m/s的射流速度、放置吸力和相互吹离是减阻的关键。
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引用次数: 0
Parametric Study for Runner Modifications of Die Casted Part with Venting Systems 带排气系统的压铸件流道修正的参数化研究
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.010
M.D. Ibrahim, J. Jendia, Y. Kashiwabara, Y. Sunami
High-pressure die casting (HPDC) is a process used for creating complex components by injecting the molten metal inside the cavity at high pressure. Failure in die casting may reduce product mechanical properties, surface quality, and life cycle. In this paper, the die-casting process of an inspection instrument – test piece is investigated for parametric study and Computational fluid dynamics (CFD) analysis. Parameters used in the die-casting process are important since it affects the molten flow quality inside the cavity. Thus, a parametric study is done to investigate the optimum parameter use in the die-casting process of the test piece. Runner gating system design is also one of the important criteria to maintain the quality of products. This paper also investigated the effect of runner gating system design optimization in reducing gas porosity. The CT scan of the sample mold is included to compare the relationships between gas porosity occurrence with CFD results. This paper proposed a new runner design named outward curvature runner with an air vent that can improve velocity and temperature distributions in reducing die-casting defects. In addition to that, air vents are installed to extend the volume and promote higher suction, to eliminate gas bubbles entrapment inside the cavity.
高压压铸(HPDC)是一种通过在高压下向腔内注入熔融金属来制造复杂部件的工艺。压铸件的故障会降低产品的机械性能、表面质量和寿命周期。本文对一种检测仪器-试样的压铸过程进行了参数化研究和计算流体力学分析。压铸过程中使用的参数很重要,因为它影响腔内的熔融流动质量。为此,进行了参数化研究,以探讨试件压铸过程中最佳参数的使用。流道浇注系统的设计也是保持产品质量的重要标准之一。研究了流道浇注系统优化设计对降低气孔率的影响。为了比较气体孔隙度的发生与CFD结果之间的关系,采用了样品模具的CT扫描。本文提出了一种新的流道设计,即带气孔的外曲率流道,它可以改善速度和温度分布,减少压铸缺陷。除此之外,还安装了通风口,以扩大体积并提高吸力,以消除腔内的气泡。
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引用次数: 0
A Numerical Model for Analysis of Heat Transfer in MHD Casson Fluid with Radiation and Viscous Dissipation 具有辐射和粘性耗散的MHD卡森流体传热分析的数值模型
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.016
Gollapalli Shankar, Siva Reddy Sheri
This article is, concerned a numerical model for analysis of heat transfer (HT) in MHD Casson fluid (CF) with radiation and viscous dissipation. The governing PDE's are developed for the physical model and converted into non-dimensional form and then with the help of Galerkin finite element method (GFEM) solution is obtained. The impact of dimensionless parameters which are supervising the flow such as Magnetic parameter , Casson parameter ( ) thermal Grashof number Permeability of porous medium Prandtl number Heat absorption parameter Viscous dissipation and Radiation parameter are analyzed through graphs for fluid properties. The results obtained were compared with earlier reported results for correctness.
本文建立了具有辐射和粘性耗散的MHD卡森流体(CF)传热分析的数值模型。建立了物理模型的控制偏微分方程,并将其转化为无量纲形式,利用伽辽金有限元法求解。通过流体性质图分析了磁参数、卡森参数、热格拉索夫数、多孔介质渗透率、普朗特数、吸热参数、粘滞耗散和辐射参数等无量纲参数对流体流动的影响。所得结果与先前报道的结果进行了正确性比较。
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引用次数: 0
Investigating The Surface Characteristics of Dip Coated 3D Printed ABS Specimens 浸渍涂层3D打印ABS试样表面特性研究
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.006
Poornaganti Satyanarayana, Yeole Shivraj Narayan, Kode Jaya Prakash, Jyotsna Cherukuri, Maneiah D.
In the past few years, FDM basedpolymer 3D printing process has flourished mainly with ABS filaments as a thermoplastic source. Food packing, medical, marine and agriculture industries employdevices and other usable items made of polymers. Utilizing layered fabrication components in these areascompelthem to have self-cleansing, anti-freezing and corrosion resistant surfaces. It is generally complex and expensive to prepare hydrophobic coatings.The present work is related to the development of a surface coating on 3D printed ABS specimens with the mentioned properties. 3D printed specimens were fabricated using Flash Forge 3D printer without any modifications, and the hydrophobic coatings were achieved by dip coating process using Tricalcium phosphate-chitin solutions with a ratio of 70:30. Static contact angle measurement was employedin gaging wettability impact on dip coated 3D printed specimens. By using digital vernier calipers and profilometer (SJ410), dimensional accuracy and surface roughness were assessed pre and post-coating. According to ASTM D570-98, water absorption tests were conducted at different time intervals. Results of the experiment showed that the hydrophobic solutions had been successfully synthesized. The maximum contact angle was achieved for solution 1(4g of tricalcium phosphate solution with 0.3g chitin solution) i.e., 109.3°. Improvement in the textureof 3D printed ABS surfaceswas observed after dip coating. Dip-coated 3D printed ABS specimens exhibited minimal absorption based on their weight gain per area.
在过去的几年里,以FDM为基础的聚合物3D打印工艺主要以ABS长丝作为热塑性源而蓬勃发展。食品包装、医疗、海洋和农业行业使用由聚合物制成的设备和其他可用物品。在这些区域使用分层制造组件,迫使它们具有自清洁,防冻和耐腐蚀的表面。疏水涂层的制备通常复杂且昂贵。目前的工作是与具有上述性能的3D打印ABS样品表面涂层的开发有关。采用Flash Forge 3D打印机制作3D打印样品,不做任何修改,采用磷酸三钙-甲壳素溶液以70:30的比例浸涂工艺获得疏水涂层。采用静态接触角测量方法研究了浸渍涂层对3D打印样品润湿性的影响。采用数字游标卡尺和轮廓仪(SJ410)对涂覆前后的尺寸精度和表面粗糙度进行了评定。根据ASTM D570-98,在不同的时间间隔进行吸水试验。实验结果表明,成功地合成了疏水溶液。溶液1(4g磷酸三钙溶液和0.3g甲壳素溶液)的最大接触角为109.3°。3D打印ABS表面的纹理在浸渍涂层后得到改善。浸渍涂层3D打印ABS样品显示最小的吸收基于他们的重量增加每面积。
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引用次数: 0
Rheological Analysis of Zirconia-Hydroxyapatite with Bi-Modal System of Binders; Low-Density Polyethylene and Palm Stearin 双峰系氧化锆-羟基磷灰石的流变学分析低密度聚乙烯和棕榈硬脂
Q4 ENGINEERING, MULTIDISCIPLINARY Pub Date : 2023-10-19 DOI: 10.30880/ijie.2023.15.05.019
Muhammad Mohamed Amin, Nur Syamimi Zainal Adelin, Abu Bakar Sulong, Norhamidi Muhamad
The two component micro-powder injection molding (2C-μPIM) process has evolved from μPIM process because of the increasing demand for multi-functional micro-components applications. In this research work, the selected materials to fabricate micro-sized bi-material parts are zirconia (ZrO2) and hydroxyapatite (HA). ZrO2 is chosen for structural integrity and bio-inert, while HA is mainly chosen for bio-active properties. The reason of employing the multi-component binders is to ensure the flowability of the feedstock. Feedstock rheological characteristics needs to be carefully investigated to avoid any undesirable and inhomogeneous mixture between powder and binder. A common binder system which is comprised of palm stearin and low-density polyethylene (LDPE) were mixed with individual ZrO2 and HA powder particles to prepare for ZrO2 and HA feedstocks. Typically, the feedstocks were obtained ZrO2 and HA powders independently with a binder ratio of 60 wt.% of palm stearin and 40wt.% low-density polyethylene (LDPE). The mixing was carried out in Brabender mixer. Before mixing, critical powder volume percentage (CPVP) analysis was carried out to determine the optimal powder loadings required to prepare the ZrO2 and HA feedstocks. In this research work, the obtained CPVP of ZrO2 and HA powders were 47.0 and 59.0 vol.%, respectively. Based on CPVP analysis, six feedstocks with optimal powder loadings of 43, 44 and 45 vol.% for ZrO2 and 54, 55 and 56 vol.% for HA were prepared. The rheological analysis involving viscosity, shear rate, flow behavior index, activation energy and moldability index was investigated using capillary rheometer. Based on the obtained rheology result, it shows that the overall shear rate and viscosity are within the 2C-μPIM process recommended range. All tested composition shows pseudoplastic behavior. The results of the study found that ZrO2 and HA with optimal powder loadings of 55 vol.% and 44 vol.% have good rheological properties compared to feedstocks with other powder loadings. This is because both materials meet the criteria of good rheological properties which are low viscosity, high shear rate, flow behavior index less than one, low activation energy and high moldability index.
双组分微粉末注射成型工艺(2C-μPIM)是从μPIM工艺发展而来的,是多功能微元件应用需求的不断增长。在本研究中,选择了氧化锆(ZrO2)和羟基磷灰石(HA)作为制备微尺寸双材料部件的材料。选择ZrO2是为了结构的完整性和生物惰性,而选择HA主要是为了生物活性。采用多组分粘结剂的原因是为了保证原料的流动性。需要仔细研究原料的流变特性,以避免粉末和粘合剂之间出现任何不希望的和不均匀的混合物。将棕榈硬脂和低密度聚乙烯(LDPE)组成的普通粘结剂体系与单独的ZrO2和HA粉末颗粒混合,制备ZrO2和HA原料。通常,原料分别为ZrO2和HA粉末,粘合剂比例为60 wt.%棕榈硬脂和40wt. %。%低密度聚乙烯(LDPE)混合在Brabender混合器中进行。在混合前,进行临界粉末体积百分比(CPVP)分析,以确定制备ZrO2和HA原料所需的最佳粉末负荷。在本研究中,ZrO2和HA粉体的CPVP分别为47.0和59.0 vol.%。基于CPVP分析,制备了ZrO2的最佳粉量为43、44和45 vol.%, HA的最佳粉量为54、55和56 vol.%的6种原料。利用毛细管流变仪对其进行了粘度、剪切速率、流动性能指标、活化能和可塑性指标的流变分析。所得的流变学结果表明,总体剪切速率和粘度均在2C-μPIM工艺推荐范围内。所有测试成分均表现出假塑性行为。研究结果发现,ZrO2和HA的最佳粉载率分别为55 vol.%和44 vol.%,与其他粉载率的原料相比,具有良好的流变性能。这是因为这两种材料都符合良好流变性能的标准,即低粘度、高剪切速率、流动行为指数小于1、低活化能和高成型指数。
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引用次数: 0
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International Journal of Integrated Engineering
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