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Volume 3: Advanced Materials: Design, Processing, Characterization and Applications; Advances in Aerospace Technology最新文献

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Impact of Imperfect Kolsky Bar Experiments Across Different Scales Using Finite Elements 不同尺度下不完善科尔斯基杆实验的有限元影响
Thomas H. Hannah, Reuben H. Kraft, V. Martin, Stephen Ellis
Typical Kolsky bars are 10–20mm in diameter with the lengths of each main bar being on the scale of meters. To push 104 and higher strain rates smaller diameter bars, accompanied by shorter lengths, are needed. As the diameters of the bars decreases the precision in the alignment of the system must increase to maintain the same relative tolerance as the larger experimental systems. Conversely, as the size of the bars decreases so does the magnitude of gravity based frictional forces due to the decreased mass of the system. Finite Element (FE) models are typically generated assuming a perfect experiment with exact alignment and no gravity. Additionally, these simulations tend to take advantage of the radial symmetry of an ideal experiment which removes any potential for modeling non-symmetric effects but has the added benefit of a reduced computational load. In this work, we discuss some of the results of these fast-running symmetry models to establish a baseline and demonstrate the first-order use case of such methods. We then take advantage of high-performance computing techniques to generate several three-dimensional, half symmetry simulations using Abaqus® allowing modeling of gravity and misalignment. The imperfection is initially modeled using the static general process followed by a dynamic explicit simulation in which the impact portion of the test is conducted. This multi-step simulation structure creates a system that can properly investigate the impact of these real-world, non-axis symmetric effects. These simulations fully explore the impacts of these experimental realities and are described in detail to allow other researchers to implement a similar FE modeling structure to aid in their experimentation and diagnostic efforts. Both a 12.7 mm and 3.16 mm diameter bar system are evaluated to quantify the degree that these various experimental imperfections have across two size scales of Kolsky bar systems.
典型的科尔斯基棒材直径为10-20mm,每个主棒材的长度以米为单位。为了推动104和更高的应变率,需要更小直径的棒材和更短的长度。随着杆的直径减小,系统的对准精度必须提高,以保持与较大的实验系统相同的相对公差。相反,随着杆的尺寸减小,由于系统质量减小,基于重力的摩擦力的大小也随之减小。有限元(FE)模型通常是假设一个完美的实验,具有精确的对准和无重力。此外,这些模拟倾向于利用理想实验的径向对称性,它消除了建模非对称效应的任何可能性,但具有减少计算负荷的附加好处。在这项工作中,我们讨论了这些快速运行的对称模型的一些结果,以建立一个基线,并展示了这些方法的一阶用例。然后,我们利用高性能计算技术生成几个三维,半对称模拟使用Abaqus®允许重力和不对准建模。缺陷最初使用静态一般过程建模,然后进行动态显式模拟,其中进行了试验的冲击部分。这种多步骤模拟结构创建了一个系统,可以正确地研究这些真实世界的非轴对称效果的影响。这些模拟充分探讨了这些实验现实的影响,并进行了详细描述,以允许其他研究人员实现类似的有限元建模结构,以帮助他们的实验和诊断工作。两个12.7毫米和3.16毫米直径棒系统进行评估,以量化的程度,这些不同的实验缺陷有跨科尔斯基棒系统的两个尺寸尺度。
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引用次数: 0
A Digital Twin Framework for Mechanical Testing Powered by Machine Learning 基于机器学习的机械测试数字孪生框架
M. Kahya, Cem Söyleyici, Mete Bakir, H. Ö. Ünver
The aviation industry demands innovation in new materials and processes which can demonstrate high performance with minimum weight. Strength-to-weight ratio (STR) is the key metric that drives the value justification in this demand stream. However, aviation’s test and certification procedures are time-consuming, expensive, and heavily regulated. This study proposes a Digital Twin (DT) framework to address the time and high costs of mechanical testing procedures in the aviation industry. The proposed DT utilizes new Machine Learning (ML) techniques such as Transfer Learning (TL). Hence, a proof-of-concept study using TL in the Aluminum material group has been demonstrated. The promising results revealed that it was possible to reduce the test load of new material to 40% without any significant error.
航空工业需要新材料和新工艺的创新,以最小的重量展示高性能。强度-重量比(STR)是驱动需求流中价值合理性的关键指标。然而,航空的测试和认证程序耗时、昂贵且监管严格。本研究提出了一个数字孪生(DT)框架来解决航空工业机械测试程序的时间和高成本问题。提出的DT利用新的机器学习(ML)技术,如迁移学习(TL)。因此,在铝材料组中使用TL进行了概念验证研究。有希望的结果表明,有可能将新材料的测试载荷降低到40%而不会产生任何显着误差。
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引用次数: 0
Blast-Resistant Ballistic Materials 防爆弹道材料
Nishant Thakkar
Several bomb explosion assaults against military personnel, police officers, and public and civil structures have occurred in recent years, resulting in a significant loss. As a result, society requires increased protection and defense for current constructions from loads of oblasts. In the middle of the many options, retrofitting reinforced concrete and masonry structures with numerous forms and types of materials of composite and fiber is an excellent way to improve resistance to the blast. This paper provides a recent review of extant works & papers on polymers, composite & fibrous materials used for elements of structure defense from the blast, as well as a list of research gaps that need to be filled. Various innovative materials such as polymers, nanomaterials, composite materials, as well as fibrous materials are taken into consideration while writing this review paper. Composite materials have been employed in the blast and ballistic impact applications and are regarded as effective materials for absorbing blast energy. The stitching boosted the composite’s Mode I interlaminar fracture toughness, resulting in increased damage resistance. The basic composite system tested is carbon-fiber-reinforced polymer (CFRP) composite skins on a styrene-acrylonitrile (SAN) polymer closed-cell foam core. In a comparable sandwich structure, glass-fiber-reinforced polymer (GFRP) composite skins were also incorporated for comparison.
近年来发生了几起针对军事人员、警察以及公共和民用建筑的炸弹爆炸袭击事件,造成重大损失。因此,社会需要加强对现有建筑的保护和防御。在众多选择中,用多种形式和类型的复合材料和纤维材料改造钢筋混凝土和砌体结构是提高抗爆炸能力的绝佳方法。本文综述了用于结构防爆元件的聚合物、复合材料和纤维材料的最新研究成果和论文,并列出了需要填补的研究空白。在撰写这篇综述论文时,考虑了各种创新材料,如聚合物,纳米材料,复合材料以及纤维材料。复合材料被认为是吸收爆炸能量的有效材料,已被应用于爆炸和弹道冲击领域。缝线提高了复合材料的I型层间断裂韧性,从而提高了抗损伤能力。测试的基本复合材料系统是在苯乙烯-丙烯腈(SAN)聚合物闭孔泡沫芯上的碳纤维增强聚合物(CFRP)复合材料表皮。在类似的三明治结构中,玻璃纤维增强聚合物(GFRP)复合材料表皮也被纳入比较。
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引用次数: 0
A Dynamics Model of Locomotive Mechanism Drilling Into Lunar Regolith 机车机构钻入月球风化层的动力学模型
Zihao Yuan, Ruinan Mu, Jiafeng Yang, Ke Wang, Haifeng Zhao
In this work, a dynamic model is proposed to simulate the drilling and steering processing of an autonomous burrowing mole to access scientific samples from the deep subsurface of the Moon. The locomotive module is idealized as a rigid beam. The characteristic parameters are considered including the length, cross-section diameter and centroid of a cylindrical rod. Based on the Lagrangian mechanics, a 3-DOF dynamic model for the locomotion of autonomous device underground is developed. By introducing the contact algorithm and resistive force theory, the interaction scheme between the locomotive body and regolith is described. The effect of characteristic parameters on resistive force and torque is studied and discussed through numerical experiments. The simulation results show that this method may adapt to a variety of drilling and burrowing motions in the lunar subsurface environments. Overall, the proposed method actually provides a reduced-order model to simulate the operating and controlling scenarios an autonomous burrowing robot in lunar subsurface. It may be further generalized to consider more complex conditions, including depth-dependent regolith model, 3D trajectory planning and navigation algorithms, etc. This model may provide intuitive inputs to plan the space missions of a drilling robot to obtain surface samples in an extraterrestrial planet, such as the Moon or Mars, etc.
在这项工作中,提出了一个动态模型来模拟自主挖洞鼹鼠的钻探和转向过程,以获取月球深层地下的科学样本。机车模块被理想化为刚性梁。考虑了圆柱杆的长度、截面直径和质心等特征参数。基于拉格朗日力学,建立了井下自主装置运动的三自由度动力学模型。通过引入接触算法和阻力理论,描述了机车本体与风化层的相互作用方案。通过数值实验研究和讨论了特征参数对阻力和转矩的影响。仿真结果表明,该方法可以适应月球地下环境中的多种钻孔和挖洞运动。总体而言,所提出的方法实际上提供了一个降阶模型来模拟月球地下自主挖洞机器人的操作和控制场景。可以进一步推广到考虑更复杂的条件,包括深度相关的风土模型、三维轨迹规划和导航算法等。该模型可以为规划钻探机器人的太空任务提供直观的输入,以获取月球或火星等地外行星的表面样本。
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引用次数: 0
Experimental and Numerical Investigation of the Influence of Crack Front Orientation in Mode 1 Plane Strain Fracture Toughness of a Vero Material System via Poly Jet Additive Manufacturing 聚流射流增材制造Vero材料体系1型平面应变断裂韧性影响的实验与数值研究
Vishwanath Khapper, R. Mohan
Polyjet printing, a multi-jet Additive Manufacturing technique, has been used to fabricate 3-Dimensional structures for various polymeric material systems. This technique uses a layer-by-layer deposition method and allows for the fabrication of parts with different material compositions and varying thermomechanical properties. The current research investigates the influence of process-induced variation on Mode 1(K1C) fracture toughness of the Vero material system. Compact Tension (C-T) specimens with crack fronts parallel and perpendicular to the print direction were fabricated. The orientation of the crack front relative to the print and build directions influenced the Mode I fracture toughness values. When the crack front was parallel to the print plane, K1C decreased by 49.54%, G1C decreased by 41.56%, and peak load intensity decreased by 52.76% compared to the perpendicular crack front orientation. C-T samples were modeled in CAD to correlate with the experimental results and then analyzed in the Ansys workbench. The FEA yielded a Mode 1 fracture toughness value of 2.48 MPa m0.5 for a perpendicular configuration of the crack front and a fracture toughness value of 1.15 MPa m0.5 for a parallel configuration of the crack front. The Representative Volume Element method is used for a composite containing the Vero material system as a matrix and carbon nanofibers as reinforcement. Carbon nanofibers are integrated using a customized material configuration, and their influence on fracture is studied. A tailored network perpendicular to the crack front in a 3D printed C-T specimen stiffens the specimen. In contrast, a tailored network parallel to the crack front has a relaxing impact, indicating that an additively created part may be prone to softening under certain conditions.
多射流打印是一种多射流增材制造技术,已被用于制造各种聚合物材料体系的三维结构。该技术采用逐层沉积方法,允许制造具有不同材料成分和不同热机械性能的部件。本研究探讨了过程诱导的变化对Vero材料体系的1型断裂韧性(K1C)的影响。制备了裂纹前沿平行于打印方向和垂直于打印方向的致密拉伸(C-T)试样。裂纹前缘相对于打印方向和构建方向的方向影响I型断裂韧性值。当裂纹前沿平行于打印平面时,与垂直裂纹前沿相比,K1C降低了49.54%,G1C降低了41.56%,峰值载荷强度降低了52.76%。C-T样品在CAD中建模,与实验结果相关联,然后在Ansys workbench中进行分析。有限元分析结果表明,裂缝前缘垂直形态下的1型断裂韧性值为2.48 MPa m0.5,裂缝前缘平行形态下的断裂韧性值为1.15 MPa m0.5。采用代表性体积元方法制备了以Vero材料体系为基体,以纳米碳纤维为增强材料的复合材料。采用定制的材料结构集成了碳纳米纤维,研究了其对断裂的影响。在3D打印的C-T样品中,垂直于裂纹前沿的定制网络使样品变硬。相比之下,与裂纹前缘平行的定制网络具有松弛影响,这表明增材制造的部件在某些条件下可能容易软化。
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引用次数: 0
Study on Heat Resistance of PLA Based Biodegradable Injection Molded Components 聚乳酸基可生物降解注塑件的耐热性研究
Can Yang, Ruifeng Chen, Jianzhong Xie, Zuguang Ding, Yang Shu, Xiao-Hong Yin
With the increasingly serious problem of white pollution, biodegradable substitutes that can replace the existing plastic materials are in urgent need. In the present work, thermal shock experiments were carried out to investigate the heat resistance of injection molded F6510 products under specific humidity/temperature conditions. Specifically, two groups of experiments were designed at a constant humidity of 90%. For single-point temperature (SPT) experiments, the testing temperature was varied from 30°C to 75 °C with an interval of 5/10 °C, and for the thermal cycle (TC) experiments, samples underwent 60 °C -(-20 °C)-60 °C thermal cycles. The SPT experiments showed that samples began to deform at 45 °C, with 0.05mm increase in length, and 0.02mm decrease in both width and height, and the shape variation increases with enhanced temperature. Meanwhile, TC experiment samples showed obvious shrinkage during the nine-day testing period, with a maximal size variation of 0.44mm for the length. In addition, DSC results showed a higher crystallinity degree for the inner layer of samples. This is due to the slower cooling rate of the inner layer, facilitating polymer molecular chain migration and thus the crystal nucleus growing, which was supported by Moldex3D simulation analyses. Double melting peaks appeared in the heating stage of DSC test, indicating the formation of both α and α’ crystal forms, which has been verified by both thermal shock experiments and DSC tests. The findings of this work indicate that the crystallinity, crystal form, and thus the products’ heat resistance of F6510 can be improved by reasonably controlling injection molding parameters such as the mold temperature and cooling time.
随着白色污染问题的日益严重,迫切需要能够替代现有塑料材料的生物降解替代品。本文通过热冲击实验研究了F6510注塑成型制品在特定湿度/温度条件下的耐热性。具体来说,两组实验设计在恒定湿度为90%的条件下。对于单点温度(SPT)实验,测试温度在30°C到75°C之间变化,间隔为5/10°C,对于热循环(TC)实验,样品经历60°C -(-20°C)-60°C的热循环。SPT实验表明,试样在45℃时开始变形,长度增加0.05mm,宽度和高度减少0.02mm,形状变化随温度升高而增大。同时,TC实验样品在9天的测试期内表现出明显的收缩,长度的最大尺寸变化为0.44mm。此外,DSC结果显示样品的内层结晶度较高。这是由于内层的冷却速度较慢,促进了聚合物分子链的迁移,从而促进了晶核的生长,这一点得到了Moldex3D模拟分析的支持。热冲击实验和DSC测试均证实了热冲击实验和DSC测试结果表明,在加热阶段出现了双熔融峰,表明形成了α和α '两种晶型。研究结果表明,通过合理控制模具温度和冷却时间等注塑工艺参数,可以提高F6510的结晶度和结晶形态,从而提高产品的耐热性。
{"title":"Study on Heat Resistance of PLA Based Biodegradable Injection Molded Components","authors":"Can Yang, Ruifeng Chen, Jianzhong Xie, Zuguang Ding, Yang Shu, Xiao-Hong Yin","doi":"10.1115/imece2022-88662","DOIUrl":"https://doi.org/10.1115/imece2022-88662","url":null,"abstract":"\u0000 With the increasingly serious problem of white pollution, biodegradable substitutes that can replace the existing plastic materials are in urgent need. In the present work, thermal shock experiments were carried out to investigate the heat resistance of injection molded F6510 products under specific humidity/temperature conditions. Specifically, two groups of experiments were designed at a constant humidity of 90%. For single-point temperature (SPT) experiments, the testing temperature was varied from 30°C to 75 °C with an interval of 5/10 °C, and for the thermal cycle (TC) experiments, samples underwent 60 °C -(-20 °C)-60 °C thermal cycles. The SPT experiments showed that samples began to deform at 45 °C, with 0.05mm increase in length, and 0.02mm decrease in both width and height, and the shape variation increases with enhanced temperature. Meanwhile, TC experiment samples showed obvious shrinkage during the nine-day testing period, with a maximal size variation of 0.44mm for the length. In addition, DSC results showed a higher crystallinity degree for the inner layer of samples. This is due to the slower cooling rate of the inner layer, facilitating polymer molecular chain migration and thus the crystal nucleus growing, which was supported by Moldex3D simulation analyses. Double melting peaks appeared in the heating stage of DSC test, indicating the formation of both α and α’ crystal forms, which has been verified by both thermal shock experiments and DSC tests. The findings of this work indicate that the crystallinity, crystal form, and thus the products’ heat resistance of F6510 can be improved by reasonably controlling injection molding parameters such as the mold temperature and cooling time.","PeriodicalId":146276,"journal":{"name":"Volume 3: Advanced Materials: Design, Processing, Characterization and Applications; Advances in Aerospace Technology","volume":"216 1","pages":"0"},"PeriodicalIF":0.0,"publicationDate":"2022-10-30","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"122389462","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Vision Based Safe Navigation of UAV for Overhead Line Inspection Enabled by Virtual Safety Bubble 基于虚拟安全气泡的架空线路巡检无人机视觉安全导航
Rufaidah Salim, Mahmoud Rezk, Mohammed Minhas Anzil, Nawal Aljasmi, Amit Shukla
Energy transmission systems have expanded significantly, given the increase in demand for power generation. This increase in size has led to the need of a robust inspection method. Overhead Line (OHL) systems consist of many critical components such as insulators, poles, and power lines, which need to be inspected regularly. With recent advancements, drones equipped with multiple sensors are flown, either manually or autonomously, for inspection. This paper proposes autonomous vision-based navigation of the drone over OHL. The navigation is achieved through the feedback from the camera onboard the drone. A deep learning-based model is developed for the detection of the various OHL components, which are then utilized to design the path for the drone to navigate. Furthermore, a virtual safety bubble (VSB) is developed around the drone upon the detection of the components. This VSB is part of local autonomy of the drone and ensures that a constant safe distance is always maintained from the components. This approach can help reduce the overall inspection time of OHL with less cognitive load on the operator. It also ensures the safety of the OHL installations and drone. Although the paper focuses mainly on running the experiments in a simulation environment, this could be imitated in real-life situations.
由于发电需求的增加,能源传输系统已显著扩大。这种尺寸的增加导致需要一种强大的检查方法。架空线路(OHL)系统由许多关键部件组成,如绝缘子、电线杆和电力线,需要定期检查。随着最近的进步,配备了多个传感器的无人机可以手动或自动飞行,以进行检查。本文提出了一种基于视觉的无人机在OHL上的自主导航方法。导航是通过无人机上的摄像头反馈来实现的。开发了一种基于深度学习的模型,用于检测各种OHL组件,然后利用这些组件设计无人机导航的路径。此外,在检测到组件后,在无人机周围形成虚拟安全气泡(VSB)。该VSB是无人机局部自治的一部分,并确保始终与组件保持恒定的安全距离。该方法减少了操作者的认知负荷,减少了OHL的整体检测时间。它还确保了OHL装置和无人机的安全。虽然本文主要侧重于在模拟环境中进行实验,但这可以在现实生活中进行模拟。
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引用次数: 0
Design and Development of Novel α-SiAlON/Co and α-SiAlON/TiCN Composites for Cutting Tool Inserts 新型刀具刀具用α-SiAlON/Co和α-SiAlON/TiCN复合材料的设计与开发
Amer D. Alotaibi, A. Abubakar, S. S. Akhtar, A. Hakeem, K. Al-Athel, A. Arif
The present study deals with the development of α-SiAlON-4%Co and α-SiAlON-20%TiCN ceramic composites with desirable properties tailored for enhanced high-cutting tool performance. The effective medium theories and mean-field homogenization schemes are used to design and optimize the volume fractions, the interfacial thermal resistance, and reinforcement particle sizes while incorporating the influence of porosity on the effective properties of the ceramic composites. The designed composites are fabricated via the spark plasma sintering process. The ceramic samples are characterized/analyzed via scanning electron microscopy, energy dispersive spectroscopy, and x-ray diffraction. The effective thermal and structural properties of the composites are measured and compared to that of the computational predictions. The results indicate that excellent densification in α-SiAlON-based composites can be achieved by the use of spark plasma sintering process. Experimentally measured properties of SiAlON-20%TiCN composite compare well with that of the computational predictions and have shown significant enhancement in its effective thermal conductivity and fracture toughness. The measured properties of SiAlON-4%Co composite did not meet the predictions due to Co agglomeration and the large thermal mismatch between the matrix and the inclusion, which emphasizes the need to optimize the synthesis process and establish volume fraction limits of Co in α-SiAlON ceramic composites.
本研究涉及α-SiAlON-4%Co和α-SiAlON-20%TiCN陶瓷复合材料的开发,这些复合材料具有增强高切削刀具性能所需的理想性能。利用有效介质理论和平均场均匀化方法,设计和优化了体积分数、界面热阻和增强颗粒尺寸,同时考虑了孔隙率对陶瓷复合材料有效性能的影响。所设计的复合材料采用火花等离子烧结工艺制备。陶瓷样品通过扫描电子显微镜、能量色散光谱和x射线衍射进行表征/分析。测量了复合材料的有效热性能和结构性能,并与计算预测结果进行了比较。结果表明,火花等离子烧结工艺可使α- sialon基复合材料获得良好的致密化效果。SiAlON-20%TiCN复合材料的实验测量性能与计算预测结果吻合良好,有效导热系数和断裂韧性均有显著提高。结果表明,α-SiAlON -4%Co复合材料由于Co的团聚和基体与夹杂物之间存在较大的热失配,其性能不符合预测结果,需要优化合成工艺,建立Co在α-SiAlON陶瓷复合材料中的体积分数限制。
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引用次数: 0
An Evolutionary Aeroelastic Design Approach for Spars and Ribs of Flying Wing Aircraft 飞翼飞机翼梁和肋部气动弹性演化设计方法
M. Moshtaghzadeh, N. Rangel, A. Bejan, Pezhman Mardanpour
The purpose of this paper is to examine how rib configurations and spar configurations influence flying wing stability. Flying wing aircraft exhibit enhanced flutter characteristics when stresses flow smoothly through the wing. We prevent stress strangulation through spar cross-sections by changing the configuration in the plunge direction. We employ and develop computer programs Gmsh, Variational Asymptotic Beam Sectional Analysis, MATLAB scripts, and Nonlinear Aeroelastic Trim and Stability of High Altitude Long Endurance Aircraft. The configurations are designed by considering the same material, mass, and flight conditions. The results indicate that the design with the smoother stress distribution through the wing has a higher flutter speed. It is shown that the σ11 and Von-Misses stress distributions have an important effect on the stability of a flying wing aircraft.
本文的目的是研究翼肋结构和翼梁结构对飞翼稳定性的影响。当应力平稳流过机翼时,飞翼飞机表现出增强的颤振特性。我们通过改变纵深方向的结构来防止应力扼杀。我们采用并开发了Gmsh、变分渐近波束截面分析、MATLAB脚本和高空长航时飞机非线性气动弹性配平与稳定等计算机程序。这些配置是通过考虑相同的材料、质量和飞行条件来设计的。结果表明,翼内应力分布更平滑的设计具有更高的颤振速度。结果表明,σ11和Von-Misses应力分布对飞翼飞机的稳定性有重要影响。
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引用次数: 0
Thermo-Mechanical Properties of SiC-Mineral Binder Composites for Space Applications 空间应用sic -矿物粘结剂复合材料的热力学性能
S. Chandrasekaran, A. el-Ghannam, J. Monroe, Chengying Xu
Due to its excellent stiffness, thermal stability and low density, silicon carbide (SiC) is an excellent candidate for fabrication of lightweight substrates for space mirrors in telescopes and satellites. However, the strong Si-C covalent bond induces high thermal stability and mechanical strength which makes it difficult to manufacture dense SiC. Other ceramic mirror materials such as Cordierite (CO720) by Kyocera® and Spodumene (ZERODUR®) by Schott® are characterized by their light weight, near zero thermal expansion coefficient and excellent thermal properties. However, mirrors made of cordierite or spodumene have relatively low stiffness and unsatisfactory thermal conductivity. We hypothesize that composites made of SiC-Cordierite and SiC-Spodumene can serve as better mirror substrates characterized by high stiffness, high thermal conductivity and improved thermomechanical stability. The present study reports on the synthesis and characterization of SiC-Cordierite (SiC-Cord) and SiC-Spodumene (SiC-Spod) using powder metallurgy method. The densification and thermomechanical stability of the SiC-mineral composites are enhanced by a novel in situ mineralization mechanism at the interface between the SiC and mineral binders between 800 °C and 1200 °C. The densities of SiC-Cord and SiC-Spod composites were 2.74 g/cc and 2.61 g/cc, respectively, while the thermal conductivities were 6.737 W/m. K and 3.281 W/m. K, respectively. Polishing the SiC-Cord with SiC grit numbers 400–1200 and diamond/silica slurry resulted in a mirror surface with an average roughness of 2.32 nm on SiC particles. The nano indentation stiffness of the polished SiC-Cordierite composite measured 239.9 ± 20.6 GPa. The stiffness of the SiC-Cord composite is superior to that of pure cordierite (140 GPa) or Zerodur (80 GPa). The average Vickers hardness of SiC-Cordierite was 8.12 ± 4.5 GPa which was superior to that of Zerodur (6.08 GPa) and comparable to that of pure cordierite (8–8.5 GPa). The composite samples demonstrated high thermal shock resistance as indicated by their comparable compressive strength and dimensional stability before and after quenching from 1200 °C to room temperature in water. Taken altogether, the superior thermomechanical properties of SiC-Cordierite and SiC-Spodumene suggest their suitability for mirrors in space-based telescopes.
碳化硅(SiC)由于其优异的刚度、热稳定性和低密度,是制造望远镜和卫星空间反射镜的轻质衬底的理想候选材料。然而,由于硅碳共价键强,其热稳定性和机械强度较高,因此难以制造致密的碳化硅。其他陶瓷镜面材料,如京瓷(Kyocera®)的堇青石(CO720)和肖特(Schott®)的锂辉石(ZERODUR®),其特点是重量轻,热膨胀系数接近于零,热性能优异。然而,堇青石或锂辉石制成的镜子刚度相对较低,导热性也不理想。我们假设sic -堇青石和sic -锂辉石复合材料具有高刚度、高导热性和更好的热机械稳定性,可以作为更好的镜面基板。本文报道了采用粉末冶金方法合成sic -堇青石(SiC-Cord)和sic -锂辉石(SiC-Spod)并对其进行了表征。SiC-矿物复合材料的致密性和热机械稳定性在800 ~ 1200℃之间通过SiC-矿物结合剂界面的原位矿化机制得到增强。SiC-Cord和SiC-Spod复合材料的密度分别为2.74 g/cc和2.61 g/cc,导热系数为6.737 W/m。K和3.281 W/m。分别K。用SiC颗粒数400-1200和金刚石/硅浆抛光SiC- cord, SiC颗粒的镜面平均粗糙度为2.32 nm。抛光后的sic -堇青石复合材料的纳米压痕刚度为239.9±20.6 GPa。SiC-Cord复合材料的刚度优于纯堇青石(140 GPa)或Zerodur (80 GPa)。sic -堇青石的平均维氏硬度为8.12±4.5 GPa,优于Zerodur (6.08 GPa),与纯堇青石的维氏硬度(8 ~ 8.5 GPa)相当。复合材料样品在1200°C至室温水中淬火前后具有相当的抗压强度和尺寸稳定性,表明其具有较高的抗热震性。综上所述,sic -堇青石和sic -锂辉石优越的热机械性能表明它们适合用作天基望远镜的反射镜。
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引用次数: 0
期刊
Volume 3: Advanced Materials: Design, Processing, Characterization and Applications; Advances in Aerospace Technology
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