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Effect of molar concentration on the optical and structural properties of ZnO thin films prepared by chemical bath deposition method 摩尔浓度对化学浴沉积法制备ZnO薄膜光学和结构性能的影响
Pub Date : 2020-12-10 DOI: 10.31257/2018/jkp/2020/120110
Qasim Chfat Abdulridha, H. A. Noor
Article history: Received: 30 JUN, 2020 Accepted: 20 ABR., 2020 Available Online: 25 JUN., 2020 This research included the preparation of (ZnO) thin films by CBD technique for the deposition of chemical bath thickness (150 ± 20nm). X-ray diffraction was analyzed and showed that the films crystallize in a polycrystalline hexagonal structure, with a preferred direction along the level (100). Increased volume of calculated crystals for deposited films was found by increasing molar concentration. The surface morphology of films was studied by SEM, and the surface morphology of ZnO films is a heterogeneous distribution. The optical properties of all deposited ZnO films contained a spectral permeability and absorption spectrum in the wavelength range (300-1100nm), and the transmittance decreased with increasing molar concentration, it was found that the value of the light energy gap (Eg) increases with increasing molecular concentration band gap between 3.1 and 3.2 eV. DOI: http://dx.doi.org/10.31257/2018/JKP/2020/120110 K e y w o r d s : Zinc oxide chemical bath deposition method structural properties Optical Properties تيشغلأ تيبيكرتلاو تيرصبلا صاوخلا ىلع يلوملا زيكرتلا ريثأت ZnO مامحلا بيسرت تقيرطب ةرضحملا تقيقرلا يئايميكلا رون يلع نيسح اضرلا دبع ثافج نساق قاشعلا ، ةيسداملا ةعهاج ، ةيبشتلا ةيلك ءايضيفلا نسل :تيحاتفملا ثاملكلا لا ــــ خ ـــ صلا ـــ ت ZnO يئايويكلا ماوحلاب بيسشتلا ةميشط ةيبيكشتلا صئاصخلا ةيشصبلا صئاصخلا ييل ةييميلشلا ةيييةقيا شيييضحح يوييضح ،ةييساسذلا ازييا يييف ZnO ةيييٌمتب ) CBD نييح تيييح كوسب يئايويك ماوح بيسشح 051 ± 01 ى يييبحأ ةيٌييسلا ةعيايا دمييح يييلحح نيح )شتهمًايً متييسولا مييط ييل يييضفه ٍايي حا ييه ، فاسمييلبلا دذييعته ةيييساذس ةيييٌب يييف سمييلبتح ةيييةقيا 011 داييص كييشط يي ةبيسشتولا ةييةق ل ةبميسحولا فاسميلبلا ني ح داييص يل سمثعلا نح ) ضيكشتلا ةحيسامب م يف ل يححيسلا يكةتلا ةساسد نح كلزك يلمولا SEM يححيسلا يكيةتلاأ ، م يفي ZnO ييو ل ةيشيصبلا اميخلا ى بئايتٌلا حيجأ تييح وًاي ته شييق ييصمح ميا ةيةق ZnO يجميولا ميحلا قايحً ييف ايصتها اييطأ ةييفيط ةيرافً ل يمتحح ةبسشولا JOURNAL OF KUFA–PHYSICS | Vol. 12, No. 1 (2020) Qasim Chfat Abdulridha, Hussein Ali Noor 67
文章历史:收稿日期:2020年6月30日本研究包括用CBD技术制备(ZnO)薄膜,用于化学浴厚度(150±20nm)的沉积。x射线衍射分析表明,薄膜结晶为六角形多晶结构,沿水平(100)方向优先结晶。随着摩尔浓度的增加,沉积膜的计算晶体体积增加。通过扫描电镜对薄膜的表面形貌进行了研究,发现ZnO薄膜的表面形貌呈非均匀分布。所得ZnO薄膜的光学性质在300 ~ 1100nm波长范围内均具有光谱渗透率和吸收光谱,透射率随摩尔浓度的增加而降低,光能隙(Eg)值随分子浓度的增加而增加,带隙在3.1 ~ 3.2 eV之间。[DOI: http://dx.doi.org/10.31257/2018/JKP/2020/120110] K . y . w .d .]氧化锌的化学浴沉积方法结构属性光学性质تيشغلأتيبيكرتلاوتيرصبلاصاوخلاىلعيلوملازيكرتلاريثأت氧化锌مامحلابيسرتتقيرطبةرضحملاتقيقرلايئايميكلارونيلعنيسحاضرلادبعثافجنساققاشعلا،ةيسداملاةعهاج،ةيبشتلاةيلكءايضيفلانسل:تيحاتفملاثاملكلالاــــخـــصلاـــت氧化锌يئايويكلاماوحلاببيسشتلاةميشطةيبيكشتلاصئاصخلاةيشصبلاصئاصخلاييلةييميلشلاةيييةقياشيييضححيوييضح،ةييساسذلاازييايييف氧化锌ةيييٌمتب)CBDنييحتيييحكوسبيئايويكماوحبيسشح051±01ىيييبحأةيٌييسلاةعيايادمييحيييلححنيح)شتهمًايًمتييسولامييطييليييضفهٍاييحاييه،فاسمييلبلادذييعتهةيييساذسةيييٌبيييفسمييلبتحةيييةقيا011داييصكييشطييةبيسشتولاةييةقلةبميسحولافاسميلبلانيحداييصيلسمثعلانح)ضيكشتلاةحيسامبميفليححيسلايكةتلاةساسدنحكلزكيلمولاSEMيححيسلايكيةتلاأ،ميفي氧化锌ييولةيشيصبلااميخلاىبئايتٌلاحيجأتييحوًايتهشييقييصمحمياةيةق氧化锌يجميولاميحلاقايحًييفايصتهااييطأةييفيطةيرافًليمتححةبسشولا杂志刘建军,刘建军,刘建军,等。物理学报,Vol. 12, No. 1 (2020
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引用次数: 0
Study the Effect of Thickness on Optical Properties of Titanium Dioxide (TiO2) That Preparation of Via the Sol-Gel Process 研究厚度对溶胶-凝胶法制备二氧化钛(TiO2)光学性能的影响
Pub Date : 2020-12-10 DOI: 10.31257/2018/jkp/2020/120111
Mohammed Sami Abdali, Ahmed S. Hussein, M. H. Shinen
This research, study the effect of the thickness on titanium dioxide (TiO2) , that prepared by the Sol-Gel Process method on the optical properties of (TiO2) thin film with different thickness (54, 64 and 89 nm), the thickness effect on optical properties (energy gap , absorbance spectrum, transmittance spectrum, reflectance, refractive index, extinction coefficient, absorption coefficient, real and imaginary dielectric constant) ,this study shows that thickness have an effect on all these parameters .
本研究研究了溶胶-凝胶法制备的二氧化钛(TiO2)薄膜厚度对不同厚度(54、64、89 nm)薄膜光学性能的影响,厚度对薄膜光学性能(能隙、吸光光谱、透射光谱、反射率、折射率、消光系数、吸收系数、光谱线、光谱线等)的影响。实介电常数和虚介电常数),研究表明厚度对这些参数都有影响。
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引用次数: 0
Variable Optical Buffer Using EIT in Three Level System Based on Semiconductor Conical Quantum Dots 基于半导体圆锥量子点的三能级系统中使用EIT的可变光缓冲器
Pub Date : 2020-12-10 DOI: 10.31257/2018/jkp/2020/120108
N. Yaqoob, S. M. Ameen
A variable semiconductor optical buffer based on the electromagnetically induced transparency (EIT) in a three level conical quantum dot system (CQD) is theoretically investigated. The system is interacting with two (control and signal) laser beams. Signal light with subluminal velocity is possible in such system through the quantum interference effect induced by the control pump field. We investigate the refractive index and absorption spectra of the QD waveguide at different pump levels, which exhibit an optimal pump power for maximum slow-down factor (SDF). The group velocity SDF is theoretically analyzed as a function of the pump intensity at different broadened linewidths. The present study is based on the assumption that the medium is homogeneous. In this paper, a SDF as a function of CQD radius was studied. The simulation results indicate that the SDF increases with decreasing CQD radius.
从理论上研究了三能级圆锥量子点系统中基于电磁感应透明的可变半导体光缓冲器。该系统与两个(控制和信号)激光束相互作用。通过控制泵浦场诱导的量子干涉效应,可以在该系统中产生亚光速的信号光。我们研究了不同泵浦水平下QD波导的折射率和吸收光谱,得出了最大慢化因子(SDF)的最佳泵浦功率。从理论上分析了不同加宽线宽下泵浦强度对群速度SDF的影响。目前的研究是基于假设介质是均匀的。本文研究了SDF作为CQD半径的函数。仿真结果表明,SDF随CQD半径的减小而增大。
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引用次数: 0
Study the Characteristics of the nanocomposite prepared by two steps laser ablation in liquids 研究了液体中两步激光烧蚀制备的纳米复合材料的特性
Pub Date : 2020-12-10 DOI: 10.31257/2018/jkp/2020/120109
R. S. Alnayli, Zeena Hakim
In the present work, structural, optical, electrical and sensing properties have been studied for the (TiO2/rGO) nanocomposite prepared by the pulse laser ablation method in the liquid, where the Nd-Yag laser was used, and the two wave pulses (1064-532) and 300mJ, which were deposited on glass bases , The structural properties have been investigated by X-Ray diffraction technique analysis and morphological by atomic force microscope (AFM), The particle size of the membranes is less in the films prepared using wavelength (1064) than in the prepared films using wavelength (532). The optical properties of the nanocomposites have been determined by using the optical transmittance measurements in the spectral region from (300- 1100) nm. Electrical properties such as I-V properties was also studied. sensing properties measurements showed good Humidity sensitivity within the range (20-80) % RH.
本文研究了脉冲激光烧蚀法制备的(TiO2/rGO)纳米复合材料的结构、光学、电学和传感性能,采用Nd-Yag激光器,以1064-532和300mJ两个波脉冲沉积在玻璃基上,通过x射线衍射技术分析和原子力显微镜(AFM)形态学研究了其结构性能。使用波长(1064)制备的膜中的膜的颗粒尺寸小于使用波长(532)制备的膜。在(300 ~ 1100)nm光谱范围内测定了复合材料的光学性能。并对其电学性能进行了研究。传感性能测量显示在(20-80)% RH范围内具有良好的湿度灵敏度。
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引用次数: 0
Structural and Optical Properties of ZnO Nanorods Thin Films Prepared Using Hydrothermal Technique and Effect of growth time 水热法制备ZnO纳米棒薄膜的结构、光学性质及生长时间的影响
Pub Date : 2020-12-10 DOI: 10.31257/2018/JKP/2020/120208
Ahmed Ahmed S. Abed, Sattar J. Qasim, A. F. Abbas
This paper describes, Synthesis of zinc oxide nanorods (ZnO NRs) using hydrothermal technique at different growth time. The structural and morphological properties were characterized by X-ray diffraction (XRD), Energy Dispersive X-Ray (EDX) and Field Emission Scanning Electron Microscope (FE-SEM). The ZnO NRs were obvious hexangular wurtzite structure and preferentially oriented along the c-axis (002) and growth vertically to the substrates. The optical properties were studied. From UV-Visible spectrophotometer and Photoluminescence (PL), the optical band gap energy of all ZnO NRs samples (S1, S2 and S3) were calculated to be (3.425 eV, 3.4 eV, 3.425 eV) respectively. Also, the effect of growth time on ZnO nanorods was studied.
采用水热法在不同生长时间下合成氧化锌纳米棒。采用x射线衍射(XRD)、能量色散x射线(EDX)和场发射扫描电镜(FE-SEM)对其结构和形态进行了表征。ZnO NRs具有明显的六角形纤锌矿结构,优先沿c轴(002)取向,垂直于衬底生长。对其光学性质进行了研究。通过紫外可见分光光度计和光致发光(PL),计算出所有ZnO NRs样品(S1, S2和S3)的光学带隙能分别为(3.425 eV, 3.4 eV, 3.425 eV)。同时,研究了生长时间对ZnO纳米棒的影响。
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引用次数: 0
Measurements of radium and uranium concentrations in blood samples of lung cancer patients in Iraq 伊拉克肺癌患者血液样本中镭和铀浓度的测量
Pub Date : 2020-12-10 DOI: 10.31257/2018/JKP/2020/120211
F. Shaker, Iraq. Najaf, S. A. Kadhim, Emad Kareem Alsabari
In this study, 30 samples of lung cancer patients were collected from Middle Euphrates Oncology Center in Najaf, Iraq. A plastic track CR-39 Reagent technique, strippable was used to measure radium and uranium concentrations. Normality was a washing solution) NaOH ) was6.25 to clarify chemical drilling to read under the electron microscope to calculate alpha particles paths. Effective radium content values were ranged from 0.1592 Bq / kg to 3.2278 Bq / kg with an average value of 1.246Bq/kg where uranium concentrations values were ranged from 5.5671ppm to 112.8615ppm with an average value of 43.5883ppm for healthy human compared with patients were effective radium content values were found from 0.261Bq/ kg to 3.286 Bq/ kg with an average value of 1.345 Bq/kg where uranium concentrations values were found to be from 9.1099 ppm to 114.8859 ppm with an average value of 47.052ppm. A positive relationship was observed between Radium concentration and uranium concentrations in blood samples. Measurements of Radium and uranium concentrations in lung cancer patients, this research important in terms of health protection, simple and reliable analysis methods which available. DOI: http://dx.doi.org/10.31257/2018/JKP/2020/120211
本研究从伊拉克纳杰夫幼发拉底河中部肿瘤中心收集了30例肺癌患者的样本。采用可剥离的CR-39塑料磁道技术测定了镭和铀的浓度。正态是洗涤液(NaOH)为6.25澄清,在电子显微镜下读取化学钻孔,计算α粒子路径。有效镭含量值的范围从0.1592 Bq /公斤到3.2278 Bq /公斤,平均价值1.246 Bq /公斤的铀浓度范围从5.5671 ppm值112.8615 ppm的平均值43.5883 ppm人类健康与患者有效发现镭含量值从0.261 Bq /公斤到3.286 Bq /公斤,平均价值1.345 Bq /公斤的铀浓度的值被发现从9.1099 ppm, 114.8859 ppm的平均价值47.052 ppm。在血液样本中观察到镭浓度和铀浓度呈正相关关系。测定肺癌患者体内镭和铀的浓度,本研究在健康保护方面具有重要意义,分析方法简便可靠。DOI: http://dx.doi.org/10.31257/2018/JKP/2020/120211
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引用次数: 0
Study the Structural Properties and Surface Morphology of CdO Thin Films Prepared by Chemical Spray pyrolysis 化学喷雾热解法制备CdO薄膜的结构性能和表面形貌研究
Pub Date : 2020-12-10 DOI: 10.31257/2018/JKP/2020/120201
K. Saleh
CdO films were prepared using a chemical spray paralysis (CSP) method on the glass substrate at a temperature of 350 ° C and thickness (260 ± 15 nm), and study the effect annealing time (0, 1, 1.5, 2, 2.5) h at annealing temperature 450 °C on structural properties. The X-ray diffraction pattern the results showed that all CdO thin films have a polycrystalline structure and a prevalent growth in the direction (111), and the average grain size (G) in this direction ranges (29.80 - 33.23) nm. It generally increases in value while the agitation values, extraction density, number of crystals decrease by increasing the annealing time (0-2)h at annealing temperature 450 ° C of thin films. From the resulted of the atomic force microscope (AFM), the surface roughness, medium square root (RMS) and average grain size increase with the increasing of the annealing time (0-2) h, at annealing temperature 450 ° C. The thin film with annealing time 2.5 h at annealing temperature 450 °C . We note a slight decrease in the values of the coefficients ( XRD and AFM) Due to the changes in the crystal structure of thin films and beginning of cracks and crystal defects generated on the surface of the thin film during the annealing process. It has been observed in practice that the increase in the annealing time to 3 h at annealing temperature 450 ° C. led to the separation of the thin film from the substrates.
采用化学喷雾麻痹法(CSP)在温度为350℃、厚度为260±15 nm的玻璃基板上制备了CdO薄膜,研究了450℃退火时间(0、1、1.5、2、2.5)h对结构性能的影响。x射线衍射结果表明,所有CdO薄膜均呈多晶结构,且普遍沿111方向生长,该方向的平均晶粒尺寸(G)在29.80 ~ 33.23 nm之间。在450°C退火温度下,随着退火时间(0 ~ 2)h的增加,薄膜的搅拌值、萃取密度、结晶数均有所减少。从原子力显微镜(AFM)的结果来看,在450℃退火温度下,薄膜的表面粗糙度、中方根(RMS)和平均晶粒尺寸随退火时间(0-2)h的增加而增大,在450℃退火温度下退火时间为2.5 h。我们注意到系数(XRD和AFM)值略有下降,这是由于薄膜的晶体结构发生了变化,并且在退火过程中薄膜表面产生了裂纹和晶体缺陷。在实践中观察到,在450℃退火温度下,将退火时间延长至3 h会导致薄膜与衬底分离。
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引用次数: 1
The Effect of adding First Order Aberrations To Third Order Aberrations on Point Spread Function for Triangular Aperture 一阶像差加三阶像差对三角形孔径点扩散函数的影响
Pub Date : 2020-06-10 DOI: 10.31257/2018/jkp/2020/120104
Widad Hamza Tarkhan, Ahlam Habeeb Hussien, Areej Saeed Abdul Shaheed
In this work, Point Spread Function (PSF) for triangular aperture was studied, in case of ideal optical system, also in case of presence first order aberrations )focal error and tilt aberration) and third order aberrations (spherical ,coma, and astigmatism aberrations) individually, and for the same values of aberration factor )W=0.1λ …..0.5 λ ) for angle of rotation (ѱ =0). First order aberrations were added to third order aberrations, to obtain the best balance and to reduce the curve width of the (PSF), and to increase the Strehl ratio, like adding a tilt aberration to the coma aberration and adding focal error to spherical aberration and astigmatism aberration. There are some aberrations effects impact negatively on point spread function, such as focal error with coma aberration and tilt aberration with spherical aberration.
本文研究了在理想光学系统下,分别存在一阶像差(焦像差和倾斜像差)和三阶像差(球面像差、彗差和像散像差)的情况下三角孔径的点扩散函数(PSF),并且在相同的像差因子W=0.1λ .....0.5 λ)的情况下,旋转角度( =0)。在三阶像差的基础上增加一阶像差,达到最佳平衡,减小(PSF)曲线宽度,提高Strehl比,如在彗差基础上增加一个倾斜像差,在球差和像差基础上增加焦差。有些像差对点扩散函数有负面影响,如焦差与彗差、倾斜像差与球差。
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引用次数: 0
New Design of Cylindrical Rectangular Microstrip Antenna (CRMA) By Using The Slots Technique 利用槽技术设计圆柱矩形微带天线
Pub Date : 2020-06-10 DOI: 10.31257/2018/jkp/2020/120101
Nabeel A. Areebi, Zeki A. Ahmed, Mahmoud M. Aubais
A conformal antennas are plays an important role due to its multitasking possibilities , which have many opportunities in several applications. In this study, a new design of cylindrical rectangular microstrip antenna(CRMA ) excited at 〖TM〗_01 mode, was achieved in order to operate at the frequency of 5.6GHz. The simulation was done by Finite Difference Time Domain(FDTD) method using MATLAB program. The input impedance , return loss and radiation pattern of antenna were calculated and plotted. By using the slots technique and dual-layers substrate technique , the bandwidth(BW) is increased to 88.88% . Also BW is increased as the dielectric constant value is decreased.
共形天线由于其多任务处理的可能性而发挥着重要的作用,在许多应用中都有很多机会。本文设计了一种新的圆柱形矩形微带天线(CRMA),激励方式为〖TM〗_01模式,工作频率为5.6GHz。利用MATLAB程序,采用时域有限差分(FDTD)方法进行了仿真。计算并绘制了天线的输入阻抗、回波损耗和辐射方向图。采用槽技术和双层衬底技术,将带宽(BW)提高到88.88%。随着介电常数值的减小,BW也随之增大。
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引用次数: 1
Physical study of Nickel Serum Level in blood samples from Iraqi populations 伊拉克人群血液样本中镍血清水平的物理研究
Pub Date : 2020-06-10 DOI: 10.31257/2018/jkp/2020/120102
Fatima Abbas Shaker, Shaymaa Awad Kadhim alshebly
Trace elements examining of basic biological components in the human and animal body, is essential due to the increase and the decrease in them may lead to toxicity. In this study, 32 patients who were diagnosed with lung cancer in 32 healthy volunteers were compared. Serum level concentrations of Fe trace elements were measured using Atomic Absorption Spectrometry. There was statistical significance difference in nickel serum levels when comparing the mean of healthy with patient concentration, where the value of P (0.05 > p) was found. The level of serum components in the patient may be important in causing lung cancer.
微量元素对人体和动物体内基本生物成分的检测是必不可少的,因为它们的增加和减少可能导致毒性。在这项研究中,32名被诊断为肺癌的患者与32名健康志愿者进行了比较。采用原子吸收光谱法测定血清铁元素浓度。健康人与患者血清中镍含量比较,差异有统计学意义,P值< 0.05 > P。患者血清成分的水平可能是导致肺癌的重要因素。
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引用次数: 0
期刊
Journal of Kufa - Physics
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