Pub Date : 2024-01-01DOI: 10.1107/s1600577523009670
Nentwich, M., Zschornak, M., Weigel, T., Köhler, T., Novikov, D., Meyer, D.C., Richter, C.
{"title":"Treatment of multiple-beam X-ray diffraction in energy-dependent measurements","authors":"Nentwich, M., Zschornak, M., Weigel, T., Köhler, T., Novikov, D., Meyer, D.C., Richter, C.","doi":"10.1107/s1600577523009670","DOIUrl":"https://doi.org/10.1107/s1600577523009670","url":null,"abstract":"","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"105 1","pages":""},"PeriodicalIF":2.5,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138715442","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-01-01DOI: 10.1107/s1600577523009852
Silveira, A., Greving, I., Longo, E., Scheel, M., Weitkamp, T., Fleck, C., Shahar, R., Zaslansky, P.
{"title":"Deep learning to overcome Zernike phase-contrast nanoCT artifacts for automated micro-nano porosity segmentation in bone","authors":"Silveira, A., Greving, I., Longo, E., Scheel, M., Weitkamp, T., Fleck, C., Shahar, R., Zaslansky, P.","doi":"10.1107/s1600577523009852","DOIUrl":"https://doi.org/10.1107/s1600577523009852","url":null,"abstract":"","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"49 1","pages":""},"PeriodicalIF":2.5,"publicationDate":"2024-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"138716013","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-01DOI: 10.1107/S1600577523007269
Junjing Deng, Antonino Miceli, Chris Jacobsen
A fast charge-integrating detector has been showcased for high-resolution X-ray ptychography. The advancement in developing detectors of this kind, with rapid framing capabilities, holds paramount significance in harnessing the full potential of emerging diffraction-limited synchrotron sources for X-ray nanoimaging.
{"title":"Counting on the future: fast charge-integrating detectors for X-ray nanoimaging.","authors":"Junjing Deng, Antonino Miceli, Chris Jacobsen","doi":"10.1107/S1600577523007269","DOIUrl":"https://doi.org/10.1107/S1600577523007269","url":null,"abstract":"<p><p>A fast charge-integrating detector has been showcased for high-resolution X-ray ptychography. The advancement in developing detectors of this kind, with rapid framing capabilities, holds paramount significance in harnessing the full potential of emerging diffraction-limited synchrotron sources for X-ray nanoimaging.</p>","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"30 Pt 5","pages":"859-860"},"PeriodicalIF":2.5,"publicationDate":"2023-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10481263/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10169445","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Tissue density measured by synchrotron-based X-ray phase computed tomography is shown to be associated with the fragility of the ruptured mitral chordae tendineae.
二尖瓣复合体的结构特性与腱索断裂之间的联系尚不清楚。基于同步辐射的x射线相位计算机断层扫描(SR-XPCT)成像是一种定量分析三维形态的创新方法。本研究采用XPCT对二尖瓣返流患者的腱索进行评价,并分析二尖瓣返流患者腱索断裂的结构变化。在二尖瓣反流手术修复中获得6例二尖瓣腱索断裂,并用福尔马林固定。此外,从尸检中获得了12条健康的腱索。采用XPCT(有效像素尺寸,3.5µm;密度分辨率为1 mg cm-3),测量每个样品中腱索的密度。随后对标本进行病理分析。破裂组平均年龄为70.2±3.0岁,对照组平均年龄为67.2±14.1岁(p = 0.4927)。所有的SR-XPCT腱索扫描均成功完成。破裂组的平均密度为1.029±0.004,对照组的平均密度为1.085±0.015 g cm-3 (p < 0.0001)。基于SR-XPCT的二尖瓣腱索破裂的密度明显低于健康的腱索。组织学检查显示断裂腱索结缔组织成分发生变化,与SR-XPCT低密度测量一致。SR-XPCT使测量二尖瓣腱索组织密度成为可能。二尖瓣腱索的低密度与破裂的二尖瓣腱索的脆性有关。
{"title":"Structural properties in ruptured mitral chordae tendineae measured by synchrotron-based X-ray phase computed tomography.","authors":"Yojiro Koda, Takuro Tsukube, Masato Hoshino, Naoto Yagi, Hatsue Ishibashi-Ueda, Kenji Okada","doi":"10.1107/S1600577523005167","DOIUrl":"https://doi.org/10.1107/S1600577523005167","url":null,"abstract":"Tissue density measured by synchrotron-based X-ray phase computed tomography is shown to be associated with the fragility of the ruptured mitral chordae tendineae.","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"30 Pt 5","pages":"995-1002"},"PeriodicalIF":2.5,"publicationDate":"2023-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10481270/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10176197","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-01DOI: 10.1107/S1600577523006355
Wan Zhang, Dechong Zhu, Yanfeng Sui, Junhui Yue, Jianshe Cao, Jun He
Vertical beam size measurements were carried out at Beijing Electron-Positron Collider II (BEPCII) using a phase grating and an absorption grating based on the Talbot effect. The transverse coherence of synchrotron radiation is closely related to beam size. Due to the partial coherence of the synchrotron radiation source, the coherence length can be calculated by measuring the visibility decay of interferograms recorded at different distances behind the gratings. A vertical beam size of 68.19 ± 2 µm was obtained based on the relationship between the coherence length and beam size at the 3W1 beamline of BEPCII. A comparison of the vertical emittance derived from the grating Talbot method and the synchrotron radiation visible light interferometer method was presented. The vertical emittances from the two methods are 1.41 nm rad and 1.40 nm rad, respectively. The 0.1% difference indicates that the grating Talbot method for beam size measurement is reliable. This technique has great potential for small beam size measurement of fourth-generation synchrotron radiation light sources, considering its small diffraction limitation and simple experimental setups.
{"title":"Exploring beam size measurement based on the Talbot effect at BEPCII.","authors":"Wan Zhang, Dechong Zhu, Yanfeng Sui, Junhui Yue, Jianshe Cao, Jun He","doi":"10.1107/S1600577523006355","DOIUrl":"https://doi.org/10.1107/S1600577523006355","url":null,"abstract":"<p><p>Vertical beam size measurements were carried out at Beijing Electron-Positron Collider II (BEPCII) using a phase grating and an absorption grating based on the Talbot effect. The transverse coherence of synchrotron radiation is closely related to beam size. Due to the partial coherence of the synchrotron radiation source, the coherence length can be calculated by measuring the visibility decay of interferograms recorded at different distances behind the gratings. A vertical beam size of 68.19 ± 2 µm was obtained based on the relationship between the coherence length and beam size at the 3W1 beamline of BEPCII. A comparison of the vertical emittance derived from the grating Talbot method and the synchrotron radiation visible light interferometer method was presented. The vertical emittances from the two methods are 1.41 nm rad and 1.40 nm rad, respectively. The 0.1% difference indicates that the grating Talbot method for beam size measurement is reliable. This technique has great potential for small beam size measurement of fourth-generation synchrotron radiation light sources, considering its small diffraction limitation and simple experimental setups.</p>","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"30 Pt 5","pages":"910-916"},"PeriodicalIF":2.5,"publicationDate":"2023-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10481274/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10169449","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-09-01DOI: 10.1107/S1600577523005374
Tommaso Mandolini, Julien Chantel, Sébastien Merkel, Yann Le Godec, Nicolas Guignot, Andrew King, Jerome Hosdez, Laura Henry, Nadège Hilairet
The use of a high-pressure torsion apparatus to deform multi-phase aggregates under high shear strain is explored, and in situ X-ray tomography data at high pressure and high temperature are collected. Step-by-step procedures on strain measurements and image processing are outlined, and results on the studied materials are presented in 2D and 3D.
{"title":"Deformation of two-phase aggregates with in situ X-ray tomography in rotating Paris-Edinburgh cell at GPa pressures and high temperature.","authors":"Tommaso Mandolini, Julien Chantel, Sébastien Merkel, Yann Le Godec, Nicolas Guignot, Andrew King, Jerome Hosdez, Laura Henry, Nadège Hilairet","doi":"10.1107/S1600577523005374","DOIUrl":"https://doi.org/10.1107/S1600577523005374","url":null,"abstract":"The use of a high-pressure torsion apparatus to deform multi-phase aggregates under high shear strain is explored, and in situ X-ray tomography data at high pressure and high temperature are collected. Step-by-step procedures on strain measurements and image processing are outlined, and results on the studied materials are presented in 2D and 3D.","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"30 Pt 5","pages":"962-977"},"PeriodicalIF":2.5,"publicationDate":"2023-09-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10481265/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"10530742","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2023-07-01DOI: 10.1107/S1600577523004241
Claude Pradervand, Colette Rosenberg, Hans Jörg Eckerlin, Kirsten Schnorr, Andre Al Haddad, Peter Wiegand, Christoph Hess, Nazareno Gaiffi, Luc Patthey
Gas attenuators are important devices providing accurate variation of photon intensity for soft X-ray beamlines. In the SwissFEL ATHOS beamline front-end the space is very limited and an innovative approach has been taken to provide attenuation of three orders of magnitude up to an energy of 1200 eV. Additive manufacturing of a differential pumping system vacuum manifold allowed a triple pumping stage to be realized in a space of less than half a meter. Measurements have shown that the response of the device is as expected from theoretical calculations.
{"title":"A compact gas attenuator for the SwissFEL ATHOS beamline realized using additive manufacturing.","authors":"Claude Pradervand, Colette Rosenberg, Hans Jörg Eckerlin, Kirsten Schnorr, Andre Al Haddad, Peter Wiegand, Christoph Hess, Nazareno Gaiffi, Luc Patthey","doi":"10.1107/S1600577523004241","DOIUrl":"https://doi.org/10.1107/S1600577523004241","url":null,"abstract":"<p><p>Gas attenuators are important devices providing accurate variation of photon intensity for soft X-ray beamlines. In the SwissFEL ATHOS beamline front-end the space is very limited and an innovative approach has been taken to provide attenuation of three orders of magnitude up to an energy of 1200 eV. Additive manufacturing of a differential pumping system vacuum manifold allowed a triple pumping stage to be realized in a space of less than half a meter. Measurements have shown that the response of the device is as expected from theoretical calculations.</p>","PeriodicalId":17114,"journal":{"name":"Journal of Synchrotron Radiation","volume":"30 Pt 4","pages":"717-722"},"PeriodicalIF":2.5,"publicationDate":"2023-07-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://www.ncbi.nlm.nih.gov/pmc/articles/PMC10325013/pdf/","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"9792271","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"物理与天体物理","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"OA","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}