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The synthesis and single-crystal X-ray structure of the first example of a tridentate, di-orthometallated triphenyl phosphite complex 合成和单晶x射线结构的第一个例子,三齿,二正金属化亚磷酸三苯基配合物
Pub Date : 1995-01-01 DOI: 10.1039/C39950002049
R. Bedford, P. A. Chaloner, P. Hitchcock
Reaction of [Ir(cod)(py)2][PF6] with triphenyl phosphite leads to the previously reported complex [Ir(cod){P(OC6H4)(OPh)2{P(OPh)3}], but reaction of [Ir(cod){P(OPh)3}Cl] with methyllithium and subsequent treatment with methanol yields the tridentate di-orthometallated complex [IrH(cod){P(OC6H4)2(OPh)}].
[Ir(cod)(py)2][PF6]与亚磷酸三苯酯反应得到了先前报道的配合物[Ir(cod){P(OC6H4)(OPh)2{P(OPh)3}],但[Ir(cod){P(OPh)3}Cl]与甲基锂反应并随后用甲醇处理得到了三尖二正金属配合物[IrH(cod){P(OC6H4)2(OPh)}]。
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引用次数: 7
Hydrodechlorination of tetrachloromethane over supported Pt catalysts 负载型Pt催化剂上四氯甲烷的加氢脱氯
Pub Date : 1995-01-01 DOI: 10.1039/C39950002169
S. Y. Kim, H. Choi, O. B. Yanga, Kyungeun Lee, J. S. Lee, Young Gul Kim
In the selective hydrodechlorination of tetrachloromethane to chloroform, long catalytic life as well as high selectivity to chloroform is achieved over a platinum catalyst supported on MgO.
在四氯甲烷选择性加氢脱氯制氯仿中,MgO负载的铂催化剂具有较长的催化寿命和对氯仿的高选择性。
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引用次数: 35
Synthesis and structure of Mo3Te10I10 containing TeI3– ligands coordinated to a triangular cluster fragment [Mo3(µ3-Te)(µ2-Te2)3]4+ 含TeI3 -配体的三角形簇碎片[Mo3(µ3- te)(µ2-Te2)3]4+的合成与结构
Pub Date : 1995-01-01 DOI: 10.1039/C39950001559
V. Fedin, H. Imoto, Taro Saito
High-temperature reaction of molybdenum, tellurium and iodine produces Mo3Te10I10, which contains triangular cluster fragment [Mo3(µ2-Te)(µ2-Te2)3]4+ and three Tel3– ligands.
钼、碲和碘的高温反应生成Mo3Te10I10, Mo3Te10I10含有三角形簇片[Mo3(µ2-Te)(µ2-Te2)3]4+和三个Tel3 -配体。
{"title":"Synthesis and structure of Mo3Te10I10 containing TeI3– ligands coordinated to a triangular cluster fragment [Mo3(µ3-Te)(µ2-Te2)3]4+","authors":"V. Fedin, H. Imoto, Taro Saito","doi":"10.1039/C39950001559","DOIUrl":"https://doi.org/10.1039/C39950001559","url":null,"abstract":"High-temperature reaction of molybdenum, tellurium and iodine produces Mo3Te10I10, which contains triangular cluster fragment [Mo3(µ2-Te)(µ2-Te2)3]4+ and three Tel3– ligands.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"14 1 1","pages":"1559-1560"},"PeriodicalIF":0.0,"publicationDate":"1995-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86829410","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 17
A homogeneous solution method for the detection of point mutations in DNA 一种检测DNA点突变的齐次溶液方法
Pub Date : 1995-01-01 DOI: 10.1039/C39950001107
J. Coates, P. Sammes, R. West
A simple, direct method is described for the detection of point mutations in single-strand DNA, under homogeneous conditions, that uses time-resolved fluorescence spectroscopy involving EuIII ions.
本文描述了一种简单、直接的方法,用于在均匀条件下检测单链DNA中的点突变,该方法使用涉及EuIII离子的时间分辨荧光光谱。
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引用次数: 5
Peptide assembly in the absence of base via Fmoc amino acid fluorides 在没有碱基的情况下,通过Fmoc氨基酸氟化物组装肽
Pub Date : 1995-01-01 DOI: 10.1039/C39950000669
H. Wenschuh, M. Beyermann, A. El‐Faham, S. Ghassemi, L. A. Carpino, M. Bienert
Fmoc amino acid fluorides are highly efficient reagents for peptide assembly in the absence of tertiary bases, the presence of which may cause a variety of side reactions.
Fmoc氨基酸氟化物是在没有三级碱基的情况下组装肽的高效试剂,三级碱基的存在可能引起各种副反应。
{"title":"Peptide assembly in the absence of base via Fmoc amino acid fluorides","authors":"H. Wenschuh, M. Beyermann, A. El‐Faham, S. Ghassemi, L. A. Carpino, M. Bienert","doi":"10.1039/C39950000669","DOIUrl":"https://doi.org/10.1039/C39950000669","url":null,"abstract":"Fmoc amino acid fluorides are highly efficient reagents for peptide assembly in the absence of tertiary bases, the presence of which may cause a variety of side reactions.","PeriodicalId":17282,"journal":{"name":"Journal of The Chemical Society, Chemical Communications","volume":"60 1","pages":"669-670"},"PeriodicalIF":0.0,"publicationDate":"1995-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"87004126","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 18
Total synthesis of milbemycin G: synthesis of the C(1)–C(10) fragment 米贝霉素G的全合成:C(1) -C(10)片段的合成
Pub Date : 1995-01-01 DOI: 10.1039/C39950002519
Simon R. Bailey, A. Teerawutgulrag, E. Thomas
The hydroxybutenolide 5, a precursor of the C(1)–C(10) fragment of the 5-methoxy a-miibemycins, is synthesised by stereo- and regio-selective modification of the hydroxycyclohexanone 8.
羟基丁烯内酯5是5-甲氧基a-米贝霉素的C(1) - C(10)片段的前体,通过对羟基环己酮8的立体和区域选择性修饰合成。
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引用次数: 7
Electrochemical generation of a new type of dioxygen carrier complex. Reversible fixation of dioxygen by the highly electron-deficient two-electron oxidized derivative of a dicobalt face-to-face diporphyrin 一种新型二氧载体配合物的电化学生成。由高度缺电子的双电子氧化衍生物的双钴面对面双卟啉的可逆固定
Pub Date : 1995-01-01 DOI: 10.1039/C39950001441
Y. L. Mest, M. L’Her
The two-electron oxidized form of the dicobalt(II) face-to-face porphyrin dimer Co2FTF4, electrogenerated in strictly anhydrous conditions, reversibly binds dioxygen.
在严格无水条件下电生成的二钴(II)面对面卟啉二聚体Co2FTF4的双电子氧化形式可逆地结合了二氧。
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引用次数: 6
Metal-assisted activation of the C–O bond of 2-hydroxyethylmethacrylate. Synthesis and molecular structure of Ti5(OPri)9(µ-OPri)(µ,η2-OC2H4O)(µ3,η2-OC2H4O)3(µ4,η2-OC2H4O) 金属辅助活化2-羟乙基甲基丙烯酸酯的C-O键。Ti5(OPri)9(µ-OPri)(µ,η2-OC2H4O)(µ3,η2-OC2H4O)3(µ4,η2-OC2H4O)的合成及分子结构
Pub Date : 1995-01-01 DOI: 10.1039/C39950001817
N. Pajot, R. Papiernik, L. Hubert-Pfalzgraf, J. Vaissermann, S. Parraud
Ti5(OPri)9(µ-OPri)(OC2H4O)5 is formed by the reaction between Ti(OPri)4 and 2-hydroxyethylmethacrylate in toluene at room temperature; the pentanuclear aggregate is asymmetric with the titanium atoms displaying coordination numbers of five, six and seven.
Ti5(OPri)9(µ-OPri)(oc2h40o)5是由Ti(OPri)4与甲基丙烯酸2-羟乙酯在甲苯中室温反应生成的;五核聚集体是不对称的,钛原子的配位数为5、6和7。
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引用次数: 13
Synthesis and structural characterization of the first donor-stabilized phosphanetriylphosphonium cation: [Ar*PP(PPh3)]+(Ar*= 2,4,6-But3C6H2) 首个供体稳定磷酸三基磷酸阳离子[Ar*PP(PPh3)]+(Ar*= 2,4,6- but3c6h2)的合成与结构表征
Pub Date : 1995-01-01 DOI: 10.1039/C39950001383
V. Romanenko, V. L. Rudzevich, E. Rusanov, A. N. Chernega, A. Senio, J. Sotiropoulos, G. Pfister-guillouzo, Michel Sanchez
Reaction of Ar*PPNR2(Ar*= 2,4,6-But3C6H2) with CF3SO3H in the presence of triphenylphosphane in CH2Cl2produces the isolable salt [Ar*PP(PPh3)]+[CF3SO3]– which is characterized by X-ray crystallography; the triphenylphosphane ligand of [Ar*PP(PPh3)]+ readily participates in nucleophilic substitution reactions affording a novel entry to donor-stabilized phosphanetriylphosphonium cations and P-functionalized diphosphenes.
在三苯基膦存在下,Ar*PPNR2(Ar*= 2,4,6- but3c6h2)与CF3SO3H在ch2cl2中反应生成可分离盐[Ar*PP(PPh3)]+[CF3SO3] -,并用x射线晶体学对其进行了表征;[Ar*PP(PPh3)]+的三苯基膦配体容易参与亲核取代反应,为供体稳定的磷酸三基磷阳离子和p功能化的二膦提供了新的入口。
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引用次数: 22
Regioselective ortho substitution of diphenyl sulfoxide chromium tricarbonyl: complementary stereoselectivities for the mono- and di-anions 二苯基亚砜铬三羰基的区域选择性邻位取代:对单阴离子和二阴离子的互补立体选择性
Pub Date : 1995-01-01 DOI: 10.1039/C39950000817
S. Davies, Tracey Loveridge, J. Clough
The mono- and di-anions derived from diphenyl sulfoxide chromium tricarbonyl and lithium diisopropylamide show complementary Stereoselectivities in their reactions with electrophiles (D+, MeI, Me3SiCl).
由二苯基亚砜、三羰基铬和二异丙酰胺锂衍生的单阴离子和二阴离子在与亲电试剂(D+、MeI、Me3SiCl)的反应中表现出互补的立体选择性。
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引用次数: 18
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