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Strengths and Microstructure of SUS316L Fabricated by Selective Laser Melting 选择性激光熔化制备SUS316L的强度和显微组织
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-03-01 DOI: 10.2320/JINSTMET.JAW201610
Kazuki Akino, K. Kakehi
The additive manufacturing (AM) process, which can produce highly complex components, has been getting signi cant attention in both industry and academic research. Ti-based alloys, Ni-based superalloys, and Co-Cr-based alloys have been widely investigated. However, as Ni-based superalloys have precipitated phases such as the γ′ and γ′′ phases, and Ti-based alloys and Co-Cr-based alloys are multiphase alloys which have phase transformation, it is dif cult to clarify the factors in the AM process that in uence the strength of these alloys. In this study, SUS316L stainless steel, which is a single-phase solid-solution alloy and does not have precipitated phases, was used to investigate the effect of speci c factors in the AM process on anisotropy or mechanical properties, and the strengthening mechanism in the AM process in comparison with SUS316L plastic-forming (PF) material. The AM SUS316L was fabricated by selective laser melting using an ytterbium ber laser from ne metallic powder. We found that the coarse columnar grains grew up along the built direction and the dislocation cell structures which were induced during the AM process into the AM material. During the solution heat treatment, dislocation recovery was observed. The AM specimens showed higher tensile and creep strength compared with the conventional material (the PF material) because of the high dislocation density. The ductility of the AM specimens was lower than that of the conventional material because of defects caused by a lack of fusion at the molten pool boundaries. Furthermore, the specimens whose loading direction corresponds to the built direction showed lower strength and elongation than the specimens whose loading direction was perpendicular to the built direction due to the oriented defects. [doi:10.2320/matertrans.M2017163]
增材制造(AM)工艺可以生产高度复杂的部件,在工业界和学术界都受到了极大的关注。ti基合金、ni基高温合金和co - cr基合金得到了广泛的研究。然而,由于ni基高温合金存在γ′和γ′相等析出相,而ti基合金和co - cr基合金是多相合金,具有相变,因此在AM过程中影响这些合金强度的因素很难明确。本研究以不存在析出相的单相固溶合金SUS316L不锈钢为研究对象,研究增材制造过程中特定因素对其各向异性或力学性能的影响,以及增材制造过程中与SUS316L塑性成形(PF)材料相比的强化机理。以金属粉末为原料,采用选择性激光熔融法制备了AM SUS316L合金。结果表明,在AM过程中,AM材料中出现了沿构建方向生长的粗柱状晶粒和位错胞结构。固溶热处理过程中,观察到位错恢复。与常规材料(PF材料)相比,AM材料具有较高的位错密度,具有较高的拉伸和蠕变强度。增材制造试样的延展性低于常规材料,这是由于熔池边界处缺乏熔合而导致的缺陷。同时,由于取向缺陷的存在,加载方向与构建方向相对应的试件的强度和伸长率低于加载方向与构建方向垂直的试件。(doi: 10.2320 / matertrans.M2017163)
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引用次数: 7
Formation Mechanism of Lath Martensite in Steels 钢中板条马氏体的形成机理
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-02-01 DOI: 10.2320/JINSTMET.J2016033
Y. Murata
Lath martensite formed in low carbon steels plays a crucial role in the mechanical properties of heat-resistant steels containing approximately 0.1 mass%C. Lath martensite exhibits a hierarchical microstructure comprising packets, blocks and laths. Martensitic transformation is the phase transformation accompanying ordered shear deformation without atom diffusion. The hierarchical microstructure is formed as a result of the relaxation of the strain energy caused by the deformation; however, to the best of our knowledge, the formation mechanism of this microstructure has not been understood thus far. In this paper, the experimental results and phenomenological formation mechanism reported thus far are reviewed, and a new mechanism (including two types of slip deformation (TTSD) model) is introduced, which is constructed by independently considering two kinds of slip deformations using the slip deformation model proposed by Khachaturyan. In addition, the TTSD model allows for the simulation of the martensite phase formation by the phaseeld method. Furthermore, the TTSD model permits the prediction of lath martensite features including the existence of sub-blocks and high density of dislocations in lath. In particular, the presence of laths in a block structure is clearly explained by the TTSD model for the rst time. [doi:10.2320/matertrans.M2016430]
低碳钢中形成的板条马氏体对含0.1%质量%C的耐热钢的力学性能起着至关重要的作用。板条马氏体呈现由包、块和板条组成的分层微观结构。马氏体相变是伴随有序剪切变形而不发生原子扩散的相变。由于变形引起的应变能松弛,形成了分层微观结构;然而,据我们所知,这种微观结构的形成机制迄今尚未被理解。本文综述了迄今为止报道的实验结果和现象学形成机制,并介绍了一种新的机制(包括两种滑移变形(TTSD)模型),该机制是在哈查图尔良提出的滑移变形模型的基础上,独立考虑两种滑移变形而构建的。此外,TTSD模型允许通过相场法模拟马氏体相的形成。此外,TTSD模型允许预测板条马氏体特征,包括板条中存在子块和高密度位错。特别是,TTSD模型第一次清楚地解释了块结构中板条的存在。(doi: 10.2320 / matertrans.M2016430)
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引用次数: 7
Effect of Indentation Orientation on the Onset of Plastic Deformation for a MAX Phase Ti 2 AlC 压痕取向对MAX相ti2alc塑性变形开始的影响
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-01-01 DOI: 10.2320/JINSTMET.J2017042
Wada Yusuke, Sekido Nobuaki, Ohmura Takahito, Yoshimi Kyosuke
Polycrystalline Ti2AlC alloys were prepared by spark plasma sintering of high purity elemental materials, and subsequently annealed at 1500°C for 24 h. Nanoindentation behavior was studied on the grains with their surface normal directions parallel to 〈3362〉, 〈4481〉, 〈0001〉 and 〈1120〉. During loading of nanoindentation, pop–in events were found to occur for all the indentation directions. The critical loads of the first pop–in observed for the indentation directions parallel to 〈1120〉 and 〈0001〉 were higher than those for 〈3362〉 and 〈4481〉. Surface topography around the residual indents suggests that the basal slip dominates the plastic deformation upon indentation. These results suggest that the nucleation of the basal dislocation is a major barrier for the onset of plastic deformation underneath the indenter. [doi:10.2320/jinstmet.J2017042]
采用火花等离子烧结法制备了高纯度元素材料Ti2AlC多晶合金,并在1500℃下退火24 h,研究了表面法向平行于< 3362 >、< 4481 >、< 0001 >和< 1120 >晶粒的纳米压痕行为。在纳米压痕加载过程中,所有压痕方向都发生了弹出事件。平行于< 1120 >和< 0001 >的压痕方向上观察到的首次弹出临界载荷高于< 3362 >和< 4481 >。残余压痕周围的表面形貌表明,压痕后的塑性变形主要是基底滑移。这些结果表明,基底位错的形核是压头下方塑性变形发生的主要障碍。(doi: 10.2320 / jinstmet.J2017042)
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引用次数: 1
Hyperbaric-Oxygen Accelerated Corrosion Test of Iron in Cement Paste and Mortar 水泥浆和砂浆中铁的高压氧加速腐蚀试验
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-01-01 DOI: 10.2320/JINSTMET.J2017030
K. Doi, S. Hiromoto, E. Akiyama
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引用次数: 0
Hydroxyapatite Dispersed Magnesium-Based Composite Produced from Pulverized Magnesium Alloy Powder and Its Mechanical Properties 镁合金粉末制备羟基磷灰石分散镁基复合材料及其力学性能
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-01-01 DOI: 10.2320/JINSTMET.J2017036
H. Watanabe, Takane Motoyama, N. Ikeo, T. Mukai
A magnesium matrix composite made of Mg–1mass%Ca and 10 vol% hydroxyapatite (HAp) particles was synthesized. The alloy powder was processed by pulverization of the small blocks of the alloy ingot using a high–speed blade grinder. Unreacted composite was successfully produced by extruding the two component powders at a temperature of 538 K. In the extruded composites, the grains of the magnesium matrix were equiaxed and the matrix grain size was 3.9 μm. As for the HAp particles, both thin clustering and severe agglomeration with the size of ~30 μm were observed. The Young's modulus, tensile yield strength and tensile strength of the extruded composite were 39 GPa, 101 MPa and 153 MPa, respectively. The damping capacity of the composite was higher than that of extruded magnesium. The composite also showed good forgeability at a temperature of 523 K. However, quite high impurity contents of Fe (0.130 mass%) and Ni (0.010 mass%) were introduced in the magnesium matrix of the composite, probably as a result of contamination that accumulates during the processing (pulverization) of the alloy powder. [doi:10.2320/jinstmet.J2017036]
合成了由Mg-1mass %Ca和10vol %羟基磷灰石(HAp)颗粒组成的镁基复合材料。采用高速叶片磨床对合金锭块进行粉碎加工。通过在538 K的温度下挤压两组分粉末,成功制备了未反应复合材料。在挤压复合材料中,镁基晶粒呈等轴状,晶粒尺寸为3.9 μm。羟基磷灰石颗粒在~30 μm范围内存在薄团聚和严重团聚现象。挤压复合材料的杨氏模量、抗拉屈服强度和抗拉强度分别为39 GPa、101 MPa和153 MPa。复合材料的减振能力高于挤压镁合金。该复合材料在523 K温度下也表现出良好的可锻性。然而,复合材料的镁基体中引入了相当高的杂质含量Fe(0.130质量%)和Ni(0.010质量%),这可能是合金粉末加工(粉碎)过程中积累的污染造成的。(doi: 10.2320 / jinstmet.J2017036)
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引用次数: 2
Dynamic Material Flow Analysis of Copper and Copper Alloy in Global Scale —Forecast of In-Use Stock and Inputs and the Estimation of Scrap Recovery Potential— 全球范围内铜及铜合金的动态物料流分析-在用库存和投入预测及废料回收潜力估算
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-01-01 DOI: 10.2320/JINSTMET.J2017034
Akihiro Yoshimura, Yasunari Matsuno
The recovery of copper ( Cu ) from secondary sources has received much attention because of its scarcity of natural resources. In this work, we estimated the input, in - use stock and discard of copper and copper alloy during 1950 - 2015 in global scale, and forecast them until 2050. In addition, we estimated the potential of scrap recovery for copper / copper alloys. It was estimated that the total amount of in - use stock of copper and copper alloy were 177 , 000 kt and 44 , 200 kt in 2015, respectively. The in - use stock, discard and input of copper in 2050 will reach 381 , 000 - 588 , 000 kt, 15 , 400 - 22 , 200 kt and 18 , 990 - 33 , 000 kt, respectively, whereas those for copper alloy will reach 77, 500 - 134 , 000 kt, 3 , 020 - 4 , 680 kt and 3 , 760 - 7 , 200 kt, respectively. The copper content in recov - erable scraps of copper and copper alloy will reach 15 , 100 - 27 , 300 kt, and this accounts for 55 . 1 - 79 . 0 % of copper content in annual input of copper and copper alloy in 2050. The range in forecast was caused by the difference in the saturation amount
从二次源中回收铜由于其天然资源的稀缺性而备受关注。在这项工作中,我们估计了1950 - 2015年全球范围内铜和铜合金的投入、在用库存和丢弃量,并预测了它们到2050年的变化。此外,我们估计了铜/铜合金废料回收的潜力。据估计,2015年中国铜及铜合金在用库存总量分别为17.7万吨和44.20万吨。2050年,铜的使用存量、丢弃量和投入量将分别达到38.1万~ 58.8万kt、1.54万~ 2.22万kt和1.990万~ 3.33万kt,而铜合金的使用存量、丢弃量和投入量将分别达到7.75万~ 13.4万kt、3.020 ~ 4.68万kt和3.760 ~ 7.20万kt。铜及铜合金可回收废料中铜的含量可达15、100 ~ 27、300 kt,占总铜的55%。1 - 79。2050年铜及铜合金年投入中铜含量达到0%。预报偏差是由于饱和量的差异造成的
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引用次数: 4
Dependence of Load Angle on Static Strength of Resistance Spot Welded Lap Joint in Combined Load Test 组合载荷试验中载荷角对电阻点焊搭接接头静强度的影响
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-01-01 DOI: 10.2320/JINSTMET.J2017040
T. Akiyama, T. Kitamura, Tetsushi Ono
Strength of resistance spot welded lap joint is a very interesting task. JIS prescribes tensile shear test and cross tension test as a realistic environment in combined load. Then, a lot of strength prediction equations have been proposed. And these features are in the use of a threshold value based on the base material strength as a fracture condition. The relational expression between the cross tension strength and the opening angle deals only with the infl uence of the opening angle on the axial force acting geometrically on the base metal. But it explains the experimental results well. The strength of resistance spot welded lap joint in combined load is known to exhibit dependence of load angle. But it is not clear whether the cause is only the geometric infl uence as shown by the past equations or the fracture mechanism change depend on the load angle. In this study, we examined how much dependence of load angle can be explained by macro geometric factors using a material dynamics model, before studying the micro fracture mechanism depend on the load angle in the vicinity of the crack initiation part of the nugget. As a result, we were able to explain the dependence of load angle with the macro model. [doi:10.2320/jinstmet.J2017040]
电阻点焊搭接接头的强度是一个非常有趣的课题。JIS规定拉伸剪切试验和交叉拉伸试验作为组合载荷下的现实环境。然后,提出了许多强度预测方程。而这些特征都是在使用一个阈值为基础的基材强度作为断裂条件。交叉拉伸强度与开口角之间的关系式只考虑开口角对作用在母材上的几何轴向力的影响。但它很好地解释了实验结果。已知电阻点焊搭接接头在复合载荷下的强度与载荷角度有关。但断裂的原因究竟是由以往方程所显示的几何影响,还是由于载荷角度的变化导致断裂机制的改变,目前还不清楚。在本研究中,我们利用材料动力学模型考察了宏观几何因素对载荷角的依赖程度,然后研究了核块裂纹起裂部位附近载荷角对微观断裂机制的依赖程度。因此,我们能够解释载荷角与宏观模型的相关性。(doi: 10.2320 / jinstmet.J2017040)
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引用次数: 0
Incremental feeding high-pressure sliding for achieving large area of severe plastic deformation 渐进式高压滑动,实现大面积剧烈塑性变形
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2018-01-01 DOI: 10.2320/JINSTMET.J2017038
Y. Takizawa, Kyohei Watanabe, T. Kajita, Kosei Sumikawa, T. Masuda, M. Yumoto, Yoshiharu Otagiri, Z. Horita, Z. Horita
In this study, high - pressure sliding is combined with incremental feeding so that a severely deformed area is enlarged without increasing the machine capacity. With this combined process ( called the incremental feeding high - pressure sliding: IF - HPS ) , a sheet sample is lateraly fed every after sliding under high pressure. The IF - HPS process was applied to a Ni - based superalloy ( Inconel 718 ) and a Ti - 6Al - 7Nb alloy ( F1295 ) for grain refinement. The applicability of the IF - HPS process is examined with the advent of superplasticity through the grain refinement. Vickers microhardness measurement shows that the hardness is higher in the area of the second pass than the first pass for both Inconel 718 and F1295 but the hardness increase is more prominent in the area where the second passes is superimposed on the first passparticularly for the Inconel 718. After tensile testing, superplastic elongation more than 400 % appears in the superimposed areas of both Inconel 718 and F1295. For the F1295 alloy, the area of the second pass also exhibits a suplerplastic elongation of 400 % . Analysis by finte element method ( FEM ) reveals that strain introduced by outwardflow from the severely deformed area is sensitive to friction coefficient between the sample and anvil outside of the flat contact area. The strain due to this outwardflow conributes to the grain refinement in the second pass for the F1295 alloy but insuf ficient for the Inconel 718. [ doi:10 . 2320 / jinstmet.J2017038 ]
在本研究中,高压滑动与增量进给相结合,在不增加机器容量的情况下,扩大了严重变形的区域。通过这种组合过程(称为增量进料高压滑动:IF - HPS),薄片样品在高压下滑动后每次横向进料。采用IF - HPS工艺对镍基高温合金(Inconel 718)和Ti - 6Al - 7Nb合金(F1295)进行晶粒细化。通过晶粒细化,验证了IF - HPS工艺的适用性。维氏显微硬度测量表明,Inconel 718和F1295在第二道次的硬度高于第一道次,但在第二道次与第一道次叠加的区域,硬度增加更为明显,尤其是Inconel 718。经拉伸试验,Inconel 718和F1295的叠加区均出现超过400%的超塑性伸长率。对于F1295合金,第二道次的超塑性伸长率也达到400%。有限元分析表明,从严重变形区向外流动所引入的应变对试样与平面接触区外砧间的摩擦系数很敏感。由于这种向外流动而产生的应变有助于F1295合金在第二道次中细化晶粒,但对于Inconel 718则不够。[doi:10]2320 / jinstmet。J2017038]
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引用次数: 6
最高温度が 1073 KにおけるNb含有フェライト系ステンレス鋼の熱疲労過程の組織変化 最高温度为1073k的含Nb铁氧体不锈钢热疲劳过程中的组织变化
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2017-12-01 DOI: 10.2320/JINSTMET.JC201701
純一 濱田, 尚希 森弘, 治彦 梶村
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引用次数: 0
Influence of Yttrium Addition on Plastic Deformation of Magnesium 添加钇对镁塑性变形的影响
4区 材料科学 Q4 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2017-12-01 DOI: 10.2320/JINSTMET.J2017016
Hiroaki Rikihisa, Takashi Mori, M. Tsushida, H. Kitahara, S. Ando
In this study, tensile tests of Mg - Y alloy single crystals and polycrystals were carried out to investigate influence of yttrium on activities of slip systems and a relationship between ductility of magnesium and active slip systems. Tensile directions of the single crystals and the polycrystals were parallel to ( 0001 ) and its rolling direction, respectively. Both tests were carried out at room temperature. Yield stress and ductility of Mg -( 0 . 6 - 1 . 1 ) at % Y alloy single crystals were higher than that of pure Mg and the crystals were yielded due to first order pyramidal slip ( FPCS ) . Mg - 0 . 9 at % Y alloy polycrystals showed higher ductility than pure Mg. The number of grains in which second order pyramidal slip can be activated was larger than that of non - basal slips in pure Mg, while the number for FPCS was increased with increasing strain in Mg - 0 . 9 at % Y alloy. We supposed that high ductil - ity of Mg - 0 . 9 at % Y alloy would be caused activation of FPCS by yttrium addition. [ doi:10 . 2320 / jinstmet.J2017016 ]
本研究通过对Mg - Y合金单晶和多晶的拉伸试验,探讨了钇元素对滑移体系活性的影响,以及镁元素的延展性与滑移体系的关系。单晶和多晶的拉伸方向分别平行于(0001)及其轧制方向。两项试验均在室温下进行。Mg -(0)的屈服应力和塑性。6比1。1)与纯Mg相比,at % Y合金单晶含量更高,单晶是由于一阶锥体滑移(FPCS)产生的。Mg - 0。9at % Y合金多晶具有比纯Mg更高的延展性。在Mg - 0中,二级锥体滑移激活的晶粒数量大于非基滑移激活的晶粒数量,而FPCS的数量随着应变的增加而增加。9at % Y合金。我们假设Mg - 0的高延展性。添加钇会引起FPCS的活化。[doi:10]2320 / jinstmet。J2017016]
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引用次数: 15
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Journal of The Japan Institute of Metals
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