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Masthead: Materials and Corrosion. 7/2024 刊头:材料与腐蚀7/2024
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-07-04 DOI: 10.1002/maco.202470072
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引用次数: 0
RETRACTION: Fabrication of a superhydrophobic surface on al alloy 5052 via combined anodic oxidation and fluorination treatment 返回:通过阳极氧化和氟化联合处理在合金 5052 上制造超疏水表面
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-28 DOI: 10.1002/maco.202470611

RETRACTION: Lkhagvaa Telmenbayar, Tumur-Ochir Erdenebat, Minjung, Daejeong Yang, Ramu Adam Gopal, Dongjin Choi Fabrication of a superhydrophobic surface on Al alloy 5052via combined anodic oxidation and fluorination treatment, published in Materials and Corrosion, DOI 10.1002/maco.202012190. The above article, published online on 03 March 2021 in Wiley Online Library (wileyonlinelibrary.com), has been withdrawn by agreement between the journal JPM Regina Hagen, Author Dongjin Choi, and Wiley-VCH. The withdrawal has been agreed upon following that there was a minor problem with the materials authors used and they plan to resubmit after additional experiments. wileyonlinelibrary.com/journal/maco Materials and Corrosion. 2021;1–9.

撤回:Lkhagvaa Telmenbayar、Tumur-Ochir Erdenebat、Minjung、Daejeong Yang、Ramu Adam Gopal、Dongjin Choi 通过阳极氧化和氟化联合处理在铝合金 5052 上制造超疏水表面,发表于《材料与腐蚀》,DOI 10.1002/maco.202012190。上述文章于 2021 年 3 月 3 日在线发表于 Wiley Online Library (wileyonlinelibrary.com),经期刊 JPM Regina Hagen、作者 Dongjin Choi 和 Wiley-VCH 同意,已被撤回。作者使用的材料出现了小问题,他们计划在进行更多实验后重新提交。2021;1-9.
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引用次数: 0
Corrosion studies of SS 316H and Alloy 617 in thermally purified molten NaF-KF-UF4-UF3 salts SS 316H 和合金 617 在热纯化熔融 NaF-KF-UF4-UF3 盐中的腐蚀研究
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-27 DOI: 10.1002/maco.202414299
Qiufeng Yang, Amanda Leong, Jinsuo Zhang

The study investigates salt chemistry and corrosion behavior of SS 316H and Alloy 617 in thermally purified molten NaF-KF-UF4-UF3 salts (UF4/UF3 initial ratio 12–14) at 800°C for 120, 72, and 32 h. UF4/UF3 ratio increases after corrosion tests. Cr species concentration in salts keeps increasing. Fe, Co, Ni, and Mo species increase first, then decrease. Cr/Mn oxides are formed along grain boundaries in SS 316H. Cr near the surface of Alloy 617 is completely depleted. A thin layer composed of Fe, Co, Ni, and Mo is observed on the Alloy 617 surface in 72-h and 32-h tests.

本研究调查了 SS 316H 和合金 617 在 800°C、120、72 和 32 小时的热纯化熔融 NaF-KF-UF4-UF3 盐(UF4/UF3 初始比为 12-14)中的盐化学性质和腐蚀行为。盐中的铬物种浓度不断增加。铁、钴、镍和钼物种先增加后减少。在 SS 316H 中,铬/锰氧化物沿晶界形成。合金 617 表面附近的铬已完全耗尽。在 72 小时和 32 小时试验中,在合金 617 表面观察到由铁、钴、镍和钼组成的薄层。
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引用次数: 0
Study of effects of rare earth elements on the corrosion behavior of weathering steels under a simulated immersion environment and a real atmospheric environment 研究稀土元素对模拟浸泡环境和真实大气环境下风化钢腐蚀行为的影响
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-18 DOI: 10.1002/maco.202414447
Zengwei Fan, Zhong Xi, Tengshi Liu, Xintong Lian, Xicheng Wei, Han Dong

The effects of rare earth elements (REEs) on the corrosion behavior of weathering steels under a simulated immersion environment and a real atmospheric environment have been investigated in this paper. Although the corrosion rate of the indoor accelerated corrosion experiment (0.01 mol/L NaHSO3) is much higher than that of the real atmospheric exposure experiment, the addition of REEs can highly improve the corrosion resistance of test steels under both conditions. The improvement of the corrosion resistance can be attributed to the quick transformation of γ-FeOOH into α-FeOOH and the accelerated formation of a stable rust layer by REEs. Furthermore, the segregation of the REE inner rust layer increases the density of the rust layer and prevents corrosive particles from eroding the matrix. REEs can also promote the segregation of Cu, Cr, and other alloying elements in the rust layer, thus blocking the cracks and holes and enabling the formation of a continuous rust layer with good adhesion.

本文研究了稀土元素 (REE) 在模拟浸泡环境和真实大气环境下对风化钢腐蚀行为的影响。虽然室内加速腐蚀实验(0.01 mol/L NaHSO3)的腐蚀速率远高于真实大气暴露实验的腐蚀速率,但在这两种条件下,稀土元素的添加都能极大地提高试验钢的耐腐蚀性。耐腐蚀性能的提高可归因于 REEs 可使 γ-FeOOH 快速转化为 α-FeOOH,并加速形成稳定的锈层。此外,REE 内锈层的偏析可增加锈层的密度,防止腐蚀颗粒侵蚀基体。稀土元素还能促进锈层中铜、铬和其他合金元素的偏析,从而堵塞裂缝和孔洞,形成具有良好附着力的连续锈层。
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引用次数: 0
Sulfide stress corrosion (SSC) susceptibilities of duplex stainless steels 2205 produced by powder metallurgy (HIP) and hot rolling 粉末冶金(HIP)和热轧生产的双相不锈钢 2205 的硫化物应力腐蚀(SSC)敏感性
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-16 DOI: 10.1002/maco.202414418
T. S. Barros, S. S. M. Tavares, A. R. Pimenta, R. T. Batista, J. A. C. Velasco

Owing to their excellent properties, duplex stainless steels (DSSs) may be selected for the H2S environment. Operational limits are not defined and depend on fabrication processes. In this work, the susceptibilities of two DSSs 2205 to sulfide stress corrosion (SSC) in saline solutions with three pH levels were investigated. The difference between materials is the fabrication route: hot rolled (HR) tubes and powder metallurgy with compacting and sintering final operations by hot isostatic pressing (PM-HIP). The susceptibility parameters were evaluated by slow strain rate tensile tests (SSRT). Both materials suffered embrittlement in solutions with pH 3.5 and 4.5, but the susceptibility was slightly better in the HR. In the solution with pH 5.5, the HR fractured with ductile behavior, while the PM-HIP was brittle. The better resistance of HR to SSC can be explained by microstructural features, such as the lower grain size and austenite island interspace.

由于双相不锈钢(DSS)具有优异的性能,因此可用于 H2S 环境。其操作限制尚未确定,且取决于制造工艺。在这项工作中,研究了两种双相不锈钢 2205 在三种 pH 值的盐溶液中对硫化物应力腐蚀(SSC)的敏感性。两种材料的不同之处在于制造工艺:热轧(HR)管和粉末冶金,最后通过热等静压(PM-HIP)进行压实和烧结。通过慢应变速率拉伸试验(SSRT)评估了易损性参数。在 pH 值为 3.5 和 4.5 的溶液中,两种材料都发生了脆化,但 HR 材料的易脆性稍好一些。在 pH 值为 5.5 的溶液中,HR 发生韧性断裂,而 PM-HIP 则发生脆性断裂。HR对SSC的耐受性更好,这可以从微观结构特征(如较小的晶粒尺寸和奥氏体岛间隙)中得到解释。
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引用次数: 0
Corrosion and degradation behavior of bent aluminum and copper pipes for practical use in air conditioning 空调中实际使用的弯曲铝管和铜管的腐蚀和降解行为
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-12 DOI: 10.1002/maco.202414453
Seiji Uchiyama, Satoshi Uemura, Takeharu Hayashi, Yuji Kimura, Shiro Seki

Although copper (Cu) pipes are widely used in refrigerant piping owing to their high thermal conductivity and weathering resistance, there are concerns regarding the increasing price and limited supply of Cu. Consequently, our focus has shifted to aluminum (Al), which is relatively abundant and inexpensive, to investigate its application in refrigerant piping. We previously examined corrosion factors on both the internal and external surfaces of straight piping and conducted accelerated degradation tests, showing that Al has a durability comparable to that of Cu. However, bending sections are always used in addition to straight pipes, and bending induces tensile stress on the outer side of the bending curvature and compressive stress on the inner side. Notably, stress corrosion cracking may occur under tensile stress in corrosive environments. Herein, we investigate the mechanical, electrochemical, and weather resistance properties of bent Al and Cu pipes to evaluate the practicality of Al refrigerant piping.

尽管铜(Cu)管因其高导热性和耐候性而被广泛应用于制冷剂管道,但铜的价格不断上涨和供应有限的问题却令人担忧。因此,我们将重点转移到相对丰富且价格低廉的铝(Al)上,研究其在制冷剂管道中的应用。我们之前研究了直管内外表面的腐蚀因素,并进行了加速降解试验,结果表明铝的耐用性与铜相当。然而,除直管外,还经常使用弯曲部分,弯曲会在弯曲曲率的外侧产生拉应力,在内侧产生压应力。值得注意的是,在腐蚀环境中,拉应力可能会导致应力腐蚀开裂。在此,我们研究了弯曲铝管和铜管的机械、电化学和耐候性能,以评估铝制冷剂管道的实用性。
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引用次数: 0
Quantifying intergranular corrosion susceptibility in AA2098-T351 weldments through friction stir welding 通过搅拌摩擦焊量化 AA2098-T351 焊件的晶间腐蚀敏感性
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-10 DOI: 10.1002/maco.202314245
Mariana X. Milagre, Uyime Donatus, Naga V. Mogili, Caruline S. C. Machado, João Victor. S. Araujo, Rejane Maria P. Silva, Renato A. Antunes, Sajid Farooq, Isolda Costa

In this study, the intergranular corrosion (IGC) susceptibility of AA2098-T351 welds, fabricated through friction stir welding (FSW), was systematically evaluated. The evaluation employed American Society for Testing and Materials (ASTM) G110-92 practice and electrochemical impedance measurements, with comparative analyses against unwelded alloys (BS). The key findings depicted that FSW-induced microstructure changes significantly influenced IGC susceptibility across different zones. Zones affected by FSW presented distinct susceptibilities compared with the base metal (BM). The ASTM G110-92 test effectively differentiated the heat-affected zone (HAZ) into segments with changing corrosion resistances based on welding temperature gradients. Cross-sectional analyses using scanning electron microscopy (SEM) techniques correlated corrosion characteristics with microstructural features identified by transmission electron microscopy (TEM). Overall, FSW-induced microstructural alterations emerged as a predominant factor influencing the varying susceptibilities of different zones to IGC, and electrochemical impedance measurements (EIS) validated the findings from ASTM G110-92 practice.

本研究系统地评估了通过搅拌摩擦焊(FSW)制造的 AA2098-T351 焊缝的晶间腐蚀(IGC)敏感性。评估采用了美国材料与试验协会 (ASTM) G110-92 标准和电化学阻抗测量方法,并与未焊接合金 (BS) 进行了对比分析。主要研究结果表明,FSW 引起的微观结构变化对不同区域的 IGC 易感性有显著影响。与基体金属(BM)相比,受 FSW 影响的区域呈现出不同的易感性。ASTM G110-92 试验根据焊接温度梯度有效地将热影响区(HAZ)区分为耐腐蚀性能不断变化的区段。使用扫描电子显微镜(SEM)技术进行的横截面分析将腐蚀特征与透射电子显微镜(TEM)确定的微观结构特征相关联。总之,FSW 引起的微观结构变化是影响不同区域对 IGC 的不同敏感性的主要因素,电化学阻抗测量 (EIS) 验证了 ASTM G110-92 实践的结论。
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引用次数: 0
Atmospheric corrosion of AISI-1020 carbon steel in a very aggressive coastal zone of Havana, Cuba. Determination of corrosivity category using three ways of assessment 古巴哈瓦那侵蚀性极强的沿海地区 AISI-1020 碳钢的大气腐蚀。用三种评估方法确定腐蚀性类别
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-10 DOI: 10.1002/maco.202414380
Abel Castañeda, Cecilia Valdés, Francisco Corvo, Ildefonso Pech, Rigoberto Marrero
<p>The Cuban coastal line is reported to be one of the most aggressive in the world. Three ways to estimate corrosivity category of the atmosphere were considered. The influence of meteorological parameters on chloride deposition rate <span></span><math> <semantics> <mrow> <mrow> <mo>(</mo> <msub> <mi>S</mi> <mi>d</mi> </msub> <mo>)</mo> </mrow> </mrow> <annotation> $({S}_{d})$</annotation> </semantics></math> in saline solution form was considered as a first way. Corrosion rate <span></span><math> <semantics> <mrow> <mrow> <mo>(</mo> <msub> <mi>r</mi> <mtext>corr</mtext> </msub> <mo>)</mo> </mrow> </mrow> <annotation> $({r}_{text{corr}})$</annotation> </semantics></math> calculated by dose response function is considered a second way. It was confirmed that atmospheric corrosion of AISI-1020 carbon steel is influenced by <span></span><math> <semantics> <mrow> <mrow> <msub> <mi>S</mi> <mi>d</mi> </msub> </mrow> </mrow> <annotation> ${S}_{d}$</annotation> </semantics></math> and <span></span><math> <semantics> <mrow> <mrow> <msub> <mi>P</mi> <mi>d</mi> </msub> </mrow> </mrow> <annotation> ${P}_{d}$</annotation> </semantics></math> in salt solution form. A critical <span></span><math> <semantics> <mrow> <mrow> <msub> <mi>S</mi> <mi>d</mi> </msub> </mrow> </mrow> <annotation> ${S}_{d}$</annotation> </semantics></math> level from which <span></span><math> <semantics> <mrow> <mrow> <msub> <mi>r</mi> <mtext>corr</mtext> </msub>
据报道,古巴海岸线是世界上腐蚀性最强的海岸线之一。我们考虑了三种估算大气腐蚀性类别的方法。第一种方法是考虑气象参数对盐溶液形式氯化物沉积速率的影响。根据剂量反应函数计算的腐蚀率被视为第二种方法。结果证实,AISI-1020 碳钢的大气腐蚀受到盐溶液形式的影响。估算出了盐溶液腐蚀加剧的临界值。碳钢典型结晶相的存在证实了腐蚀产物层开裂的形成机制。作为第三种评估方法,它证明了 rcorr 随时间的增加而增加,直至达到极高(C5)腐蚀性类别。三种评估方法之间存在对应关系。
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引用次数: 0
Corrosion of some metallic materials embedded in gypsum 嵌入石膏中的某些金属材料的腐蚀
IF 1.6 4区 材料科学 Q4 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-06-09 DOI: 10.1002/maco.202414483
Gustavo Duffó, Jhon Torres-Ramirez, Silvia Fernandez, Silvia Farina

In the construction area, as well as in the restoration of old and historical buildings, different metallic materials are frequently in contact with gypsum plaster. Due to the high porosity of gypsum plaster, and particularly in high relative humidity environments, the risk of corrosion exists. In the present work, carbon, galvanized and stainless steel, as well as copper, were embedded in gypsum plaster (with varying water/gypsum ratios) and exposed to different environmental conditions, and the corrosion rate was assessed by electrochemical techniques. Stainless steel showed very low corrosion rates, carbon and galvanized steel showed considerable corrosion rates, and copper showed moderate corrosion rates. The higher the humidity, the higher the corrosion rate, independently of the water/gypsum ratio. A comparison with results obtained for the same materials embedded in mortar was performed. Except for stainless steel, the corrosion rates obtained in gypsum are higher than those obtained in mortar, being this difference up to two orders of magnitude. The differences in the pH of both matrices explained the lower corrosion rates measured in mortar.

在建筑领域以及古建筑和历史建筑的修复中,不同的金属材料经常与石膏抹灰接触。由于石膏灰泥的孔隙率较高,特别是在相对湿度较高的环境中,存在腐蚀的风险。在本研究中,碳钢、镀锌钢、不锈钢和铜被嵌入石膏抹灰(水/石膏比例不同)中,暴露在不同的环境条件下,并通过电化学技术对腐蚀率进行了评估。不锈钢的腐蚀率非常低,碳钢和镀锌钢的腐蚀率相当高,铜的腐蚀率适中。湿度越高,腐蚀率越高,与水/石膏比例无关。与嵌入砂浆中的相同材料的结果进行了比较。除不锈钢外,石膏中的腐蚀率均高于砂浆中的腐蚀率,两者相差两个数量级。两种基质 pH 值的不同解释了在砂浆中测得的腐蚀率较低的原因。
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引用次数: 0
Contents: Materials and Corrosion. 6/2024 内容:材料与腐蚀。6/2024
IF 1.8 4区 材料科学 Q2 Materials Science Pub Date : 2024-06-04 DOI: 10.1002/maco.202470063
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引用次数: 0
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Materials and Corrosion-werkstoffe Und Korrosion
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