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Identification and quantification of resolubilised polyphenols from fining precipitation 精制沉淀中可溶解多酚的鉴定与定量
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-10-19 DOI: 10.20870/oeno-one.2023.57.4.7568
Gauthier Lagarde, Joëlline Pocher, Jean Martin Pernier, Sandra Vanbrabant, Arnaud Massot, Virginie Moine, Soizic Lacampagne, Pierre-Louis Teissedre, Michael Jourdes
The aim of this study was to better understand the colloidal phenomenon involved in the fining process and to determine how many polyphenols are impacted in this process. Different types and compositions of fining agent were used to fine the wine. Some of them were pure and based on animal proteins and plant proteins, while others comprised a mixture of different matter, like PVPP and plant proteins, or PVPP, plant proteins and bentonite. Before and after fining, five different analyses were performed on the wine to characterise the polyphenolic composition and content. In order to determine polyphenol loss more precisely during fining, a new method was developed to quantify and characterise polyphenol precipitate using fining agents. This new method allowed us to find some drastic differences between the fining agents in term of total polyphenol precipitation, as well as in the composition of the precipitated compounds. Indeed, a group of anthocyanins present in low levels in wine (i.e., p-coumaroylated anthocyanins) became the most represented in the fining precipitate. Similarly, differences were also observed between the fining agents in the composition of precipitated condensed tannins. Fining agents without PVPP did not precipitate monomeric or dimeric flavan-3-ol or crown tannins. Some differences were also observed between the fining agent composed of plant-derived protein and that comprising gelatin.
本研究的目的是为了更好地了解在细化过程中涉及的胶体现象,并确定在此过程中有多少多酚受到影响。采用不同类型和成分的精制剂对葡萄酒进行精制。其中一些是纯的,以动物蛋白和植物蛋白为基础,而另一些则由不同物质的混合物组成,如PVPP和植物蛋白,或PVPP,植物蛋白和膨润土。在精炼前后,对葡萄酒进行了五种不同的分析,以表征多酚成分和含量。为了更精确地测定精馏过程中多酚的损失,提出了一种利用精馏剂定量表征多酚沉淀的新方法。这种新方法使我们发现精化剂之间在总多酚沉淀以及沉淀化合物的组成方面存在一些巨大差异。事实上,葡萄酒中存在的一组低水平花青素(即,对香豆素化花青素)在细化沉淀中最具代表性。同样,在沉淀缩合单宁的组成中也观察到不同的细化剂之间的差异。不含PVPP的精制剂不会沉淀单体或二聚体黄烷-3-醇或冠状单宁。用植物源性蛋白和明胶组成的增细剂也有不同之处。
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引用次数: 0
Cu fractions in Shiraz and Pinot Noir wines during bottle aging: rates of changes and capacity for conversion 设拉子和黑皮诺葡萄酒在装瓶陈酿过程中的铜组分:变化率和转化能力
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-10-16 DOI: 10.20870/oeno-one.2023.57.4.7425
Xinyi Zhang, Andrew C. Clark
The Cu fraction in wine associated with Cu(II)-organic acid complexes can suppress detrimental aromas attributed to hydrogen sulfide and methanethiol. However, the long-term stability of this Cu fraction (known as Cu fraction I) during bottle aging of red wine is not well understood. This study utilised Pinot Noir and Shiraz wines containing 0.43 ± 0.01 and 0.56 ± 0.02 mg/L respectively of total Cu, to which 0, 0.3 or 0.6 mg/L Cu(II) was further added immediately before bottling. The bottles were then stored at 14 °C for 1 yr. Cu fraction I concentrations were measured using two independent methods: i) stripping potentiometry, and ii) ICP-OES analysis of filtrate after diatomaceous earth depth filtration. Within the first 6 months of storage, Cu fraction I was found to decrease in all wines. Using stripping potentiometry, the first-order decay rates were found to be 0.012 ± 0.001 day-1 and 0.010 ± 0.001 day-1 for Pinot Noir and Shiraz respectively, corresponding to half-lives of 55 ± 4 and 67 ± 9 days. The decay rates for Shiraz versus Pinot Noir were similar for wines with different Cu addition rates, or when rates were determined using the different analysis techniques. Both wines had a high capacity for conversion of Cu fraction I to Cu fraction III during the 1-yr storage period, with 0.4-0.8 mg/L Cu forming Cu fraction III in the Pinot Noir, and 0.3-0.6 mg/L in the Shiraz. These conversion capacity ranges are higher than the typical Cu(II) additions made to wine during production. Overall, the results show that red wine has a large capacity for enabling the sulfide-binding of Cu-organic acid complexes during bottle aging and the conversion occurs at a relatively uniform rate with the concentration halving approximately every 2 months.
葡萄酒中的Cu组分与Cu(II)-有机酸配合物相结合,可以抑制硫化氢和甲硫醇的有害香气。然而,这种Cu组分(称为Cu组分I)在红酒瓶陈酿过程中的长期稳定性尚不清楚。本研究使用的黑比诺和设拉子葡萄酒的总铜含量分别为0.43±0.01和0.56±0.02 mg/L,在装瓶前立即添加0、0.3或0.6 mg/L的Cu(II)。然后在14°C下保存1年。使用两种独立的方法测量Cu组分I的浓度:I)剥离电位法和ii)硅藻土深度过滤后滤液的ICP-OES分析。在储藏的前6个月,所有葡萄酒中的Cu分数I都有所下降。采用溶出电位法,黑皮诺和设拉子的一级衰变率分别为0.012±0.001 day-1和0.010±0.001 day-1,对应的半衰期分别为55±4天和67±9天。设拉子和黑皮诺的衰减率在不同的铜添加率或使用不同的分析技术确定的速率下是相似的。两种葡萄酒在1年的储藏期中都有较高的Cu组分I转化为Cu组分III的能力,黑皮诺中有0.4-0.8 mg/L的Cu组分III,设拉子中有0.3-0.6 mg/L的Cu组分III。这些转化能力范围高于在生产过程中向葡萄酒中添加的典型Cu(II)。总体而言,结果表明,红葡萄酒在装瓶陈酿过程中具有较大的cu -有机酸配合物硫化物结合能力,并且转化速度相对均匀,大约每2个月浓度减半。
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引用次数: 0
Sensory identity of wine from the ancient and almost forgotten grape variety Timorasso 葡萄酒的感官身份,从古老的,几乎被遗忘的葡萄品种蒂莫拉索
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-10-05 DOI: 10.20870/oeno-one.2023.57.4.7639
Monica Laureati, Marta Appiani, Camilla Cattaneo, Noemi Sofia Rabitti, Zoe Verveur, Stefano Bergaglio, Dominique Valentin
Over the last few decades, there has been a gradual decrease in natural biodiversity, which is leading to the standardisation of wine products. Minor grape varieties possess key traits for producing wines with a specific territorial identity and they contribute to increasing biodiversity. Timorasso is an ancient Italian white grape variety native to the province of Alessandria in the Piedmont region. It fell into oblivion for a period of time due to the advent of phylloxera at the end of the 1800s and the abandonment of rural areas, which almost led to the extinction of this grapevine. This study aimed to identify the sensory properties that characterise Timorasso wine from different producers and production areas and to investigate the diversity of the sensory space. Sixteen Timorasso wines from the 2018 vintage and were evaluated for sensory description by a panel of nine semi-trained judges using the RATA method. The Timorasso wine was found to have a complex aromatic profile spanning fruity (citrus, tropical fruits, tree-fruit and dried/baked fruit), floral, vegetative, balsamic, honey and fuel/petroleum. The multiple factor analysis clearly differentiated wines with fruity notes from those with balsamic, vegetative and fuel/petroleum aromas. The hierarchical cluster analysis evidenced three main clusters. Cluster 1 comprised wines with pale-yellow colour and fruity-related aromas, low sourness, body and alcohol sensations. Cluster 2 comprised wines with dark yellow colour, low sourness, and high intensities of raisin and fuel aromas, probably due to specific oenological practices, such as grape maceration. Cluster 3 comprised wines with high sourness and vegetative odour. The results provide for the first time a sensory map of a grapevine that was almost forgotten until a few decades ago, but which is now considered to be among the most promising white wines on the Italian market.
在过去的几十年中,自然生物多样性逐渐减少,这导致了葡萄酒产品的标准化。小型葡萄品种具有生产具有特定地域特征的葡萄酒的关键性状,它们有助于增加生物多样性。蒂莫拉索是一种古老的意大利白葡萄品种,原产于皮埃蒙特地区的亚历山德里亚省。由于19世纪末根瘤蚜的出现和对农村地区的遗弃,它被遗忘了一段时间,这几乎导致了这种葡萄藤的灭绝。本研究旨在确定来自不同生产商和产区的蒂莫拉索葡萄酒的感官特性,并调查感官空间的多样性。来自2018年份的16款蒂莫拉索葡萄酒,由9名受过半培训的评委组成的评审团使用RATA方法对其感官描述进行了评估。Timorasso葡萄酒被发现具有复杂的芳香特征,包括水果(柑橘,热带水果,树木水果和干燥/烘烤水果),花卉,植物,香脂,蜂蜜和燃料/石油。多因素分析清楚地区分了带有水果味的葡萄酒与带有香料味、植物味和燃料/石油味的葡萄酒。分层聚类分析证明了三个主要的聚类。第一类葡萄酒颜色淡黄,带有水果香味,酸度低,酒体醇厚。第2类葡萄酒颜色深黄,酸度低,有强烈的葡萄干和燃料香气,可能是由于特殊的酿酒工艺,如葡萄浸渍。第三类葡萄酒酸度高,有植物气味。研究结果首次提供了一种葡萄藤的感官地图,这种葡萄藤直到几十年前几乎被遗忘,但现在被认为是意大利市场上最有前途的白葡萄酒之一。
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引用次数: 0
Australian Red Wines Made from Non-Traditional, Emerging Red Grape Varieties: Distinguishing Sensory Profiles and Consumer Perceptions 用非传统的、新兴的红葡萄品种酿造的澳大利亚红葡萄酒:不同的感官特征和消费者的认知
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-10-05 DOI: 10.20870/oeno-one.2023.57.4.7323
Jacob Long, Laura Mezei, Lira Souza-Gonzaga, Trent E. Johnson, Armando Corsi, Sue E. P. Bastian
To sustain the Australian wine sector, it needs to adopt innovative strategies to adapt to rising temperatures brought by climate change. A potential approach is cultivating more drought-resistant emerging grape varieties with diverse flavour profiles to reduce, in part, the current reliance on major varieties. The study aimed to 1) explore sensory profiles of Australian wines made from three emerging red wine grape varieties, 2) determine consumer perceptions and liking of these wines and 3) evaluate whether these three emerging varietal wines display similar sensory characteristics to three major Australian varietal wines. An expert sensory panel (n = 8) performed a sorting task with 38 commercially available Australian wines (10 Montepulciano, 10 Nero d’Avola and 9 Touriga Nacional) and three each produced from Shiraz, Grenache and Cabernet-Sauvignon for exploration of sensory similarity and quality screening purposes, with three wines removed from further study. A Rate-All-That-Apply (RATA) panel of trained wine tasters (n = 36) evaluated the wines to produce sensory profiles and collect preliminary liking. Finally, a subset (n = 9 total) of the emerging wines was selected for consumer trials. Red wine consumers (n = 116) liked all wine samples independent of their knowledge and wine behaviour. Similarity scores indicated that consumers found the most significant similarity between Shiraz and Montepulciano, and Cabernet-Sauvignon and Touriga Nacional wines. The expert and trained tasters also drew similar comparisons between Shiraz and Montepulciano, but also between Grenache and Nero d’Avola wines, yet not towards Cabernet-Sauvignon and Touriga Nacional wines. The findings support the consumer acceptance and perceived similarities between the sensory profile of Shiraz and Montepulciano and Nero d’Avola and Grenache varietal wines, highlighting the potential for producers to adopt these more drought-resistant varieties as alternatives in a warmer future.
为了维持澳大利亚的葡萄酒行业,它需要采取创新的策略来适应气候变化带来的气温上升。一种潜在的方法是培育更多具有不同风味的抗旱新葡萄品种,以部分减少目前对主要品种的依赖。该研究旨在1)探索用三种新兴红葡萄酒葡萄品种酿造的澳大利亚葡萄酒的感官特征,2)确定消费者对这些葡萄酒的看法和喜爱程度,3)评估这三种新兴品种葡萄酒是否表现出与三种主要澳大利亚品种葡萄酒相似的感官特征。一个专家感官小组(n = 8)对38种市售的澳大利亚葡萄酒(10种蒙特普西亚诺(Montepulciano)、10种尼罗达沃拉(Nero d’avola)和9种图里加(Touriga Nacional))和三种产自设拉子(Shiraz)、歌海娜(Grenache)和赤霞珠(Cabernet-Sauvignon)的葡萄酒进行了分类,以探索感官相似性和质量筛选目的,其中三种葡萄酒从进一步的研究中剔除。一个由训练有素的品酒师组成的RATA (Rate-All-That-Apply)小组(n = 36)对葡萄酒进行评估,以产生感官特征并收集初步的喜好。最后,选择新兴葡萄酒的一个子集(n = 9总数)进行消费者试验。红葡萄酒消费者(n = 116)喜欢所有的葡萄酒样品,与他们的知识和葡萄酒行为无关。相似度得分表明,消费者发现设拉子和蒙特普尔恰诺葡萄酒,赤霞珠和图里加国家葡萄酒之间的相似性最大。这些专家和训练有素的品酒师也对设拉子(Shiraz)和蒙特普尔恰诺(Montepulciano)、歌海娜(Grenache)和尼禄(Nero d’avola)葡萄酒进行了类似的比较,但没有对赤霞珠(Cabernet-Sauvignon)和图里加(Touriga Nacional)葡萄酒进行比较。研究结果支持了消费者对设拉子、蒙特普恰诺、尼罗达沃拉和歌海娜等品种葡萄酒的接受度和感知相似性,强调了生产商在未来更温暖的环境下采用这些更抗旱的品种作为替代品的潜力。
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引用次数: 0
Enhancing the sensory properties and consumer acceptance of warm climate red wine through blending 通过混合提高温暖气候红葡萄酒的感官特性和消费者接受度
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-10-02 DOI: 10.20870/oeno-one.2023.57.3.7651
Damian Espinase Nandorfy, Desireé Likos, Simone Lewin, Sheridan Barter, Stella Kassara, Shaoyang Wang, Allie Kulcsar, Patricia Williamson, Keren Bindon, Marlize Bekker, John Gledhill, Tracey Siebert, Robert A. Shellie, Russell Keast, Leigh Francis
Proline has recently been found to direct several sensory attributes in red wine, including viscosity, fruit flavour and sweetness. We sought to investigate whether a red wine, deemed ‘flavour deficient’ by a producer, from a warm inland region could be improved by blending with a high proline wine from the same region, compared to a high colour and flavour wine, linking consumer acceptance with sensory properties and chemical composition. Three dry red wines (two Cabernet-Sauvignon wines from a warm region and one Lagrein wine from a cooler region) were blended in a constrained mixture design. Several blends were uncovered with improved sensory properties and consumer liking scores. Increased liking scores were related to heightened perceived Viscosity (unrelated to physical viscosity), Sweetness and Berry flavours, connected to proline-rich wines with small proportions of Lagrein. PLS-R models relating blend chemical composition, sensory properties and consumer acceptance associated Astringency and Bitterness to polyphenolics and organic acids and lower liking scores. Vegetal and Leather aromas in blends also reduced consumer acceptance and were related to the concentration of the thiols 3SH, 3SHA, PMT, 2FMT and MeSH, as well as guaiacol and isobutyl methoxypyrazine. Multiple blends successfully improved consumer acceptance of the ‘flavour deficient’ wine, particularly those with an increased proportion of the proline-rich wine. Non-linear effects resulting from blending were also assessed, with most variables modelled best by linear averaging. This study demonstrates the practical application of a design of experiment approach using sensory properties, proline and polyphenolic concentrations to guide wine blending and improve wine flavour and acceptability.
脯氨酸最近被发现直接影响红酒的几个感官属性,包括粘度、水果味和甜味。我们试图调查一种被生产商认为“风味不足”的红葡萄酒,是否可以通过与来自同一地区的高脯氨酸葡萄酒混合来改善,与高色香味的葡萄酒相比,将消费者的接受程度与感官特性和化学成分联系起来。三种干红葡萄酒(两种来自温暖地区的赤霞珠(Cabernet-Sauvignon)葡萄酒和一种来自较冷地区的拉格林(Lagrein)葡萄酒)在有限的混合设计中混合。几种混合物被发现具有改善的感官性能和消费者喜欢分数。喜欢度分数的增加与感知粘度(与物理粘度无关)、甜味和浆果味的增加有关,与脯氨酸含量高、葡萄醇含量低的葡萄酒有关。与混合化学成分、感官特性和消费者接受度相关的PLS-R模型将多酚类物质和有机酸的涩味和苦味与较低的喜欢分数联系起来。混合物中的植物和皮革气味也降低了消费者的接受度,这与硫醇3SH、3SHA、PMT、2FMT和MeSH以及愈创木酚和异丁基甲氧基吡嗪的浓度有关。多次混合成功地提高了消费者对“风味不足”葡萄酒的接受度,特别是那些富含脯氨酸的葡萄酒比例增加的葡萄酒。对混合产生的非线性效应也进行了评估,大多数变量的最佳建模方法是线性平均。本研究展示了一种实验设计方法的实际应用,利用感官特性、脯氨酸和多酚浓度来指导葡萄酒调配,提高葡萄酒的风味和可接受性。
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引用次数: 1
Novel algorithms for high-resolution prediction of canopy evapotranspiration in grapevine 葡萄树冠层蒸散量高分辨率预测新算法
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-09-28 DOI: 10.20870/oeno-one.2023.57.3.7251
Matthew Jenkins, Autumn Mannsfeld, Shayla Nikzad, Jean-Jacques Lambert, Konrad Miller, Mark Burns, J. Mason Earles, David E. Block
Developing low-cost technology for custom water delivery to individual or small groups of plants is a critical next step to advance precision irrigation. Current systems for estimating evapotranspiration (ET), or plant water use, work on the scale of a full vineyard (e.g., 3–5 acres) or the scale of a single vine, but at a cost that prohibits monitoring past a small number of representative vines. To develop and evaluate low-cost ET sensors for individual grapevines, we used three head-pruned Zinfandel vines in pots and placed them on load cells to collect continuous weights indicative of actual ET. We mounted research-grade sensors for humidity, temperature, and wind speed on each vine and saved data at 2-minute intervals during three growing seasons. We developed three models based on first principles (Convective Mass Transfer or Mass Balance approaches) or simple correlations to predict actual single-plant ET from these data. We present here the results of a multi-year trial at the UC-Davis RMI vineyard to illustrate the performance of each of the models for ET estimation. Relative model performance was assessed by comparing model predictions to ground truth data provided by measurements from load cells–including assessments of estimated instantaneous ET rate, estimated cumulative water use over a one-hour window surrounding solar noon, and estimated cumulative water use over a full 24-hour period. The three algorithms developed consistently performed well, with single vine ET rate predictions showing a strong linear relationship with ground truth (range in r2 over three seasons CMT r2 = 0.61–0.86; MB r2 = 0.07–0.91; EM r2 = 0.57–0.92). The MB approach, which includes two measurements of relative humidity and temperature, was the most variable, likely due to the impact of sensor placement. In all seasons, we also examined the trend in the plant scaling factor found in each model, deemed As, which, based on model theory, is a function of vine size. Taken together, these results suggest that high-resolution irrigation (HRI) models are a promising new method for ET estimation at the single plant level.
开发低成本技术,为单个或小群植物定制供水,是推进精准灌溉的关键下一步。目前用于估算蒸发蒸腾(ET)或植物水分利用的系统,是在整个葡萄园(例如,3-5英亩)或单个葡萄藤的规模上工作的,但其成本不利于监测少数具有代表性的葡萄藤。为了开发和评估单株葡萄的低成本ET传感器,我们将三棵剪了头的馨芳葡萄放在花盆里,并将它们放在称重传感器上,以连续收集实际ET的重量。我们在每棵葡萄上安装了研究级的湿度、温度和风速传感器,并在三个生长季节每隔2分钟保存一次数据。我们开发了三个基于第一性原理(对流传质或质量平衡方法)或简单相关性的模型,以从这些数据预测实际的单厂ET。我们在这里展示了在加州大学戴维斯分校RMI葡萄园进行的多年试验的结果,以说明每个模型用于ET估计的性能。通过将模型预测与称重传感器测量提供的地面真实数据进行比较,评估了相对模型的性能,包括评估估计的瞬时ET率,估计的太阳正午周围一小时窗口内的累积用水量,以及估计的整个24小时期间的累积用水量。开发的三种算法表现一致,单藤ET率预测与地面真实值表现出很强的线性关系(三个季节的r2范围CMT r2 = 0.61-0.86;MB r2 = 0.07-0.91;EM r2 = 0.57-0.92)。MB方法,包括相对湿度和温度的两个测量,是最可变的,可能是由于传感器放置的影响。在所有季节,我们还检查了在每个模型中发现的植物比例因子的趋势,认为As,根据模型理论,它是藤蔓大小的函数。综上所述,这些结果表明,高分辨率灌溉(HRI)模型是在单株水平估算ET的一种有前景的新方法。
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引用次数: 1
How soil and climate variability within a vineyard can affect the heterogeneity of grapevine vigour and production 葡萄园内的土壤和气候变化如何影响葡萄活力和产量的异质性
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-09-20 DOI: 10.20870/oeno-one.2023.57.3.7498
Gustavo Pereyra, Anne Pellegrino, Milka Ferrer, Remi Gaudin
This study aimed to determine how within-plot soil heterogeneity combined with yearly climate variability can promote the heterogeneity of vine growth at plot level, and which soil-climate parameters influence final yield and berry composition the most. An 8-year experiment was conducted on grapevine in two zones of a vineyard (1 ha) differentiated according to grapevine vigour as determined by NDVI: high vigour (HV) and low vigour (LV). The heterogeneity of the soil properties (depth, texture and composition), plant growth (shoots and roots) and plant production (yield components and berry composition) were determined at plot level. Compared to the LV zone, the HV zone was associated with deeper soils, higher soil water and nitrogen availability, CEC and montmorillonite/illite ratio. More extended root systems, higher vegetative growth and higher yield were observed in the HV zone compared to the LV zone. Drier and warmer vintages increased the difference in heterogeneity of vine growth and yield between the two zones. Berry composition (primary and secondary metabolites) also differed between HV and LV zones but seemed unconnected to vigour and mainly depended on soil-climate-plant interactions over the years. The heterogeneity of plant vigour within the vineyard mainly resulted from differences in root exploration, soil profile and composition (notably montmorillonite/illite ratio). The present study identified soil and crop factors that, depending on weather conditions, can be drivers for reducing the heterogeneity of plant development and improving productivity at vineyard level.
本研究旨在确定样地内土壤异质性和年气候变率如何促进样地水平葡萄生长的异质性,以及哪些土壤气候参数对最终产量和果实组成的影响最大。在一个葡萄园(1公顷)的两个区域进行了为期8年的试验,根据NDVI测定的葡萄活力分为高活力区(HV)和低活力区(LV)。在样地水平上测定土壤性质(深度、质地和组成)、植物生长(芽和根)和植物生产(产量组成和浆果组成)的异质性。与低电压区相比,高电压区土壤较深,土壤水氮有效性、CEC和蒙脱土/伊利石比较高。与低压区相比,高压区根系伸长率更高,营养生长更快,产量更高。干燥和温暖的年份增加了两个区域之间葡萄生长和产量异质性的差异。果实组成(初级和次级代谢物)在高低温区和低低温区也存在差异,但似乎与活力无关,主要取决于多年来土壤-气候-植物的相互作用。葡萄园内植物活力的异质性主要是由于根系探索、土壤剖面和成分(尤其是蒙脱石/伊利石比)的差异。目前的研究确定了土壤和作物因素,根据天气条件,可以成为减少植物发育异质性和提高葡萄园水平生产力的驱动因素。
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引用次数: 0
A mobile device to investigate the response of grapevine berries to heat stress 研究葡萄莓对热胁迫反应的移动装置
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-09-19 DOI: 10.20870/oeno-one.2023.57.3.7216
Kai Konstantin Heilemann Müller, Manfred Stoll, Marco Hofmann, Matthias Friedel
Reproducibly comparing the heat stress response of grapevine berries from different cultivars in the field is often limited by weather conditions during the growing season. This work presents a mobile heating device capable of controlled heat-stress induction on grapevine berries. The heater consisted of six 150 W infrared lamps mounted in a profile frame. The heating power of the lamps could be set individually by a control unit consisting of a single board computer and six temperature sensors positioned as desired. The heat energy applied to individual berries within a cluster decreases by the squared distance to the heat source, enabling the establishment of temperature profiles within individual clusters. Infrared thermography of the fruit surface and measurements conducted with a thermocouple inserted at the epidermis level showed comparable temperatures. Berries treated with high temperatures were sampled according to their visual appearance (i.e., sunburn symptoms). Only symptomatic berries showed a significant increase in electrolyte leakage, indicating cell damage. In a field experiment, the induction of sunburn necrosis symptoms with the presented device was used to predict a Lethal Dose (LD50) for sunburn necrosis symptoms of the Vitis vinifera L. cultivars Bacchus and Silvaner. The LD50 of Bacchus, known as a heat-sensitive cultivar, was about 3.2 °C lower than that of Silvaner. The presented device offers possibilities for a wide range of applications and the induction of precise temperature dynamics in the context of heat stress on fleshy fruit.
在田间对不同品种葡萄果实热胁迫反应的重复性比较常常受到生长季节天气条件的限制。这项工作提出了一个移动加热装置能够控制热应力诱导葡萄藤浆果。加热器由六个150w的红外灯组成,安装在一个侧面框架中。灯的加热功率可以由一个由单板计算机和六个温度传感器组成的控制单元单独设置。应用于单个浆果在一个集群内的热能减少平方距离的热源,使建立温度分布在单个集群内。水果表面的红外热成像和在表皮水平插入热电偶进行的测量显示出相当的温度。根据其视觉外观(即晒伤症状)对经过高温处理的浆果进行取样。只有有症状的浆果显示电解质泄漏显著增加,表明细胞损伤。在田间试验中,利用该装置诱导葡萄品种巴克斯和西万尼的晒伤坏死症状,预测其致死剂量(LD50)。热敏感品种巴克斯的LD50比西万尼低3.2℃左右。该装置提供了广泛的应用和在肉质水果热应力背景下精确温度动态感应的可能性。
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引用次数: 0
<i>Agaricus bisporus</i> chitosan influences the concentrations of caftaric acid and furan-derived compounds in Pinot noir juice and base wine & lt; i&gt;双bisporus&lt; / i&gt;壳聚糖对黑皮诺果汁和基酒中羧酸和呋喃衍生物浓度的影响
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-09-18 DOI: 10.20870/oeno-one.2023.57.3.7565
Jacob Mederios, Shufen Xu, Gary Pickering, Belinda Kemp
Chitosan is a fining agent used in winemaking, although its use in juice and wine beyond fining has been limited until now. Therefore, this study's first aim was to determine if chitosan derived from Agaricus bisporus (button mushrooms) could reduce caffeic and caftaric acid concentrations in Pinot noir grape juice (Study A). The second aim was to determine if chitosan, when added to base wine, could influence the synthesis of furan-derived compounds during storage (Study B). In Study A, Pinot noir grape juice was stored at 10 °C for 18 hours after the following treatments: control (no addition), bentonite/activated charcoal (BAC), low molecular weight (< 3 kDa; LMW) chitosan, med. MW (250 kDa; MMW) chitosan, and high MW (422 kDa; HMW) chitosan (all 1 g/L additions). Caftaric acid was decreased, and total amino acid concentration was increased in the LMW chitosan-treated juice, while the estimated total hydroxycinnamic acid content, turbidity, and browning were decreased in the MMW chitosan-treated juice compared to the control. In Study B, Pinot noir base wine destined for sparkling wine was stored at 15 and 30 °C for 90 days with the following treatments: control (no addition), LMW chitosan, MMW chitosan, and HMW chitosan (all 1 g/L additions). The three chitosan treatments stored at 30 °C had increased furfural, homofuraneol, and 5-methylfurfural formation in the base wine compared to the control. At 15 °C, furfural and homofuraneol had greater concentrations in all chitosan-treated wines after 90 days of storage. Our results demonstrate the potential of mushroom-derived chitosan to remove caftaric acid from grape juice and suggest that chitosan can influence the synthesis of furan-derived compounds in wine after short-term storage.
壳聚糖是一种用于酿酒的精制剂,尽管迄今为止,它在果汁和葡萄酒中的使用一直受到限制。因此,本研究的第一个目的是确定从双孢蘑菇(蘑菇)中提取的壳聚糖是否能降低黑比诺葡萄汁中咖啡因和自丁酸的浓度(研究A)。第二个目的是确定将壳聚糖添加到基酒中,是否会影响储存过程中呋喃衍生化合物的合成(研究B)。在研究A中,黑比诺葡萄汁经过以下处理后,在10°C下储存18小时:对照(无添加),膨润土/活性炭(BAC),低分子量(<3 kDa;LMW)壳聚糖,med. MW (250 kDa;MMW)壳聚糖,高MW (422 kDa);HMW)壳聚糖(均添加量为1g /L)。与对照相比,低分子量壳聚糖处理的果汁中羧酸含量降低,总氨基酸浓度增加,而MMW壳聚糖处理的果汁中估计的总羟基肉桂酸含量、浊度和褐变均降低。在研究B中,用于起泡酒的黑皮诺基酒在15和30°C下保存90天,并进行以下处理:对照(不添加),LMW壳聚糖,MMW壳聚糖和HMW壳聚糖(添加量均为1g /L)。与对照相比,经30℃贮藏的三种壳聚糖处理后,基底酒中糠醛、同型糠醛醇和5-甲基糠醛的生成均有所增加。在15℃下,经过壳聚糖处理90天的葡萄酒中,糠醛和同戊烷醇的浓度更高。我们的研究结果证明了蘑菇衍生壳聚糖去除葡萄汁中羧酸的潜力,并表明壳聚糖可以影响短期储存后葡萄酒中呋喃衍生化合物的合成。
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引用次数: 0
Effect of the alcoholic strength of unaged wine distillates on the final composition of Brandy de Jerez aged in Sherry Casks® 未陈酿葡萄酒蒸馏物的酒精浓度对雪利酒桶陈酿白兰地最终成分的影响
3区 农林科学 Q1 Agricultural and Biological Sciences Pub Date : 2023-09-18 DOI: 10.20870/oeno-one.2023.57.3.7371
Daniel Butron, Manuel J. Valcárcel-Muñoz, M. Valme García-Moreno, M. Carmen Rodríguez-Dodero, Dominico A. Guillén-Sánchez
Brandy is a spirit obtained from distilled wine that has an alcohol content equal to or greater than 36 % ABV (Alcohol by Volume). It undergoes an ageing process in oak wood casks with a capacity of up to 1000 L for a minimum of six months. During this process, a series of physicochemical and sensory changes take place that confer the initial wine distillate with a series of improvements to its sensory profile. Such changes are mainly determined by the intrinsic characteristics of the wood and by those associated with the manufacturing process of the casks. The previous use of the casks, ageing time and the alcoholic strength of the wine distillate are also important factors, among others. The casks, which will have previously contained some type of Sherry wine (such as Fino, Amontillado, Oloroso and Pedro Ximénez), are known as Sherry Casks® and they must be used in the production of Brandy de Jerez. During the ageing of Brandy de Jerez, Sherry Casks® contribute to the final brandy via the compounds that are both inherent to the wood they are made of and from the wine that they initially contained and that were retained in the wood pores. The alcohol content of the wine distillate to be aged significantly affects not only the quality of the brandy, but also the financial cost of the process. This study aimed to determine the influence on brandy of the alcoholic strength of wine distillates aged in static ageing systems using Sherry Casks®. Specifically, we assessed the physicochemical composition and sensory profile of Brandy de Jerez made from wine distillates with three different alcoholic strengths (40 %, 55 % and 68 % ABV) and aged for 24 months. The Brandy de Jerez with lower alcoholic strengths (40 % - 55 % ABV) were found to contain a higher concentration of polyphenolic compounds deriving from the wood as well as from the constituents of the cask-seasoning Sherry wine. The brandies with higher alcoholic strengths exhibited a marked colour change, while the 40 % and 55 % ABV brandies were perceived to have the best sensory characteristics.
白兰地是一种从蒸馏酒中获得的烈酒,其酒精含量等于或大于36% ABV(酒精体积)。它在容量高达1000升的橡木桶中经过至少六个月的陈酿过程。在这个过程中,发生了一系列的物理化学和感官变化,赋予最初的葡萄酒蒸馏物一系列的感官改善。这些变化主要是由木材的内在特性和木桶的制造过程所决定的。以前使用的木桶、陈年时间和葡萄酒蒸馏物的酒精浓度也是重要的因素。这些木桶以前曾装过某种雪利酒(如菲诺、阿蒙蒂拉多、奥洛罗索和佩德罗·西姆萨梅斯),现在被称为雪利酒木桶®,它们必须用于生产赫雷斯白兰地。在赫雷斯白兰地的陈酿过程中,雪利酒桶®通过木材固有的化合物,以及最初含有的葡萄酒和保留在木材孔隙中的化合物,为最终的白兰地做出贡献。待陈化的葡萄酒蒸馏液的酒精含量不仅显著影响白兰地的质量,而且还影响该过程的财务成本。本研究旨在确定在静态陈酿系统中使用雪利酒桶®陈酿的葡萄酒蒸馏物的酒精强度对白兰地的影响。具体来说,我们评估了由三种不同酒精浓度(40%、55%和68% ABV)的葡萄酒蒸馏物制成的赫雷斯白兰地的物理化学成分和感官特征,并将其陈酿24个月。酒精浓度较低(40% - 55% ABV)的赫雷斯白兰地含有较高浓度的多酚化合物,这些多酚化合物来自木材以及酒桶调味雪利酒的成分。酒精浓度较高的白兰地表现出明显的颜色变化,而酒精浓度为40%和55%的白兰地被认为具有最佳的感官特征。
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引用次数: 0
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OENO One
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