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Evolution Pathway of Competitive Precipitation of Inclusions in Al–Ti-Deoxidized Steel 铝钛脱氧钢中夹杂物竞争性沉淀的演变途径
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202400500
Yuanyou Xiao, Lei Cao, Guocheng Wang, Daxian Zhang, Jianzhong He

Seven types of inclusions are observed in the Al-deoxidized steel followed by Ti-deoxidized steel, while ten types of inclusions are found in Al–Ti simultaneous deoxidized steel. Three special inclusions are only found in Al-deoxidized steel followed by Ti-deoxidized steel as Al2TiO5–TixOy, Al2TiO5–Al2O3–TiS, and Al2TiO5–Al2O3–TixOy–TiS. The precipitation order of inclusions in Al–Ti-deoxidized steel is very dependent on the value of [%Ti]/[%Al] or [%S]/[%O]. The critical value of [%Ti]/[%Al] for the precipitation of inclusions from large to small is TixOy > Al2TiO5 > Al2O3, and the critical value of [%S]/[%O] for the precipitation of inclusions from large to small is TiS > TixOy. The critical value of [%Ti]/[%Al] for the precipitation of TixOy prior to Al2TiO5, and the precipitation of Al2TiO5 prior to Al2O3 has a close relationship with the content of [%Al]. In addition, the critical value of [%S]/[%O] for the precipitation of TiS prior to TixOy inclusions increases with an increasing content of [%O] and increased with the decreasing of temperature. The precipitation order of inclusions in the two types of steel is Al2TiO5 or Al2O3 → Ti3O5 → TiO2 → Ti2O3 → TiS.

在铝脱氧钢和钛脱氧钢中发现了七种夹杂物,而在铝钛同时脱氧钢中发现了十种夹杂物。三种特殊夹杂物仅出现在铝脱氧钢中,其次是钛脱氧钢,分别为 Al2TiO5-TixOy、Al2TiO5-Al2O3-TiS 和 Al2TiO5-Al2O3-TixOy-TiS。铝钛氧化钢中夹杂物的析出顺序与[%Ti]/[%Al]或[%S]/[%O]的值有很大关系。夹杂物从大到小析出的[%Ti]/[%Al]临界值为 TixOy > Al2TiO5 > Al2O3,夹杂物从大到小析出的[%S]/[%O]临界值为 TiS > TixOy。在 Al2TiO5 之前析出 TixOy 的[%Ti]/[%Al]临界值和在 Al2O3 之前析出 Al2TiO5 的[%Al]临界值与[%Al]含量有密切关系。此外,TiS先于TixOy夹杂物析出的临界值[%S]/[%O]随[%O]含量的增加而增加,并随温度的降低而增加。两种钢中夹杂物的析出顺序为 Al2TiO5 或 Al2O3 → Ti3O5 → TiO2 → Ti2O3 → TiS。
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引用次数: 0
Formation Mechanism and Main Control Methods of Bright-Band Defects in Strip Casting Based on Numerical Simulation 基于数值模拟的带钢铸造亮带缺陷形成机理及主要控制方法
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202400350
Yuchen Wang, Xiaoming Zhang, Yuanxiang Zhang, Zongwen Ma, Zhenlei Li, Feng Fang, Yang Wang, Guo Yuan

Bright-band defects frequently occur on as-cast strips in the twin-roll strip-casting process, particularly at low-casting speeds, with intervals of ≈200 mm. Additionally, the cast-rolling force also exhibits minor fluctuations. With increasing casting speeds, the spacing between bright-band defects widens, and the severity of these defects diminishes. When the casting speed reaches a certain threshold, defects almost entirely disappear. Detailed analysis of the underlying causes of this phenomenon is essential for effectively preventing defect formation. In this study, the numerical simulation method is employed to analyze casting rolls’ thermal deformation and the melt pool's solidification behavior, based on the production site equipment and process conditions. The causes of defects in as-cast strips are thoroughly analyzed based on simulation results, in conjunction with variations in the cast-rolling force. In this study, it is demonstrated that the thermal deformation of casting rolls and the position of the solidification endpoints collectively contribute to the fluctuations in cast-rolling force and are the primary causes of bright-band defects. Fundamental principles for preventing defects are provided based on actual on-site production. Furthermore, simulation results contribute to establishing a theoretical basis for selecting process parameters and controlling cast-rolling force during production.

在双辊带材浇铸工艺中,特别是在低速浇铸时,浇铸后的带材上经常出现光亮带缺陷,间隔≈200 毫米。此外,铸轧力也会出现微小波动。随着浇铸速度的提高,亮带缺陷的间距变宽,缺陷的严重程度降低。当浇铸速度达到一定临界值时,缺陷几乎完全消失。要有效防止缺陷的形成,就必须对这一现象的根本原因进行详细分析。本研究根据生产现场的设备和工艺条件,采用数值模拟方法分析了铸造轧辊的热变形和熔池的凝固行为。根据模拟结果,结合铸轧力的变化,深入分析了铸坯带材缺陷的成因。研究表明,浇铸辊的热变形和凝固端点的位置共同导致了浇铸轧制力的波动,是造成亮带缺陷的主要原因。根据实际现场生产情况,提供了防止缺陷的基本原则。此外,模拟结果有助于为生产过程中选择工艺参数和控制轧制力奠定理论基础。
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引用次数: 0
Damage Initiation of 15V38 Steel Bar during Square-to-Round Hot Rolling Process 15V38 钢棒在从方形到圆形热轧过程中的损伤初始化
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202400344
Siva Sai Krishna Dasari, Henry Adekola Haffner, K. Chandrashekhara, Mario F. Buchley, Simon N. Lekakh, Ronald J. O’Malley

Hot rolling processes have been extensively used to produce round bars by reducing the cross-sectional area of continuously cast steel. The current trend toward increasing productivity often requires a more aggressive reduction per pass. Establishing safe and optimized hot rolling parameters must be determined to avoid damage while deforming the specific steel composition. Understanding the damage mechanism during the metal forming process is vital for product quality. Herein, a combined experimental and simulation approach is developed to track the evolution potential damage during hot bar rolling. Hot tension tests are conducted on as-cast vanadium microalloyed 15V38 steel at different hot rolling temperatures and strain rate conditions to develop Johnson–Cook-type material model. A thermomechanical finite element model is developed to simulate potential damage trends in a 12-pass square-to-round and 8-pass round-to-round standard industrial hot rolling process, employing damage criteria. Results are illustrated by creating a damage map at each rolling pass to determine the critical hot rolling conditions for damage initiation. Several parametric studies are also performed to illustrate the application of the suggested methodology for hot rolling process optimization. Results show that the probability of the damage initiation is higher at higher pass reductions and lower temperatures.

通过减小连铸钢的横截面积,热轧工艺已被广泛用于生产圆棒。当前提高生产率的趋势往往要求每道轧制工序的缩减量更大。必须确定安全和优化的热轧参数,以避免在特定钢成分变形时造成损坏。了解金属成型过程中的损伤机理对产品质量至关重要。在此,我们开发了一种实验和模拟相结合的方法,用于跟踪热轧棒材过程中潜在损伤的演变。在不同的热轧温度和应变率条件下,对铸钒微合金 15V38 钢进行了热拉伸试验,以建立约翰逊-库克型材料模型。开发了热机械有限元模型,采用损伤标准模拟 12 次方到圆和 8 次圆到圆标准工业热轧过程中的潜在损伤趋势。通过在每个轧制道次绘制损伤图来确定引发损伤的临界热轧条件,从而对结果进行说明。还进行了几项参数研究,以说明建议的热轧工艺优化方法的应用。结果表明,轧制道次减少越多、温度越低,发生损伤的概率越高。
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引用次数: 0
Effect of the Tundish Inhibitor Design on the Flotation Efficiency of Nonmetallic Inclusions: Water Modeling and Mathematical Simulations by the Reynolds Stress Model 槽底抑制剂设计对非金属夹杂物浮选效率的影响:水模型和雷诺应力模型的数学模拟
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202400087
Alfonso Nájera-Bastida, Rodolfo Dávila Morales, Javier Guarneros-Guarneros, Jafeth Rodríguez-Ávila, Oscar Joaquín Solís-Marcial

Numerical fluid simulations using the Reynolds stress model and water model experiments are conducted to test different designs of tundish turbulence inhibitors (A, B, C, D, and E) for their effectiveness in removing nonmetallic inclusions from steel. The results reveal a unique flow pattern, with a mushroom-like shape forming around the entry jet. The acceleration of small eddies within this mushroom is a significant factor in inclusion removal. This discovery has practical implications for the steel industry, leading to a longer residence time in the entry jet mushroom and improved inclusion flotation performance. Additionally, the turbulent kinematic viscosity and Reynolds stress fields in the flow mushroom influence the tracer's local dispersion rate and the interactions of the inclusions in this region. These findings are further validated using a tundish water model to track the dynamics of amine particles injected into the ladle shroud, enhancing their practical relevance.

利用雷诺应力模型和水模型试验进行了数值流体模拟,以测试不同设计的连铸湍流抑制剂(A、B、C、D 和 E)去除钢中非金属夹杂物的效果。结果发现了一种独特的流动模式,即在入口射流周围形成蘑菇状。蘑菇状流体中的小涡流加速是去除夹杂物的一个重要因素。这一发现对钢铁行业具有实际意义,可延长进入射流蘑菇状流体的停留时间,提高夹杂物浮选性能。此外,流菇中的湍流运动粘度和雷诺应力场会影响示踪剂的局部分散率以及夹杂物在该区域的相互作用。这些研究结果通过使用中间包水模型跟踪注入钢包护罩的胺颗粒动态得到了进一步验证,从而增强了其实用性。
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引用次数: 0
Constitutive Modeling of High-Temperature Deformation Behavior of Nonoriented Electrical Steels as Compared to Machine Learning 无取向电工钢高温变形行为的构造模型与机器学习的比较
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202300549
Gyanaranjan Mishra, Jubert Pasco, Thomas McCarthy, Kudakwashe Nyamuchiwa, Youliang He, Clodualdo Aranas

Hot rolling is a critical thermomechanical processing step for nonoriented electrical steel (NOES) to achieve optimal mechanical and magnetic properties. Depending on the silicon and carbon contents, the electrical steel may or may not undergo austenite–ferrite phase transformation during hot rolling, which requires different process controls as the austenite and ferrite show different flow stresses at high temperatures. Herein, the high-temperature flow behaviors of two nonoriented electrical steels with silicon contents of 1.3 and 3.2 wt% are investigated through hot compression tests. The hot deformation temperature is varied from 850 to 1050 °C, and the strain rate is differentiated from 0.01 to 1.0 s−1. The measured stress-strain data are fitted using various constitutive models (combined with optimization techniques), namely, Johnson–Cook, modified Johnson–Cook, Zener–Hollomon, Hensel–Spittel, modified Hensel–Spittel, and modified Zerilli–Armstrong. The results are also compared with a model based on deep neural network (DNN). It is shown that the Hensel–Spittel model results in the smallest average absolute relative error among all the constitutive models, and the DNN model can perfectly track almost all the experimental flow stresses over the entire ranges of temperature, strain rate, and strain.

热轧是无取向电工钢(NOES)获得最佳机械和磁性能的关键热机械加工步骤。根据硅和碳含量的不同,电工钢在热轧过程中可能会也可能不会发生奥氏体-铁素体相变,这就需要不同的工艺控制,因为奥氏体和铁素体在高温下表现出不同的流动应力。本文通过热压缩试验研究了硅含量分别为 1.3 和 3.2 wt%的两种无取向电工钢的高温流动行为。热变形温度范围为 850 至 1050 °C,应变速率范围为 0.01 至 1.0 s-1。测量到的应力-应变数据使用各种构成模型(结合优化技术)进行拟合,即约翰逊-库克模型、改进的约翰逊-库克模型、齐纳-霍洛蒙模型、亨塞尔-斯皮特尔模型、改进的亨塞尔-斯皮特尔模型和改进的泽里利-阿姆斯特朗模型。研究结果还与基于深度神经网络(DNN)的模型进行了比较。结果表明,在所有构成模型中,Hensel-Spittel 模型的平均绝对相对误差最小,而 DNN 模型可以在整个温度、应变率和应变范围内完美跟踪几乎所有的实验流动应力。
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引用次数: 0
Hot Deformation Behavior and Numerical Simulation of 40CrNiMo Steel for Wind Turbine Pulley Shafts 风力涡轮机滑轮轴用 40CrNiMo 钢的热变形行为和数值模拟
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202400134
Hongyu Wei, Wensheng Liu, Ke Zhang, Wei Wei, Qun Wu, Mingya Zhang, Xiaoping Tao, Hongyan Liu

The hot deformation behavior (T = 800–1100 °C, ε˙$$ dot{epsilon } $$ = 0.01–10 s−1) of 40CrNiMo steel for wind turbine pulley shafts was studied by Gleeble-3800 thermomechanical simulator. A constitutive equation and hot processing map are established based on the friction and temperature correction curves. The most available hot processing parameters are determined by combining microstructure analysis. The temperature fields and effective strain fields under different deformation conditions are simulated by Deform-3D software. The results indicate that the effect of friction on the flow curves is greater than that of temperature rise, the activation energy Q of hot deformation for 40CrNiMo steel calculated based on the theoretical calculation is 368.292 kJ mol−1. The constitutive model based on strain compensation has high accuracy, with an average relative error of 6.65% and a correlation coefficient of 0.987. The optimum hot processing interval is at a deformation temperature of 950–1050 °C and a strain rate of 0.03–0.25 s−1, which has a high-power dissipation value and avoids the instability region. Additionally, numerical simulation results show that the temperature field distribution is uniform in this deformation range, and the standard deviation of the effective strain is low, making it suitable for hot processing.

Gleeble-3800 热机械模拟器研究了风力涡轮机滑轮轴用 40CrNiMo 钢的热变形行为(T = 800-1100 °C, = 0.01-10 s-1)。根据摩擦和温度修正曲线建立了构成方程和热加工图。结合微观结构分析确定了最可用的热加工参数。利用 Deform-3D 软件模拟了不同变形条件下的温度场和有效应变场。结果表明,摩擦对流动曲线的影响大于温升的影响,根据理论计算得出的 40CrNiMo 钢的热变形活化能 Q 为 368.292 kJ mol-1。基于应变补偿的构效模型具有较高的精度,平均相对误差为 6.65%,相关系数为 0.987。最佳热加工区间为变形温度 950-1050 ℃、应变速率 0.03-0.25 s-1,该区间具有较高的功率耗散值,避免了不稳定区域。此外,数值模拟结果表明,在此变形范围内温度场分布均匀,有效应变的标准偏差较低,适合热加工。
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引用次数: 0
Experimental and Fractographic Study of the Hydrogen-Induced Cracking of 45CrNiMoVA Martensitic Advanced High-Strength Steel 45CrNiMoVA 马氏体高级高强度钢氢气诱发裂纹的实验和断面研究
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-29 DOI: 10.1002/srin.202400369
Yunlong Li, Xiaodong Liu

Hydrogen-induced cracking (HIC) in high-strength 45CrNiMoVA steel is investigated using smooth and notched cylindrical specimens by performing uniaxial tensile tests. Specimens with different notch geometries are used to analyze the interacting effects of the stress concentration factor and HIC micromechanism. The results show that hydrogen charging reduces the elongation at fracture and the ultimate tensile strength of smooth tensile specimens. The microscopic fracture mode changes from ductile dimples with some quasicleavage fracture without hydrogen to a mixture of brittle quasicleavage and intergranular cracking with hydrogen. For notched specimens with a lower notch root radius, significant stress concentration occurs at the notch root, which enriches hydrogen in these highly stressed regions. This causes a lower notch tensile strength and greater susceptibility to hydrogen embrittlement. Microfracture observations show that the area fraction of the intergranular cracking surface increases gradually, and the brittle zone moves farther away from the notch root upon decreasing the notch root radius, causing the embrittlement index to remain high. These results will help determine the applicability of existing steel for hydrogen service and also provide guidance for developing new high-strength martensitic steels that can resist hydrogen embrittlement.

通过单轴拉伸试验,使用光滑和有缺口的圆柱形试样研究了高强度 45CrNiMoVA 钢的氢致开裂(HIC)。采用不同缺口几何形状的试样来分析应力集中因子和 HIC 微观机制的相互作用。结果表明,充氢降低了光滑拉伸试样的断裂伸长率和极限拉伸强度。微观断裂模式从无氢情况下的韧性凹陷和一些类泡状断裂转变为有氢情况下的脆性类泡状断裂和晶间开裂的混合断裂。对于缺口根部半径较小的缺口试样,缺口根部会出现明显的应力集中,从而在这些高应力区域富集氢气。这导致缺口抗拉强度降低,更容易发生氢脆。显微断裂观察结果表明,晶间开裂面的面积分数逐渐增加,脆性区随着缺口根部半径的减小而远离缺口根部,导致脆化指数保持在较高水平。这些结果将有助于确定现有钢材在氢工况下的适用性,并为开发可抵抗氢脆的新型高强度马氏体钢提供指导。
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引用次数: 0
Effect of CaO/Al2O3 Ratio in Fluorine-Free Refining Slag with Low Basicity on the Cleanliness of SWRS82B Steel 低碱性无氟精炼渣中的 CaO/Al2O3 比对 SWRS82B 钢洁净度的影响
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-28 DOI: 10.1002/srin.202400314
Ruiqi Luo, Yudong Zhao, Linzhu Wang, Chaoyi Chen, Junqi Li

A fluorine-free quaternary CaO–Al2O3–SiO2–MgO refining slag for SWRS82B coil steel is studied by considering the requirements of the steel wire. Laboratory experiments are conducted to study the equilibrium and kinetics of steel–slag reactions. The physical and chemical properties of refining slags, including the melting temperature, viscosity, and MgO solubility, are estimated by FactSage7.2 calculation. The cleanliness of SWRS82B steel refined by slags with a basicity of 1 and C/A ratio in the range of 1.36–7.13 is studied systematically. The plasticity of inclusions is studied by phase diagram and Young modulus calculation. Deoxidizing capacity and desulfurization capacity of refining slags are discussed by kinetic calculation of steel–slag reactions based on FactSage7.2 macro-editing and the kungliga tekniska högskolan model. Slag with a composition of 42%CaO–47%SiO2–4%Al2O3–7%MgO has the best refining effect, in which impurity elements are lowest and plastic inclusions with the smallest size and least quantity are obtained. The impurity elements oxygen and sulfur in steel can be controlled for 29 and 75 ppm, respectively. The average size of inclusions is 1.54 μm. The majority of inclusions are in a liquid state at 1600 °C and Young modulus of the inclusions ranges from 99.78 to 152.87 GPa.

考虑到钢丝的要求,研究了用于 SWRS82B 卷钢的无氟四元 CaO-Al2O3-SiO2-MgO 精炼渣。通过实验室实验研究了钢渣反应的平衡和动力学。通过 FactSage7.2 计算估算了精炼渣的物理和化学特性,包括熔化温度、粘度和氧化镁溶解度。系统研究了碱性为 1、C/A 比在 1.36-7.13 范围内的炉渣精炼 SWRS82B 钢的清洁度。通过相图和杨氏模量计算研究了夹杂物的塑性。通过基于 FactSage7.2 宏编辑和 kungliga tekniska högskolan 模型的钢渣反应动力学计算,讨论了精炼炉渣的脱氧能力和脱硫能力。成分为 42%CaO-47%SiO2-4%Al2O3-7%MgO 的炉渣具有最佳的精炼效果,其中杂质元素最少,获得的塑性夹杂物尺寸最小、数量最少。钢中的杂质元素氧和硫可分别控制在 29 ppm 和 75 ppm。夹杂物的平均尺寸为 1.54 μm。大多数夹杂物在 1600 °C 时处于液态,夹杂物的杨氏模量范围为 99.78 至 152.87 GPa。
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引用次数: 0
Classification of Cast Iron Alloys through Convolutional Neural Networks Applied on Optical Microscopy Images 通过应用于光学显微镜图像的卷积神经网络对铸铁合金进行分类
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-28 DOI: 10.1002/srin.202400120
Marta Bárcena, Lara Lloret Iglesias, Diego Ferreño, Isidro Carrascal

Classification of cast iron alloys based on graphite morphology plays a crucial role in materials science and engineering. Traditionally, this classification has relied on visual analysis, a method that is not only time-consuming but also suffers from subjectivity, leading to inconsistencies. This study introduces a novel approach utilizing convolutional neural networks—MobileNet for image classification and U-Net for semantic segmentation—to automate the classification process of cast iron alloys. A significant challenge in this domain is the limited availability of diverse and comprehensive datasets necessary for training effective machine learning models. This is addressed by generating a synthetic dataset, creating a rich collection of 2400 pure and 1500 mixed images based on the ISO 945-1:2019 standard. This ensures a robust training process, enhancing the model's ability to generalize across various morphologies of graphite particles. The findings showcase a remarkable accuracy in classifying cast iron alloys (achieving an overall accuracy of 98.9 ± 0.4%—and exceeding 97% for all six classes—for classification of pure images and ranging between 84% and 93% for semantic segmentation of mixed images) and also demonstrate the model's ability to consistently identify and graphite morphology with a level of precision and speed unattainable through manual methods.

根据石墨形态对铸铁合金进行分类在材料科学和工程学中起着至关重要的作用。传统上,这种分类依赖于视觉分析,这种方法不仅耗时,而且存在主观性,会导致不一致。本研究介绍了一种利用卷积神经网络(用于图像分类的 MobileNet 和用于语义分割的 U-Net)的新方法,以实现铸铁合金分类过程的自动化。该领域的一个重大挑战是训练有效机器学习模型所需的多样化综合数据集的可用性有限。为了解决这个问题,我们根据 ISO 945-1:2019 标准生成了一个合成数据集,创建了一个包含 2400 张纯图像和 1500 张混合图像的丰富集合。这就确保了训练过程的稳健性,增强了模型对各种形态的石墨颗粒的泛化能力。研究结果表明,该模型在铸铁合金分类方面具有出色的准确性(纯图像分类的总体准确性达到 98.9 ± 0.4%,所有六个类别的准确性均超过 97%,混合图像的语义分割准确性介于 84% 和 93% 之间),同时还证明了该模型能够始终如一地识别石墨形态,其准确性和速度是人工方法无法达到的。
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引用次数: 0
Effect of Quenching Post-Intercritical Austenitizing on the Microstructure and Tensile Properties of an K55 Grade Steel for Oil and Gas Industry 跨临界奥氏体化后淬火对石油天然气工业用 K55 级钢微观结构和拉伸性能的影响
IF 1.9 3区 材料科学 Q2 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2024-08-28 DOI: 10.1002/srin.202400478
Verônica Stela da Silva Lima, Arthur Cançado Schuttenberg, Geraldo Lúcio de Faria

The API K55 grade steel is widely utilized in seamless pipes for oil and gas exploration, especially as casing pipes for wellbores. Traditionally, this steel is processed using hot rolling followed by quenching and tempering to achieve the desired dimensional and microstructural characteristics, balancing high strength with ductility. This article introduces an alternative method to attaining the required tensile properties for API K55 grade steel by employing a biphasic microstructure (ferrite/martensite) achieved through quenching post-intercritical austenitizing heat treatment to high-strength-low-alloy steel. Thermodynamic simulations and dilatometric experiments revealed that increasing the austenitizing temperature enhances austenite formation, decreasing significantly its carbon content, which facilitates martensitic transformation and increases the Ms and Mf temperatures. A complete phase transformation mapping was presented, highlighting how the austenitizing temperature influences martensitic transformation kinetics during the quenching heat treatment. It was concluded that austenitizing at 750 °C, followed by quenching and short tempering at 650 °C, produced a biphasic microstructure with 30% ferrite and 70% martensite, providing a favorable balance between mechanical strength and ductility that meets the API K55 grade requirements, surpassing traditional methods in the industry.

API K55 级钢广泛用于石油和天然气勘探用无缝钢管,尤其是井筒用套管。传统上,这种钢材的加工方法是先热轧,然后进行淬火和回火,以获得所需的尺寸和微观结构特征,同时兼顾高强度和延展性。本文介绍了一种替代方法,通过对高强度低合金钢进行临界奥氏体化后淬火热处理,获得双相显微组织(铁素体/马氏体),从而达到 API K55 级钢所需的拉伸性能。热力学模拟和稀释实验表明,提高奥氏体化温度可促进奥氏体的形成,显著降低其碳含量,从而促进马氏体转变,提高 Ms 和 Mf 温度。完整的相变图显示了奥氏体化温度如何影响淬火热处理过程中的马氏体转变动力学。结果表明,在 750 ℃ 下奥氏体化,然后在 650 ℃ 下淬火和短回火,可产生 30% 铁素体和 70% 马氏体的双相微观结构,在机械强度和延展性之间实现了良好的平衡,符合 API K55 等级要求,超越了行业内的传统方法。
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引用次数: 0
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steel research international
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