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Characterization of fluid resistance in nanostructured TiO2 (NST) film 纳米结构TiO2 (NST)薄膜的流体阻力表征
L. Nannan, C. Jing
Embedded microchannels are required in many microfluidic devices. However, the channels may reduce the strength of the bulk substrate. In this study, Nanostructured TiO2(NST) material is proposed to provide the fluid passage for the drug into the required location while still maintains very good strength. A simple method was proposed to obtain the pressure drop over NST filled channel and the fluid resistance was experimentally determined. The Darcy' equation of NST films was setup, and the permeability was measured 1.475×10-11 m2. With a relatively high fluid resistance, further optimization should be carried out for NST microfluidic devices.
许多微流控器件都需要嵌入微通道。然而,通道可能会降低体基板的强度。在本研究中,纳米结构TiO2(NST)材料可以为药物提供进入所需位置的流体通道,同时仍然保持非常好的强度。提出了一种简单的方法来获得NST填充通道上的压降,并实验确定了流体阻力。建立了NST薄膜的Darcy方程,测量了其渗透率1.475×10-11 m2。由于NST微流控器件具有较高的流体阻力,需要进一步优化。
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引用次数: 0
A comparison study on hydrogen sensing performance of Pt/MoO3 nanoplatelets coated with a thin layer of Ta2O5 or La2O3 薄层Ta2O5和La2O3包覆Pt/MoO3纳米片感氢性能的比较研究
Jerry Yu, Y. Liu, F. Cai, M. Shafiei, Gang Chen, N. Motta, W. Wlodarski, K. Kalantar-zadeh, P. Lai
In this work, we investigate how hydrogen sensing performance of thermally evaporated MoO3 nano-platelets can be further improved by RF sputtering a thin layer of tantalum oxide (Ta2O5) or lanthanum oxide (La2O3). We show that dissociated hydrogen atoms cause the thin film layer to be polarised, inducing a measurable potential difference greater than that as reported previously. We attribute these observations to the presence of numerous traps in the thin layer; their states allow a stronger trapping of charge at the Pt-thin film oxide interface as compared to the MoO3 sensors without the coating. Under exposure to H2 (10 000 ppm), the maximum change in dielectric constant is 45.6 (at 260 °C) for the Ta2O5/MoO3 nanoplatelets and 31.6 (at 220 °C) for the La2O3/MoO3 nano-platelets. Subsequently, the maximum sensitivity for the Ta2O5/MoO3 and La2O3/MoO3 based sensors is 16.8 and 7.5, respectively.
在这项工作中,我们研究了如何通过射频溅射薄层氧化钽(Ta2O5)或氧化镧(La2O3)来进一步提高热蒸发MoO3纳米片的氢传感性能。我们表明,解离的氢原子导致薄膜层极化,诱导一个可测量的电位差比以前报道的大。我们将这些观察结果归因于薄层中存在许多圈闭;与没有涂层的MoO3传感器相比,它们的状态允许在pt薄膜氧化物界面上更强的电荷捕获。暴露于H2 (10,000 ppm)下,Ta2O5/MoO3纳米片的介电常数最大变化为45.6(260°C), La2O3/MoO3纳米片的介电常数最大变化为31.6(220°C)。基于Ta2O5/MoO3和La2O3/MoO3的传感器的最大灵敏度分别为16.8和7.5。
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引用次数: 4
Piezoresistive probes for (biomolecular) force sensing 用于(生物分子)力传感的压阻式探针
J. Bausells, G. Tosolini, Y. Birhane, F. Pérez-Murano
We have developed self-sensing piezoresistive microcantilevers optimized for the measurement of (biomolecular) forces. Typical dimensions are 250 μm in length, 8-20 μm in width and 450 nm in thickness, with spring constants of about 1 mN/m. The devices have been electromechanically tested on wafer and show good force resolutions in air between 35 and 130 pN depending on the cantilever dimensions. We have also tested the electromechanical behavior of the cantilevers in liquid environment and we show that both the force sensitivity and the noise characteristics of the devices are not noticeably degraded as compared with their response in air. This opens the way to the use of the cantilevers in single molecule force spectroscopy of biomolecules.
我们已经开发了自传感压阻微悬臂,优化了(生物分子)力的测量。典型尺寸为长250 μm,宽8 ~ 20 μm,厚450 nm,弹簧常数约为1 mN/m。这些器件已经在硅片上进行了机电测试,根据悬臂尺寸的不同,在35到130 pN之间的空气中显示出良好的力分辨率。我们还测试了悬臂梁在液体环境中的机电性能,结果表明,与在空气中的响应相比,该装置的力灵敏度和噪声特性都没有明显下降。这为悬臂梁在生物分子单分子力谱中的应用开辟了道路。
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引用次数: 0
Fabrication of silicon piezoresistive pressure sensor using a reliable wet etching process 采用可靠的湿法蚀刻工艺制备硅压阻式压力传感器
Huiming Xu, Hong Zhang, Zhiqiang Deng, H. San, Yuxi Yu
Silicon-based piezoresistive pressure sensors are generally fabricated as a piezo-sensitive diaphragm by using MEMS technology and SOI wafer. Lots of innovations and improvements have been made for silicon pressure sensor to increase its performance and reliability. It is found that the quality of Si-Si bonding will directly affect the performing of SOI substrate removing processes. The main problem is that the etching liquid infiltrate into bonding interface from the defect position of bonding wafer edge, resulting in the damage and corrosion of bonding wafer. To solve this problem, the paper presents an etching fixture design for effectively protecting the bonding wafer edge. Experimentally, a SOI-Si bonding wafer with poor quality in bonding edge was used to fabricate the piezoresistive pressure sensors by using the etching fixture. The experimental results show the use of etching fixture did not damage the bonding wafer and made a nice removal of SOI substrate. The fabricated pressure sensors wafers are also presented.
硅基压阻式压力传感器一般采用MEMS技术和SOI晶圆制成压敏膜片。为了提高硅压力传感器的性能和可靠性,人们对其进行了大量的创新和改进。结果表明,硅硅结合的质量将直接影响SOI衬底去除工艺的性能。主要问题是蚀刻液从键合晶片边缘的缺陷位置渗入键合界面,造成键合晶片的损坏和腐蚀。为了解决这一问题,本文提出了一种有效保护键合晶片边缘的刻蚀夹具设计。实验中,采用粘接边缘质量较差的SOI-Si粘接晶片,利用刻蚀夹具制作压阻式压力传感器。实验结果表明,使用刻蚀夹具对键合晶片无损伤,并能很好地去除SOI衬底。介绍了压力传感器晶片的制备方法。
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引用次数: 2
Fabrication of membrane-typed metal mould with microstructures and application for roller imprinting 微结构膜型金属模具的制造及其在辊压印中的应用
Yu-Hsiang Tang, Yu-Hsin Lin, Jr-Jung Yang, M. Shiao
In this paper, we focus on the development of membrane-typed metal mould with microstructures for imprinting. This mould has several benefits including reusable, easy replaceable core, and low cost that strongly improves industrial values in microstructure mass production. The membrane-typed metal mould with a thickness of 60 μm can be attached to a level mould or a roller mould, and becomes a metal core for the polymer microstructure imprint for mass production of products over large surface area. Photolithography, electroforming, and grinding techniques have been integrated in order to develop the membrane-typed metal mould in this research. It has been proven that the metal mould of micro pillars could be successfully fabricated. This metal mould was fabricated by precision electroforming technology that Ni-Co alloy was deposited on a photoresist mould, and further peeled off to attach onto a level mould. The hardness, stiffness and toughness of the Ni-Co alloy material core structure were sufficient and strong enough for reusable duration. The durability of this membrane-typed metal mould has been greatly enhanced. Furthermore, by applying roller assisted attaching mechanism, the interface between the mould and Ni-Co alloy core became more inseparable and flat. According to the experimental measurement results, the uniformity has been controlled between ± 5 μm. The reproducing accuracy of the polymer microstructures can also be effectively enhanced.
本文重点研究了印迹用微结构膜型金属模具的研制。该模具具有可重复使用、芯易于更换、成本低等优点,大大提高了微结构批量生产的工业价值。厚度为60 μm的膜型金属模具可以附着在水平模具或滚轮模具上,成为聚合物微结构压印的金属芯,用于大表面积产品的批量生产。本研究将光刻、电铸和研磨技术相结合,以开发膜型金属模具。实践证明,该金属模具是可以成功制备微柱的。该金属模具采用精密电铸技术,将镍钴合金沉积在光刻胶模具上,再剥落附着在水平模具上。Ni-Co合金材料芯结构的硬度、刚度和韧性足够强,可重复使用。这种膜型金属模具的耐久性大大提高。此外,通过采用滚轮辅助附着机构,使模具与镍钴合金芯之间的界面更加不可分割和平整。实验测量结果表明,均匀度控制在±5 μm之间。该方法还可以有效地提高聚合物微观结构的再现精度。
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引用次数: 1
Improvement of DNA Origami's adsorption on silicon substrate DNA折纸在硅衬底上吸附性能的改进
P. Dai, Honglu Zhang, Tie Li, Yuelin Wang, J. Chao, C. Fan
DNA origami, in which a long single strand of DNA is folded into a shape using shorter `staple Strands', promises low-cost ways to create nanoscale shapes and can even display patterns of binding sites of 6-nm-resolution, in principle allowing complex arrangements of carbon nanotubes, silicon nanowires, or quantum dots [1]. However, adsorption of origami appears better results on mica substrate, which cannot compatible with the complementary metal oxide semiconductor (CMOS) process. Here we describe a method to improve the adsorption of origami on silicon substrate, by quantitative control of the adsorption conditions, which will hopefully make contributions for churning out nanoscale shapes with CMOS process in the future.
DNA折纸技术是用较短的“短链”将长单链DNA折叠成某种形状,它有望以低成本的方式创造纳米级形状,甚至可以显示6纳米分辨率的结合位点图案,原则上允许碳纳米管、硅纳米线或量子点的复杂排列[1]。然而,折纸在云母衬底上的吸附效果较好,与互补金属氧化物半导体(CMOS)工艺不兼容。本文描述了一种通过定量控制吸附条件来改善折纸在硅衬底上吸附的方法,有望为未来利用CMOS工艺生产纳米级形状做出贡献。
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引用次数: 0
Magneto-FEM analysis for micro actuator using array of magnetic elements 基于磁元件阵列的微执行器磁力有限元分析
F. Tsumori, Kenji Hatama, Hyungoo Kang, Toshiko Osada, H. Miura
This paper reports a magnetic actuator using interaction between micro magnetic elements. It was already reported that the present actuator can work even if the structure was miniaturized to nano-scale. In the present work, simple fabrication process with photolithography and PDMS casting was employed to obtain beam type structures with micro array of magnetic elements on their surface. Two samples with simple grid patterns were prepared for testing. These samples had the same grid pattern but different orientation, which caused directly opposite bending deformation under the same applied magnetic field. We used magneto finite element method (FEM) to explain the behavior of the present actuators.
本文报道了一种利用微磁元件相互作用的磁致动器。已有报道称,即使结构微型化到纳米级,该驱动器也能正常工作。本文采用光刻和PDMS铸造的简单制造工艺,获得了表面带有微阵列磁性元件的束型结构。准备了两个具有简单网格图案的样品进行测试。这些样品具有相同的网格模式,但取向不同,在相同的外加磁场下产生了相反的弯曲变形。本文采用磁元有限元法(FEM)来解释现有作动器的行为。
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引用次数: 9
Hydrogen etching effect on single-crystal graphene domains 氢蚀刻对单晶石墨烯畴的影响
C. Liang, Wenrong Wang, Tie Li, Yuelin Wang
In this paper, the anisotropic hydrogen etching effect on chemical vapor deposited sing-crystal graphene domains was reported. After synthesized by chemical vapor deposition on copper foils, the graphene domains were exposed to a mixed gas flow of argon and hydrogen for etching. By varying the etching temperature from 800°C to 1050°C, hexagonal openings inside the graphene domains were found on hydrogen etched samples. The dependence of substrate was then studied and the result indicated that copper was necessary in the etching process as catalyst. At last, etching experiments were performed on high quality single-crystal graphene domains, and the result showed that the hexagonal single-crystal graphene domains were etched to circular.
本文报道了各向异性氢蚀刻对化学气相沉积单晶石墨烯畴的影响。采用化学气相沉积法在铜箔上合成石墨烯后,将其暴露在氩气和氢气混合气流中进行蚀刻。通过改变蚀刻温度从800°C到1050°C,在氢蚀刻样品的石墨烯畴内发现了六边形的开口。然后研究了衬底的依赖性,结果表明铜作为催化剂在蚀刻过程中是必需的。最后,对高质量的单晶石墨烯畴进行了刻蚀实验,结果表明,六边形的单晶石墨烯畴被刻蚀成圆形。
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引用次数: 3
Low frequency PVDF piezoelectric energy harvester with combined d31 and d33 operating modes 低频PVDF压电能量采集器,d31和d33组合工作模式
Mengdi Han, Y. C. Chan, Wen Liu, Shouhe Zhang, Haixia Zhang
This paper reports the design, test and application of a novel low frequency piezoelectric energy harvester. To achieve high output voltage at low frequency, both d31 and d33 modes of polyvinylidene fluoride (PVDF) are utilized in this device. Output voltage of the device are tested under different frequencies and accelerations. Rectifying bridge is used to reverse signals with negative signs and capacitors can be charged to light up a light emitting diode (LED).
本文报道了一种新型低频压电能量采集器的设计、测试和应用。为了实现低频高输出电压,该器件采用了聚偏氟乙烯(PVDF)的d31和d33模式。测试了该装置在不同频率和加速度下的输出电压。整流桥用于反转带有负号的信号,电容器可以充电以点亮发光二极管(LED)。
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引用次数: 14
Fabrication of anisotropic nanomaterial by precise and large-area nanowire operation with focused-ion-beam 聚焦离子束精密、大面积纳米线加工制备各向异性纳米材料
Lurui Zhao, Can Li, D. She, Zhiqiang Wang, Jun Xu, Wengang Wu
This paper presents a fabrication method for anisotropic nanomaterial by operating nanowires by focused-ion-beam (FIB) irradiation. After the preparation of one-dimensional nanowire, FIB irradiation is applied on the nanowire to operate its orientation and morphology by choosing irradiation position and area. On one hand, localized FIB irradiation is employed to precisely operate the morphology of the planar ultra-fine nanowire prepared by FIB induced fluidization and self-perfect process driven by the material diffusion process. On the other hand, large area FIB scanning is applied to achieve the orientation adjustment of high-density nanowire bunch and nano-forest obtained by oxygen plasma etching. When nanowire is irradiated, unbalanced stress is introduced at different side, and thus nanowire bends to balance the stress. Based on this approach, both single and large area of nanowire structure can be controlled, and anisotropic nanomaterial is realized.
提出了一种利用聚焦离子束辐照操作纳米线制备各向异性纳米材料的方法。一维纳米线制备完成后,通过选择照射位置和照射面积,对纳米线进行FIB照射,对纳米线的取向和形貌进行操作。一方面,采用局部FIB辐照对材料扩散过程驱动的FIB诱导流化和自完善工艺制备的平面超细纳米线的形貌进行精确操作;另一方面,采用大面积FIB扫描实现了氧等离子体刻蚀得到的高密度纳米线束和纳米林的取向调整。当纳米线受到辐照时,在不同侧面引入不平衡应力,纳米线弯曲以平衡应力。在此基础上,实现了单纳米线和大面积纳米线结构的控制,实现了纳米材料的各向异性。
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引用次数: 1
期刊
The 8th Annual IEEE International Conference on Nano/Micro Engineered and Molecular Systems
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