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Unveiling the effect of cementite distribution on the deformation behavior of pearlitic steel wires under micropillar compression: A strain-gradient crystal plasticity approach 微柱压缩下渗碳体分布对珠光体钢丝变形行为的影响:应变梯度晶体塑性方法
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104214
Abhishek Kumar Singh , Ki-Seong Park , Saurabh Pawar , Dahye Shin , Dongchan Jang , Shi-Hoon Choi
This study examines the deformation mechanisms in cold-drawn pearlitic steel wires using micropillar compression tests. Scanning electron microscopy (SEM) identified five distinct regions characterized by varying cementite distributions, and nanoindentation tests were subsequently performed in these areas. Additionally, five micropillars were fabricated within these regions using focused ion beam (FIB) techniques. The micropillar compression results reveal a pronounced correlation between the mechanical behavior of micropillars and various microstructural parameters, including the cementite inclination angle (CIA), interlamellar spacing, and ferrite-cementite distribution. Furthermore, strain gradient crystal plasticity finite element analysis (SG-CPFEM) revealed a significant increase in geometrically necessary dislocations (GNDs) at the ferrite-cementite interfaces, which critically influences the effective slip resistance. The simulations also indicated that the presence of a ferrite-cementite interface significantly elevates GND concentrations, impacting the load-displacement behavior. Micropillars with cementite normal to the loading direction showed higher increases in GNDs, while reduced cementite spacings were found to amplify GND formation due to increased strain gradients in the ferrite phase. A shear fracture were predominant in pillars with CIA of 67.5º or higher, while kink band formations were observed in pillars with CIA of 22.5º or lower. The increase in GNDs is influenced by both the CIA and interlamellar spacing, highlighting their critical roles in determining mechanical properties.
本研究利用微柱压缩试验研究了冷拔珠光体钢丝的变形机制。扫描电子显微镜(SEM)确定了五个不同的区域,其特征是不同的雪明碳酸盐分布,随后在这些区域进行了纳米压痕测试。此外,还利用聚焦离子束(FIB)技术在这些区域内制造了五个微柱。微柱压缩结果表明,微柱的机械行为与各种微结构参数(包括雪明碳柱倾角 (CIA)、层间距和铁素体-雪明碳柱分布)之间存在明显的相关性。此外,应变梯度晶体塑性有限元分析(SG-CPFEM)显示,铁素体-水泥石界面上的几何必要位错(GND)显著增加,对有效抗滑性产生了关键影响。模拟结果还表明,铁素体-水泥石界面的存在会显著增加 GND 的浓度,从而影响负载-位移行为。与加载方向垂直的胶结物微柱显示出更高的 GND 增量,而胶结物间距的减小则由于铁素体相中应变梯度的增加而放大了 GND 的形成。剪切断裂主要出现在 CIA 为 67.5º 或更高的岩柱中,而扭结带则出现在 CIA 为 22.5º 或更低的岩柱中。GNDs 的增加受 CIA 和层间间距的影响,突出了它们在决定机械性能方面的关键作用。
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引用次数: 0
Novel distortional anisotropic hardening model mediated by microstructure evolutions in polycrystalline metals: Theory and validation 由多晶金属微观结构演变介导的新型畸变各向异性硬化模型:理论与验证
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104227
Seonghwan Choi , Soo-Chang Kang , Jinwoo Lee , Myoung-Gyu Lee
In this study, we introduce a novel anisotropic hardening model designed to capture the macroscopic mechanical responses under complex loading paths while considering the mesoscopic evolutions of crystallographic structures. Based on the framework of homogeneous distortional anisotropic hardening, this model treats the plastic shear strain of each slip system as an internal variable. Utilizing the plastic work equivalence principle, the plastic shear rate within the slip system is determined, aligning with the evolution laws of rate-independent crystal plasticity (CP) theory. The model evaluates the Bauschinger effect and transient hardening at grain level and integrates it into the macroscopic yield function to describe phenomenological hardening responses. The model has been extensively validated against experimental and computational polycrystalline CP approaches, demonstrating its efficacy in capturing both the evolution of crystal textures and complex anisotropic hardening behaviors for both FCC and BCC materials. This proposed hardening model marks a significant advancement in material behavior modeling, effectively bridging the gap between microstructural mechanisms and macroscopic mechanical behavior in better practical way.
在这项研究中,我们引入了一种新的各向异性硬化模型,旨在捕捉复杂加载路径下的宏观力学响应,同时考虑晶体结构的细观演变。该模型基于均匀变形各向异性硬化框架,将各滑移体系的塑性剪切应变作为内部变量。利用塑性功等效原理,根据速率无关晶体塑性理论的演化规律,确定了滑移体系内的塑性剪切速率。该模型评估了包辛格效应和瞬态硬化在晶粒水平上的影响,并将其整合到宏观屈服函数中来描述现象性硬化响应。该模型已经通过实验和计算多晶CP方法进行了广泛的验证,证明了它在捕获FCC和BCC材料的晶体结构演变和复杂的各向异性硬化行为方面的有效性。提出的硬化模型标志着材料行为建模的重大进步,有效地弥合了微观结构机制和宏观力学行为之间的差距,更切合实际。
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引用次数: 0
Understanding the stress-induced grain boundary migration behavior in a deformed Mg alloy: The role of deformation twin and grain rotation 形变镁合金应力诱导晶界迁移行为的研究:变形孪晶和晶粒旋转的作用
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2025.104244
Zijian Zhang , Lin Yuan , Jiaping Ma , Mingyi Zheng , Debin Shan , Bin Guo
Stress-induced grain boundary (GB) migration plays a crucial role in plastic deformation, influencing the microstructure and mechanical properties of polycrystalline materials. While twinning and grain rotation are important deformation modes, their impact on the GB migration of Mg alloys remains unclear. This work builds the internal relationship between deformation twins, grain rotation, and stress-induced GB migration in a deformed Mg alloy by experiments and simulations. During the uniaxial compression experiment, the GB migration mainly occurs during the {101¯2}tension twin thickening. Atomic simulations reveal that twin thickening results from the slip of interface dislocations along the basal plane (0001) under shear stress. When interface dislocations of twins are hindered by the GB, local stress concentrations lead to GB migration. A new factor I, derived from experimental results, serves as a criterion to differentiate migrated from non-migrated regions during twin thickening at the mesoscale. Grain rotation accompanied by GB migration occurs under mesoscale observations. The scalar disclinations density increases at the GB junctions due to rotation and the disclinations move with the GB migration. Local rotation associated with the formation of low-angle GBs accelerates local migration and contributes to GB serration. Crystal plasticity finite element simulations show that the additional shear stress caused by grain rotation promotes GB migration. Our findings help to understand the GB migration mechanisms of Mg alloys related to the application of Mg alloys through GB engineering.
应力晶界迁移在塑性变形中起着至关重要的作用,影响着多晶材料的显微组织和力学性能。虽然孪晶和晶粒旋转是重要的变形模式,但它们对镁合金GB迁移的影响尚不清楚。本文通过实验和模拟建立了变形孪晶、晶粒旋转和变形镁合金应力诱导GB迁移之间的内在关系。在单轴压缩实验中,GB迁移主要发生在{101¯2}拉伸孪晶增厚过程中。原子模拟表明,孪晶增厚是由界面位错在剪切应力作用下沿基面(0001)滑移引起的。当晶界位错受到晶界位错的阻碍时,局部应力集中导致晶界位错的迁移。从实验结果中得到一个新的因子I,作为在中尺度上区分双胞胎增厚过程中迁移和非迁移区域的标准。在中尺度观测下,粮食轮作伴随着GB迁移。由于旋转的作用,标量偏差密度在GB结点处增加,偏差随GB迁移而移动。局部旋转与低角度GB的形成有关,加速了局部迁移,促进了GB的分离。晶体塑性有限元模拟表明,晶粒旋转产生的附加剪切应力促进了晶态迁移。研究结果有助于了解镁合金在GB工程中应用的GB迁移机制。
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引用次数: 0
Strategic enhancement of CoCrFeMnNi high-entropy alloy mechanical properties through a high-strength nano-scale nitride layer without geometrical or tolerance constraints 通过无几何或公差约束的高强度纳米氮化层战略性地增强CoCrFeMnNi高熵合金的力学性能
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104235
Gang Hee Gu , Shin Hyun Kim , Sung-Gyu Heo , Yongju Kim , Soo-Hyun Kim , Hyeonseok Kwon , Donghwa Lee , Goo-Hwan Jeong , Yoon-Uk Heo , Dong Jun Lee , Hyoung Seop Kim
Plasma nitriding is a class of surface treatment method that improves wear, corrosion, and fatigue properties along with the benefits of excellent geometry freedom and minimal dimensional distortion. Yet, previous plasma nitriding studies related to tensile properties have mostly compromised strength or ductility mainly due to grain growth or the brittle nature of bulky micrometer-scale nitride layer. We propose a strategy to simultaneously improve mutually exclusive strength and elongation through a high-strength nano-scale nitride layer fabricated via plasma nitriding, overcoming the typical trade-off relationship; for example, ultimate tensile strength and uniform elongation were improved by ∼74.6 MPa and ∼7.9 %, respectively. Using extraordinarily controlled processing parameters (e.g., low-pressure, short-time, warm-temperature), we successfully produced CoCrFeMnNi HEA with a nano-scale nitride layer of ∼291.9 nm near the surface without any change in grain size. The enhanced mechanical properties of the plasma nitrided CoCrFeMnNi HEA are attributed to the combined effects of pre-existing dislocation density, high-strength nano-scale nitride layer, and compressive residual stress. This work introduces an innovative approach to nano-scale hard regions, providing a novel framework for post-processing strategies ranging from fundamental research to various industrial applications.
等离子氮化是一类能改善磨损、腐蚀和疲劳性能的表面处理方法,同时还具有出色的几何自由度和最小尺寸变形的优点。然而,以往与拉伸性能有关的等离子氮化研究大多会损害强度或延展性,这主要是由于晶粒长大或大块微米级氮化层的脆性造成的。我们提出了一种策略,通过等离子氮化制造高强度纳米级氮化层,同时提高互斥的强度和伸长率,克服了典型的权衡关系;例如,极限拉伸强度和均匀伸长率分别提高了 ∼ 74.6 MPa 和 ∼ 7.9%。利用超常控制的加工参数(如低压、短时间、高温),我们成功制备出了在表面附近具有 ∼291.9 nm 纳米级氮化层的 CoCrFeMnNi HEA,且晶粒大小没有发生任何变化。等离子氮化 CoCrFeMnNi HEA 机械性能的增强归因于预先存在的位错密度、高强度纳米级氮化层和压缩残余应力的共同作用。这项工作为纳米级硬质区域引入了一种创新方法,为从基础研究到各种工业应用的后处理策略提供了一个新的框架。
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引用次数: 0
Advancing material simulations: Physics-Informed Neural Networks and Object-Oriented Crystal Plasticity Finite Element Methods 先进的材料模拟:物理信息神经网络和面向对象的晶体塑性有限元方法
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104221
Shahriyar Keshavarz , Yuwei Mao , Andrew C.E. Reid , Ankit Agrawal
An innovative method for predicting the behavior of crystalline materials is presented by integrating Physics-Informed Neural Networks (PINNs) with an object-oriented Crystal Plasticity Finite Element (CPFE) code within a large deformation framework. The CPFE platform is utilized to generate reference data for training the PINNs, ensuring precise and fast predictions of material responses. The object-oriented design of the CPFE system facilitates the coherent incorporation of complex constitutive models and numerical methods, enhancing simulation flexibility and scalability. To demonstrate the adaptability of this approach, two problems are addressed: a fundamental power-law and a complex dislocation density-based constitutive models for predicting the behavior of Ni3Al-based alloys. Both models are implemented within an object-oriented CPFE system powered by its flexible plug-in architecture. The resulting PINN model accurately captures intricate deformation mechanisms in crystalline materials, as validated through comparisons with CPFE simulations and experimental data. This work offers a promising alternative for efficient and accurate material behavior prediction, paving the way for advanced simulations in materials science.
提出了一种预测晶体材料行为的创新方法,即在大变形框架内将物理信息神经网络(pinn)与面向对象的晶体塑性有限元(CPFE)代码相结合。CPFE平台用于生成用于训练pin的参考数据,确保准确快速地预测材料响应。CPFE系统的面向对象设计有利于复杂本构模型和数值方法的连贯结合,提高了仿真的灵活性和可扩展性。为了证明这种方法的适应性,我们解决了两个问题:用于预测ni3alni3al基合金行为的基本幂律和基于复杂位错密度的本构模型。这两个模型都是在一个由其灵活的插件体系结构提供支持的面向对象的CPFE系统中实现的。由此产生的PINN模型准确地捕获了晶体材料中复杂的变形机制,并通过与CPFE模拟和实验数据的比较进行了验证。这项工作为有效和准确的材料行为预测提供了一个有希望的替代方案,为材料科学的高级模拟铺平了道路。
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引用次数: 0
Enhancing the strain-hardening rate and uniform tensile ductility of lightweight refractory high-entropy alloys by tailoring multi-scale heterostructure strategy 采用定制多尺度异质结构策略提高轻质难熔高熵合金的应变硬化率和均匀拉伸延展性
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104237
Yansong Zhang, Huaming Wang, Junwei Yang, Yanyan Zhu, Jia Li, Zhuo Li, Bing Su, Bingsen Liu, Chunjie Shen
During the deformation of body-centered cubic (BCC) structured lightweight refractory high-entropy alloys (LRHEAs), strain localization caused by a low strain-hardening rate (SHR) induces premature alloy necking, resulting in poor uniform tensile ductility (UTD) and restricts their processability and applicability. In this study, we improved the SHR of the alloys from negative to 1.5 GPa by tailoring multi-scale heterostructures, including the microscopic bimodal grain distribution, submicron spherical C14 Laves phase, nanoscale local chemical fluctuations (LCFs), and atomic clusters less than 1nm. The strength of the alloy was raised by 13.8 %, and the UTD increased by 710 % compared with the initial homogenized sample, and overall performance was superior to most LRHEAs. Bimodal grain interfaces can effectively coordinate the strain distribution between the two during deformation, accelerating the generation and storage of geometrically necessary dislocations (GNDs), and the back stress accumulates and increases with strain, stabilizing the hardening ability. Meanwhile, the meticulously dispersed C14 Laves phase plays a role in precipitation strengthening without compromising plasticity. The matrix's LCFs and Al-Zr atomic clusters can further regulate the morphology and distribution of statistically stored dislocations (SSDs). On the one hand, they could effectively pin dislocations and cause them to bend, increasing the migration resistance of SSDs; on the other hand, dislocation tangles resulting from microbands blocking and the interaction of multi-slip systems activate new dislocation sources, which lead to the rapid expansion of secondary microbands in a reticular manner. Those significantly increase the synchronous dislocation multiplication rate and dynamic dislocation density during plastic deformation, maintaining high and sustained SHR of alloys. Therefore, the SHR of LRHEA can be effectively improved by introducing multi-scale heterogeneous structures to optimize the coordination of GND and SSD density and distribution, thus achieving an excellent match between strength and UTD.
在体心立方(BCC)结构轻质耐火高熵合金(LRHEAs)变形过程中,由于低应变硬化率(SHR)导致的应变局部化导致合金过早颈缩,导致均匀拉伸延展性(UTD)较差,限制了其加工性能和适用性。在这项研究中,我们通过调整多尺度异质结构,包括微观双峰晶粒分布、亚微米球形C14 Laves相、纳米尺度局部化学波动(LCFs)和小于1nm的原子团簇,将合金的SHR从负提高到1.5 GPa。与初始均质样品相比,合金强度提高了13.8%,UTD提高了710%,整体性能优于大多数LRHEAs。双峰型晶粒界面能有效协调变形过程中两者之间的应变分布,加速几何必要位错(GNDs)的产生和储存,背应力随应变积累和增大,稳定了硬化能力。同时,精心分散的C14 Laves相在不影响塑性的前提下起到了沉淀强化的作用。矩阵的LCFs和Al-Zr原子团簇可以进一步调节统计存储位错(ssd)的形态和分布。一方面,它们可以有效地钉住位错并使其弯曲,增加ssd的迁移阻力;另一方面,微带阻塞和多滑移系统相互作用导致的位错缠结激活了新的位错源,导致次级微带以网状方式快速扩展。显著提高了塑性变形过程中的同步位错倍增率和动态位错密度,保持了合金的高持久SHR。因此,通过引入多尺度异质结构,优化GND和SSD密度和分布的协调性,可以有效提高LRHEA的SHR,从而实现强度和UTD的良好匹配。
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引用次数: 0
Influences of dislocation configuration and texture optimization on obtaining exceptional cryogenic strength-ductility synergy in a dynamic-recovered heterogeneous high-manganese steel 位错结构和织构优化对动态回收非均相高锰钢获得超常低温强度-塑性协同效应的影响
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104225
Hao Xiong , Yu Li , Chun Xu , Wei Li , Xiaoshuai Jia
In this study, an innovative strategy of dislocation configuration and texture optimization is employed to achieve a heterogeneous dynamic-recovered (DRV) high-manganese steel via successive cold-warm-rolling (CWR). Compared with single-step warm-rolling (WR) treatment, the imposed cold deformation of CWR process not only results in more and finer dislocation cells in DRV grains, but also leads to texture optimization with intensity weakening and component changing. Hence, the CWR sample shows a higher yield strength (YS, ∼1.35 GPa) and ultimate tensile strength (UTS, ∼1.6 GPa) without sacrificing the tensile elongation (TEL, ∼57%) at LNT (liquid nitrogen temperature), accompanied with a significantly lower mechanical anisotropy. The exceptional cryogenic strength-ductility synergy can be attributed to following: i) the difference of YS comes from the additional Taylor hardening effect (∼150 MPa); ii) the prefer-orientated DRV grains with a high Schmid factor (SFR) of twinning induces the twin deflections or kinks at the dislocation boundary in the early deformation stage; and iii) the refined cell structure can increase the critical resolved shear stress (CRSS) of twin, act as twin nucleus and impede its growth, leading to the occurrence of high-density of nano-twin segment (thickness: ∼15 nm, number density: ∼1.1 × 108 m-3) at a high stress and strain level. Thus, the cooperative forest dislocation hardening (∼870 MPa) and dynamic Hall-Petch strengthening (∼220 MPa) effects can provide continuous strain hardening capacity. In contrast, the high ductility of the WR sample primarily originates from the abundant microband-induced plasticity correlated with limited twinning- (TWIP) and transformation-induced plasticity (TRIP) due to a coarse twin (∼22.5 nm) and martensite thickness (∼55 nm).
在本研究中,采用一种创新的位错构型和织构优化策略,通过连续冷温轧制(CWR)实现了高锰钢的非均质动态恢复(DRV)。与单步温轧(WR)处理相比,CWR工艺的冷变形不仅使DRV晶粒中出现了更多更细的位错细胞,而且使织构优化,强度减弱,成分变化。因此,CWR样品在LNT(液氮温度)下表现出更高的屈服强度(YS, ~ 1.35 GPa)和极限抗拉强度(UTS, ~ 1.6 GPa),而不牺牲抗拉伸长率(TEL, ~ 57%),同时力学各向异性显著降低。特殊的低温强度-延性协同作用可归因于以下原因:1)YS的差异来自额外的泰勒硬化效应(~ 150 MPa);ii)高施密德因子(SFR)的择优取向DRV晶粒在变形初期在位错边界处诱发孪晶挠曲或扭结;精细的晶胞结构增加了孪晶的临界分解剪切应力(CRSS),起到孪晶核的作用,阻碍孪晶的生长,导致在高应力应变水平下出现纳米孪晶段高密度(厚度:~ 15 nm,数密度:~ 1.1 × 108 m-3)。因此,协同森林位错硬化(~ 870 MPa)和动态Hall-Petch强化(~ 220 MPa)效应可以提供连续应变硬化能力。相比之下,WR样品的高延展性主要源于丰富的微带诱导塑性,这与有限的孪晶(TWIP)和由粗孪晶(~ 22.5 nm)和马氏体厚度(~ 55 nm)引起的相变诱导塑性(TRIP)有关。
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引用次数: 0
Bulging of grain boundaries and core-shell dislocation structures enhance mechanical properties of equiatomic high-entropy alloys 晶界胀形和核壳位错结构提高了等原子高熵合金的力学性能
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104224
Jungwan Lee , Sun Ig Hong , Hyoung Seop Kim
Regulating elemental compositions of structural materials has been at the heart of interests for metallurgists to ensure target properties under harsh environments. For instance, metastability engineering that exploits phase transformation or deformation twinning depends on a minor modification in atomic compositions. Distinct from the well-studied control of elemental compositions, this work centers on a straightforward thermomechanical process of hot rolling to induce bulging of grain boundaries and core-shell dislocation cell structures. During the hot rolling, the bulging of grain boundaries releases high-density dislocation walls and more dislocations are distributed around the grain boundaries in equiatomic CoCrFeMnNi, one of the most studied high-entropy alloys. Under the tensile deformation at cryogenic temperatures with decreased stacking fault energy, the less stable grain boundaries promote the emanation of partial dislocations and the consequent formation of deformation twinning. As a result, the hot-rolled alloy exhibits an enhanced combination of yield strength of ∼941 MPa and uniform elongation of ∼54% at –196 °C, which is counterintuitive to low ductility of as-rolled metallic materials. This lies at the upper bound in comparison with tensile responses of precipitation-strengthened high-entropy alloys and high-strength steels. The higher propensity of deformation twins in hot-rolled alloy compared to that of cold-rolled and annealed one enhances strain hardening despite the hot-rolled state. Regarding the benefits of the streamlined thermomechanical history, this study validates the academic and industrial worth of hot-rolled metallic materials to develop the alloy science and fabricating technology.
调节结构材料的元素组成一直是冶金学家感兴趣的核心,以确保在恶劣环境下的目标性能。例如,利用相变或变形孪晶的亚稳态工程依赖于原子组成的微小改变。不同于已被充分研究的元素成分控制,这项工作集中在一个直接的热轧热力学过程中,以诱导晶界膨胀和核-壳位错细胞结构。等原子CoCrFeMnNi是研究最多的高熵合金之一,在热轧过程中,晶界的胀形释放出高密度的位错壁,晶界周围分布着更多的位错。在低温拉伸变形下,层错能降低,晶界不稳定,促进了部分位错的发散,从而形成变形孪晶。结果表明,热轧合金在-196℃时屈服强度达到~ 941 MPa,延伸率达到~ 54%,这与轧制时金属材料的低延展性相反。与析出强化高熵合金和高强钢的拉伸响应相比,这是上界。与冷轧和退火合金相比,热轧合金的变形孪晶倾向较高,在热轧状态下强化了应变硬化。考虑到热轧金属材料在热轧过程中所带来的好处,本研究验证了热轧金属材料在合金科学和制造技术发展中的学术和工业价值。
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引用次数: 0
Study of orientation-dependent residual strains during tensile and cyclic deformation of an austenitic stainless steel 奥氏体不锈钢拉伸和循环变形过程中取向相关残余应变的研究
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104228
Namit Pai, Indradev Samajdar, Anirban Patra
<div><div>This work presents a combined experimental and crystal plasticity finite element modeling study on the development of bulk and local residual strains during tensile and cyclic deformation of an austenitic stainless steel. The <span><math><mrow><mo>(</mo><mi>h</mi><mi>k</mi><mi>l</mi><mo>)</mo></mrow></math></span>-specific bulk (residual) lattice strains are measured using X-ray Diffraction, while the local residual strains are measured using High Resolution Electron Back Scatter Diffraction. The residual strains are predicted using a dislocation density-based crystal plasticity model, with consideration for directional hardening due to backstress evolution. The work emphasizes on residual strain developments for four specific grain families: <span><math><mrow><mo>(</mo><mn>111</mn><mo>)</mo></mrow></math></span>, <span><math><mrow><mo>(</mo><mn>001</mn><mo>)</mo></mrow></math></span>, <span><math><mrow><mo>(</mo><mn>101</mn><mo>)</mo></mrow></math></span> and <span><math><mrow><mo>(</mo><mn>311</mn><mo>)</mo></mrow></math></span>, specifically in terms of their correlation with the underlying microstructure, studied using crystallographic orientation, misorientation, dislocation density and backstress evolution. Large intragranular orientation gradients, dislocation densities and backstress are observed during tensile deformation for the texturally dominant <span><math><mrow><mo>(</mo><mn>101</mn><mo>)</mo></mrow></math></span> grain family, indicating that these grains have higher plastic deformation as compared to the <span><math><mrow><mo>(</mo><mn>001</mn><mo>)</mo></mrow></math></span> and <span><math><mrow><mo>(</mo><mn>111</mn><mo>)</mo></mrow></math></span> grain families. This also contributes to the observed relaxation in lattice strains for the <span><math><mrow><mo>(</mo><mn>101</mn><mo>)</mo></mrow></math></span> grain family, with the resulting load shed being primarily accommodated by the <span><math><mrow><mo>(</mo><mn>001</mn><mo>)</mo></mrow></math></span> grain family. In contrast, no such orientation gradients or lattice strain relaxations are observed in the cyclically deformed material. The measured local residual strains, which are also qualitatively predicted by the crystal plasticity simulations, highlight the additional effect of spatial heterogeneity and neighboring grains on the development of residual strains. Finally, statistical analysis of the simulated residual strains reveals that the hierarchy in the development of lattice strains is in the following order for the different grain families: <span><math><mrow><mrow><mo>(</mo><mn>001</mn><mo>)</mo></mrow><mo>></mo><mrow><mo>(</mo><mn>311</mn><mo>)</mo></mrow><mo>></mo><mrow><mo>(</mo><mn>111</mn><mo>)</mo></mrow><mo>></mo><mrow><mo>(</mo><mn>101</mn><mo>)</mo></mrow></mrow></math></span> for tensile deformation, and <span><math><mrow><mrow><mo>(</mo><mn>001</mn><mo>)</mo></mrow><mo>></mo><mrow><mo>(</mo><mn>311</mn><mo>)</mo></mrow><mo>></
本研究结合实验和晶体塑性有限元模型研究了奥氏体不锈钢在拉伸和循环变形过程中的体应变和局部残余应变的发展。(hkl)特异体(残余)晶格应变采用x射线衍射测量,局部残余应变采用高分辨率电子背散射衍射测量。利用基于位错密度的晶体塑性模型预测了残余应变,并考虑了背应力演化引起的定向硬化。本研究着重于(111)、(001)、(101)和(311)四个特定晶粒族的残余应变发展,特别是它们与底层微观结构的相关性,利用晶体取向、错取向、位错密度和背应力演化进行了研究。在拉伸变形过程中观察到较大的晶内取向梯度、位错密度和背应力,表明与(001)和(111)晶族相比,这些晶族具有更高的塑性变形。这也有助于观察到(101)晶粒族晶格应变的松弛,由此产生的载荷脱落主要由(001)晶粒族承担。相反,在循环变形材料中没有观察到这种取向梯度或晶格应变弛豫。实测的局部残余应变也通过晶体塑性模拟进行了定性预测,突出了空间异质性和邻近晶粒对残余应变发展的附加影响。最后,对模拟残余应变的统计分析表明,不同晶粒族的晶格应变发展顺序如下:拉伸变形(001)>(311)>(111)>(101),循环变形(001)>(311)>(111) ~(101)。在拉伸和循环变形过程中,不同晶粒族的弹性刚度和晶粒旋转(或缺乏旋转)是导致观察到的分层的主要因素。
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The residual strains are predicted using a dislocation density-based crystal plasticity model, with consideration for directional hardening due to backstress evolution. The work emphasizes on residual strain developments for four specific grain families: &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;111&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt;, &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;001&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt;, &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;101&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; and &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;311&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt;, specifically in terms of their correlation with the underlying microstructure, studied using crystallographic orientation, misorientation, dislocation density and backstress evolution. Large intragranular orientation gradients, dislocation densities and backstress are observed during tensile deformation for the texturally dominant &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;101&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; grain family, indicating that these grains have higher plastic deformation as compared to the &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;001&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; and &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;111&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; grain families. This also contributes to the observed relaxation in lattice strains for the &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;101&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; grain family, with the resulting load shed being primarily accommodated by the &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;001&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; grain family. In contrast, no such orientation gradients or lattice strain relaxations are observed in the cyclically deformed material. The measured local residual strains, which are also qualitatively predicted by the crystal plasticity simulations, highlight the additional effect of spatial heterogeneity and neighboring grains on the development of residual strains. Finally, statistical analysis of the simulated residual strains reveals that the hierarchy in the development of lattice strains is in the following order for the different grain families: &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;001&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;mo&gt;&gt;&lt;/mo&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;311&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;mo&gt;&gt;&lt;/mo&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;111&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;mo&gt;&gt;&lt;/mo&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;101&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;/mrow&gt;&lt;/math&gt;&lt;/span&gt; for tensile deformation, and &lt;span&gt;&lt;math&gt;&lt;mrow&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;001&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;mo&gt;&gt;&lt;/mo&gt;&lt;mrow&gt;&lt;mo&gt;(&lt;/mo&gt;&lt;mn&gt;311&lt;/mn&gt;&lt;mo&gt;)&lt;/mo&gt;&lt;/mrow&gt;&lt;mo&gt;&gt;&lt;/","PeriodicalId":340,"journal":{"name":"International Journal of Plasticity","volume":"185 ","pages":"Article 104228"},"PeriodicalIF":9.4,"publicationDate":"2025-02-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"142911523","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":1,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Multiscale modeling of the damage and fracture behaviours of TA15 titanium alloy with trimodal microstructure TA15钛合金三模态组织损伤断裂行为的多尺度模拟
IF 9.4 1区 材料科学 Q1 ENGINEERING, MECHANICAL Pub Date : 2025-02-01 DOI: 10.1016/j.ijplas.2024.104238
M.Y. Fei , P.F. Gao , Z.N. Lei , H.W. Li , M. Zhan , M.W. Fu
Trimodal microstructure, consisting of equiaxed α (αp), lamellar α (αl), and transformed β (βt), has become an ideal target microstructure of titanium alloys. However, the complex microstructure morphologies and the differences in mechanical property among the three constituent phases of the trimodal microstructure significantly influence its microscopic crack propagation behaviour and further affect its fracture toughness. To address this issue, a multiscale finite element (FE) model, including a microscopic crack propagation (micro-CP) model and a macroscopic fracture toughness (macro-FT) model, was established for analysis and prediction of the damage fracture behaviour and property of the trimodal microstructure. In this model, the deformation, damage and fracture behaviours of the trimodal microstructure at both micro and macro scales were described by bridging the constitutive laws of constituent phases and deformation responses. In tandem with this, the micro-CP model adopted a macro-micro nested structure, and the macro-FT model was developed based on a virtual fracture toughness test. Using the established multiscale FE model, the dependence of microscopic crack propagation and macroscopic fracture behaviours on the constituent phases of the trimodal microstructure was revealed. It is found that both αp and αl improved the path tortuosity and energy consumption of microscopic crack propagation, and αl decreased the microscopic crack propagation rate simultaneously. In addition, αp and αl contributed to the fracture toughness of the trimodal microstructure from both the intrinsic toughening mechanism (suppressing the heterogeneous deformation and damage and then decreasing the strength and increasing the plasticity) and the extrinsic toughening mechanism (increasing the tortuosity and energy consumption of crack propagation). The research provided an in-depth understanding of the damage and fracture behaviours of TA15 titanium alloy with the trimodal microstructure.
由等轴α (αp)、片层α (αl)和转化β (βt)组成的三峰组织已成为钛合金理想的靶组织。然而,三模态组织中复杂的组织形态和三个组成相之间力学性能的差异显著影响其微观裂纹扩展行为,进而影响其断裂韧性。为了解决这一问题,建立了包括微观裂纹扩展(micro-CP)模型和宏观断裂韧性(macro-FT)模型在内的多尺度有限元(FE)模型,对三模态微观结构的损伤断裂行为和性能进行了分析和预测。在该模型中,通过连接组成相的本构规律和变形响应,在微观和宏观尺度上描述了三模态微观结构的变形、损伤和断裂行为。与此相对应,微观cp模型采用宏观微观嵌套结构,宏观ft模型基于虚拟断裂韧性试验建立。利用所建立的多尺度有限元模型,揭示了微观裂纹扩展和宏观断裂行为与三模态组织组成相的关系。结果表明,αp和αl均提高了细观裂纹扩展的路径弯曲度和能量消耗,αl同时降低了细观裂纹扩展速率。此外,αp和αl对三模态组织的断裂韧性有内在的增韧机制(抑制非均质变形和损伤,降低强度,提高塑性)和外在的增韧机制(增加弯曲度和裂纹扩展能耗)。该研究为深入了解TA15钛合金的三模态组织损伤和断裂行为提供了依据。
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引用次数: 0
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International Journal of Plasticity
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