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Investigating laser intensity profile and light scattering effects in the transmission laser welding process of 3D printed parts 研究三维打印部件透射激光焊接过程中的激光强度曲线和光散射效应
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-01-07 DOI: 10.1016/j.jajp.2024.100186
Thi-Ha-Xuyen Nguyen, André Chateau Akué Asséko, Anh-Duc Le, Benoît Cosson

Transmission Laser Welding (TLW) is a promising technique for joining thermoplastic and composite components, especially those produced through additive manufacturing or 3D printing processes. However, achieving optimal welding quality and efficiency in TLW of 3D printed parts is challenging due to the presence of highly heterogeneous and anisotropic materials, which introduce light scattering and absorption issues. Light scattering is caused by the refraction phenomenon. These phenomena significantly impact the laser intensity profile within the materials and at the welding interface, thereby affecting the energy required for successful welding and the mechanical strength of the final assembly. In this paper, we present an in-depth investigation into the laser intensity profile and the effects of laser-matter interaction on the welding of 3D-printed parts. Our approach combines experimental measurements using a heat flux sensor and an analytical inverse model to measure the laser intensity distribution within the materials at the welding interface. The results obtained from the experimental measurements and numerical identification are compared and analyzed, providing insights into the laser intensity profile in TLW of 3D printed parts.

透射激光焊接(TLW)是一种很有前途的热塑性塑料和复合材料部件连接技术,尤其是那些通过增材制造或三维打印工艺生产的部件。然而,在三维打印部件的透射激光焊接中实现最佳焊接质量和效率具有挑战性,这是因为存在高度异质和各向异性的材料,会带来光散射和吸收问题。光散射是由折射现象引起的。这些现象会严重影响材料内部和焊接界面的激光强度曲线,从而影响成功焊接所需的能量和最终装配的机械强度。在本文中,我们深入研究了激光强度曲线以及激光与物质相互作用对 3D 打印部件焊接的影响。我们的方法结合了使用热通量传感器的实验测量和分析逆模型,以测量焊接界面材料内部的激光强度分布。通过对实验测量结果和数值识别结果进行比较和分析,我们可以深入了解三维打印部件 TLW 焊接过程中的激光强度分布。
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引用次数: 0
Investigations to improve the tool life during thermomechanical and incremental forming of steel auxiliary joining elements 在钢制辅助连接部件的热机械和增量成形过程中提高工具寿命的研究
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-01-07 DOI: 10.1016/j.jajp.2024.100185
T Borgert, AB Nordieker, E Wiens, W Homberg

Modern vehicles as well as structures consist more and more often of a multi material mix. In addition to the use of light materials (e. g. aluminium) to optimise lightweight construction potential, higher strength alloys are being used more and more frequently. With the different material combinations, the requirements for the joining technology also increase. Thus (due to restrictions in the area of thermal joining processes) the joining of different material combinations is often realised by mechanical joining technology. Even though different joining tasks (dissimilar material or sheet thicknesses) can be solved by mechanical joining technology in general, it is often required to switch between appropriate auxiliary joining elements and even joining technique. To adapt the auxiliary elements to the individual requirements of each joint an innovative manufacturing process of customisable auxiliary joining elements has been developed. The use of the incremental, thermomechanical manufacturing process called friction-spinning for the manufacturing of adaptive auxiliary joining elements enables to individualise each element for the subsequent joining process. However, this advantage comes at the cost of a high mechanical and thermal loads on the forming tools. These loads also depend on the process design (trajectory, feed, rotational speed) and have to be controlled in order to improve the tool life. For a more profound process knowledge and to better understand the corellation of the individual process variables, a series of tests with varying process parameters were carried out in a partial factorial design of experiments. The results show not only an possible improvement in the tool life, but also the required process design for a higher reproducibility of the auxiliary joining element geometry and the possibility of positively influencing the geometry to achieve a force-closure of the joint.

现代车辆和结构越来越多地由多种材料组合而成。除了使用轻质材料(如铝)来优化轻质结构外,高强度合金的使用也越来越频繁。随着材料组合的不同,对连接技术的要求也随之提高。因此(由于热连接工艺的限制),不同材料组合的连接通常采用机械连接技术。尽管不同的连接任务(不同的材料或板材厚度)一般都可以通过机械连接技术来解决,但往往需要在适当的辅助连接元件甚至连接技术之间进行切换。为了使辅助元件适应每个接合点的个性化要求,我们开发了一种可定制辅助接合元件的创新制造工艺。在自适应辅助连接元件的制造过程中,使用了一种名为摩擦纺丝的增量热机械制造工艺,从而使每个元件都能在后续连接过程中实现个性化。然而,这一优势的代价是成型工具要承受较高的机械和热负荷。这些载荷也取决于工艺设计(轨迹、进料、转速),必须加以控制,以提高工具的使用寿命。为了更深入地了解工艺知识,更好地理解各个工艺变量之间的核心关系,我们在部分因子实验设计中进行了一系列改变工艺参数的测试。结果表明,不仅刀具寿命有可能提高,而且工艺设计所需的辅助接合元件几何形状的再现性更高,并有可能对几何形状产生积极影响,从而实现接合处的力闭合。
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引用次数: 0
A novel joining technology for metal and polymer sheets 金属和聚合物板材的新型连接技术
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-01-04 DOI: 10.1016/j.jajp.2024.100184
MM Kasaei , RJC Carbas , EAS Marques , LFM da Silva

This paper introduces a novel joining process for producing hybrid metal-polymer joints. The process, called hole hemming, involves deforming the metal sheet to establish a mechanical interlock with the polymer sheet, requiring neither heating nor auxiliary elements. The applicability of this process is tested for joining aluminum and polycarbonate (PC) sheets. Initially, an analytical design method is presented to achieve a connection without failure and with a mechanical interlock. Subsequently, the accuracy of the predictions is assessed through experiments and finite element simulations, employing the modified Mohr-Coulomb criterion for the prediction of ductile damage. Additionally, a new design for hole-hemmed joints, involving the incorporation of branches in the hole of the outer sheet, is introduced to expand the process window of this novel joining technology. Finally, the mechanical behavior of four different types of hybrid hole-hemmed joints (HHH joints) are evaluated through single-lap shear tests. The results show that the hole hemming process can successfully join AA6082-T4 and PC sheets, validating the proposed designs and ideas. The new hybrid joints demonstrate a maximum force and displacement of 1.6 kN and 12.9 mm, respectively, in the shear test, indicating significant potential of the proposed technology for joining metal and polymer sheets.

本文介绍了一种用于生产金属-聚合物混合接头的新型连接工艺。这种工艺被称为 "孔折边",它通过使金属板变形来与聚合物板建立机械互锁,既不需要加热,也不需要辅助元件。我们对铝板和聚碳酸酯(PC)板的连接工艺进行了测试。首先提出了一种分析设计方法,以实现无故障连接和机械互锁。随后,通过实验和有限元模拟,采用修正的莫尔-库仑准则来预测韧性破坏,评估了预测的准确性。此外,还介绍了一种新的孔铰接设计,即在外层板的孔中加入分支,以扩大这种新型连接技术的工艺窗口。最后,通过单圈剪切试验评估了四种不同类型的混合孔铰接接头(HHH 接头)的机械性能。结果表明,孔边工艺可以成功连接 AA6082-T4 和 PC 板,验证了所提出的设计和想法。在剪切试验中,新型混合接头的最大力和位移分别达到 1.6 kN 和 12.9 mm,这表明所提出的技术在连接金属和聚合物板材方面具有巨大潜力。
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引用次数: 0
Investigation of the influence of pulse parameters on the resulting weld seam quality in pulsed electron beam welding of AW 6061 研究脉冲参数对 AW 6061 脉冲电子束焊接焊缝质量的影响
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-28 DOI: 10.1016/j.jajp.2023.100183
M. Troise, T. Krichel, S. Olschok, U. Reisgen

Utilizing pulsed lasers in favor of a continuous wave in laser beam welding is a well-established method to achieve higher process efficiency and reduce heat input into the workpiece, which is especially useful for thin-walled workpieces (Steen, 2005). In addition, pulsed processes have shown to lead to smaller grain sizes due to higher cooling rates, which can lead to a reduction in hot cracks in some aluminum alloys (Beiranvand et al., 2019). Since an electron beam can also be pulsed, a technique industrially utilized in electron beam drilling, the same principles apply (Schultz, 2000). However, pulsed electron beam welding is rarely used in industrial welding applications due to the risk of pores, spiking and sputtering resulting from the pulsed process dynamic, especially in the deep welding regime (Kautz, 1991). This study aims to develop a pulsed electron beam welding process for AW 6061 sheet metal, which is susceptible to hot cracking. The influence of the welding and pulse parameters, as well as the combination of a pulsed beam with high frequency beam oscillation is discussed. Furthermore, suitable welding parameters for pulsed electron beam welding of AW 6061 are developed, and the increased efficiency of pulsed welding is shown by comparison to continuous welds.

在激光束焊接中使用脉冲激光而非连续波激光是一种行之有效的方法,可提高加工效率并减少输入工件的热量,这对薄壁工件尤其有用(Steen,2005 年)。此外,脉冲工艺由于冷却率更高,因此晶粒尺寸更小,这可以减少某些铝合金的热裂纹(Beiranvand 等人,2019 年)。由于电子束也可以是脉冲式的,这种技术在工业上用于电子束钻孔,因此原理相同(Schultz,2000)。然而,脉冲电子束焊接在工业焊接应用中很少使用,因为脉冲过程动态会产生气孔、尖峰和溅射风险,尤其是在深层焊接过程中(Kautz,1991)。本研究旨在为容易产生热裂纹的 AW 6061 金属板开发一种脉冲电子束焊接工艺。研究讨论了焊接和脉冲参数的影响,以及脉冲光束与高频光束振荡的结合。此外,还为 AW 6061 的脉冲电子束焊接制定了合适的焊接参数,并通过与连续焊缝的比较显示了脉冲焊接效率的提高。
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引用次数: 0
In situ localised post-weld heat treatment with electron beam welding of S690QL steel 利用电子束焊接对 S690QL 钢进行局部焊后热处理
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-27 DOI: 10.1016/j.jajp.2023.100182
Raghawendra Sisodia , Marek Weglowski , Piotr Sliwinski

The objective of this research is to assess the influence of in-situ localised electron beam post-weld heat treatment (LEB-PWHT) on the microstructure and mechanical properties of high-strength S690QL steel welded joints utilising highly sophisticated electron beam welding (EBW) technology. Although EBW is well-known for creating high-quality welds, the addition of the novel LEB-PWHT technique may significantly improve the characteristics of the welded joints. To systematically analyse the impacts of PWHT on the welded joints, the study employs microstructural analysis like optical microscopy and mechanical properties like microhardness testing, bending, tensile, and impact tests. Furthermore, tensile fractography analysed by scanning electron microscopy (SEM) to provide detailed insights into the fracture behaviour of the welded joints. The results show that the in-situ PWHT approach improves the microstructure and mechanical characteristics of the welded joints, such as a lower hardness peak in the heat affected zone (HAZ), increased tensile strength (5%), and improved toughness by 7 times. LEB-PWHT fractured surface revealed smaller, more sharply defined dimples and micro-voids. These results suggest that in-situ PWHT is an attractive option for improving the quality and performance of welds in a wide range of applications incorporating S690QL steel.

本研究旨在评估原位局部电子束焊后热处理(LEB-PWHT)对采用高精密电子束焊接(EBW)技术的高强度 S690QL 钢焊接接头的微观结构和机械性能的影响。尽管 EBW 以制造高质量焊缝而闻名,但加入新颖的 LEB-PWHT 技术可显著改善焊接接头的特性。为了系统分析 PWHT 对焊接接头的影响,该研究采用了光学显微镜等微观结构分析方法和显微硬度测试、弯曲、拉伸和冲击测试等机械性能分析方法。此外,还通过扫描电子显微镜(SEM)进行拉伸断裂分析,以详细了解焊接接头的断裂行为。结果表明,原位 PWHT 方法改善了焊接接头的微观结构和机械特性,如降低了热影响区(HAZ)的硬度峰值,提高了抗拉强度(5%),并将韧性提高了 7 倍。LEB-PWHT 的断裂表面显示出更小、更清晰的凹陷和微空洞。这些结果表明,在使用 S690QL 钢的各种应用中,原位 PWHT 是提高焊缝质量和性能的一种有吸引力的选择。
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引用次数: 0
Electropolymerization of acrylic acid on steel for enhanced joining by plastic deformation 在钢上电聚合丙烯酸,通过塑性变形增强接合效果
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-25 DOI: 10.1016/j.jajp.2023.100181
B. Duderija , F. Sahin , D. Meinderink , J.C. Calderón-Gómez , H.C. Schmidt , W. Homberg , G. Grundmeier , A. González-Orive

Resource-efficient electrochemical polymerization of acrylic acid (AA) on steel (DC04), from mildly acid Zn2+/ AA-containing aqueous solutions, is presented as an effective and sustainable thin film technology which allows for a precise control of the polymer thickness and morphology. The steel substrates were potentiostatically polarized to -1.4 V (vs. Ag/AgCl) or cycled between +0.1 to -1.4 V (vs. Ag/AgCl) in a degassed 2.0 M AA and 0.2 M ZnCl2-containing aqueous electrolyte solution at pH 6. FE-SEM, AFM, FT-IRRAS, XPS, and electrochemical measurements shed light on the structural and chemical features exhibited by the as-prepared polyacrylic acid (PAA) thin films. When PAA-modified DC04 plates are joined to Al EN AW-1050A H24 specimens by plastic deformation using cold pressure welding (CPW), tensile strength testing unveiled the macroscopic interfacial adhesion-promoting capabilities exhibited by PAA layers to the opposing aluminum oxide surfaces. Carboxylate moieties present in the PAA are shown to form stable chemical bonds with metal oxide surfaces and with amine-epoxy-based resins. Interestingly, higher maximum shear force values are obtained for the PAA films when Zn metallic deposits are not present in the organic layer, but, when these welded specimens are heated up to 200 °C in a N2 atmosphere, it occurred exactly the opposite: Zn particle-containing PAA films showed the highest maximum shear force values for the same deposition time.

在钢 (DC04) 上利用含弱酸性 Zn2+/ AA 的水溶液进行丙烯酸 (AA) 的资源节约型电化学聚合,是一种有效且可持续的薄膜技术,可精确控制聚合物的厚度和形态。在 pH 值为 6 的脱气 2.0 M AA 和 0.2 M ZnCl2- 含水电解质溶液中,将钢基板静电极化至 -1.4 V(相对于 Ag/AgCl),或在 +0.1 至 -1.4 V(相对于 Ag/AgCl)之间循环。FE-SEM、AFM、FT-IRRAS、XPS 和电化学测量揭示了制备的聚丙烯酸 (PAA) 薄膜的结构和化学特征。当使用冷压焊(CPW)通过塑性变形将 PAA 改性的 DC04 板与 Al EN AW-1050A H24 试样连接在一起时,拉伸强度测试揭示了 PAA 层对对立的氧化铝表面所表现出的宏观界面粘附促进能力。PAA 中的羧酸盐分子可与金属氧化物表面和胺环氧树脂形成稳定的化学键。有趣的是,当有机层中不存在金属锌沉积物时,PAA 薄膜会获得更高的最大剪切力值,但当这些焊接试样在氮气环境中加热到 200 °C 时,情况恰恰相反:在相同的沉积时间内,含锌微粒的 PAA 薄膜显示出最高的最大剪切力值。
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引用次数: 0
Feasibility of friction stir welding using a hemispherical tool tilted towards the retreating side 使用向后退一侧倾斜的半球形工具进行搅拌摩擦焊接的可行性
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-21 DOI: 10.1016/j.jajp.2023.100180
D. Ambrosio, A. Sharma, M. Mukuda, Y. Morisada, H. Fujii

The use of a hemispherical tool tilted towards the retreating side for friction stir welding 6061-T6 aluminum alloy is investigated. Joints with smooth surfaces and without internal voids are obtained. Under the same welding and rotational speeds, adapting the tilt angle makes it possible to weld various thicknesses up to 3.5 mm. Plunge depth and tilt angle are demonstrated to be key geometrical parameters driving material flow when using the hemispherical tool. Microstructural features in the weld are equiaxed and refined grains below 5 µm in the stirred zone and narrow thermo-mechanical affected zones. The through-thickness thermomechanical gradient developing beneath the hemispherical tool leads to different extents of dynamic recrystallization and recovery in the stirred zone. The tool orientation towards the retreating side and the division of the tool-workpiece interaction in continuous and intermittent contact leads to an asymmetrical thermal field around the stirred zone. Hence, the new derivative friction stir welding solution allows the welding of multiple aluminum alloy blank thicknesses using the same tool.

研究了使用向后退侧倾斜的半球形工具对 6061-T6 铝合金进行搅拌摩擦焊接的方法。焊接接头表面光滑且无内部空隙。在相同的焊接和旋转速度下,调整倾斜角度可以焊接厚度达 3.5 毫米的各种材料。事实证明,在使用半球形工具时,切入深度和倾斜角度是驱动材料流动的关键几何参数。焊缝的微观结构特征是在搅拌区和狭窄的热机械影响区内出现 5 微米以下的等轴和细化晶粒。半球形工具下方形成的通厚热机械梯度导致搅拌区出现不同程度的动态再结晶和恢复。工具朝向后退侧的方向以及工具与工件在连续和间歇接触中的相互作用导致了搅拌区周围不对称的热场。因此,新的衍生搅拌摩擦焊接解决方案允许使用同一工具焊接多种厚度的铝合金坯料。
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引用次数: 0
Cold spot joining of high-strength steel sheets 高强度钢板的冷点连接
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-21 DOI: 10.1016/j.jajp.2023.100179
Takumi Aibara , Masayoshi Kamai , Yoshiaki Morisada , Kohsaku Ushioda , Takaaki Miyauchi , Shinichi Hasegawa , Hidetoshi Fujii

A novel solid-state joining method, called cold spot joining (CSJ), has been successfully developed. In this method, the material near the joining interface undergoes plastic deformation under high pressure, forming a joining interface, while oxide layers at the interface are fragmented and expelled to the exterior. High-strength steel sheets (HSS) with strengths of 780 MPa were joined under various conditions. The joining temperature can be adjusted by applying pressure during CSJ. Applying suitable pressure results in solid-state joining, and microstructural observations, alongside fracture morphology, indicate that the formation of a brittle structure was effectively prevented. Furthermore, cross-tensile strength measurements were conducted on steel sheets of varying strength grades, ranging from 270 to 1180 MPa and exhibited that the cross-tensile strength increased with increasing tensile strength.

一种名为冷点连接(CSJ)的新型固态连接方法已经研制成功。在这种方法中,接合界面附近的材料在高压下发生塑性变形,形成接合界面,同时界面上的氧化层破碎并被排出到外部。强度为 780 兆帕的高强度钢板(HSS)在不同条件下进行了接合。在 CSJ 过程中,可以通过施加压力来调节连接温度。施加适当的压力会导致固态连接,而微观结构观察和断裂形态表明,脆性结构的形成得到了有效防止。此外,还对 270 至 1180 兆帕不同强度等级的钢板进行了交叉拉伸强度测量,结果表明交叉拉伸强度随拉伸强度的增加而增加。
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引用次数: 0
Thermographic procedure for the assessment of Resistance Projection Welds (RPW): Investigating parameters and mechanical performances 用于评估电阻凸焊 (RPW) 的热成像程序:研究参数和机械性能
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-15 DOI: 10.1016/j.jajp.2023.100177
G. Dell'Avvocato, D. Palumbo

This study presents a non-destructive testing (NDT) thermographic procedure for assessing the quality and mechanical strength of Resistance Projection Welded (RPW) joints with rectangular embossments. We analysed twelve RPW joints by systematically varying process parameters based on a factorial design. These joints underwent flash thermography followed by mechanical tests to evaluate the maximum breaking force (Fmax). Significant statistical correlations between process parameters (time and force) and Fmax were established. Furthermore, we found a correlation (p-value 0.86) between the optically measured fused region and Fmax. Subsequently, we developed a pulsed phase thermography-based procedure for non-destructively measuring the fused region, resulting in an average difference of approximately 4 % compared to optical measurements. An empirical linear relationship was derived to correlate the welded area obtained by thermal data with Fmax, enabling the estimation of mechanical joint strength through non-destructive pulsed thermography. This research offers a promising approach for assessing the mechanical integrity of RPW joints using thermal imaging techniques.

本研究介绍了一种无损检测(NDT)热成像程序,用于评估带有矩形压纹的电阻凸焊(RPW)接头的质量和机械强度。我们通过系统地改变基于因子设计的工艺参数,对十二个 RPW 接头进行了分析。对这些接头进行了闪光热成像,然后进行了机械测试,以评估最大断裂力(Fmax)。结果表明,工艺参数(时间和力)与 Fmax 之间存在显著的统计相关性。此外,我们还发现光学测量的熔合区域与 Fmax 之间存在相关性(p 值为 0.86)。随后,我们开发了一种基于脉冲相位热成像的程序,用于非破坏性地测量熔合区域,结果与光学测量相比,平均差异约为 4%。我们得出了一种经验线性关系,将热数据获得的焊接区域与 Fmax 相关联,从而能够通过非破坏性脉冲热成像技术估算机械接头强度。这项研究为利用热成像技术评估 RPW 接头的机械完整性提供了一种可行的方法。
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引用次数: 0
The effect of vacuum brazing time on the microstructure and mechanical properties of Ti-6Al-4 V to 316 L dissimilar joint using BNi-2 filler metal 使用 BNi-2 填充金属的真空钎焊时间对 Ti-6Al-4 V 至 316 L 异种接头的微观结构和机械性能的影响
IF 4.1 Q2 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2023-12-12 DOI: 10.1016/j.jajp.2023.100176
Milad Foumani, Homam Naffakh-Moosavy

Due to the distinct differences in physical and metallurgical properties, it is hard to join titanium alloys to stainless steels directly via conventional welding processes. In this research, the grade 5 titanium alloy was subjected to brazing with austenitic stainless steel through the vacuum furnace, and the process was conducted above the β transition temperature (BTT). In order to reduce brittle intermetallic formation, a nickel base filler metal (Ni-6.6Cr-4.5Si-3B) was employed under a vacuum condition, and the effect of time on the microstructure and mechanical properties of the joints was investigated. The brazing temperature led to the thickening of the interface to 400 µm, toward the titanium alloy, and the FeTi formed adjacent to the diffusion affected zone (DAZ). Moreover, the isothermal solidified zone (ISZ) widened during the whole process, which, led to higher dissolution of the titanium base metal in the ISZ. Because of the widening of the interfaces, there were no Ni-rich compounds or residual filler metal in this region. SEM result showed that TiB strengthening borides, which were distributed after 45 min, and this evolution caused an increase in the shear strength of the joint up to 67 MPa. Fractography analyses and XRD results of the fractured surfaces revealed that the Ti2Ni phase, which formed in the athermaly solidified zone (ASZ) during a two-step solidification reaction, caused the brittle fracture in all joints.

由于物理和冶金性能的明显差异,很难通过传统焊接工艺将钛合金与不锈钢直接连接起来。在这项研究中,5 级钛合金通过真空炉与奥氏体不锈钢进行了钎焊,钎焊过程在 β 转变温度(BTT)以上进行。为了减少脆性金属间化合物的形成,在真空条件下采用了镍基填充金属(Ni-6.6Cr-4.5Si-3B),并研究了时间对接头微观结构和机械性能的影响。钎焊温度导致界面向钛合金方向增厚至 400 µm,并在扩散影响区(DAZ)附近形成了铁钛。此外,在整个过程中,等温凝固区(ISZ)变宽,导致等温凝固区中钛基合金的溶解度增加。由于界面变宽,该区域没有富镍化合物或残余填充金属。扫描电子显微镜结果表明,钛硼化物在 45 分钟后分布加强,这种演变使接头的剪切强度增加到 67 兆帕。断裂表面的断口形貌分析和 XRD 结果表明,在两步凝固反应过程中在非热凝固区(ASZ)形成的 Ti2Ni 相导致了所有接头的脆性断裂。
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引用次数: 0
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