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An Approach For Microencapsulation Of Melaleuca alternifolia Oil Using Different Techniques And Its Application 不同工艺制备互花千层油的微胶囊化方法及其应用
Pub Date : 2023-09-15 DOI: 10.2174/2666145417666230915103802
Samidha Shelar, Subhalaxmi Pradhan, Chandu S. Madankar
Abstract: Tea tree oil (TTO) is a widely known essential oil extracted from Melaleuca alternifolia leaves naturally having antimicrobial and antibacterial activities. Tea tree oil is widely used in a variety of industries, including agrochemicals, pharmaceuticals, medicine, food, textiles, as well as cosmetic and hygiene products. To overcome the limitation of tea tree oil being highly volatile and reactive, microencapsulation has become one of the preferred methods to retain and control these compounds. This review explores the different techniques for encapsulating tea tree oil. Along with a comprehensive overview of the most recent research and applications of microencapsulated tea tree oil, microencapsulation techniques and the available technologies are also discussed.
摘要:茶树油是一种从互花千层树叶中提取的具有抗菌和抑菌活性的天然精油。茶树油被广泛应用于各种行业,包括农化、制药、医药、食品、纺织以及化妆品和卫生产品。为了克服茶树精油挥发性强、反应性强的限制,微胶囊化已成为保留和控制这些化合物的首选方法之一。这篇综述探讨了不同的茶树油包封技术。综述了微胶囊化茶树油的最新研究和应用,并对微胶囊化技术和现有技术进行了讨论。
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引用次数: 0
Recent progress in layered double hydroxides-based materials as sustainable nanoadsorbents for hazardous pollutants recovery from aqueous medium 层状双氧水基材料在水介质中回收有害污染物的可持续纳米吸附剂研究进展
Pub Date : 2023-09-14 DOI: 10.2174/2666145417666230914104249
Mustapha Dib, Marieme Kacem, Nazrizawati A. Tajuddin
Abstract: The increasing prevalence of hazardous pollutants in water poses a significant global threat to the environment and human health. To address this issue, various methodologies have been developed for the determination and removal of harmful contaminants, with layered double hydroxides (LDHs)-based materials emerging as promising adsorbents. This review focuses on recent advancements in the application of LDHs-based materials for the removal of specific harmful pollutants, such as selenium, fluoride, heavy metals, and organic dyes, from aqueous solutions. Heavy metals and organic dyes, in particular, are major contributors to environmental pollution, necessitating effective and eco-friendly treatment methods.
摘要:水体中有害污染物的日益普遍,对环境和人类健康构成了重大的全球性威胁。为了解决这个问题,人们开发了各种方法来测定和去除有害污染物,分层双氢氧化物(LDHs)基材料成为有前途的吸附剂。本文综述了ldhs基材料在去除水中特定有害污染物,如硒、氟化物、重金属和有机染料等方面的研究进展。特别是重金属和有机染料是造成环境污染的主要因素,因此需要有效和环保的处理方法。
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引用次数: 0
Synthesis and characterisation of porous carbide-derived carbon from SiC in Molten Salt 熔融盐中碳化硅多孔碳化物衍生碳的合成与表征
Pub Date : 2023-09-05 DOI: 10.2174/2666145417666230905150410
Kai Zheng, Cuilian Shi, Jierui Li, Xiangdong Su
Introduction: The nanoporous carbide-derived carbon (CDC) have been prepared by electrochemical etching of SiC in molten CaCl2 at 900 ºC for 15 h in argon at an applied constant voltage of 3.0 V. SiC powder was pressed to form a pellet which was then served as the anode, and a graphite rod was used as the cathode Method: The results show that the obtained SiC-CDC is a mixture of amorphous carbon and ordered graphite phase with a highly degree of graphitization. The Raman analysis confirms that the ID/IG ratio of the CDC nanosheets is 0.46, indicating a lower degree of graphitization. Result: The layered CDC nanosheets possess a specific surface area of 561.39 m2/g and a total pore volume of 0.39 cm3/g with an average pore diameter of 2.8 nm. Conclusion: It is suggested that the molten salt electrochemical etching process is a novel method for the production of porous carbon material, and has the penitential to be used for a variety of applications.
摘要:采用恒电压3.0 V,在900℃的氩气中电解腐蚀SiC,制备了纳米多孔碳化物衍生碳(CDC)。将碳化硅粉末压成球团作为阳极,用石墨棒作为阴极。结果表明,所制得的碳化硅- cdc是一种非晶态碳与有序石墨相的混合物,石墨化程度高。拉曼分析证实,CDC纳米片的ID/IG比为0.46,表明石墨化程度较低。结果:层状CDC纳米片的比表面积为561.39 m2/g,总孔容为0.39 cm3/g,平均孔径为2.8 nm。结论:熔盐电化学蚀刻工艺是制备多孔碳材料的一种新方法,具有广阔的应用前景。
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引用次数: 0
Hybrid Aluminized Fiberglass Reinforced Composite Pipes: A Framework for Safety Use in Industries 混合铝化玻璃纤维增强复合管道:工业安全使用的框架
Pub Date : 2023-09-04 DOI: 10.2174/2666145417666230904122507
A. Vasanthanathan, U. P. S. Narayanan, K. Amudhan
Polymer matrix composites have been utilized in various industries due to their low cost and good strength-to-weight ratios. AIM: This study aims to investigate the effectiveness of filament-wound fiber-reinforced polymer composite pipes. The focus is on aluminized fabric tubes, which are flexible and heat-resistant tubes made from a glass fabric and laminated with a layer of aluminum.These tubes offer unique properties that make them suitable for various applications, especially in environments with high temperatures or exposure to radiant heat. Fiber Reinforced Plastic (FRP) pipes are highlighted for their lightweight, easy transportation, low maintenance, corrosion resistance, design flexibility, and anti-freezing performance. The study delves into the use of aluminized glass fiber for high-temperature applications, with a specific focus on enhancing high-temperature withstanding properties.In addition, the present research also conducts tests to study the structural strength of normal glass fabric tubes and aluminized glass fabric tubes. The fabrication of composite pipes is achieved through a filament winding process with a zero-degree winding angle using a manually operated filament winding machine. Mechanical testing and Finite Element Analysis (FEA) simulations using ANSYS® are also performed to compare glass fiber-reinforced plastic pipes with hybrid aluminized fiber-reinforced plastic pipes.The application of aluminized glass fiber in both the internal and external layers of the pipes improves the pipe’s strength and ability to endure high temperatures.
聚合物基复合材料由于其低成本和良好的强度重量比而被广泛应用于各个行业。目的:研究长丝缠绕纤维增强聚合物复合管材的性能。重点是镀铝织物管,这是一种柔性和耐热的管,由玻璃织物制成,并与铝层压在一起。这些管提供独特的性能,使其适用于各种应用,特别是在高温或暴露于辐射热的环境中。FRP (Fiber Reinforced Plastic)管材具有重量轻、运输方便、维护成本低、耐腐蚀、设计灵活、防冻等特点。该研究深入研究了铝化玻璃纤维在高温应用中的应用,特别关注增强高温耐受性。此外,本研究还对普通玻璃布管和镀铝玻璃布管的结构强度进行了试验研究。复合材料管道的制造是通过人工操作的缠绕机以零度缠绕角缠绕长丝工艺实现的。利用ANSYS®进行了力学测试和有限元分析(FEA)模拟,比较了玻璃纤维增强塑料管与混合镀铝纤维增强塑料管。镀铝玻璃纤维在管道内外两层的应用,提高了管道的强度和耐高温能力。
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引用次数: 0
Utilization of Polysaccharides-Based Nanoparticles for Gene Delivery: Advances and Prospective 利用基于多糖的纳米颗粒进行基因传递:进展与展望
Pub Date : 2023-09-04 DOI: 10.2174/2666145417666230904150858
Bilkisu Ibrahim Goni, Sonali Sundram, Rishav Sharma
Many industries use polysaccharide materials, such as those dealing with food, food packaging, medicine delivery, tissue engineering, wound dressing, wastewater treatment, and bioremediation. They were implemented in these spheres because of their efficacy, low cost, non-toxicity, biocompatibility, and biodegradability. It's well-known that many quick and easy techniques can be used to synthesize polysaccharides successfully. Nanotechnology and biotechnology have combined to create nanoparticles that are effective carriers for a wide range of medicines. Numerous researchers in the field of drug delivery are interested in polysaccharides because of their countless desirable properties, including biocompatibility, biodegradability, low toxicity, and amenability to modification. Gene delivery nanoparticles can be prepared from a variety of polysaccharides and their derivatives, with chitosan, hyaluronic acid, and dextran being popular choices. This manuscript provides an overview of the chemical and physical properties of polysaccharides that are of particular interest for use in biomedical applications and then discusses recent advances in the production of polysaccharide-based nanoparticles for gene delivery.
许多行业都使用多糖材料,如食品、食品包装、药物输送、组织工程、伤口敷料、废水处理和生物修复。由于其高效、低成本、无毒性、生物相容性和可生物降解性等优点,在这些领域得到了广泛应用。众所周知,有许多快速简便的方法可以成功地合成多糖。纳米技术和生物技术结合在一起,创造出了纳米粒子,它们是多种药物的有效载体。许多药物传递领域的研究人员对多糖感兴趣,因为它们具有无数理想的特性,包括生物相容性、生物可降解性、低毒性和易修饰性。基因传递纳米颗粒可以由多种多糖及其衍生物制备,壳聚糖、透明质酸和葡聚糖是常用的选择。本文概述了生物医学应用中特别感兴趣的多糖的化学和物理性质,然后讨论了用于基因传递的基于多糖的纳米颗粒的生产的最新进展。
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引用次数: 0
Facile synthesis of dysprosium oxide/bismuth oxide nanocomposite electrode materials with good electrocatalytic performance 简便合成了具有良好电催化性能的氧化镝/氧化铋纳米复合电极材料
Pub Date : 2023-08-31 DOI: 10.2174/2666145417666230831114021
Zizhan Sun, Xiaoyu Wang, Qianmin Cong, Chenxu Feng, Xu Zhang, Zhengyu Cai, Yong Zhang, Lizhai Pei
Benzoic acid is widely applied in the food field, including beverages as the antimicrobial preservative due to its strong inhabitation role to bacteria and yeasts. However, excessive intake of benzoic acid can easily cause abdominal pain and diarrhea and can even result in metabolic diseases. Hence, it is important to seek simple, accurate and sensitive strategies to detect low-trace benzoic acid.The aim of this study is to synthesize dysprosium oxide/bismuth oxide nanocomposites using dysprosium sulphate and sodium bismuthate as the raw materials and research the electrochemical sensing properties for the detection of benzoic acid.Dysprosium oxide/bismuth oxide nanocomposites were synthesized by a facile hydrothermal route. The dysprosium oxide/bismuth oxide nanocomposites were characterized by X-ray diffraction, electron microscopy, X-ray photoelectron spectroscopy and electrochemical impedance spectroscopy.The dysprosium oxide/bismuth oxide nanocomposites are composed of nearly circular-shaped particles with polycrystalline cubic Dy2O3 and triclinic Bi2O3 phases. The size of the nearly circular-shaped particles is about 50 to 200 nm. The electrons are easier to transfer by the dysprosium oxide/bismuth oxide nanocomposite-modified electrode than the bare electrode. A pair of quasi-reversible cyclic voltammetry (CV) peaks located at -0.155 V and -0.582 V exist in the CV curve of 0.1 M KCl buffer solution containing 2 mM benzoic acid. The nanocomposite-modified electrode shows a linear detection range and detection limit of 0.001-2 mM and 0.18 μM, respectively, for benzoic acid detection.The dysprosium oxide/bismuth oxide nanocomposite-modified electrode reveals superior electro-catalytic activity towards benzoic acid.
苯甲酸因其对细菌和酵母菌具有较强的居住作用,在食品领域,包括饮料中作为抗菌防腐剂得到了广泛的应用。然而,过量摄入苯甲酸容易引起腹痛和腹泻,甚至可能导致代谢性疾病。因此,寻找简单、准确、灵敏的低痕量苯甲酸检测方法具有重要意义。本研究以硫酸镝和铋酸钠为原料合成氧化镝/氧化铋纳米复合材料,并研究其检测苯甲酸的电化学传感性能。采用水热法合成了氧化镝/氧化铋纳米复合材料。采用x射线衍射、电子显微镜、x射线光电子能谱和电化学阻抗谱对氧化镝/氧化铋纳米复合材料进行了表征。氧化镝/氧化铋纳米复合材料由多晶立方Dy2O3和三斜Bi2O3相组成的近圆形颗粒组成。近圆形颗粒的大小约为50 ~ 200nm。氧化镝/氧化铋纳米复合修饰电极比裸电极更容易转移电子。在含2mm苯甲酸的0.1 M KCl缓冲溶液中,CV曲线上存在一对位于-0.155 V和-0.582 V的准可逆循环伏安峰。纳米复合材料修饰电极对苯甲酸的线性检测范围为0.001 ~ 2 mM,检出限为0.18 μM。氧化镝/氧化铋纳米复合修饰电极对苯甲酸具有优异的电催化活性。
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引用次数: 0
Antibacterial activity of Ag-graphene nanocomposites against Gram-Positive and Gram-negative bacteria 银-石墨烯纳米复合材料对革兰氏阳性和革兰氏阴性细菌的抑菌活性
Pub Date : 2023-08-25 DOI: 10.2174/2666145417666230825163555
P. Chamoli, Anuskha Kala, Dr Rashmi Verma, M. Meenu, L. Gambhir, K. Kar
Many pathogenic microorganisms, including bacteria, viruses, and fungi, which are common sources of disease and infection in both humans and animals, have a significant impact on human health. To combat these microorganisms, scientists and technicians are steadily attempting to develop novel and potent antimicrobial agents. Recently, graphene nanosheets (GNs) based nanocomposites (NCs) have shown promising potential as antibacterial activity against microorganisms. The present is an attempt to examine the antimicrobial effect of Silver (Ag)/GNs NCs against gram-positive (Bacillus thuringiensis, Staphylococcus aureus, and Enterococcus faecalis) and gram-negative (Salmonella typhi) bacteria.In this study, Ag/GNs NCs have been synthesized by the solvothermal method. X-ray diffraction (XRD), Raman spectroscopy, Fourier transform infrared spectroscopy (FTIR), UV-vis spectroscopy, field emission scanning electron microscopy (FESEM), and X-ray photoelectron spectroscopy have all been used to study the Ag/GNs NCs. The antibacterial activity of synthesized GO and Ag/GNs NCs was evaluated against microorganisms using the disk diffusion method.The elemental analysis of synthesized nanomaterial revealed that GO and Ag ions have been reduced by citric acid, and led to the successful formation of Ag/GNs NCs. The resultant NCs have been examined for their antibacterial activity against gram-positive (Bacillus thuringiensis, Staphylococcus aureus, and Enterococcus faecalis) and gram-negative (Salmonella typhi) bacteria. It was observed that Ag/GNs NCs markedly inhibit gram-positive and gram-negative bacteria.The prepared Ag/GNs NCs have the potential for long-term gram-positive and gram-negative bacteria-targeting antibacterial activities and grasp the ability in combating public health threats.
许多致病微生物,包括细菌、病毒和真菌,是人类和动物疾病和感染的常见来源,对人类健康产生重大影响。为了对抗这些微生物,科学家和技术人员正在稳步尝试开发新型有效的抗菌剂。近年来,基于石墨烯纳米片(GNs)的纳米复合材料(NCs)在抗菌微生物方面表现出了良好的潜力。本研究旨在研究银(Ag)/GNs NCs对革兰氏阳性(苏云金芽孢杆菌、金黄色葡萄球菌和粪肠球菌)和革兰氏阴性(伤寒沙门氏菌)细菌的抗菌作用。本研究采用溶剂热法合成了Ag/GNs纳米材料。利用x射线衍射(XRD)、拉曼光谱(Raman spectroscopy)、傅里叶变换红外光谱(FTIR)、紫外可见光谱(UV-vis spectroscopy)、场发射扫描电镜(FESEM)、x射线光电子能谱(photoelectron spectroscopy)等方法对Ag/GNs纳米材料进行了研究。采用圆盘扩散法对合成的氧化石墨烯和Ag/GNs纳米粒进行抑菌活性评价。对合成的纳米材料进行元素分析,发现氧化石墨烯和银离子被柠檬酸还原,并成功形成了Ag/GNs纳米结构。已检测所得nc对革兰氏阳性(苏云金芽孢杆菌、金黄色葡萄球菌和粪肠球菌)和革兰氏阴性(伤寒沙门氏菌)细菌的抑菌活性。Ag/GNs NCs对革兰氏阳性菌和革兰氏阴性菌均有明显抑制作用。制备的Ag/GNs NCs具有长期靶向革兰氏阳性和革兰氏阴性细菌的抗菌活性,具有应对公共卫生威胁的能力。
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引用次数: 0
Static and Dynamic Analysis of Automated Car Parking Tower Systems 自动泊车塔系统的静态和动态分析
Pub Date : 2023-08-23 DOI: 10.2174/2666145417666230823111030
M. Bajad, Yogini V. Deshpande
Our country has dramatically evolved over the decades, and now we have a large number of well-connected roads, public buildings and a rising number of automobiles. With the passage of time, the manual car parking system in commercial spaces has become a stumbling block and wastes time. As a result, it requires a solution that can address these issues. Automated car parking systems are the answer to these issues.In this study, the static and dynamic response spectrum approach was used to analyze G+13 storey automated car parking by using ETABS-2018 systemsThe storey displacement, storey stiffness, storey shear and overturning moment of steel and Reinforced cement concrete (RCC) automated car parking tower subjected to static and dynamic load for seismic zone III and zone IV in India have been determined.The RCC automated car parking tower was found to be not only stiffer but also lowered the displacement of construction
我们的国家在过去的几十年里发生了巨大的变化,现在我们有大量连接良好的道路,公共建筑和越来越多的汽车。随着时间的推移,人工停车系统在商业空间已经成为一个绊脚石,浪费时间。因此,它需要一个能够解决这些问题的解决方案。自动停车系统是解决这些问题的答案。本研究利用ETABS-2018系统,采用静动力响应谱方法对G+13层自动泊车进行了分析,确定了印度III区和IV区静动力荷载作用下钢和钢筋水泥混凝土(RCC)自动泊车塔的层位移、层刚度、层剪力和倾覆力矩。发现碾压混凝土自动停车塔不仅刚度更大,而且降低了结构位移
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引用次数: 0
Study on the Influence of Carbonation on the Microstructure of Cement-based Materials Based on BSE Technique 基于BSE技术的碳化对水泥基材料微观结构影响研究
Pub Date : 2023-08-23 DOI: 10.2174/2666145417666230823094321
Qizhen Shen, Gaoxiang Lou
The influence of carbonation on the interfacial transition zone (ITZ) microstructure of cement-based materials was significant. However, the width of ITZ is about tens of microns, and studying its micro-characteristics (such as porosity, hydration products, content of unhydrated cement, etc.) by macro test was difficult.Backscattered electron (BSE) imaging technology and gray scale analysis method were used to analyze the cement-based materials with water-binder (W/B) ratios of 0.53 and 0.35, respectively.BSE and gray scale analysis showed that in the ITZ, the porosity of 0.53P (Portland cement paste), 0.35P (Portland cement paste), 0.53F (fly ash), and 0.35F (fly ash) decreased by 24.1%, 28.9%, 49.5%, and 64.2% respectively, whereas the content of hydration products increases after carbonation, and the matrix also shows the same rule. At the same time, the smaller W/B ratio, the greater the porosity reduction, and the filling effect of carbonation on the specimens with supplementary cementitious material (SCM) was more significant than that of pure cement specimens.The porosity of the ITZ decreased after carbonation, however it remained higher than that of the matrix. Consequently, the ITZ remained a vulnerable zone with a greater diffusion rate of CO2 compared to the matrix even after carbonation.
碳化对水泥基材料界面过渡区微观结构的影响是显著的。然而,ITZ的宽度约为几十微米,通过宏观试验研究其微观特性(如孔隙率、水化产物、未水化水泥含量等)比较困难。采用背散射电子(BSE)成像技术和灰度分析方法对水胶比(W/B)分别为0.53和0.35的水泥基材料进行分析。BSE和灰阶分析表明,在ITZ中,0.53P(硅酸盐水泥浆体)、0.35P(硅酸盐水泥浆体)、0.53F(粉煤灰)和0.35F(粉煤灰)的孔隙率分别降低了24.1%、28.9%、49.5%和64.2%,而水化产物含量在碳化后增加,基质也表现出相同的规律。同时,W/B比越小,孔隙率降低越大,且添加了补充胶凝材料(SCM)的试件的碳化充填效果比纯水泥试件更为显著。碳化后孔隙率降低,但仍高于基体孔隙率。因此,即使在碳化后,与基体相比,ITZ仍然是CO2扩散速率较大的脆弱区。
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引用次数: 0
Characterization of ceria powders as a continuous search for new rare-earth based materials for radiation dosimetry 表征铈粉作为辐射剂量学新稀土基材料的不断探索
Pub Date : 2023-08-23 DOI: 10.2174/2666145417666230823091126
S. Santos, O. Rodrigues, L. Campos
Ceria (CeO2) belongs to rare-earth series and due to its profitable properties, presents a wide commercial use such as catalysis, energy, biological, biomedical, and pharmaceutical. The features of the starting materials in the form of free powders influence notably the processing, formation, as well as characteristics of the final structuresbodies obtained by colloidal processing. This study aims to characterize CeO2 powders. The results obtained are worthwhile data to advance toward new rare-earth based materials for radiation dosimetry.CeO2 powders were evaluated by the following techniques: PCS, SEM, XRD, FT-IR, EPR, IPC, and pycnometric density (ρ). The stability of particles in aqueous solvent was evaluated by zeta potential (ζ) determination.CeO2 powders exhibited cubic C-type form, Fm-3m space group, a mean particle size (d50) of 19.3nm, and a pycnometric density (ρ) of 7.01g.cm-3. Based on the results of zeta potential determination, CeO2 powders exhibited high stability at pH 6.4 with ζ-value of |34.0|mV.The evaluation of CeO2 powders was reported. The results presented and discussed in this study contribute to advance in the search of new rare-earth based materials for radiation dosimetry.
铈(CeO2)属于稀土系列,由于其有利的性质,在催化、能源、生物、生物医学和制药等领域具有广泛的商业用途。以游离粉末形式存在的起始材料的特征显著地影响通过胶体加工获得的最终结构体的加工、形成和特性。本研究旨在对CeO2粉末进行表征。所得结果为开发新型稀土基辐射剂量学材料提供了有价值的数据。采用PCS、SEM、XRD、FT-IR、EPR、IPC和密度(ρ)等技术对CeO2粉末进行了表征。采用ζ电位(ζ)测定法评价颗粒在水溶液中的稳定性。CeO2粉末呈立方c型,空间群为Fm-3m,平均粒径(d50)为19.3nm,比密度(ρ)为7.01g.cm-3。zeta电位测定结果表明,CeO2粉体在pH 6.4时表现出较高的稳定性,ζ值为34.0|mV。报道了对CeO2粉末的评价。本研究提出和讨论的结果有助于推动寻找新的稀土基辐射剂量学材料。
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引用次数: 0
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Current Materials Science
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