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Application of thermotolerant petroleum microbes at reservoir conditions for enhanced oil recovery 耐热石油微生物在储层条件下提高采收率的应用
Q2 ENERGY & FUELS Pub Date : 2023-06-01 DOI: 10.1016/j.petlm.2022.01.008
Emmanuel E. Okoro , Ewarezi A. Efajemue , Samuel E. Sanni , Oluwasanmi A. Olabode , Oyinkepreye D. Orodu , Temiloluwa Ojo

Primary oil recovery is the first stage of hydrocarbon production in which a reservoir uses its natural energy to force hydrocarbon to its wellbore. Secondary oil recovery comes to play when hydrocarbons can no longer be further produced by natural means. The purpose of secondary recovery is to maintain reservoir pressure so as to displace hydrocarbons toward the wellbore. Both primary and secondary recovery processes cannot displace more than 50% of the available hydrocarbons in a reservoir. The remaining hydrocarbons are further recovered through Tertiary/Enhanced Oil Recovery techniques. According to literature, microbial enhanced oil recovery has been identified as a tertiary method used to improve the efficiency of hydrocarbon production from reservoirs. Microbial enhanced oil recovery is a feasible reservoir technology, which has not been widely used in the oil and gas industry owing to the attainment of the requisite reservoir conditions such as temperature within which microbes can thrive. Literature has shown that thermotolerant microbes can withstand optimum temperatures of 50–90°C, while deep and ultra-deep hydrocarbon reservoir temperatures are often above 100°C. This study identifies some isolated thermotolerant microbes from a sandstone reservoir that can withstand temperatures as high as 110°C via conventional methods and molecular analysis. The identified thermotolerant petroleum microbes: Bacillus amyloliquefaciens (A) and Bacillus nealsonii (B) were used to enhance oil recovery from a reservoir. The results showed that the microbial species A and B at a confined pressure of 3.0 MPa and temperature of 27°C, gave 46.4% and 48.6% oil recoveries, respectively, which is comparably higher than the value (26.9%) obtained for the water flooded samples. At temperatures of 80, 90, 100, 110 and 120°C, the oil recovery results show that the recovery factor (55.2%–64.1%) of species B were higher compared to the range (46.7–57.5%) recorded for species A. At the onset of the core flooding experiments, there was an initial increment in oil recovery factor as the temperature increased from 80 to 110°C, whereas, it remained constant within 110–120°C. This trend coincides with the drop in the thermal resistance exhibited by the microbes when exposed to such conditions. The cumulative oil production from the commercial Eclipse simulation closely matched those of the experiment results, whereas, the slight difference can be attributed to the adjustment of the simulation input parameters. The experimental results show that species B can be used to enhance oil recovery at reservoir temperature conditions above 100°C.

一次采油是油气生产的第一个阶段,在这个阶段,油藏利用其自然能量迫使油气进入井筒。当碳氢化合物不能再通过自然方式进一步开采时,就需要进行二次采油。二次采油的目的是保持储层压力,以便将油气驱入井筒。一次和二次采油过程都不能取代油藏中50%以上的可用碳氢化合物。剩余的油气通过三次采油技术进一步回收。根据文献,微生物提高采收率已被确定为提高储层油气生产效率的第三种方法。微生物提高采收率是一种可行的油藏技术,但由于需要达到微生物可以繁殖的必要油藏条件(如温度),该技术尚未在油气工业中得到广泛应用。文献表明,耐热微生物可以承受50-90°C的最佳温度,而深层和超深层油气储层温度通常超过100°C。本研究通过常规方法和分子分析,从砂岩储层中分离出一些耐热微生物,这些微生物可以承受高达110°C的高温。利用鉴定出的耐高温石油微生物:解淀粉芽孢杆菌(A)和尼氏芽孢杆菌(B)来提高油藏的采收率。结果表明,在承压压力为3.0 MPa、温度为27℃条件下,A、B两种微生物的采收率分别为46.4%和48.6%,明显高于水淹样品的26.9%。在80、90、100、110和120℃温度下,采收率结果表明,B种的采收率(55.2% ~ 64.1%)高于a种的采收率(46.7 ~ 57.5%)。岩心驱油实验开始时,温度从80℃升高到110℃,采收率有一个初始增量,在110℃~ 120℃范围内基本保持不变。这种趋势与微生物暴露在这种条件下所表现出的热阻下降相吻合。商业Eclipse模拟的累积产油量与实验结果非常接近,而模拟输入参数的调整可能导致了细微的差异。实验结果表明,在100℃以上的储层温度条件下,B种可以提高采收率。
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引用次数: 3
Experimental study on the sandstone abrasiveness via mineral composition and microstructure analysis 通过矿物成分和微观结构分析对砂岩磨蚀性的实验研究
IF 4.2 Q2 ENERGY & FUELS Pub Date : 2023-05-11 DOI: 10.1016/j.petlm.2023.05.002

Rock abrasiveness is an important factor affecting the tool's lifetime and efficiency in breaking a rock. Characterizing rock abrasiveness helps in the design, optimization, and mean-life prediction of tools. X-ray diffraction, cast thin section analysis, and CERCHAR abrasiveness tests were performed on 18 different sandstones to characterize rock abrasiveness and explore new methods for characterization. The relationship between the mineral composition and microstructure of sandstone and abrasiveness was investigated. The results show that different structural maturities have varying effects on abrasiveness. In addition, the higher the structural maturity, the more the abrasiveness. Furthermore, in sandstones of the same structural maturity, the abrasiveness increases with equivalent quartz content (EQC). The texture coefficient (TC) and CERCHAR abrasiveness index (CAI) of sandstones with the same structural maturity showed a good linear relationship. Moreover, the correlation coefficients considering the combined parameters are above 0.85. Therefore, obtaining the microstructure and mineral composition of sandstone can effectively characterize rock abrasiveness. It also provides a new method for predicting the abrasiveness of the rock in the well.

岩石磨蚀性是影响工具使用寿命和破岩效率的重要因素。表征岩石磨蚀性有助于工具的设计、优化和平均寿命预测。我们对 18 种不同的砂岩进行了 X 射线衍射、铸造薄片分析和 CERCHAR 磨蚀性测试,以确定岩石磨蚀性的特征,并探索新的表征方法。研究了砂岩的矿物成分和微观结构与磨蚀性之间的关系。结果表明,不同的结构成熟度对磨蚀性有不同的影响。此外,结构成熟度越高,磨蚀性越强。此外,在结构成熟度相同的砂岩中,磨蚀性随等效石英含量(EQC)的增加而增加。结构成熟度相同的砂岩的质地系数(TC)和 CERCHAR 耐磨性指数(CAI)呈良好的线性关系。此外,综合参数的相关系数均在 0.85 以上。因此,获取砂岩的微观结构和矿物成分可以有效地表征岩石的磨蚀性。这也为预测井中岩石的磨蚀性提供了一种新方法。
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引用次数: 0
Axial-torsional nonlinear vibration of bottom hole assembly in the air drilling technology 气钻技术中底孔组件的轴向-扭转非线性振动
IF 4.2 Q2 ENERGY & FUELS Pub Date : 2023-05-10 DOI: 10.1016/j.petlm.2023.05.001

The safety and efficiency of drilling engineering are greatly impeded by destructive vibrations of drill string in air drilling, such as stick-slip, bit-bounce and their coupled vibrations. To avoid or suppress these vibrations improving the stability of drilling operations, revealing the occurrence mechanisms of abovementioned harmful vibrations are indispensable by investigating dynamics characteristics of drill string system. In this paper, an axial-torsional coupled dynamics model that can capture the motion behaviors of bottom hole assembly (BHA) is established adopting the lumped parameter method. Subsequently, a rate of penetration (ROP) model appropriating for air drilling is obtained firstly by linear fitting means. Meanwhile, a novel discontinuous support model is established to describe the bit-formation interactions. Then, BHA dynamics are discussed using numerical simulations under different vibration scenarios: normal operation; stick-slip; bit-bounce; bit-bounce and stick-slip combination. Subsequently, in two drilling modes: the continuous and intermittent drilling, the vibration mitigation strategies and dynamics sensibility study of BHA are carried out based on the parametric analysis. The results show that increasing torsional stiffness of drill-pipes, appropriately adjusting rotation speed of top driven system and dynamic weight on bit (WOB) are deemed as an effective strategy suppressing or eliminating stick-slip and bit-bounce vibrations of BHA. Suggest that the rotation speed of top driven system and dynamic WOB are 5 rad/s and 3.5 kN, respectively. Finally, the constructed probability maps allow to driller to choose reasonable mechanical parameters, thereby realizing smooth drilling operation in the air drilling.

空气钻井中钻杆的破坏性振动,如粘滑、钻头弹跳及其耦合振动,极大地影响了钻井工程的安全和效率。为了避免或抑制这些振动,提高钻井作业的稳定性,必须通过研究钻杆系统的动力学特性来揭示上述有害振动的发生机理。本文采用集合参数法建立了一个能捕捉底孔组件(BHA)运动行为的轴向-扭转耦合动力学模型。随后,首先通过线性拟合方法得到了适合空气钻井的钻进速度(ROP)模型。同时,建立了一个新颖的非连续支撑模型来描述钻头与变形之间的相互作用。然后,通过数值模拟讨论了不同振动情况下的 BHA 动态:正常工作;粘滑;钻头反弹;钻头反弹和粘滑组合。随后,在连续钻进和间歇钻进两种钻进模式下,基于参数分析对 BHA 的振动缓解策略和动力学敏感性进行了研究。结果表明,增加钻杆扭转刚度、适当调整顶部驱动系统转速和动态钻头重量(WOB)被认为是抑制或消除 BHA 粘滑和钻头反弹振动的有效策略。建议顶部驱动系统的转速和动态 WOB 分别为 5 rad/s 和 3.5 kN。最后,通过所构建的概率图,钻井人员可以选择合理的机械参数,从而在空气钻井中实现平稳的钻进操作。
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引用次数: 0
The rock cutting simulation of heterogeneous granite using FDEM method 非均质花岗岩的FDEM切割模拟
Q2 ENERGY & FUELS Pub Date : 2023-04-01 DOI: 10.1016/j.petlm.2023.04.002
Weiji Liu, Hongxing Deng, X. Zhu, Yanxin Lv, Yunxu Luo
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引用次数: 0
Experimental study on sand production and coupling response of silty hydrate reservoir with different contents of fine clay during depressurization 不同细粘土含量粉质水合物储层减压产砂及耦合响应试验研究
Q2 ENERGY & FUELS Pub Date : 2023-03-01 DOI: 10.1016/j.petlm.2021.11.008
Xiangyu Fang , Dianheng Yang , Fulong Ning , Linjie Wang , Zhichao Liu , Yanjiang Yu , Wenwei Xie , Hongfeng Lu , Yanlong Li , Meng Xu

To further understand the characteristics of clay and sand production (hereafter collectively referred to as sand production) and to provide optimization designs of sand control schemes are critical for gas production from clayey silt natural gas hydrate reservoirs in the South China Sea. Thus, gas-water-sand production behavoirs and coupling reservoir subsidence characteristics before, during, and after hydrate dissociation of the clayey silt hydrate reservoirs with different clay contents (5%, 10%, 15%, 20%, 25%, and 30%) have been studied through a self-developed experimental system. The results show that with the increase of clay content, the total mass of sand production first increases and then decreases, and it reaches maximum when the clayey content is 20%. The sand production is the lowest before hydrate dissociation and increases significantly during hydrate dissociation, which mainly occurs in the high-speed gas and water production stage at the beginning of hydrate dissociation. After hydrate dissociation, the sand production decreases significantly. During the whole depressurization process, the clay and free sand particles generally move to the sand outlet due to the fluid driving force and overlying stress extrusion. However, for conditions of high clay contents, those particles fail to pass through the sand control screen and gradually accumulate and block the screen by forming a mud cake, which greatly reduce the permeability of the screen and limite sand production as well as gas and water production. Our research lays a foundation for sand production prediction and sand control scheme selection during gas recovery from clayey silty hydrate reservoirs that greatly need to consider a balance between sand control and gas productivity.

为了进一步了解粘土和出砂(以下统称为出砂)的特征,并提供防砂方案的优化设计,对于从南海粘性淤泥质天然气水合物储层中开采天然气至关重要。因此,通过自行开发的实验系统,研究了不同粘土含量(5%、10%、15%、20%、25%和30%)的粘质粉土水合物储层在水合物分解前后的气水砂生产行为和耦合储层沉降特征。结果表明,随着粘土含量的增加,出砂总质量先增大后减小,当粘土含量为20%时,出砂总量达到最大值。水合物解离前出砂量最低,在水合物解离过程中出砂量显著增加,主要发生在水合物解离初期的高速产气和产水阶段。水合物分解后,出砂量显著下降。在整个降压过程中,由于流体驱动力和上覆应力挤压,粘土和自由砂粒通常会向出砂口移动。然而,在粘土含量高的条件下,这些颗粒无法通过防砂筛管,并逐渐积聚并堵塞筛管,形成泥饼,这大大降低了筛管的渗透率,限制了出砂以及产气和产水。我们的研究为粘土质粉质水合物油藏采气过程中的出砂预测和防砂方案选择奠定了基础,这些油藏需要考虑防砂和产气之间的平衡。
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引用次数: 3
Development and performance evaluation of a high temperature resistant, internal rigid, and external flexible plugging agent for water-based drilling fluids 耐高温、内刚性、外柔性水基钻井液封堵剂的研制与性能评价
Q2 ENERGY & FUELS Pub Date : 2023-03-01 DOI: 10.1016/j.petlm.2022.07.004
Zhe Xu , Jinsheng Sun , Li Li , Kaihe Lv , Jingping Liu , Zhiwen Dai , Xianfa Zhang , Zonglun Wang

During the drilling process for oil and gas production, a larger number of drilling fluids invade the formation, causing severe formation damage and wellbore collapsing, which seriously hinders the efficient production of deep oil and gas. Although several plugging agents have been developed for efficient fracture sealing in recent years, the development of high-performance plugging agents with self-adaptive ability and high-temperature resistance remain a challenge. Herein, we report the synthesis of an internal rigid and external flexible plugging agent PANS by reversed-phase emulsion polymerization with nano-silica as the rigid core and poly (acrylamide-co-N-vinylpyrrolidone) as a flexible shell. The plugging agent has a median particle size of 10.5 μm and can self-adapt to seal the microfractures and fractures in the formation, leading to an effective reduction in the filtration loss of bentonite water-based drilling fluid under both low temperature and low pressure (LTLP) and high temperature and high pressure (HTHP) conditions. In addition, compared with the neat nano-silica (500 nm), the sealing efficiency of PANS toward 100–120 mesh sand bed was increased by 71.4% after hot rolling at 180°C.

在油气开采的钻井过程中,大量钻井液侵入地层,造成严重的地层破坏和井筒坍塌,严重阻碍了深层油气的高效开采。尽管近年来已经开发了几种用于高效裂缝密封的堵剂,但开发具有自适应能力和耐高温性能的高性能堵剂仍然是一个挑战。本文报道了以纳米二氧化硅为刚性核,聚(丙烯酰胺-co-N-乙烯基吡咯烷酮)为柔性壳,通过反相乳液聚合合成内刚性和外柔性堵剂PANS。该堵剂的中粒径为10.5μm,可自适应封堵地层中的微裂缝和裂缝,有效降低膨润土水基钻井液在低温低压和高温高压条件下的过滤损失。此外,与纯纳米二氧化硅(500 nm)相比,在180°C下热轧后,PANS对100–120目砂床的密封效率提高了71.4%。
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引用次数: 5
Production optimization under waterflooding with long short-term memory and metaheuristic algorithm 基于长短期记忆和元启发式算法的水驱生产优化
Q2 ENERGY & FUELS Pub Date : 2023-03-01 DOI: 10.1016/j.petlm.2021.12.008
Cuthbert Shang Wui Ng , Ashkan Jahanbani Ghahfarokhi , Menad Nait Amar

In petroleum domain, optimizing hydrocarbon production is essential because it does not only ensure the economic prospects of the petroleum companies, but also fulfills the increasing global demand of energy. However, applying numerical reservoir simulation (NRS) to optimize production can induce high computational footprint. Proxy models are suggested to alleviate this challenge because they are computationally less demanding and able to yield reasonably accurate results. In this paper, we demonstrated how a machine learning technique, namely long short-term memory (LSTM), was applied to develop proxies of a 3D reservoir model. Sampling techniques were employed to create numerous simulation cases which served as the training database to establish the proxies. Upon blind validating the trained proxies, we coupled these proxies with particle swarm optimization to conduct production optimization. Both training and blind validation results illustrated that the proxies had been excellently developed with coefficient of determination, R2 of 0.99. We also compared the optimization results produced by NRS and the proxies. The comparison recorded a good level of accuracy that was within 3% error. The proxies were also computationally 3 times faster than NRS. Hence, the proxies have served their practical purposes in this study.

在石油领域,优化碳氢化合物生产至关重要,因为它不仅确保了石油公司的经济前景,而且满足了全球日益增长的能源需求。然而,应用油藏数值模拟(NRS)来优化生产可能会导致高计算足迹。建议使用代理模型来缓解这一挑战,因为它们在计算上要求较低,并且能够产生相当准确的结果。在本文中,我们演示了如何将机器学习技术,即长短期记忆(LSTM)应用于开发三维油藏模型的代理。采用采样技术创建了大量模拟案例,这些案例作为建立代理的训练数据库。在对训练的代理进行盲验证后,我们将这些代理与粒子群优化相结合,以进行生产优化。训练和盲验证结果都表明,代理已经得到了很好的开发,确定系数R2为0.99。我们还比较了NRS和代理产生的优化结果。比较记录了良好的准确度,误差在3%以内。代理在计算上也比NRS快3倍。因此,代理人在本研究中达到了其实际目的。
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引用次数: 11
Sealing performance and mechanical response of mud pump piston 泥浆泵柱塞的密封性能及力学响应
Q2 ENERGY & FUELS Pub Date : 2023-03-01 DOI: 10.1016/j.petlm.2021.12.004
Jie Zhang , Wenjie Jiang , Pai Zhu , Ting Zheng

In order to explore the effect of piston cup structure on its sealing characteristics and mechanical properties, a numerical simulation model of the piston cup in the BW-160 mud pump was established. Effects of work load, friction coefficient and cup structure parameters on the sealing and mechanical properties of the piston were discussed under mud discharge condition. The results show that stress concentration on the root and lips of the cup is becoming more and more obvious with the working load increases. The average contact pressure increases with the friction coefficient increases, but an excessive friction coefficient accelerate the wear of the cup and the heat generation. Effect of the piston lip interference and thickness on the sealing performance of the cup is greater than that of the inner wall width. The piston with groove structure can effectively improve the sealing performance of the piston. The mechanical properties of triangular groove cup are better than that of semicircular and trapezoidal groove cup.

为了探讨活塞杯结构对其密封特性和力学性能的影响,建立了BW-160泥浆泵活塞杯的数值模拟模型。讨论了在排泥条件下,工作载荷、摩擦系数和杯形结构参数对活塞密封性能和力学性能的影响。结果表明,随着工作载荷的增加,杯根部和唇部的应力集中越来越明显。平均接触压力随着摩擦系数的增加而增加,但过大的摩擦系数会加速杯的磨损和热量的产生。活塞唇过盈量和厚度对杯密封性能的影响大于内壁宽度的影响。采用凹槽结构的活塞可以有效地提高活塞的密封性能。三角槽杯的力学性能优于半圆形和梯形槽杯。
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引用次数: 1
Anti-drilling ability of Ziliujing conglomerate formation in Western Sichuan Basin of China 川西地区自流井砾岩组抗钻能力
Q2 ENERGY & FUELS Pub Date : 2023-03-01 DOI: 10.1016/j.petlm.2022.03.007
Nian Peng , Tianshou Ma , Gongsheng Zhu , Qiang Su

The conglomerate rock is usually featured by strong heterogeneity, high abrasiveness, and poor drillability due to its complex composition and texture, which brought a huge challenge for drilling efficiency. In order to guide the drill bit selection and high-efficiency drilling, the physical, mechanical, and drillability characteristics were investigated for conglomerate rock that collected from the lower Jurassic Ziliujing formation in the Western Sichuan Basin of China. The mineral composition, SEM micro-structure, P- and S-wave velocities, uniaxial and triaxial compressive testing, drillability, abrasiveness were systematically tested and analyzed. The mechanical properties and anti-drilling ability of Ziliujing formation were proposed for a typical deep well of S-07, and the distribution characteristics were analyzed. The results indicated that the Ziliujing rock is rich-in quartz and clay minerals, due to the co-existing of strong quartz gravel and weak argillaceous cement, the Ziliujing rock shows strong heterogeneity. The relationships are roughly linear among UCS, drillability, and grinding weight loss with P-wave velocity. The Young's modulus, UCS, internal friction angle, drillability, and abrasiveness meet the Weibull distribution pattern, while only the Poisson's ratio meets the Kernel Smooth distribution pattern. Logging interpretation results reval that the Ziliujing formation has the Young's modulus of 38.61 ± 17.08 GPa, the Poisson's ratio of 0.327 ± 0.006, the internal friction angle of 49.21 ± 11.00°, the drillability of 8.04 ± 1.54, and the abrasiveness grade of 4.32 ± 1.94. The mechanical properties and anti-drilling ability of logging interpretation are in good agreement with the experimental data. The Ziliujing formation is a kind of hard rock with strong heterogeneity, high strength, poor drillability, and medium abrasiveness. Based on the characteristics of Ziliujing formations, the SV516TAUL PDC bit with non-planar cutters was selected for the field application due to the good abrasion resistance, impact resistance, self-sharpening and thermal stability of the non-planar cutters. The field application shows that the average ROP of the new type drill bit in Ziliujing formation is 2.93 m/h, and the average footage is 225.9 m. Comparing with the traditional PDC bit, the ROP of the new drill bit with non-planar cutters has increased by 67.4%, and the footage has increased by 92.1%. The results of this paper can be utilized to guide the drill bit selection and high-efficiency drilling in conglomerate formation.

砾岩由于其成分和质地复杂,通常具有非均质性强、耐磨性高、可钻性差的特点,这给钻井效率带来了巨大挑战。为了指导钻头的选择和高效钻井,研究了四川盆地西部侏罗系自流井组下部砾岩的物理、力学和可钻性特征。系统地测试和分析了矿石成分、SEM微观结构、P波和S波速度、单轴和三轴抗压试验、可钻性和耐磨性。针对S-07某典型深井,提出了自流井组的力学性能和抗钻能力,并对其分布特征进行了分析。结果表明,自流井岩石富含石英和粘土矿物,由于强石英砾石和弱泥质胶结物的共同存在,自流井岩石表现出强烈的非均质性。UCS、可钻性和研磨重量损失与P波速度之间的关系大致呈线性。杨氏模量、无侧限抗压强度、内摩擦角、可钻性和耐磨性符合威布尔分布模式,而只有泊松比符合核光滑分布模式。测井解释结果表明,自流井组的杨氏模量为38.61±17.08GPa,泊松比为0.327±0.006,内摩擦角为49.21±11.00°,可钻性为8.04±1.54,耐磨性等级为4.32±1.94。测井解释的力学性能和抗钻能力与实验数据吻合较好。自流井组是一种非均质性强、强度高、可钻性差、磨蚀性中等的坚硬岩石。根据自流井组的特点,非平面刀具具有良好的耐磨性、抗冲击性、自锐性和热稳定性,选用SV516TAUL非平面刀具PDC钻头进行现场应用。现场应用表明,新型钻头在自流井组的平均钻速为2.93m/h,平均进尺为225.9m。与传统PDC钻头相比,非平面刀具新型钻头的钻速提高了67.4%,研究结果可用于指导砾岩地层钻头的选择和高效钻井。
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引用次数: 4
Super gas wet and gas wet rock surface: State of the art evaluation through contact angle analysis 超气湿和气湿岩石表面:通过接触角分析进行的最新评估
Q2 ENERGY & FUELS Pub Date : 2023-03-01 DOI: 10.1016/j.petlm.2021.09.004
Mohammad Azadi Tabar , Abolfazl Dehghan Monfared , Flor Shayegh , Farzad Barzegar , Mohammad Hossein Ghazanfari

Recently, super gas wet and gas wet surfaces have been extensively attended in petroleum industry, as supported by the increasing number of publications in the last decade related to wettability alteration in gas condensate reservoirs. In many cases, contact angle measurement has been employed to assess the wettability alteration. Even though contact angle measurement seems to be a straightforward approach, there exist many misuses of this technique and consequently misinterpretation of the corresponding results. In this regard, a critical inspection of the most recent updated concepts and the intervening parameters in the contact angle based wettability evaluation of liquid-solid-gas systems could aid to provide some remediation to alleviate this problem. To this end, this work presents a survey on the accurate terms and rigorous protocols based on the community of surface science and chemistry. As a preliminary step, advancing, receding, static, and the most stable contact angle terminology are defined. The study is followed by the definition of the contact angle hysteresis effect. The application of surface free energy in the selection of the best gas wet agent is then analyzed. Afterward, the impact of the size-dependent behavior of drop on contact angle is discussed. Finally, a sessile drop experiment is explained to achieve the defined parameters. For future contributions to petroleum industry journals, like this journal, this work could offer an easy use of the conceptual framework for analyzing the results and comparative evaluations in chemical wettability modifier agents.

最近,超气湿和气湿表面在石油工业中得到了广泛的关注,在过去十年中,越来越多的出版物与凝析油储层的润湿性变化有关。在许多情况下,接触角测量已被用于评估润湿性变化。尽管接触角测量似乎是一种简单的方法,但该技术存在许多误用,从而导致对相应结果的误解。在这方面,在基于接触角的液固气系统润湿性评估中,对最新更新的概念和干预参数进行关键检查,可能有助于提供一些补救措施来缓解这一问题。为此,这项工作基于表面科学和化学社区,对准确的术语和严格的协议进行了调查。作为初步步骤,定义了前进、后退、静态和最稳定的接触角术语。接着对接触角磁滞效应进行了定义。分析了表面自由能在选择最佳气体润湿剂中的应用。然后,讨论了液滴尺寸依赖行为对接触角的影响。最后,对实现所定义参数的固着跌落实验进行了解释。对于未来对石油工业期刊(如本期刊)的贡献,这项工作可以为分析化学润湿性改性剂的结果和比较评估提供一个简单的概念框架。
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引用次数: 1
期刊
Petroleum
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