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Sm-Co ALLOYS COERCIVITY PREDICTION USING STACKING HETEROGENEOUS ENSEMBLE MODEL 用叠加非均匀镶嵌模型预测Sm-Co合金矫顽力
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-07 DOI: 10.36547/ams.27.4.1173
A. Trostianchyn, Z. Duriagina, I. Izonin, R. Tkachenko, V. Kulyk, O. Pavliuk
The use of machine learning tools in modern materials science can significantly reduce the duration and cost of developing new materials and improving the properties of existing ones. This is especially true in studying expensive and strategic importance materials like alloys of rare earth metals, which are used to manufacture high-energy permanent magnets. At the same time, single machine learning algorithms do not always provide the accuracy required to solve a particular applied task. Therefore, the current paper aimed to develop an ensemble model for predicting the magnetic properties of Sm-Co system alloys with high accuracy. Based on literature data, we have collected the dataset of the relationship between phase composition, sample state, crystallographic orientation, microstructure, and magnetic properties. We have compared different machine learning algorithms. A stacking ensemble model was designed based on high-precision machine learning algorithms: Neural Networks, AdaBoost, Gradient Boosting, and Random Forest algorithm. The proposed ensemble scheme showed a significant increase in the accuracy for predicting the magnetic properties of Sm-Co alloys on the example of coercivity.
在现代材料科学中使用机器学习工具可以显著减少开发新材料的时间和成本,并改善现有材料的性能。在研究昂贵且具有战略重要性的材料时尤其如此,比如用于制造高能永磁体的稀土金属合金。同时,单个机器学习算法并不总是提供解决特定应用任务所需的准确性。因此,本文旨在建立一种高精度预测Sm-Co系合金磁性能的系综模型。在文献资料的基础上,我们收集了相组成、样品状态、晶体取向、微观结构和磁性能之间关系的数据集。我们比较了不同的机器学习算法。基于高精度机器学习算法:神经网络、AdaBoost、梯度增强和随机森林算法,设计了一个叠加集成模型。以矫顽力为例,所提出的系综方案在预测Sm-Co合金磁性能精度上有显著提高。
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引用次数: 4
The effect of eggshell as a reinforcement on the mechanical and Corrosion properties of Mg-Zn-Mn matrix composite 蛋壳增强剂对Mg-Zn-Mn基复合材料力学性能和腐蚀性能的影响
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-07 DOI: 10.36547/ams.27.4.1088
Hasan A. Fattah, M. Gouda, S. Salman, A. Elsayed
Magnesium is a promising lightweight metal required in many industries such as automobile, aerospace, electronics, etc. It is also a biodegradable material, which eliminates the secondary removal procedure of the implant. Furthermore, its mechanical properties are similar to the mechanical properties of human bone.  In this research, eggshells were used as an environmentally friendly composite reinforcement material in the Mg-2.5Zn-1Mn matrix. Composites were prepared using the powder metallurgy route.  The effect of eggshells on the morphology, mechanical, and corrosion behaviour of Mg-2.5Zn-1Mn alloy was investigated. The results revealed an enhancement in grain refining ability and mechanical properties of Mg-2.5Zn-1Mn with eggshell additives. The corrosion behaviour improved at a higher percentage of eggshells (10%).
镁是一种很有前途的轻质金属,在汽车、航空航天、电子等许多行业都需要。它也是一种可生物降解的材料,可以消除植入物的二次移除过程。此外,它的力学性能与人体骨骼的力学性能相似。在本研究中,蛋壳被用作Mg-2.5Zn-1Mn基体中的环保复合增强材料。采用粉末冶金方法制备了复合材料。研究了蛋壳对Mg-2.5Zn-1Mn合金形态、力学性能和腐蚀行为的影响。结果表明,添加蛋壳添加剂可提高Mg-2.5Zn-1Mn的晶粒细化能力和力学性能。蛋壳百分比越高(10%),腐蚀行为就越好。
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引用次数: 2
PRODUCTION OF IRON ORE PELLETS BY UTILIZATION OF SUNFLOWER HUSKS 利用向日葵壳生产铁矿石球团
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-07 DOI: 10.36547/ams.27.4.1052
A. Koveria, L. Kieush, M. Boyko, Maksym Yaholnyk, Natalia Poliakova
Steel production is the most dynamic industry and one of the key sectors for the development of the global economy. The growing production of iron ore increases the need for its beneficiation and granulating for subsequent use in the production of iron and steel. As a result, the number of CO2 emissions and harmful substances increases, which negatively affects both society and the environment. It is important to study the use of biomass for the production of iron ore pellets. Lignocellulosic biomass is a renewable and sustainable source of heat and energy that can mitigate climate change. The efficiency of using sunflower husks on the combined machine “straight grate - rotary kiln - annular cooler” to partially replace natural gas in the production of iron ore pellets has been studied. The influences of alternative fuel use on technological indicators of the process and quality of iron ore pellets have been analyzed. It was found that the combustion of sunflower husks generates enough heat to obtain iron ore pellets with good strength. The main indicators of the quality of iron ore pellets remain at the same level as the iron ore pellet quality when using natural gas.
钢铁生产是最具活力的行业,也是全球经济发展的关键部门之一。铁矿石产量的不断增长增加了对其选矿和制粒的需求,以供随后用于钢铁生产。因此,二氧化碳排放量和有害物质的数量增加,对社会和环境都产生了负面影响。研究生物质在铁矿石球团生产中的应用具有重要意义。木质纤维素生物质是一种可再生和可持续的热能和能源,可以缓解气候变化。研究了葵花籽在“直篦-回转窑-环冷机”组合机上部分替代天然气生产铁矿石球团的效果。分析了替代燃料的使用对球团生产工艺指标和质量的影响。研究发现,向日葵皮燃烧产生的热量足以获得强度良好的铁矿石球团。使用天然气时,铁矿石球团质量的主要指标与铁矿石球团的质量保持在同一水平。
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引用次数: 3
FORMING PROCESS SIMULATION OF BIMETALLIC BILLET BY EXTRUSION FOR REW METHOD REW法挤压双金属坯料成形过程模拟
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-07 DOI: 10.36547/ams.27.4.1254
A. Schrek, A. Brusilová, P. Sejč, B. Vanko
The bimetallic joining elements were designed for lap joints of thin metallic (Fe-Fe, Fe-Al) as well as metallic – nonmetallic (Fe-PMMA, Al-PMMA) sheets by Resistance Element Welding (REW). The Cu tubes with an outer diameter of 4 mm, wall thickness of 0.5 mm, and a length of 11 mm filled with a solder Sn60Pb40 were used for the bimetallic joining elements producing. The required shape of joining elements is obtained by cold forming. Simulation by ANSYS software was chosen for the optimization of the forming process and geometry of functional parts of the forming tool allowing to use only one extrusion forming operation. The simulation results are stresses, strains, and modification of cross-section geometry of elements for the three proposed forming modes. The geometry of functional parts of the forming tool was compared with the results of cross-section macroanalysis of joining elements.
双金属连接元件是为薄金属(Fe-Fe,Fe-Al)以及金属-非金属(Fe-PMMA,Al-PMMA)片的搭接设计的,采用电阻元件焊接(REW)。将外径为4mm、壁厚为0.5mm、长度为11mm的填充有焊料Sn60Pb40的铜管用于生产双金属连接元件。连接元件的所需形状是通过冷成型获得的。选择ANSYS软件进行模拟,以优化成形过程和成形工具功能部件的几何形状,从而只允许使用一次挤压成形操作。模拟结果是三种提出的成形模式的应力、应变和元件截面几何形状的修改。将成形工具功能部件的几何形状与连接元件的横截面宏观分析结果进行了比较。
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引用次数: 1
The Effect of Different Pre-Surface Finishing Method on the Aluminium Anodization of the 6XXX Series Alloy 不同表面前处理方法对6XXX系列合金铝阳极氧化的影响
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-12-07 DOI: 10.36547/ams.27.4.1109
Merve Özcan, Bilge Tunca, Ipek Biltaş, T. Tuken
In this study, the effect of different pre-surface finishing method on the aluminium anodization was investigated for AA 6063 alloy. Within the scope of pre-surface finishing method which is acidic solution concentrations and process time were determined. Acidic solution was determined by using hydrofluoric acid (HF) and nitric acid (HNO3). Also Gresoff LIM-5 LV chemical was used with different concentrations and process time for degreasing process. The etching effect of acidic solution on aluminium samples was investigated. The optimal etching behaviour was obtained with 1.0% concentration of HF and 3.2% concentration of HNO3 at 10 minutes process time. Also optimal surface properties were observed with 1.0% concentration of Gresoff LIM-5 LV at 12 minutes process time. Then anodic oxidation was performed by using 180 g / L sulfuric acid (H2SO4) and 18 volt (V). Surface morphology of the final aluminium profiles were examined with SEM analysis, Roughness, Gloss and Thickness tests.
研究了不同表面预处理方法对AA 6063铝合金阳极氧化性能的影响。在预表面处理方法的范围内,确定了酸性溶液的浓度和处理时间。酸性溶液用氢氟酸(HF)和硝酸(HNO3)测定。并采用Gresoff LIM-5 LV化学剂,在不同浓度和工艺时间下进行脱脂处理。研究了酸性溶液对铝样品的腐蚀作用。当HF浓度为1.0%,HNO3浓度为3.2%,工艺时间为10 min时,刻蚀效果最佳。当Gresoff LIM-5 LV浓度为1.0%时,处理时间为12分钟,表面性能最佳。然后用180 g / L硫酸(H2SO4)和18伏(V)进行阳极氧化。通过SEM分析、粗糙度、光泽和厚度测试来检测最终铝型材的表面形貌。
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引用次数: 1
EFFECT OF COOLING RATE ON MICROSTRUCTURE AND HARDNESS IN GRAY CAST IRON CASTING PROCESS 灰口铸铁冷却速度对组织和硬度的影响
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-09-13 DOI: 10.36547/ams.27.3.996
A. Yulianto, R. Soenoko, W. Suprapto, A. Sonief
This study aims to investigate the thermal conditions of the molds, changes in microstructure and hardness of casting products using sand mold and permanent mold. The use of sand mold and permanent mold results in different cooling rates. Thermal analysis was performed using a thermocouple to obtain a temperature versus time curve. Metallographic observations were carried out using a Scanning Electron Microscope equipped with Energy-Dispersive X-ray Spectroscopy. The Vickers hardness test was carried out in three areas with different thicknesses. The results showed a constant temperature at 691 oC where the eutectoid phase reaction occurred. Testing with sand mold showed that cast iron with flake graphite was finer and spreader than graphite in cast iron produced by permanent mold. Meanwhile, gray cast iron from a casting process with a permanent mold has a higher hardness than gray cast iron from a casting process using a sand mold.
本研究旨在研究砂型和永久型铸造模具的热条件、铸件微观结构和硬度的变化。砂模和永久模的使用导致不同的冷却速率。使用热电偶进行热分析以获得温度与时间的关系曲线。使用配备有能量分散X射线光谱的扫描电子显微镜进行金相观察。维氏硬度试验在三个不同厚度的区域进行。结果表明,在691℃的恒定温度下发生共析相反应。砂型试验表明,片状石墨铸铁比永久模生产的铸铁更细、更分散。同时,使用永久模具的铸造工艺产生的灰铸铁比使用砂型的铸造工艺的灰铸铁具有更高的硬度。
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引用次数: 0
IMPACT OF COLD PLASTIC DEFORMATION AND THERMAL POST-TREATMENT ON THE PHYSICAL PROPERTIES OF COPPER BASED ALLOYS Al-BRONZE AND α-BRASS 冷塑性变形和热后处理对铜基合金Al、青铜和α-黄铜物理性能的影响
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-09-13 DOI: 10.36547/ams.27.3.951
Samiul Kaiser, M. S. Kaiser
The copper based alloys Al-bronze and α-brass containing each of 10wt% aluminum and zinc were prepared by casting. Afterwards, the specimens were cold-rolled with various percentages of deformation and the cold-rolled samples were aged subsequently at the varied time for four hours and temperatures ranging up to 500°C. Samples underwent characterizations by microhardness testing, electrical resistivity, optical properties, differential scanning calorimetry as well as microstructure analysis using an optical microscope. The results showed that the hardening of Cu-based alloys was taken place due to solid-solution hardening. Al addition accelerated the hardness through ageing due to the formation of various intermetallic copper aluminites into the aged alloy which was hard and brittle in nature. The resistivity decreased marginally through heat treatment due to the stage of stress relieving, recovery, precipitation coarsening as well as recrystallization and increased for arranging different intermetallics into the alloys. The microstructural study revealed that the cold rolled alloys content the different phases of elongated grain at the rolling direction. Meanwhile higher ageing temperatures at 500°C for one hour led to recrystallization and grain growth especially in pure copper and Cu-10Zn alloys.
通过铸造制备了铝和锌含量分别为10wt%的铜基合金Al青铜和α-黄铜。然后,以不同的变形百分比对试样进行冷轧,随后在不同的时间和高达500°C的温度范围内对冷轧试样进行老化4小时。样品通过显微硬度测试、电阻率、光学性能、差示扫描量热法以及光学显微镜微观结构分析进行表征。结果表明,铜基合金的硬化是由于固溶硬化引起的。铝的添加通过时效加速了硬度,这是由于在时效合金中形成了各种金属间铜铝盐,而时效合金本质上是硬脆的。由于应力消除、恢复、沉淀粗化和再结晶阶段,电阻率在热处理过程中略有下降,而在合金中排列不同的金属间化合物时电阻率增加。微观组织研究表明,冷轧合金在轧制方向上含有不同的细长晶粒相。同时,在500°C下一小时的较高时效温度会导致再结晶和晶粒生长,尤其是在纯铜和Cu-10Zn合金中。
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引用次数: 1
THE EFFECT OF MATERIAL MODELS IN THE FEM SIMULATION ON THE SPRINGBACK PREDICTION OF THE TRIP STEEL 有限元模拟中材料模型对TRIP钢回弹预测的影响
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-09-13 DOI: 10.36547/ams.27.3.899
P. Mulidrán, E. Spišák, M. Tomáš, J. Majerníková, Ján Varga
In this work, the influence of material models used in the FEM simulation on the springback prediction is investigated. The interest of this paper is to extend the knowledge base regarding springback predictions in numerical simulation. The springback effect of a V-shaped sheet metal part made of TRIP steel, with a thickness of 0.75 mm was investigated. The bending angle was set to 90°.  In the numerical simulation, Hill48 and Barlat yield criteria were used in combination with Ludwik's and Swift's hardening models. Achieved data from the numerical simulations were compared and evaluated with experimental test results. The experimental results showed the relation between springback and calibration force. The effect of specimen cut direction on the springback was smaller in comparison with the calibration force. The numerical results of the springback were not identical with the experimentally achieved springback values in most cases. Particularly, when a calibration force of 1 800 N was used in the simulation. The simulation results showed a good correlation between experimental and numerical results, when Hill48 and Barlat yield criteria were used in combination with Ludwik hardening law and calibration force F with the value 900 N was applied.
本文研究了有限元模拟中使用的材料模型对回弹预测的影响。本文的兴趣在于扩展数值模拟中回弹预测的知识库。研究了由TRIP钢制成的厚度为0.75mm的V形金属板件的回弹效应。弯曲角度设置为90°。在数值模拟中,Hill48和Barlat屈服准则与Ludwik和Swift的硬化模型相结合。将数值模拟获得的数据与实验测试结果进行了比较和评估。实验结果表明回弹与标定力之间存在一定的关系。与标定力相比,试样切割方向对回弹的影响较小。在大多数情况下,回弹的数值结果与实验获得的回弹值不一致。特别是当在模拟中使用1800N的校准力时。模拟结果表明,当Hill48和Barlat屈服准则与Ludwik硬化定律结合使用,并施加值为900N的校准力F时,实验结果与数值结果之间具有良好的相关性。
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引用次数: 2
ELECTROCHEMICAL POLYMORPHIC PHASE FORMATION IN METALS 金属中电化学多晶相的形成
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-09-13 DOI: 10.36547/ams.27.3.1011
O. Girin
The phenomenon of electrochemical phase formation in metals and alloys via a supercooled liquid state stage was discussed. Assuming the electrodeposited metal to be a product of formation and ultrarapid solidification of supercooled metallic liquid, a possibility of metastable phase formation during electrodeposition of polymorphous metals was suggested. It was anticipated that the polymorphic transition of the metal’s metastable form to the stable one occurs by shear, as does the martensitic transformation. To enable revealing an orientation relationship between grains of the two phases, a method for X-ray texture analysis of metals was developed using a combination of direct pole figures. It was established that the phase formation during electrodeposition of polymorphous metals produces metastable modifications typical of entities that crystallized from a liquid state at extremely high rates. In regards polymorphic transitions in metal electrodeposition, certain orientation relationships were observed between grains of the stable and the metastable phase, which is typical of phase transformations proceeding at extremely high rates. The results obtained provided additional arguments in favor of the phenomenon under discussion.
讨论了金属和合金在过冷液相阶段的电化学相形成现象。假设电沉积的金属是过冷金属液体形成和超快固化的产物,提出了在多晶金属电沉积过程中形成亚稳相的可能性。正如马氏体相变一样,金属亚稳形态向稳定形态的多晶型转变是通过剪切发生的。为了揭示两相晶粒之间的取向关系,开发了一种使用直接极图组合的金属X射线织构分析方法。已经确定,在多晶型金属的电沉积过程中的相形成产生亚稳改性,这是以极高的速率从液态结晶的实体的典型改性。关于金属电沉积中的多晶型转变,在稳定相和亚稳相的晶粒之间观察到某些取向关系,这是以极高速率进行的相变的典型情况。所获得的结果为支持正在讨论的现象提供了更多的论据。
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引用次数: 0
Strain Hardening and Stretch Formability Behavior of Triple Phase (TP) Steel Strips 三相(TP)钢带的应变硬化和拉伸成形性能
IF 1 Q3 METALLURGY & METALLURGICAL ENGINEERING Pub Date : 2021-09-13 DOI: 10.36547/ams.27.3.1048
Maha ElMeligy, T. El-Bitar
The current work explores the strain hardening and stretches formability behaviour of the developed Triple Phase (TP) steel. Double quenched TP steel strips posse three distinguished stages of strain hardening on tensile forming. 1st stage represents the highest n-value reflecting resistance to homogeneous deformation, where steel can be safely stretched. 2nd and 3rd stage reveals lower n-values, where localized thinning exist. On Erichsen testing, the relationship between punch forming force and punch stroke exhibits two forming regions. The 1st region is delineated by a straight line showing an ultra-high strain-hardening rate, which represents a reversible elastic stretch forming.  The 2nd forming region continues to a higher Erichsen punch stroke than that of the 1st region and presents the permanent plastic stretch forming behaviour.  It is found that bainite and martensite clusters created, by double quenching, in TP-steel exaggerated the elastic stretch forming limit 10 times higher than the as-hot rolled condition. 7 min. holding time of strips in the salt bath is considered the most effective for the creation of a useful volume fraction of the bainite phase. However, 21 min. holding time in salt bath grows martensite laths through the bainite aggregates, affecting negatively on stretch formability.
目前的工作探索了开发的三相(TP)钢的应变硬化和拉伸成形性能。双淬火TP钢带在拉伸成形过程中具有三个不同的应变硬化阶段。第一阶段代表反映均匀变形阻力的最高n值,其中钢可以安全拉伸。第二和第三阶段显示出较低的n值,其中存在局部稀疏。在Erichsen试验中,冲压成形力和冲压行程之间的关系表现为两个成形区域。第一区域由显示超高应变硬化率的直线描绘,其表示可逆弹性拉伸成形。第二成形区域继续到比第一区域更高的Erichsen冲压行程,并且呈现永久塑性拉伸成形行为。研究发现,TP钢中通过双重淬火产生的贝氏体和马氏体团簇使弹性拉伸成形极限比热轧条件提高了10倍。在盐浴中保持带材7分钟的时间被认为是产生有用的贝氏体相体积分数的最有效的。然而,在盐浴中保持21分钟,马氏体板条通过贝氏体聚集体生长,对拉伸成形性产生负面影响。
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引用次数: 0
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Acta Metallurgica Slovaca
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