首页 > 最新文献

Journal of Micro and Nano-Manufacturing最新文献

英文 中文
Automatic Screw Detection and Tool Recommendation System for Robotic Disassembly 机器人拆卸螺丝自动检测与工具推荐系统
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85403
Xinyao Zhang, Kareem A. Eltouny, Xiao Liang, S. Behdad
Disassembly is an essential process for the recovery of end-of-life (EOL) electronics in remanufacturing sites. Nevertheless, the process remains labor-intensive due to EOL electronics’ high degree of uncertainty and complexity. The robotic technology can assist in improving disassembly efficiency, however, the characteristics of EOL electronics pose difficulties for robot operation, such as removing small components. For such tasks, detecting small objects is critical for robotic disassembly systems. Screws are widely used as fasteners in ordinary electronic products while having small sizes and varying shapes in a scene. To achieve robotic disassembly of screws, the location information and the required tools need to be predicted. This paper proposes a framework to automatically detect screws and recommend related tools for disassembly. First, the YOLOv4 algorithm is used to detect screw targets in EOL electronic devices, and then a screw image extraction mechanism is executed based on the position coordinates predicted by YOLOv4. Second, after obtaining the screw images, the EfficientNetv2 algorithm is applied for screw shape classification. In addition to proposing a framework for automatic small-object detection, we explore how to modify the object detection algorithm to improve its performance and discuss the sensitivity of tool recommendations to the detection predictions. A case study of three different types of screws is used to evaluate the performance of the proposed framework.
拆卸是回收报废电子产品的一个重要过程。然而,由于EOL电子产品的高度不确定性和复杂性,该过程仍然是劳动密集型的。机器人技术可以帮助提高拆卸效率,然而,EOL电子器件的特性给机器人操作带来了困难,例如拆卸小部件。对于此类任务,检测小物体对机器人拆卸系统至关重要。螺钉作为紧固件广泛应用于普通电子产品中,但其尺寸小,在场景中形状多变。为了实现机器人拆卸螺钉,需要预测位置信息和所需的工具。本文提出了一种自动检测螺钉的框架,并推荐了相应的拆卸工具。首先利用YOLOv4算法对EOL电子器件中的螺旋目标进行检测,然后根据YOLOv4预测的位置坐标执行螺旋图像提取机制。其次,在获得螺旋图像后,应用effentnetv2算法对螺旋形状进行分类。除了提出一个自动小目标检测框架外,我们还探讨了如何修改目标检测算法以提高其性能,并讨论了工具推荐对检测预测的敏感性。通过对三种不同类型螺钉的案例研究来评估所提出框架的性能。
{"title":"Automatic Screw Detection and Tool Recommendation System for Robotic Disassembly","authors":"Xinyao Zhang, Kareem A. Eltouny, Xiao Liang, S. Behdad","doi":"10.1115/msec2022-85403","DOIUrl":"https://doi.org/10.1115/msec2022-85403","url":null,"abstract":"\u0000 Disassembly is an essential process for the recovery of end-of-life (EOL) electronics in remanufacturing sites. Nevertheless, the process remains labor-intensive due to EOL electronics’ high degree of uncertainty and complexity. The robotic technology can assist in improving disassembly efficiency, however, the characteristics of EOL electronics pose difficulties for robot operation, such as removing small components. For such tasks, detecting small objects is critical for robotic disassembly systems. Screws are widely used as fasteners in ordinary electronic products while having small sizes and varying shapes in a scene. To achieve robotic disassembly of screws, the location information and the required tools need to be predicted. This paper proposes a framework to automatically detect screws and recommend related tools for disassembly. First, the YOLOv4 algorithm is used to detect screw targets in EOL electronic devices, and then a screw image extraction mechanism is executed based on the position coordinates predicted by YOLOv4. Second, after obtaining the screw images, the EfficientNetv2 algorithm is applied for screw shape classification. In addition to proposing a framework for automatic small-object detection, we explore how to modify the object detection algorithm to improve its performance and discuss the sensitivity of tool recommendations to the detection predictions. A case study of three different types of screws is used to evaluate the performance of the proposed framework.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"2013 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86467912","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 4
Pre-Crosslinked Hybrid Hydrogels for 3D Bio-Printing Process: Rheological Analysis 预交联混合水凝胶用于3D生物打印过程:流变分析
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85700
Slesha Tuladhar, Cartwright Nelson, Md. Ahasan Habib
Bioprinting for regenerative medicine has been gaining a lot of popularity in today’s world. Despite being one of the rigorously studied fields, there are still several challenges yet to be solved. Geometric fidelity and mechanical complexities stand as roadblocks when it comes to the printability of the customized scaffolds. Exploring the rheological properties of the compositions helps us understand the physical and mechanical properties of the biomaterials which are closely tied to the printability of the filament and eventually, geometric fidelity of the scaffolds. To ensure the structural integrity of the scaffolds, viscosity enhancers such as Carboxymethyl Cellulose (CMC) and crosslinkers like CaCl2 and CaSO4 were used. These crosslinkers can be used before (pre-crosslinking) and after (post-crosslinking) the extrusion of considered compositions to investigate and compare the outcome. To do this, mixtures of Carboxymethyl Cellulose (CMC, viscosity enhancer), Alginate, and CaCl2 and CaSO4 (crosslinkers) were prepared at various concentrations maintaining minimum solid content (≤ 8%). Each composition was subjected to a set of rheological tests like Flow curve for shear thinning behavior, three-point thixotropic for recovery rate, amplitude test for gelation point, and frequency tests. This research thoroughly investigates compositions when they are introduced to crosslinkers and viscosity enhancers which can be crucial for 3D printing world.
在当今世界,用于再生医学的生物打印技术越来越受欢迎。尽管这是一个被严格研究的领域,但仍有一些挑战有待解决。几何保真度和机械复杂性是定制支架可打印性的障碍。探索组合物的流变特性有助于我们了解生物材料的物理和机械特性,这些特性与长丝的可打印性以及最终支架的几何保真度密切相关。为了保证支架的结构完整性,使用了羧甲基纤维素(CMC)等增粘剂和CaCl2、CaSO4等交联剂。这些交联剂可以在(交联前)和(交联后)挤出所考虑的组合物之前使用,以研究和比较结果。为此,制备了不同浓度的羧甲基纤维素(CMC,粘度增强剂)、海藻酸盐、CaCl2和CaSO4(交联剂)的混合物,保持最低固含量(≤8%)。每种组合物都进行了一系列流变学测试,如剪切变薄行为的流动曲线,恢复速率的三点触变,凝胶点的振幅测试和频率测试。这项研究彻底调查了组合物,当它们被引入交联剂和粘度增强剂时,这对3D打印世界至关重要。
{"title":"Pre-Crosslinked Hybrid Hydrogels for 3D Bio-Printing Process: Rheological Analysis","authors":"Slesha Tuladhar, Cartwright Nelson, Md. Ahasan Habib","doi":"10.1115/msec2022-85700","DOIUrl":"https://doi.org/10.1115/msec2022-85700","url":null,"abstract":"\u0000 Bioprinting for regenerative medicine has been gaining a lot of popularity in today’s world. Despite being one of the rigorously studied fields, there are still several challenges yet to be solved. Geometric fidelity and mechanical complexities stand as roadblocks when it comes to the printability of the customized scaffolds. Exploring the rheological properties of the compositions helps us understand the physical and mechanical properties of the biomaterials which are closely tied to the printability of the filament and eventually, geometric fidelity of the scaffolds. To ensure the structural integrity of the scaffolds, viscosity enhancers such as Carboxymethyl Cellulose (CMC) and crosslinkers like CaCl2 and CaSO4 were used. These crosslinkers can be used before (pre-crosslinking) and after (post-crosslinking) the extrusion of considered compositions to investigate and compare the outcome. To do this, mixtures of Carboxymethyl Cellulose (CMC, viscosity enhancer), Alginate, and CaCl2 and CaSO4 (crosslinkers) were prepared at various concentrations maintaining minimum solid content (≤ 8%). Each composition was subjected to a set of rheological tests like Flow curve for shear thinning behavior, three-point thixotropic for recovery rate, amplitude test for gelation point, and frequency tests. This research thoroughly investigates compositions when they are introduced to crosslinkers and viscosity enhancers which can be crucial for 3D printing world.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"31 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"75891946","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Physics-Informed Artificial Intelligence for Temperature Prediction in Metal Additive Manufacturing: A Comparative Study 基于物理的人工智能在金属增材制造中的温度预测:比较研究
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85159
Suyog Ghungrad, B. Gould, S. Wolff, Azadeh Haghighi
Prediction of the temperature history of printed paths in additive manufacturing is crucial towards establishing the process-structure-property relationship. Traditional approaches for predictions such as physics-based simulations are computationally costly and time-consuming, whereas data driven approaches are highly dependent on huge, labeled datasets. Moreover, these labeled datasets are mostly scarce and costly in additive manufacturing owing to its unique application domain (mass customization) and complicated data-gathering stage. Recently, model-based or physics-informed artificial intelligence approaches have shown promising potential in overcoming the existing limitations and challenges faced by purely analytical or data driven approaches. In this work, a novel physics-informed artificial intelligent structure for scenarios with limited data is presented and its performance for temperature prediction in the selective laser melting additive manufacturing process is compared with one of the state-of-the-art data driven approaches, namely long short-term memory (LSTM) neural networks. Temperature data for training and testing was extracted from infrared images of single-track layer-based experiments for Ti64 material with different combinations of process parameters. Compared to LSTM, the proposed approach has higher computational efficiency and achieves better accuracy in limited data scenarios, making it a potential candidate for real-time closed-loop control of the additive manufacturing process under limited and sparse data scenarios. In other words, the proposed model is capable to learn more efficiently under such scenarios in comparison to LSTM model.
预测增材制造中打印路径的温度历史对于建立工艺-结构-性能关系至关重要。传统的预测方法,如基于物理的模拟,在计算上是昂贵和耗时的,而数据驱动的方法高度依赖于巨大的、标记的数据集。此外,这些标记数据集由于其独特的应用领域(大规模定制)和复杂的数据收集阶段,在增材制造中大多是稀缺和昂贵的。最近,基于模型或物理信息的人工智能方法在克服纯分析或数据驱动方法面临的现有限制和挑战方面显示出了很大的潜力。在这项工作中,提出了一种新的基于物理的人工智能结构,用于有限数据的场景,并将其在选择性激光熔化增材制造过程中的温度预测性能与最先进的数据驱动方法之一,即长短期记忆(LSTM)神经网络进行了比较。从不同工艺参数组合下的Ti64材料单层实验红外图像中提取温度数据,用于训练和测试。与LSTM相比,该方法在有限数据场景下具有更高的计算效率和更好的精度,使其成为有限和稀疏数据场景下增材制造过程实时闭环控制的潜在候选。换句话说,与LSTM模型相比,所提出的模型能够在这些场景下更有效地学习。
{"title":"Physics-Informed Artificial Intelligence for Temperature Prediction in Metal Additive Manufacturing: A Comparative Study","authors":"Suyog Ghungrad, B. Gould, S. Wolff, Azadeh Haghighi","doi":"10.1115/msec2022-85159","DOIUrl":"https://doi.org/10.1115/msec2022-85159","url":null,"abstract":"\u0000 Prediction of the temperature history of printed paths in additive manufacturing is crucial towards establishing the process-structure-property relationship. Traditional approaches for predictions such as physics-based simulations are computationally costly and time-consuming, whereas data driven approaches are highly dependent on huge, labeled datasets. Moreover, these labeled datasets are mostly scarce and costly in additive manufacturing owing to its unique application domain (mass customization) and complicated data-gathering stage. Recently, model-based or physics-informed artificial intelligence approaches have shown promising potential in overcoming the existing limitations and challenges faced by purely analytical or data driven approaches. In this work, a novel physics-informed artificial intelligent structure for scenarios with limited data is presented and its performance for temperature prediction in the selective laser melting additive manufacturing process is compared with one of the state-of-the-art data driven approaches, namely long short-term memory (LSTM) neural networks. Temperature data for training and testing was extracted from infrared images of single-track layer-based experiments for Ti64 material with different combinations of process parameters. Compared to LSTM, the proposed approach has higher computational efficiency and achieves better accuracy in limited data scenarios, making it a potential candidate for real-time closed-loop control of the additive manufacturing process under limited and sparse data scenarios. In other words, the proposed model is capable to learn more efficiently under such scenarios in comparison to LSTM model.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"8 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"84719718","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Machine Vision Tracking and Automation of a Microrobot (sAFAM) 微型机器人(sAFAM)的机器视觉跟踪与自动化
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85424
Colin Warn, A. Sherehiy, Moath H. A. Alqatamin, Brooke Ritz, Ruoshi Zhang, S. Chowdhury, Danming Wei, D. Popa
In this paper, we propose a method for tracking a microrobot’s three-dimensional position using microscope machine vision. The microrobot, theSolid Articulated Four Axis Microrobot (sAFAM), is being developed to enable the assembly and manipulation of micro and nanoscale objects. In the future, arrays of sAFAMS working together can be integrated into a wafer-scale nanofactory, Prior to use, microrobots in this microfactory need calibration, which can be achieved using the proposed measurement technique. Our approach enables faster and more accurate mapping of microrobot translations and rotations, and orders of magnitude larger datasets can be created by automation. Cameras feeds on a custom microscopy system is fed into a data processing pipeline that enables tracking of the microrobot in real-time. This particular machine vision method was implemented with a help of OpenCV and Python and can be used to track the movement of other micrometer-sized features. Additionally, a script was created to enable automated repeatability tests for each of the six trajectories traversable by the robot. A more precise microrobot workable area was also determined thanks to the significantly larger datasets enabled by the combined automation and machine vision approaches.
本文提出了一种利用显微镜机器视觉跟踪微型机器人三维位置的方法。这种微型机器人被称为固体铰接四轴微型机器人(sAFAM),正在开发中,以实现微型和纳米级物体的组装和操作。在未来,协同工作的sAFAMS阵列可以集成到晶圆级纳米工厂中。在使用之前,该微工厂中的微型机器人需要校准,这可以使用所提出的测量技术来实现。我们的方法可以更快,更准确地映射微型机器人的平移和旋转,并且可以通过自动化创建数量级更大的数据集。在定制的显微镜系统上输入的摄像头被送入数据处理管道,从而能够实时跟踪微型机器人。这种特殊的机器视觉方法是在OpenCV和Python的帮助下实现的,可用于跟踪其他微米尺寸特征的运动。此外,还创建了一个脚本,以便对机器人可穿越的六条轨迹中的每一条进行自动化的可重复性测试。由于自动化和机器视觉相结合的方法提供了更大的数据集,因此还确定了更精确的微型机器人工作区域。
{"title":"Machine Vision Tracking and Automation of a Microrobot (sAFAM)","authors":"Colin Warn, A. Sherehiy, Moath H. A. Alqatamin, Brooke Ritz, Ruoshi Zhang, S. Chowdhury, Danming Wei, D. Popa","doi":"10.1115/msec2022-85424","DOIUrl":"https://doi.org/10.1115/msec2022-85424","url":null,"abstract":"\u0000 In this paper, we propose a method for tracking a microrobot’s three-dimensional position using microscope machine vision. The microrobot, theSolid Articulated Four Axis Microrobot (sAFAM), is being developed to enable the assembly and manipulation of micro and nanoscale objects. In the future, arrays of sAFAMS working together can be integrated into a wafer-scale nanofactory, Prior to use, microrobots in this microfactory need calibration, which can be achieved using the proposed measurement technique. Our approach enables faster and more accurate mapping of microrobot translations and rotations, and orders of magnitude larger datasets can be created by automation. Cameras feeds on a custom microscopy system is fed into a data processing pipeline that enables tracking of the microrobot in real-time. This particular machine vision method was implemented with a help of OpenCV and Python and can be used to track the movement of other micrometer-sized features. Additionally, a script was created to enable automated repeatability tests for each of the six trajectories traversable by the robot. A more precise microrobot workable area was also determined thanks to the significantly larger datasets enabled by the combined automation and machine vision approaches.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"76 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"80545364","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Tiling of Cellular Structures Into 3D Parts According to the Density Values of SIMP Topology Optimization 根据SIMP拓扑优化的密度值将细胞结构平铺成三维零件
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85307
Damla Ozkapici Helvaci, U. Yaman
In this study, a novel approach is proposed to enhance the performance of the parts optimized by Solid Isotropic Material with Penalization (SIMP) method. SIMP is a topology optimization method that aims the optimum distribution of material in a design domain subjected to predefined loads, constraints and boundary conditions. The method forces every finite element composing the geometry to have a density of either 1 or 0. The main reason behind penalizing is that regions with intermediate densities are difficult to fabricate. However, including these regions in the optimization output may provide better performance results. Based on this idea, a method is proposed to utilize intermediate densities in a manufacturable form and is applied to 3D geometries. Besides, the remodeled topology is checked against any unconnected cells. In contrast to many methods, which delete the unconnected elements, the proposed method provides connectivity by adding cells. The outputs of the proposed method are fabricated by using Electron Beam Melting (EBM) and Stereolithography (SLA) technologies. EBM uses material powder and a heat source to melt and fuse the powders while SLA uses photosensitive resin and an ultraviolet light to cure the resin. A common limitation of both technologies is that powder/resin may remain inside the internal features which do not have access to outer surface of the part through the channels. The proposed method ensures the easy removal of excess powder/resin after fabrication. Performance of the method is compared with the SIMP method through test and analysis.
本文提出了一种提高固体各向同性材料惩罚法优化零件性能的新方法。SIMP是一种拓扑优化方法,其目的是在预定义的载荷、约束和边界条件下,在设计域中实现材料的最佳分布。该方法强制组成几何图形的每个有限元元素的密度为1或0。惩罚背后的主要原因是中等密度的区域难以制造。但是,在优化输出中包含这些区域可能会提供更好的性能结果。基于这一思想,提出了一种利用可制造形式的中间密度的方法,并将其应用于三维几何形状。此外,根据任何未连接的单元检查重构的拓扑。与许多删除未连接元素的方法相反,该方法通过添加单元来提供连接。采用电子束熔化(EBM)和立体光刻(SLA)技术制备了该方法的输出。EBM使用材料粉末和热源来熔化和融合粉末,而SLA使用光敏树脂和紫外光来固化树脂。这两种技术的一个共同限制是粉末/树脂可能会残留在内部特征中,而这些内部特征无法通过通道进入零件的外表面。所提出的方法确保在制造后容易去除多余的粉末/树脂。通过试验和分析,比较了该方法与SIMP方法的性能。
{"title":"Tiling of Cellular Structures Into 3D Parts According to the Density Values of SIMP Topology Optimization","authors":"Damla Ozkapici Helvaci, U. Yaman","doi":"10.1115/msec2022-85307","DOIUrl":"https://doi.org/10.1115/msec2022-85307","url":null,"abstract":"\u0000 In this study, a novel approach is proposed to enhance the performance of the parts optimized by Solid Isotropic Material with Penalization (SIMP) method. SIMP is a topology optimization method that aims the optimum distribution of material in a design domain subjected to predefined loads, constraints and boundary conditions. The method forces every finite element composing the geometry to have a density of either 1 or 0. The main reason behind penalizing is that regions with intermediate densities are difficult to fabricate. However, including these regions in the optimization output may provide better performance results. Based on this idea, a method is proposed to utilize intermediate densities in a manufacturable form and is applied to 3D geometries. Besides, the remodeled topology is checked against any unconnected cells. In contrast to many methods, which delete the unconnected elements, the proposed method provides connectivity by adding cells.\u0000 The outputs of the proposed method are fabricated by using Electron Beam Melting (EBM) and Stereolithography (SLA) technologies. EBM uses material powder and a heat source to melt and fuse the powders while SLA uses photosensitive resin and an ultraviolet light to cure the resin. A common limitation of both technologies is that powder/resin may remain inside the internal features which do not have access to outer surface of the part through the channels. The proposed method ensures the easy removal of excess powder/resin after fabrication. Performance of the method is compared with the SIMP method through test and analysis.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"58 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81019838","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
3D Co-Printability of PCL and Hybrid Hydrogels PCL和混合水凝胶的3D共打印性能
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85685
Connor Quigley, Md. Ahasan Habib
3D bioprinting has recently gained popularity due to its inherent capability of releasing cell-seeded and cell-laden biomaterials in a defined location to fabricate patient-specific scaffolds. Multi-nozzle extrusion-based 3D bio-printing allows the fabrication of various natural and synthetic biopolymers and the investigations of material to material and cell to material interactions, and eventually with a high percentage of cell viability and proliferation. Although natural hydrogels are demanding candidates for bio-printing because of their biocompatibility and high-water content, ensuring the scaffold’s fidelity with only natural hydrogel polymers is still challenging. Polycaprolactone (PCL) is a potential synthetic bioprinting material that can provide improved mechanical properties for fabricated scaffolds, especially bone and cartilage scaffolds. In this paper, application-oriented structural viability such as 3D printability, shape fidelity, and mechanical properties of the scaffolds fabricated by PCL and other natural hydrogel materials will be investigated. Scaffolds will be fabricated using various natural hybrid hydrogels such as Alginate-Carboxymethyl Cellulose; Alginate-Carboxymethyl Cellulose-TEMPO NFC, and PCL simultaneously using various infill densities, applied pressures, print speeds, and toolpath patterns. Shape fidelities of printed scaffolds will be analyzed. This research can help identify optimum natural-synthetic polymer combinations based on the materials interaction, external and internal geometries, and mechanical properties for large-scale multi-material bio fabrication.
生物3D打印由于其在特定位置释放细胞种子和细胞负载生物材料以制造患者特异性支架的固有能力,最近获得了普及。基于多喷嘴挤出的3D生物打印允许制造各种天然和合成生物聚合物,以及材料与材料和细胞与材料相互作用的研究,最终具有高比例的细胞活力和增殖。尽管天然水凝胶因其生物相容性和高含水量而成为生物打印的候选材料,但仅用天然水凝胶聚合物确保支架的保真度仍然具有挑战性。聚己内酯(PCL)是一种有潜力的合成生物打印材料,它可以为制备支架,特别是骨和软骨支架提供更好的力学性能。本文将研究PCL和其他天然水凝胶材料制备的支架的3D打印性、形状保真度和力学性能等面向应用的结构可行性。支架将使用各种天然混合水凝胶,如海藻酸盐-羧甲基纤维素;海藻酸盐-羧甲基纤维素- tempo NFC和PCL同时使用不同的填充密度、应用压力、打印速度和刀具轨迹模式。将分析打印支架的形状保真度。这项研究可以帮助确定基于材料相互作用、外部和内部几何形状以及大规模多材料生物制造的机械性能的最佳天然合成聚合物组合。
{"title":"3D Co-Printability of PCL and Hybrid Hydrogels","authors":"Connor Quigley, Md. Ahasan Habib","doi":"10.1115/msec2022-85685","DOIUrl":"https://doi.org/10.1115/msec2022-85685","url":null,"abstract":"\u0000 3D bioprinting has recently gained popularity due to its inherent capability of releasing cell-seeded and cell-laden biomaterials in a defined location to fabricate patient-specific scaffolds. Multi-nozzle extrusion-based 3D bio-printing allows the fabrication of various natural and synthetic biopolymers and the investigations of material to material and cell to material interactions, and eventually with a high percentage of cell viability and proliferation. Although natural hydrogels are demanding candidates for bio-printing because of their biocompatibility and high-water content, ensuring the scaffold’s fidelity with only natural hydrogel polymers is still challenging. Polycaprolactone (PCL) is a potential synthetic bioprinting material that can provide improved mechanical properties for fabricated scaffolds, especially bone and cartilage scaffolds. In this paper, application-oriented structural viability such as 3D printability, shape fidelity, and mechanical properties of the scaffolds fabricated by PCL and other natural hydrogel materials will be investigated. Scaffolds will be fabricated using various natural hybrid hydrogels such as Alginate-Carboxymethyl Cellulose; Alginate-Carboxymethyl Cellulose-TEMPO NFC, and PCL simultaneously using various infill densities, applied pressures, print speeds, and toolpath patterns. Shape fidelities of printed scaffolds will be analyzed. This research can help identify optimum natural-synthetic polymer combinations based on the materials interaction, external and internal geometries, and mechanical properties for large-scale multi-material bio fabrication.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"109 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"81203515","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Nanoporous Carbon Nanotube Coating for 3D Printing of High-Performance Continuous Fiber Reinforced Polymer Composites 用于高性能连续纤维增强聚合物复合材料3D打印的纳米多孔碳纳米管涂层
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85758
J. M. Pappas, Xiangyang Dong
High strength and lightweight continuous carbon fiber reinforced composites are desirable structural materials for applications in various industries including aerospace, automotive, and defense. Additive manufacturing (AM) of such important materials may provide multiple benefits including reduced cost, improved manufacturing efficiency, and the ability to fabricate complex structures not possible with traditional methods. Despite these benefits, a significant challenge with AM of continuous carbon fiber composites is poor impregnation of the fiber bundle with matrix material. When there is a lack of matrix material, voids develop within the fiber bundle and reduce mechanical properties of the composite including strength and stiffness. To minimize void formation, low speed manufacturing is typically necessary to facilitate impregnation. In this work, it was shown that fiber bundle impregnation can be significantly improved by applying thin, nanoporous coatings to the continuous fiber bundle. Using an electrophoretic deposition process, the coating microstructure, including thickness and nano pore size, was easily controlled through effective tuning of process parameters. Ultimately, individually coated carbon fibers were obtained and provided improvements in fiber bundle impregnation without sacrificing the flexibility of the fiber bundle. A highly absorbent yet flexible fiber bundle was desirable for 3D printing applications and would facilitate fabrication of complex geometries. With such tailored nanoporous coatings, fifteen-fold improvement in resin absorption time due was observed due to improved wicking by the nanoporous structure. Such improvements in absorption characteristics have a great potential for drop on demand or other resin-based 3D printing techniques. Furthermore, mechanical characterization demonstrated the potential of nanoporous coatings for additive manufacturing of high performance carbon fiber reinforced composites.
高强度、轻量化连续碳纤维增强复合材料是应用于航空航天、汽车和国防等各个行业的理想结构材料。这种重要材料的增材制造(AM)可以提供多种好处,包括降低成本,提高制造效率,以及制造传统方法无法实现的复杂结构的能力。尽管有这些优点,但连续碳纤维复合材料增材制造的一个重大挑战是纤维束与基体材料的浸渍不良。当缺乏基体材料时,纤维束内部会产生空洞,从而降低复合材料的机械性能,包括强度和刚度。为了尽量减少空洞的形成,通常需要低速制造以促进浸渍。在这项工作中,研究表明,在连续的纤维束上涂上薄的纳米多孔涂层可以显著改善纤维束的浸渍。采用电泳沉积工艺,通过对工艺参数的有效调整,可以很容易地控制涂层的微观结构,包括厚度和纳米孔径。最终,获得了单独涂层的碳纤维,并在不牺牲纤维束柔韧性的情况下改善了纤维束的浸渍。高吸水性且灵活的纤维束对于3D打印应用是理想的,并且可以促进复杂几何形状的制造。使用这种定制的纳米孔涂层,由于纳米孔结构改善了排芯,树脂吸收时间提高了15倍。这种吸收特性的改进对于按需滴或其他基于树脂的3D打印技术具有很大的潜力。此外,力学表征表明纳米多孔涂层在增材制造高性能碳纤维增强复合材料方面的潜力。
{"title":"Nanoporous Carbon Nanotube Coating for 3D Printing of High-Performance Continuous Fiber Reinforced Polymer Composites","authors":"J. M. Pappas, Xiangyang Dong","doi":"10.1115/msec2022-85758","DOIUrl":"https://doi.org/10.1115/msec2022-85758","url":null,"abstract":"\u0000 High strength and lightweight continuous carbon fiber reinforced composites are desirable structural materials for applications in various industries including aerospace, automotive, and defense. Additive manufacturing (AM) of such important materials may provide multiple benefits including reduced cost, improved manufacturing efficiency, and the ability to fabricate complex structures not possible with traditional methods. Despite these benefits, a significant challenge with AM of continuous carbon fiber composites is poor impregnation of the fiber bundle with matrix material. When there is a lack of matrix material, voids develop within the fiber bundle and reduce mechanical properties of the composite including strength and stiffness. To minimize void formation, low speed manufacturing is typically necessary to facilitate impregnation. In this work, it was shown that fiber bundle impregnation can be significantly improved by applying thin, nanoporous coatings to the continuous fiber bundle. Using an electrophoretic deposition process, the coating microstructure, including thickness and nano pore size, was easily controlled through effective tuning of process parameters. Ultimately, individually coated carbon fibers were obtained and provided improvements in fiber bundle impregnation without sacrificing the flexibility of the fiber bundle. A highly absorbent yet flexible fiber bundle was desirable for 3D printing applications and would facilitate fabrication of complex geometries. With such tailored nanoporous coatings, fifteen-fold improvement in resin absorption time due was observed due to improved wicking by the nanoporous structure. Such improvements in absorption characteristics have a great potential for drop on demand or other resin-based 3D printing techniques. Furthermore, mechanical characterization demonstrated the potential of nanoporous coatings for additive manufacturing of high performance carbon fiber reinforced composites.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"23 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"83731018","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Characterizing the Conductivity of Aerosol Jet Printed Silver Traces on Glass Using Intense Pulsed Light (IPL) 用强脉冲光(IPL)表征玻璃上气溶胶喷射印刷银迹的电导率
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85649
Connor Ferris, Dilan Ratnayake, Alexander Curry, Danming Wei, Erin Gerber, T. Druffel, K. Walsh
Aerosol Jet Printing is a novel micron-scale printing technology capable of handling a variety of materials due to a large print material viscosity range and high substrate standoff distance of 3–5 mm. To finalize the properties of printed materials, a form of post-processing is often required. A current widely applicable post-processing technique exists in traditional oven curing. However, oven curing greatly restricts the viable substrates as well as curing time. Intense Pulsed Light (IPL) offers the chance to greatly expand this substrate variety and decrease curing time. However, limited models currently exist to relate the finished material properties to the unique settings of current IPL technology. In this paper, an experiment is developed through a General Full Factorial Design of Experiments (DOE) model to characterize conductivity of Ag ink using IPL as a post processing technique. This is conducted through Novacentrix Ag ink (JSA426) by 3 × 3 mm Van der Pauw sensor pads cured using IPL. Sample pads were generated in triplicate over a range of Energy Levels, Counts and Durations for IPL and the resulting conductivity measured. The collected conductivity data was then analyzed using ANOVA to determine the significant interactions. From this, a regression model is developed to predict the conductivity for any Energy-Count-Duration value. The methods employed are applicable to any post-processing technique, and further optimization of the model is proposed for future work.
气溶胶喷射印刷是一种新型的微米级印刷技术,由于印刷材料粘度范围大,基材距离高,可达3-5毫米,因此能够处理各种材料。为了最终确定印刷材料的特性,通常需要一种形式的后处理。传统烘箱腌制是目前应用广泛的后处理技术。然而,烘箱固化极大地限制了可行的基材以及固化时间。强脉冲光(IPL)提供了机会,大大扩大这种基板的品种和减少固化时间。然而,目前存在的有限模型将成品材料属性与当前IPL技术的独特设置联系起来。本文通过实验的一般全析因设计(DOE)模型,利用IPL作为后处理技术来表征银油墨的电导率。这是通过Novacentrix Ag油墨(JSA426)通过3 × 3 mm的Van der Pauw传感器衬垫进行的,使用IPL固化。样品垫在IPL的能级,计数和持续时间范围内生成三份,并测量由此产生的电导率。然后使用方差分析分析收集的电导率数据,以确定显著的相互作用。由此,开发了一个回归模型来预测任何能量计数-持续时间值的电导率。所采用的方法适用于任何后处理技术,并为今后的工作提出了进一步优化模型的建议。
{"title":"Characterizing the Conductivity of Aerosol Jet Printed Silver Traces on Glass Using Intense Pulsed Light (IPL)","authors":"Connor Ferris, Dilan Ratnayake, Alexander Curry, Danming Wei, Erin Gerber, T. Druffel, K. Walsh","doi":"10.1115/msec2022-85649","DOIUrl":"https://doi.org/10.1115/msec2022-85649","url":null,"abstract":"\u0000 Aerosol Jet Printing is a novel micron-scale printing technology capable of handling a variety of materials due to a large print material viscosity range and high substrate standoff distance of 3–5 mm. To finalize the properties of printed materials, a form of post-processing is often required. A current widely applicable post-processing technique exists in traditional oven curing. However, oven curing greatly restricts the viable substrates as well as curing time. Intense Pulsed Light (IPL) offers the chance to greatly expand this substrate variety and decrease curing time. However, limited models currently exist to relate the finished material properties to the unique settings of current IPL technology. In this paper, an experiment is developed through a General Full Factorial Design of Experiments (DOE) model to characterize conductivity of Ag ink using IPL as a post processing technique. This is conducted through Novacentrix Ag ink (JSA426) by 3 × 3 mm Van der Pauw sensor pads cured using IPL. Sample pads were generated in triplicate over a range of Energy Levels, Counts and Durations for IPL and the resulting conductivity measured. The collected conductivity data was then analyzed using ANOVA to determine the significant interactions. From this, a regression model is developed to predict the conductivity for any Energy-Count-Duration value. The methods employed are applicable to any post-processing technique, and further optimization of the model is proposed for future work.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"1947 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"91210235","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 1
Effect of Porosity on Tool Wear During Micromachining of Additive Manufactured Titanium Alloy 增材钛合金微加工过程中孔隙率对刀具磨损的影响
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-80096
V. Varghese, Soham Mujumdar
Porosity is a major quality issue in additively manufactured (AM) materials due to improper selection of raw material or process parameters. While porosity is kept to a minimum for structural applications, parts with intentional (engineered) porosity find applications in prosthetics, sound dampeners & mufflers, catalytic converters, electrodes, heat exchangers, filters, etc. During post-processing of additive manufactured components using secondary machining to obtain required dimensional tolerance and/or surface quality, part porosity could lead to fluctuating cutting forces and reduced tool life. The machinability of the porous AM material is poor compared to the homogenous wrought material due to the intermittent cutting and anisotropy of AM materials. The cutting parameters for machining are generally optimized for continuous wrought material and are not applicable for porous AM material. Micromilling experiments were carried out on AM Ti6Al4V alloy with different porosity levels and cutting speed using a 1 mm diameter end mill. The progression of tool wear and associated mechanisms during micro-milling of additive manufactured Ti6Al4V samples with different porosity levels are experimentally investigated. Insights into tool-workpiece interaction during micro-machining are obtained in cases where pore size could be comparable to the cutting tool diameter. This research could lead to efficient hybrid additive-subtractive manufacturing technologies with improved tool life and reduced costs.
由于原材料或工艺参数选择不当,孔隙率是增材制造(AM)材料的主要质量问题。虽然孔隙度在结构应用中保持在最小,但有意(工程)孔隙度的部件可以应用于假肢,消声器和消声器,催化转换器,电极,热交换器,过滤器等。为了获得所需的尺寸公差和/或表面质量,在使用二次加工的增材制造部件的后处理过程中,零件孔隙率可能导致切削力波动和刀具寿命缩短。由于AM材料的间歇性切削和各向异性,多孔AM材料的可加工性较均匀变形材料差。加工的切削参数一般是针对连续变形材料进行优化的,而不适用于多孔增材制造材料。采用直径为1mm的立铣刀对不同孔隙率和切削速度的AM Ti6Al4V合金进行了微铣削实验。实验研究了不同孔隙率的添加剂制备的Ti6Al4V试样在微铣削过程中刀具磨损的进展及其机理。在微加工过程中,在孔径可与刀具直径相当的情况下,获得了对刀具-工件相互作用的见解。这项研究将带来高效的增材减材混合制造技术,提高刀具寿命,降低成本。
{"title":"Effect of Porosity on Tool Wear During Micromachining of Additive Manufactured Titanium Alloy","authors":"V. Varghese, Soham Mujumdar","doi":"10.1115/msec2022-80096","DOIUrl":"https://doi.org/10.1115/msec2022-80096","url":null,"abstract":"\u0000 Porosity is a major quality issue in additively manufactured (AM) materials due to improper selection of raw material or process parameters. While porosity is kept to a minimum for structural applications, parts with intentional (engineered) porosity find applications in prosthetics, sound dampeners & mufflers, catalytic converters, electrodes, heat exchangers, filters, etc. During post-processing of additive manufactured components using secondary machining to obtain required dimensional tolerance and/or surface quality, part porosity could lead to fluctuating cutting forces and reduced tool life. The machinability of the porous AM material is poor compared to the homogenous wrought material due to the intermittent cutting and anisotropy of AM materials. The cutting parameters for machining are generally optimized for continuous wrought material and are not applicable for porous AM material. Micromilling experiments were carried out on AM Ti6Al4V alloy with different porosity levels and cutting speed using a 1 mm diameter end mill. The progression of tool wear and associated mechanisms during micro-milling of additive manufactured Ti6Al4V samples with different porosity levels are experimentally investigated. Insights into tool-workpiece interaction during micro-machining are obtained in cases where pore size could be comparable to the cutting tool diameter. This research could lead to efficient hybrid additive-subtractive manufacturing technologies with improved tool life and reduced costs.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"31 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86911894","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Real-Time Structured Light Scanning Characterization of Surface Topography of Direct Energy Deposited 316L Stainless Steel 直接能量沉积316L不锈钢表面形貌的实时结构光扫描表征
IF 1 Q4 ENGINEERING, MANUFACTURING Pub Date : 2022-06-27 DOI: 10.1115/msec2022-85783
Weijun Shen, Xing Zhang, Y. Liao, Beiwen Li
Direct energy deposition (DED) has been widely used for additive manufacturing of metallic components toward a variety of applications. Surface characteristics of DED-fabricated components play key roles in determining the property and performance. Besides the average surface roughness which has been extensively investigated in literature, surface skewness and kurtosis are critical for surface integrity, particularly its durability due to stress concentration points. In this work, surface skewness and kurtosis of DED-fabricated 316L stainless steel as affected by processing parameters are investigated. In particular, the surface quality is measured using a microscopic structured light scanning (SLS) system, which is a relatively fast, low-cost, high-efficiency dimensional inspection metrology as compared to other methods. The results demonstrated the correlations between the printing parameters (laser power and scanning speed) and the surface topography of DED printed parts. It is found that the skewness and kurtosis of the surface are more sensitive to the change in scanning speed within a relatively low laser power range. Skewness is positively correlated with the scanning speed, while kurtosis shows a negative correlation with the scanning speed. Given a high scanning speed, Kurtosis and Skewness are more sensitive to the changes of scanning speed. Understanding the relationship between DED processing parameters and areal surface characteristics provides guidance and insights for process optimization and post-processing design towards additive manufacturing of high-performance metallic components.
直接能量沉积(DED)技术在金属部件的增材制造中得到了广泛的应用。ded制造的部件的表面特性对其性能起着关键作用。除了文献中广泛研究的平均表面粗糙度外,表面偏度和峰度对表面完整性至关重要,特别是由于应力集中点导致的耐用性。研究了316L不锈钢的表面偏度和峰度随工艺参数的变化规律。特别是,使用微观结构光扫描(SLS)系统测量表面质量,与其他方法相比,这是一种相对快速、低成本、高效率的尺寸检测计量方法。结果表明了打印参数(激光功率和扫描速度)与DED打印件表面形貌之间的相关性。在较低的激光功率范围内,表面的偏度和峰度对扫描速度的变化更为敏感。偏度与扫描速度呈正相关,峰度与扫描速度呈负相关。当扫描速度较高时,峰度和偏度对扫描速度的变化更为敏感。了解DED加工参数与面表面特性之间的关系,可以为高性能金属部件增材制造的工艺优化和后处理设计提供指导和见解。
{"title":"Real-Time Structured Light Scanning Characterization of Surface Topography of Direct Energy Deposited 316L Stainless Steel","authors":"Weijun Shen, Xing Zhang, Y. Liao, Beiwen Li","doi":"10.1115/msec2022-85783","DOIUrl":"https://doi.org/10.1115/msec2022-85783","url":null,"abstract":"\u0000 Direct energy deposition (DED) has been widely used for additive manufacturing of metallic components toward a variety of applications. Surface characteristics of DED-fabricated components play key roles in determining the property and performance. Besides the average surface roughness which has been extensively investigated in literature, surface skewness and kurtosis are critical for surface integrity, particularly its durability due to stress concentration points. In this work, surface skewness and kurtosis of DED-fabricated 316L stainless steel as affected by processing parameters are investigated. In particular, the surface quality is measured using a microscopic structured light scanning (SLS) system, which is a relatively fast, low-cost, high-efficiency dimensional inspection metrology as compared to other methods. The results demonstrated the correlations between the printing parameters (laser power and scanning speed) and the surface topography of DED printed parts. It is found that the skewness and kurtosis of the surface are more sensitive to the change in scanning speed within a relatively low laser power range. Skewness is positively correlated with the scanning speed, while kurtosis shows a negative correlation with the scanning speed. Given a high scanning speed, Kurtosis and Skewness are more sensitive to the changes of scanning speed. Understanding the relationship between DED processing parameters and areal surface characteristics provides guidance and insights for process optimization and post-processing design towards additive manufacturing of high-performance metallic components.","PeriodicalId":45459,"journal":{"name":"Journal of Micro and Nano-Manufacturing","volume":"16 1","pages":""},"PeriodicalIF":1.0,"publicationDate":"2022-06-27","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"86179941","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
期刊
Journal of Micro and Nano-Manufacturing
全部 Acc. Chem. Res. ACS Applied Bio Materials ACS Appl. Electron. Mater. ACS Appl. Energy Mater. ACS Appl. Mater. Interfaces ACS Appl. Nano Mater. ACS Appl. Polym. Mater. ACS BIOMATER-SCI ENG ACS Catal. ACS Cent. Sci. ACS Chem. Biol. ACS Chemical Health & Safety ACS Chem. Neurosci. ACS Comb. Sci. ACS Earth Space Chem. ACS Energy Lett. ACS Infect. Dis. ACS Macro Lett. ACS Mater. Lett. ACS Med. Chem. Lett. ACS Nano ACS Omega ACS Photonics ACS Sens. ACS Sustainable Chem. Eng. ACS Synth. Biol. Anal. Chem. BIOCHEMISTRY-US Bioconjugate Chem. BIOMACROMOLECULES Chem. Res. Toxicol. Chem. Rev. Chem. Mater. CRYST GROWTH DES ENERG FUEL Environ. Sci. Technol. Environ. Sci. Technol. Lett. Eur. J. Inorg. Chem. IND ENG CHEM RES Inorg. Chem. J. Agric. Food. Chem. J. Chem. Eng. Data J. Chem. Educ. J. Chem. Inf. Model. J. Chem. Theory Comput. J. Med. Chem. J. Nat. Prod. J PROTEOME RES J. Am. Chem. Soc. LANGMUIR MACROMOLECULES Mol. Pharmaceutics Nano Lett. Org. Lett. ORG PROCESS RES DEV ORGANOMETALLICS J. Org. Chem. J. Phys. Chem. J. Phys. Chem. A J. Phys. Chem. B J. Phys. Chem. C J. Phys. Chem. Lett. Analyst Anal. Methods Biomater. Sci. Catal. Sci. Technol. Chem. Commun. Chem. Soc. Rev. CHEM EDUC RES PRACT CRYSTENGCOMM Dalton Trans. Energy Environ. Sci. ENVIRON SCI-NANO ENVIRON SCI-PROC IMP ENVIRON SCI-WAT RES Faraday Discuss. Food Funct. Green Chem. Inorg. Chem. Front. Integr. Biol. J. Anal. At. Spectrom. J. Mater. Chem. A J. Mater. Chem. B J. Mater. Chem. C Lab Chip Mater. Chem. Front. Mater. Horiz. MEDCHEMCOMM Metallomics Mol. Biosyst. Mol. Syst. Des. Eng. Nanoscale Nanoscale Horiz. Nat. Prod. Rep. New J. Chem. Org. Biomol. Chem. Org. Chem. Front. PHOTOCH PHOTOBIO SCI PCCP Polym. Chem.
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
0
微信
客服QQ
Book学术公众号 扫码关注我们
反馈
×
意见反馈
请填写您的意见或建议
请填写您的手机或邮箱
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
现在去查看 取消
×
提示
确定
Book学术官方微信
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术
文献互助 智能选刊 最新文献 互助须知 联系我们:info@booksci.cn
Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。
Copyright © 2023 Book学术 All rights reserved.
ghs 京公网安备 11010802042870号 京ICP备2023020795号-1