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The effect of temperature on injection-induced shear slip of laboratory faults in sandstone 温度对砂岩实验室断层注入诱导剪切滑移的影响
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-15 DOI: 10.1007/s11440-024-02329-5
Nao Shen, Lei Wang, Xiaochun Li

Fluid injection into subsurface reservoirs may cause existing faults/fractures to slip seismically. To study the effect of temperature on injection-induced fault slip, at a constant confining pressure of 10 MPa, we performed a series of injection-induced shear slip experiments on critically stressed sandstone samples containing saw-cut fractures (laboratory-simulated faults) under varying fluid pressurization rates (0.1 and 0.5 MPa/min, respectively) and temperatures (25, 80, and 140 °C, respectively). At 25 °C, slow fault slip events with a peak slip velocity of about 0.13 μm/s were observed on a tested sample in response to a low fluid pressurization rate of 0.1 MPa/min. In contrast, fluid injection with a high pressurization rate of 0.5 MPa/min caused fault slip events with a peak slip rate up to about 0.38 μm/s. In response to a given fluid pressurization rate, several episodes of slip events with a higher slip velocity were induced at an elevated temperature of 140 °C, indicating an appreciable weakening effect at elevated temperatures. We also experimentally constrained the rate-and-state frictional (RSF) parameters at varying effective normal stresses and temperatures by performing velocity-stepping tests. The obtained RSF parameters demonstrate that for a relatively high normal stress, increasing temperature tends to destabilize fault slip. Post-mortem microstructural observations reveal that elevated temperatures promote the generation of abundant fine-grained gouge particles associated with injection-induced shear slip. Our experiments highlight that injection-induced fault slip is affected by temperature-related wear production over the fault surface.

向地下储层注入流体可能会导致现有断层/裂缝发生地震滑移。为了研究温度对注入诱发断层滑移的影响,我们在 10 兆帕的恒定约束压力下,对含有锯切裂缝(实验室模拟断层)的临界应力砂岩样本进行了一系列注入诱发剪切滑移实验,实验条件为不同的流体加压速率(分别为 0.1 和 0.5 兆帕/分钟)和温度(分别为 25、80 和 140 °C)。在 25 °C时,测试样本在 0.1 MPa/min 的低流体加压速率下出现了缓慢的断层滑动,滑动速度峰值约为 0.13 μm/s。相比之下,以 0.5 兆帕/分钟的高加压率注入流体时,断层滑移事件的峰值滑移速度高达约 0.38 μm/s。在给定的流体加压速率下,140 °C的高温诱发了几次滑移速度更高的滑移事件,这表明在高温下存在明显的削弱效应。我们还通过速度步进试验,对不同有效法向应力和温度下的速率与状态摩擦(RSF)参数进行了实验约束。所获得的 RSF 参数表明,对于相对较高的法向应力,温度升高往往会破坏断层滑动的稳定性。死后微观结构观察表明,温度升高会促进大量细粒刨花颗粒的产生,与注入诱发的剪切滑移有关。我们的实验突出表明,注入诱发的断层滑移受到断层表面与温度相关的磨损产生的影响。
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引用次数: 0
Estimation of coefficient of earth pressure at rest for coral sand considering the effect of density and stress 考虑密度和应力的影响,估算珊瑚砂静止时的土压力系数
IF 5.7 1区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-04-15 DOI: 10.1007/s11440-024-02325-9
Jiru Zhang, Weike Peng, Xiaoxuan Liu, Mingxing Luo

The coefficient of earth pressure at rest (K0) is a crucial parameter in geotechnical design. In this study, coral sands with various initial relative densities were subjected to K0 consolidation tests and consolidated-drained triaxial compression tests to investigate the impact of the relative density, stress level, and particle breakage on K0. Based on the Mohr–Coulomb failure law and experimental data, a formula for estimating K0 related to the effective stress and effective friction angle was proposed. The results revealed that the K0 of coral sand decreased with an increase in effective stresses, while the impact of the initial relative density on K0 was more obvious. At the same effective stress, the smaller the initial relative density was, the larger the K0 can be. In the tested stress range, minimal particle breakage was observed during the K0 consolidation, whereas a greater degree of particle breakage occurred during triaxial shear. This particle breakage has the potential to undermine the stress-dilatancy and interparticle locking characteristics in coral sands, leading to a diminished effective friction angle and potentially affecting K0. The proposed formula for estimating K0 can be expressed as a function of the effective stresses and effective friction angle, and the effect of initial relative density on K0 can be reflected by the function parameters. This formula provides a reasonable estimate of the K0 value for coral sand within a certain range of relative densities and stress levels. Furthermore, it demonstrates favorable applicability to other types of granular soils, such as quartz sand and rockfills.

静止时的土压力系数(K0)是岩土工程设计中的一个重要参数。本研究对不同初始相对密度的珊瑚砂进行了 K0 固结试验和固结排水三轴压缩试验,以研究相对密度、应力水平和颗粒破碎对 K0 的影响。根据莫尔-库仑失效定律和实验数据,提出了与有效应力和有效摩擦角相关的 K0 估算公式。结果表明,珊瑚砂的 K0 随有效应力的增加而减小,而初始相对密度对 K0 的影响更为明显。在相同的有效应力下,初始相对密度越小,K0 越大。在测试的应力范围内,K0固结过程中观察到的颗粒断裂极少,而在三轴剪切过程中发生的颗粒断裂程度更大。这种颗粒断裂可能会破坏珊瑚砂的应力膨胀和颗粒间锁定特性,导致有效摩擦角减小,并可能影响 K0。拟议的 K0 估算公式可表示为有效应力和有效摩擦角的函数,初始相对密度对 K0 的影响可通过函数参数反映出来。该公式可在一定的相对密度和应力水平范围内合理估算珊瑚砂的 K0 值。此外,它还证明了对其他类型颗粒土(如石英砂和岩石填料)的良好适用性。
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引用次数: 0
Experimental investigations of water retention curves of fresh and decomposed municipal solid wastes under multiple drying and wetting cycles 多次干燥和湿润循环下新鲜和分解城市固体废物保水曲线的实验研究
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-15 DOI: 10.1007/s11440-024-02314-y
Yuekai Xie, Jianfeng Xue

Municipal solid wastes (MSWs) disposed in landfills are generally exposed to drying and wetting cycles because of the variation in environmental conditions, decomposition of organics and leachate recirculation. This paper studies the water retention curves (WRCs) of fresh and degraded MSWs under various numbers of drying and wetting cycles with water and leachate exposure. The result indicates that the water retention capacities of MSWs decrease with drying and wetting cycles. The maximum hysteresis between the drying and wetting cycles is observed in the first cycles for all MSW samples. The WRCs of medium to highly decomposed MSWs under drying and wetting cycles are similar to those of soils. The WRCs of fresh MSWs can undergo substantial changes due to the discharge of intra-particle moisture caused by decomposition and compression. For both fresh and decomposed MSWs, the WRCs stabilize after 3 drying and wetting cycles. However, only the MSWs of one initial composition with similar void ratios were investigated. Further research should be conducted to investigate the water retention behavior of MSWs with diverse initial compositions (e.g., food contents) and void ratios.

由于环境条件的变化、有机物的分解和沥滤液的再循环,在垃圾填埋场处置的城市固体废物(MSWs)通常会经历干燥和湿润循环。本文研究了新鲜和降解的 MSW 在不同次数的干燥和湿润循环以及水和沥滤液暴露下的保水曲线(WRC)。结果表明,随着干燥和湿润循环次数的增加,城市固体废物的保水能力降低。在干燥和湿润循环的第一个循环中,所有都市固体废物样本都观察到了干燥和湿润循环之间的最大滞后现象。在干燥和湿润循环下,中度至高度分解的城市固体废物的水分保持率与土壤的水分保持率相似。由于分解和压缩会导致颗粒内水分的排出,因此新鲜都市固态固体废物的湿度分布系数会发生很大变化。无论是新鲜还是已分解的都市固态固体废物,在经过 3 次干燥和湿润循环后,其可湿性粉尘浓度都会趋于稳定。不过,我们只研究了空隙率相近、初始成分相同的城市固体废物。应进一步研究具有不同初始成分(如食物含量)和空隙率的都市固体废物的保水行为。
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引用次数: 0
Stability evaluation of gentle slopes in spatially variable soils using discretized limit analysis method: a probabilistic study 利用离散极限分析法评估空间可变土壤中缓坡的稳定性:一项概率研究
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-13 DOI: 10.1007/s11440-024-02289-w
Tianzheng Li, Wenping Gong, Chun Zhu, Huiming Tang

The stability of gentle slopes is rarely accessed in existing studies, which are at risk of below-toe failure in soils with low shear strength. The inherent spatial variability of soil shear strength poses a huge complication to the probabilistic stability evaluation of large-scale three-dimensional gentle slopes, which usually forces a trade-off between precision and efficiency. In view of this, a semi-analytical method is developed in the framework of discretized limit analysis, which gives a unified mathematical representation of toe failure and below-toe failure of slopes. The proposed method inherits the high efficiency of analytical methods and has the ability to integrate spatially variable shear strengths into the slope mechanical model. The model validation is conducted by comparisons with a widely recognized analytical method developed for uniform soils. The random fields are introduced to achieve a relatively accurate characterization of soil shear strength, and the Monte Carlo simulation is employed to obtain a sufficient number of factors of safety of slopes for the subsequent statistical analyses. In the parametric study, spatial variability-related parameters, including the coefficient of variation of soil cohesion covc or internal friction angle covφ, the autocorrelation lengths along vertical and horizontal directions ξ and k, the cross-correlation coefficient ρ, are varied systematically to reveal their influences on the slope stability from a statistical perspective. It is found that the ranking of the impact on the probabilistic stability of a gentle slope is given as: covc or covφ > ξ > k > ρcφ. Finally, the failure probabilities of the gentle slope are computed considering the variations of key parameters, which may have implications for practical slope designs.

现有的研究很少涉及缓坡的稳定性问题,因为在剪切强度较低的土壤中,缓坡有可能出现趾部以下崩塌。土壤剪切强度固有的空间变异性给大规模三维缓坡的概率稳定性评估带来了巨大的复杂性,通常需要在精度和效率之间做出权衡。有鉴于此,我们在离散极限分析的框架下开发了一种半解析方法,该方法给出了斜坡坡脚破坏和坡脚以下破坏的统一数学表征。所提出的方法继承了分析方法的高效率,并能将空间可变剪切强度纳入斜坡力学模型。模型验证是通过与针对均匀土壤开发的广受认可的分析方法进行比较而实现的。通过引入随机场来实现对土壤剪切强度的相对精确描述,并采用蒙特卡罗模拟来获得足够数量的斜坡安全系数,以便进行后续的统计分析。在参数研究中,系统地改变了与空间变异性相关的参数,包括土壤内聚力变异系数 covc 或内摩擦角 covφ、沿垂直和水平方向的自相关长度 ξ 和 k、交叉相关系数 ρcφ,从统计学角度揭示了它们对边坡稳定性的影响。结果发现,对缓坡概率稳定性影响的排序为:covc 或 covφ > ξ > k > ρcφ。最后,考虑到关键参数的变化,计算了缓坡的破坏概率,这可能会对实际的斜坡设计产生影响。
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引用次数: 0
Effects of subgrade spatial variability on critical strains and effectiveness of geogrid reinforcement in flexible pavement 路基空间变化对柔性路面临界应变和土工格栅加固效果的影响
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-12 DOI: 10.1007/s11440-024-02326-8
Li Xiao, Jianfeng Xue

The objective of this study is to assess the impact of spatial variability in the subgrade layer on the critical response of pavements and the effectiveness of geogrid reinforcement, employing the random field finite difference analysis (RFFDA). A comprehensive parametric study was conducted to examine the influence of two crucial factors: the coefficient of variation (({{text{COV}}}_{E})) and scale of fluctuation (SOF) of the subgrade modulus. Further investigation was conducted to uncover the statistical and mechanical mechanisms underlying the impact of subgrade spatial variability with emphasis on the critical strain distributions and their correlation with both the overall modulus and the local spatial variability of the key influence zone. Furthermore, this study explored the influence of subgrade spatial variability on the effectiveness of geogrid in reducing critical strains, considering various placement positions and geogrid moduli. The following main conclusions are drawn: (a) subgrade spatial variability has a substantial amplifying effect on critical pavement strains due to low modulus dominating effect, (b) there exists a worst value of SOF that results in the most unfavorable statistics of critical subgrade strain, (c) the effect of subgrade spatial variability on critical subgrade strain is more pronounced compared to its effect on critical asphalt strain, (d) the mean value of critical subgrade strain in RFFDA can be significantly underestimated when assuming fixed location for the strain, and (e) the effectiveness of geogrid in reducing critical strains is impacted by subgrade spatial variability, with the impact varying with the type of critical strain and geogrid location. Specifically, when placed at the base course–subgrade interface, the ability of geogrid to reduce critical subgrade strain is significantly compromised due to the subgrade spatial variability.

本研究的目的是采用随机场有限差分分析法(RFFDA),评估基层空间变异性对路面临界响应和土工格栅加固效果的影响。通过全面的参数研究,考察了两个关键因素的影响:路基模量的变异系数({text{COV}}}_{E})和波动尺度(SOF)。研究还进一步揭示了影响路基空间变异性的统计和力学机制,重点是临界应变分布及其与整体模量和关键影响区局部空间变异性的相关性。此外,考虑到不同的铺设位置和土工格栅模量,本研究还探讨了路基空间变化对土工格栅降低临界应变效果的影响。主要结论如下(a) 由于低模量主导效应,路基空间变异性对路面临界应变有显著的放大效应;(b) SOF 存在一个最差值,导致最不利的路基临界应变统计;(c) 与对沥青临界应变的影响相比,路基空间变异性对路基临界应变的影响更为明显、(e) 土工格栅降低临界应变的效果受基层空间变化的影响,其影响因临界应变的类型和土工格栅的位置而异。具体来说,当土工格栅被放置在基层-路基界面时,由于路基的空间变化,土工格栅减小路基临界应变的能力会大打折扣。
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引用次数: 0
Experimental determination of hypoplastic parameters and cyclic numerical analysis for railway bridge backfills 铁路桥梁回填土低塑性参数的实验测定和循环数值分析
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-11 DOI: 10.1007/s11440-024-02312-0
A. Stastny, L. Knittel, T. Meier, F. Tschuchnigg

Long integral bridges experience an enhanced cyclic soil structure interaction with their granular backfills, especially due to seasonal thermal loading. For numerical modelling of this interaction behaviour under cyclic loading, it is important to employ a suitable constitutive model and calibrate it thoroughly. However, up to the present, experimental data and calibrated soil models for this purpose with focus on typical well-graded coarse-grained bridge backfill materials are rarely available in the literature. Therefore, one aim of this paper is to present results of a comprehensive cyclic laboratory testing programme on highly compacted gravel backfill material. Based on this, a hypoplastic constitutive model with intergranular strain extension for small strain and cyclic behaviour is calibrated and evaluated against the experimental test data. The soil model’s abilities and limitations are discussed at element test level. In addition, cyclic FE analyses of an integral bridge are conducted with several hypoplastic parameter sets from the literature and compared to the calibrated gravel backfill material. The investigation highlights that poorly-graded sands show significantly smaller cyclic earth pressures compared to well-graded gravels intended for the backfilling of a bridge. The soil structure interaction behaviour is clearly governed by the general soil model stiffness, including the small strain stiffness.

整体式长桥与其颗粒状回填土之间的周期性土体结构相互作用增强,特别是由于季节性热荷载的影响。要对循环荷载下的这种相互作用行为进行数值建模,必须采用合适的构成模型并对其进行全面校准。然而,到目前为止,文献中还很少有针对典型的级配良好的粗粒桥梁回填材料的实验数据和经过校准的土壤模型。因此,本文的目的之一是介绍对高度压实的砾石回填材料进行综合循环实验室测试的结果。在此基础上,针对小应变和循环行为校准并评估了具有晶间应变扩展的低塑性构造模型。在元素测试层面讨论了土壤模型的能力和局限性。此外,还利用文献中的几组次塑性参数对一座整体桥梁进行了循环有限元分析,并与校准后的砾石回填材料进行了比较。研究结果表明,与用于桥梁回填的级配良好的砾石相比,级配不良的砂土所表现出的循环土压力要小得多。土壤结构相互作用行为明显受制于一般土壤模型刚度,包括小应变刚度。
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引用次数: 0
Dynamic effects in soil water retention curves: an experimental exploration by full-scale soil column tests using spatial time-domain reflectometry and tensiometers 土壤保水曲线的动态效应:利用空间时域反射仪和张力计进行的全尺度土柱试验探索
IF 5.7 1区 工程技术 Q1 Earth and Planetary Sciences Pub Date : 2024-04-10 DOI: 10.1007/s11440-024-02328-6
Guanxi Yan, Thierry Bore, Stefan Schlaeger, Alexander Scheuermann, Ling Li

The dynamic effects in soil water retention curves (SWRCs) have been the focus of much research. However, most studies implemented short column tests in a few centimeters, under which a semi-permeable porous media inevitably minimizes or magnifies the dynamic effects. In this study, full-scale sand column tests were conducted to eliminate this flaw by preparing a saturated zone under the unsaturated one. The soil suction and moisture profiles were monitored using high-precision tensiometers and spatial time-domain reflectometry, thereby providing a rational overshooting range of the dynamic SWRC. The results confirm that the dynamic primary drainage curve overshoots the static one. The dynamic effects were estimated quantitatively from the soil moisture re-equilibrium time (τS) and dynamic coefficient (τp), falling within reasonable ranges from previous studies. The τp increases log-linearly with decreasing moisture content and can be estimated well from the corresponding τS and the first derivative of SWRC. Also, the τp increases as the soil becomes finer and better graded, which agrees with more-prominent dynamic effects for lower-permeability reservoirs from petroleum studies but disagrees with more-significant dynamic effects for higher-permeability sand from soil-hydrology studies. The analysis shows that the dynamic effects are not dominated solely by the τp or permeability but also by the groundwater dynamics, which can be seen as a pressure boundary from the saturated zone. This finding explains the significant dynamic effects for both high- and ultra-low-permeability geomaterial. Therefore, the present full-scale soil column setup with a prepared saturated zone is recommended for academic investigations of dynamic SWRCs.

土壤保水曲线(SWRC)中的动态效应一直是许多研究的重点。然而,大多数研究采用的是几厘米的短柱试验,在这种情况下,半渗透多孔介质不可避免地会使动态效应最小化或放大。在本研究中,为了消除这一缺陷,我们进行了全尺寸砂柱试验,在非饱和区下准备了一个饱和区。使用高精度张力计和空间时域反射测量法监测了土壤吸力和湿度剖面,从而为动态 SWRC 提供了合理的超调范围。结果证实,动态主排水曲线与静态曲线存在过冲。根据土壤水分再平衡时间(τS)和动态系数(τp)对动态效应进行了定量估算,结果在以往研究的合理范围内。τp 随含水量的降低呈对数线性增长,可以很好地根据相应的 τS 和 SWRC 的一阶导数进行估算。此外,τp 随着土壤变得更细、分级更好而增大,这与石油研究中渗透率较低的储层更突出的动力效应一致,但与土壤-水文研究中渗透率较高的砂土更显著的动力效应不同。分析表明,动态效应并非仅受 τp 或渗透率的影响,还受地下水动态的影响。这一发现解释了高渗透性和超低渗透性土工材料的显著动态效应。因此,建议在对动态 SWRC 进行学术研究时,采用目前这种带有预制饱和区的全尺度土柱设置。
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引用次数: 0
Formation and evolution of particle migration zones for different drilling fluid compositions in porous media 多孔介质中不同钻井液成分的颗粒迁移区的形成和演变
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-10 DOI: 10.1007/s11440-024-02316-w
Jithin S. Kumar, Ramesh Kannan Kandasami, Jitendra S. Sangwai

Flow of suspensions through the complex porous network is typically characterized by the initial spurt and then the formation of internal/ external filter cake which impedes the flow velocity. The transient mechanisms involved during the particle migration phenomenon need to be studied carefully as it is crucial for effectively managing the flow characteristics of drilling fluids and their impact on subsurface reservoirs. In this study, constant pressure permeation experiments are carried out using a specially designed apparatus to quantify the formation and evolution of particle migration zones using advanced image processing algorithms. Additionally, a comprehensive pre-test and post-test characterization of drilling fluids/ filtrates and the porous medium revealed intricate insights into the dynamics of particle migration. Four distinct particle migration/ filtration zones such as internal filter cake, primary filtration, secondary filtration and fluid loss are identified based on the change in the concentration gradient. The influence of additives on the growth of these zones is quantified during the filtration process. The concentration of barite/ micronized calcium carbonate and xanthan gum predominantly controls the filtration process by enhancing the particle plugging and retention time, respectively. In addition to the in-depth understanding of the particle migration zones, the transition from kinetic to capillary flow is identified by performing the fractal analysis. The analysis revealed that drilling fluid containing more barite exhibits a dominant capillary flow. Finally, an analytical model has been modified by considering the influence of different additives to predict the depth of penetration, which is comparable with the experimental results.

悬浮液在复杂多孔网络中流动的典型特征是最初的喷涌,然后形成内部/外部滤饼,阻碍流速。需要仔细研究颗粒迁移现象中涉及的瞬态机制,因为这对有效管理钻井液的流动特性及其对地下储层的影响至关重要。在这项研究中,使用专门设计的仪器进行了恒压渗透实验,利用先进的图像处理算法对颗粒迁移区的形成和演变进行量化。此外,还对钻井液/滤液和多孔介质进行了全面的试验前和试验后表征,揭示了颗粒迁移动态的深刻内涵。根据浓度梯度的变化,确定了四个不同的颗粒迁移/过滤区,如内部滤饼、一次过滤、二次过滤和流体流失。在过滤过程中,对添加剂对这些区域增长的影响进行了量化。重晶石/微粉碳酸钙和黄原胶的浓度分别通过增强颗粒堵塞和保留时间来控制过滤过程。除了深入了解颗粒迁移区外,还通过分形分析确定了从动能流到毛细管流的过渡。分析结果表明,含重晶石较多的钻井液主要表现为毛细管流。最后,考虑到不同添加剂的影响,对分析模型进行了修改,以预测渗透深度,结果与实验结果相当。
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引用次数: 0
Effects of aqueous nanoparticle suspension injection on a shale’s mechanical properties 水性纳米颗粒悬浮液注入对页岩力学性能的影响
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-10 DOI: 10.1007/s11440-024-02282-3
Yongkang Wu, Yucheng Li, Shengmin Luo, Meng Lu, Nancy Zhou, Li He, Yongfeng Deng, Guoping Zhang

This paper presents the first effort to unravel and quantify the strengthening of a shale induced by nanoparticle injection from the perspectives of cross-scale and multi-constituent mechanical properties. After being subject to injection of pure water and an aqueous suspension of carbon black nanoparticle of ~ 50 nm in diameter under a differential pressure of 850 kPa, the shale specimens were characterized by big data nanoindentation (BDNi) to probe the mechanical properties of both individual constituents at the microscale and the bulk rock at the macroscale, leading to comparatively assessing the effects of injecting pure water and aqueous nanoparticle suspension on the mechanical properties. Microstructural characterization by electron microscopy and X-ray computed tomography validates the successful injection of nanoparticles into the microcracks and micropores of the rock. While the nanoparticles can infiltrate to depths of up to 100 s μm in zones with densely populated microcracks, the maximum depths of injection in crack-free zones are only 2–5 μm. Moreover, the injected nanoparticles mostly act as inert fillers in the interconnected micropores and microcracks but can seldom enter the isolated micropores. Comparison of the BDNi results from pure water versus nanoparticle-injected specimens shows that the Young’s modulus of the clay matrix experiences the highest increase by 23.1%, while the counterpart of non-porous quartz the lowest by 12.8%. Overall, the bulk shale’s Young’s modulus increases by 21.5%. Such data are consistent with the microcharacterization results that the injected nanoparticles mainly remain in the micropores and microcracks within the clay matrix. Owing to their hydrophobic nature, the carbon black nanoparticles have little effect on the rock’s hardness. The findings can shed light on the practical applications of nanoparticle injection for improved wellbore stability in shale formations.

本文首次从跨尺度和多成分力学性能的角度揭示并量化了纳米粒子注入对页岩的强化作用。在 850 kPa 压差下注入纯水和直径约 50 nm 的碳黑纳米粒子水悬浮液后,页岩试样通过大数据纳米压痕(BDNi)表征,探测微观尺度上单个成分和宏观尺度上岩体的力学性能,从而比较评估注入纯水和纳米粒子水悬浮液对力学性能的影响。通过电子显微镜和 X 射线计算机断层扫描进行的微观结构表征验证了纳米颗粒成功注入岩石的微裂缝和微孔。在微裂缝密集区,纳米颗粒的渗透深度可达 100 s μm,而在无裂纹区,最大注入深度仅为 2-5 μm。此外,注入的纳米粒子大多在相互连接的微孔和微裂缝中充当惰性填充物,但很少能进入孤立的微孔。对比纯水和注入纳米粒子试样的 BDNi 结果发现,粘土基质的杨氏模量增幅最大,为 23.1%,而无孔石英的杨氏模量增幅最小,为 12.8%。总体而言,块状页岩的杨氏模量增加了 21.5%。这些数据与微观表征结果一致,即注入的纳米颗粒主要停留在粘土基质的微孔和微裂缝中。由于纳米炭黑具有疏水性,因此对岩石硬度的影响很小。这些发现可以为注入纳米粒子提高页岩层井筒稳定性的实际应用提供启示。
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引用次数: 0
Influence of non-plastic fines and density state on stress-dilatancy behavior of coral sand: an experimental investigation 非塑性细粒和密度状态对珊瑚砂应力膨胀行为的影响:实验研究
IF 5.6 1区 工程技术 Q1 ENGINEERING, GEOLOGICAL Pub Date : 2024-04-10 DOI: 10.1007/s11440-024-02286-z
Xue Li, Wan-Huan Zhou, Jiankun Liu, Chao Wang

Understanding accurately the influence of non-plastic fines on stress-dilatancy of coral sand mixture-packing is crucial for marine engineering in various geotechnical applications. This work experimentally examined the effects of non-plastic fines and initial test conditions on stress-dilatancy behavior of mixture. Based on test results, equivalent void ratio (({e}^{*})) was determined to quantify the global effect of fines on shear behavior across different shear stages. Test results show that ({e}^{*}) exhibits a reduction as the mean effective stress (({p}{^prime})) increases, following a power function relationship. Besides, ({e}^{*}) variation under phase transformation, peak state, and critical state can be described by a normalized curve. Reduced fines content and increased relative density can contribute to the enhancement of both peak strength and internal friction angle within the mixture. However, the smooth shape and lubrication function facilitated by fines actively contribute to initiation of shear contraction. Furthermore, the stress paths observed in the CD shear tests manifest as a sequence of parallel straight lines within the (q)-({p}{^prime}) plane. The length of these lines progressively extends as the stress level escalates. Moreover, deviator stress in (q)-({p}{^prime}) curves under character state presents lower and upper limits which are 0.334 and 0.639 corresponding to tested samples determined by fines content and relative density. Elevated fines content combined with reduced relative density can lead to a reduction in both peak-state friction angle and maximum angle of dilation.

准确了解非塑性细粒对珊瑚砂混合物填料应力膨胀的影响,对于海洋工程中的各种岩土工程应用至关重要。这项工作通过实验研究了非塑性细粒和初始试验条件对混合物应力膨胀行为的影响。根据试验结果,确定了等效空隙率(({e}^{*})),以量化细颗粒在不同剪切阶段对剪切行为的总体影响。试验结果表明,随着平均有效应力(({p}{^prime}))的增加,等效空隙率(({e}^{*}}))呈下降趋势,这与幂函数关系有关。此外,({e}^{*})在相变、峰值状态和临界状态下的变化可以用归一化曲线来描述。细粒含量的降低和相对密度的增加有助于提高混合物的峰值强度和内摩擦角。然而,细粒材料的光滑形状和润滑功能会积极促进剪切收缩的产生。此外,CD 剪切试验中观察到的应力路径表现为 (q)-({p}{^prime}) 平面内的一系列平行直线。这些直线的长度随着应力水平的增加而逐渐延长。此外,在特征状态下的(q)-({p}{^prime})曲线中的偏离应力呈现出下限和上限,分别为 0.334 和 0.639,与根据细粒含量和相对密度确定的测试样品相对应。细粒含量的增加与相对密度的降低会导致峰值状态摩擦角和最大扩张角的减小。
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Acta Geotechnica
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