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Synthesis of Fluorescent Carbon Dots (CDs) Using Laser Ablation Method for Bioimaging Application 激光烧蚀法合成荧光碳点在生物成像中的应用
Pub Date : 2023-05-06 DOI: 10.25077/jif.15.2.91-105.2023
J. Jumardin, A. Maddu, Kokoeh Santoso, I. Isnaeni
Carbon Dots (CDs) were synthesized using laser ablation by focusing the laser beam on carbon (Tea) material in colloid (CH3) for 3 hours. UV-Vis spectroscopic and fluorometric characterization showed absorption of the wavelength peaks caused by the control treatment and after laser ablation and coating using Poly Ethylene Glycol (PEG400). The excitation and emission energies are formulations of CDs absorbance wavelength and fluorescence intensity. The absorbance coefficient is obtained based on the absorbance value of the cuvette thickness. The transmittance value (T) is obtained based on the absorption coefficient multiplied by 100%. CD fluorescence wavelength based on control parameters was 489 nm. After laser ablation was 496 nm, and after coating was 511 nm. CDs morphology and size characteristics are 4 nm to 10 nm based on TEM measurements. Fluorescence analysis for bioimaging applications on the luminescence intensity value of internalized blue CDs in zebrafish eye organs. The average intensity of CDs in the eye organs, gill, intestinal, dorsal, and tail injection points was 88.15 %, 91.58 %, 92.76 %, and 0.00 %.
通过将激光束聚焦在胶体(CH3)中的碳(Tea)材料上3小时,使用激光烧蚀合成碳点(CDs)。UV-Vis光谱和荧光表征显示了由对照处理以及使用聚乙二醇(PEG400)进行激光烧蚀和涂覆之后引起的波长峰值的吸收。激发能和发射能是CDs吸收波长和荧光强度的公式。吸光度系数是基于比色杯厚度的吸光度值而获得的。透射率值(T)是基于吸收系数乘以100%而获得的。基于对照参数的CD荧光波长为489nm。激光烧蚀后为496nm,涂覆后为511nm。基于TEM测量,CD的形态和尺寸特征为4nm至10nm。荧光分析在斑马鱼眼睛器官内内化蓝CD发光强度值的生物成像应用。眼器官、鳃、肠、背侧和尾部注射点的CD平均强度分别为88.15%、91.58%、92.76%和0.00%。
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引用次数: 0
Recent Progress of ZnO-Based Nanoparticle: Synthesizing Methods of Various Dopant and Applications zno基纳米颗粒的研究进展:各种掺杂剂的合成方法及应用
Pub Date : 2023-05-02 DOI: 10.20527/flux.v20i1.16044
N. Rauf
This review focus on the effect of doping rare earth metals, transition metals, noble metals, poor metals, and non-metals on ZnO nanoparticles. ZnO is a semiconductor material with an average wide energy band gap of 3.2 eV. The doping is used to improve the properties of ZnO which strongly depend on their application. The concentration of doping, the type of doping and the process using sol-gel, hydrothermal and precipitation methods are affected in modifying the ZnO lattice parameters. The transition metal widely used for photocatalysts and sensors. The doped application of ZnO nanoparticles as a semiconductor material has proven advantageous in enabling various photocatalytic, glucose biosensors, VOC detection sensors, antibacterial, biomedical, and optoelectronic spintronic, LED, NLO, and silicon solar cells. This review provided information for scientist in choosing the synthesizing methods of ZnO with desired properties and application in future.
本文综述了稀土金属、过渡金属、贵金属、贫金属和非金属掺杂对ZnO纳米粒子的影响。ZnO是一种半导体材料,其平均能带宽度为3.2 eV。掺杂是提高ZnO性能的重要手段,其性能的提高与掺杂的应用密切相关。掺杂浓度、掺杂类型、溶胶-凝胶法、水热法和沉淀法对ZnO晶格参数的修饰均有影响。过渡金属广泛用于光催化剂和传感器。ZnO纳米粒子作为半导体材料的掺杂应用已被证明在实现各种光催化、葡萄糖生物传感器、VOC检测传感器、抗菌、生物医学、光电自旋电子、LED、NLO和硅太阳能电池方面具有优势。这一综述为今后选择具有理想性能和应用前景的氧化锌合成方法提供了参考。
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引用次数: 0
Utilization of LDPE Plastic Waste, Coconut Shell and Coconut Husk as Basic Material for Briquettes with Tapioca Starch Adhesive 利用LDPE塑料废料、椰子壳和椰子壳作为木薯淀粉粘合剂成型基料
Pub Date : 2023-04-29 DOI: 10.25077/jif.15.2.81-90.2023
Sheilla Rully Anggita, Renanda Fasha Devarasalya, I. Istikomah, A. Bawono
Bio-briquettes of organic waste can be used as alternative energy to solve the waste problem. This study aimed to determine the quality of bio-briquettes made of LDPE, coconut husk, and coconut shell with tapioca adhesive. The coconut husk and shell were carbonized at 300 °C for 60 minutes. Charcoal that has been ground and sieved with 40 mesh is mixed with tapioca flour adhesive, and pieces of LDPE are added. Then, the sample is pressed with a cylindrical mold with a matrix strength of 5 tons. Bio-briquettes were dried in an oven at 80 °C for 12 hours. The quality of the briquette was evaluated through proximate analysis, including the calorific value, moisture content, ash content, volatile matter content, and fixed carbon content. The calorific value of all samples complied with the regulation of the Ministry of Energy and Mineral Resources (ESDM) No. 047 of 2006, which is above 4400 cal/g. The maximum moisture content is 15%, which fulfills SNI 06–3730-1995 standards, and the ESDM regulation, especially for the composition of 40% shell: 40% coconut: LDPE 20%. The ash content, volatile matter content, and fixed carbon content of all samples did not comply with SNI briquette standards and ESDM regulations.
有机废物的生物压块可以作为替代能源来解决废物问题。研究了以LDPE、椰壳和椰壳为原料,用木薯淀粉胶粘剂制备生物型煤的质量。椰壳和椰壳在300°C下碳化60分钟。用40目筛过的木炭与木薯粉胶粘剂混合,并加入LDPE片。然后,用基体强度为5吨的圆柱形模具对样品进行压制。生物型煤在80°C的烤箱中干燥12小时。通过热值、水分含量、灰分含量、挥发物含量和固定碳含量等近似分析来评价型煤的质量。所有样品的热值均符合能源和矿产资源部2006年第047号规定,均在4400 cal/g以上。最大含水率为15%,符合SNI 06-3730-1995标准,符合ESDM规定,特别适用于40%壳:40%椰子:20% LDPE的组成。所有样品的灰分含量、挥发物含量、固定碳含量均不符合SNI型煤标准和ESDM规定。
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引用次数: 0
Effect of TiO2 on Orange Peel Activated Carbon Composite in Reducing Carbon Monoxide and Hydrocarbon Gas Emissions TiO2对柑桔皮活性炭复合材料减少一氧化碳和碳氢化合物气体排放的影响
Pub Date : 2023-04-21 DOI: 10.25077/jif.15.2.73-80.2023
Ya' Muhammad Arsyad, D. Wahyuni, N. Nurhasanah, Bintoro Siswo Nugroho, Riza Adriat, Agus Prasetiono, Wahyu Tri Hidayat
study aims to see the effect of adding TiO2 on activated carbon as a material for reducing CO and HC gas emissions. Activated carbon (AC) was synthesized from orange peel waste at a carbonization temperature of 600  with a 10% (w/v) ZnCl2 activator. Composite AC/TiO2 was prepared by a simple mixing method. This process obtained TiO2-modified activated carbon material with variations in TiO2 concentrations of 0%, 10%, 15%, 20%, and 25%. Scanning Electron Microscope (SEM) was performed to obtain information on the AC/TiO2 surface morphology. In the application as a CO and HC gas emission reduction material, the results of mixing AC/TiO2 are mixed with a 10% (w/v) solution of Polyvinyl Alcohol (PVA) as an adhesive and molded in the shape of a filter with two variations hole sizes with a diameter of 1 cm and 0.3 cm. Composite filter performance tests were carried out using a gas analyzer. The best result for reducing gas emissions occurred at a concentration of TiO2 15% with reduction power to reduce CO gas emission up to 53.79% and HC gas emission up to 55.57%.
研究的目的是观察在活性炭材料上添加TiO2对减少CO和HC气体排放的影响。采用10% (w/v) ZnCl2活化剂,在600℃的炭化温度下合成了活性炭(AC)。采用简单的混合法制备了AC/TiO2复合材料。该工艺得到TiO2浓度为0%、10%、15%、20%和25%的TiO2改性活性炭材料。用扫描电镜(SEM)观察了AC/TiO2的表面形貌。在作为CO和HC气体减排材料的应用中,将混合AC/TiO2的结果与10% (w/v)的聚乙烯醇(PVA)溶液作为粘合剂混合,并模压成直径为1 cm和0.3 cm的两种孔径的过滤器形状。利用气体分析仪对复合过滤器进行了性能测试。TiO2浓度为15%时的气体减排效果最好,CO和HC气体减排功率分别为53.79%和55.57%。
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引用次数: 0
GIS Scoring and Overlay Methods for Mapping Landslide Vulnerability in Lebak Regency, Banten 万丹勒巴克县滑坡易损性GIS评分与叠加方法
Pub Date : 2023-04-08 DOI: 10.20527/flux.v20i1.15057
Sandri Erfani, Muhammad Naimullah, Denta Winardi
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引用次数: 2
Alternative Energy of Biomass Briquettes from Alaban Wood and Rubber Seed Shells with Rubber Sap Adhesive and Dyeing Used Cooking Oil 用橡胶液胶粘剂和废油染色制备阿拉木和橡胶籽壳生物质压块的替代能源研究
Pub Date : 2023-03-21 DOI: 10.20527/flux.v20i1.15026
N. H. Haryanti, N. Annisa, S. Suryajaya, Surini Surini
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引用次数: 0
Identification of Landslide-Prone Areas in Sanggau Regency, West Kalimantan using GIS and Resistivity Method 基于GIS和电阻率法的西加里曼丹Sanggau县滑坡易发区识别
Pub Date : 2023-03-20 DOI: 10.20527/flux.v20i1.12449
R. Perdhana, N. Nurhasanah, R. Adriat
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引用次数: 0
Neutron Generated during Proton Bombardment in Water Molecule 水分子中质子轰击产生的中子
Pub Date : 2023-03-15 DOI: 10.20527/flux.v20i1.14684
Gusti Atika Urfa, N. Sari, A. V. Nasrulloh
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引用次数: 0
Analysis of Liquefaction Potential Based on Seismic Wave Velocity in Bengkulu City 基于地震波速度的明古鲁市液化潜力分析
Pub Date : 2023-03-10 DOI: 10.20527/flux.v20i1.15243
A. Setiawan, Della Zakia Sholeha, Alfata Kausari, Arif Ismul Hadi
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引用次数: 0
Analysis of Seismicity Level and Coulomb Stress Changes in the Central Sulawesi Region in 1996-2022 1996-2022年苏拉威西中部地区地震活动水平和库仑应力变化分析
Pub Date : 2023-03-08 DOI: 10.20527/flux.v20i1.14273
L. H. Lubis, Ratni Sirait, Dhiau Rahman Fikri
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引用次数: 0
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