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Study of Forming Accuracy and Surface Finish in Multi-Stage Robot-Assisted Incremental Sheet Hydroforming of AA6061 AA6061多阶段机器人辅助增厚成形精度及表面光洁度研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-23 DOI: 10.1007/s11665-025-12397-7
Ravi Prakash Singh, Santosh Kumar, Sudarshan Choudhary, Edward James Brambley, Pankaj Kumar Singh, Amrut Mullay

This study presents the development of multi-stage robot-assisted incremental sheet hydroforming (MSRAISHF), an innovative process that integrates multi-stage incremental sheet forming (MSISF) with hydroforming to enhance formability, thickness uniformity, and surface finish in aluminum alloy AA6061 sheets. MSRAISHF was compared with single-stage RAISHF, revealing that multi-stage processing produced fixed wall angle conical frustums (FWACF) with improved forming depths and enhanced thickness uniformity along the wall of the cone. Notably, MSRAISHF reduced spring back by 60%, significantly improving the geometric accuracy of the formed parts. Surface quality also improved markedly, with reduced surface roughness and the suppression of undesired waviness commonly observed in single-stage RAISHF. To further assess the effect of multiple forming stages on surface characteristics, a Variable Wall Angle Stepped Conical Frustum (VWASCF) was designed. This sample was used to analyze the influence of forming stages on thickness distribution and surface finish. The results indicate that MSRAISHF is effective for producing sheet metal parts with improved surface finish and dimensional stability, making it suitable for applications requiring high accuracy and surface quality.

本研究提出了多阶段机器人辅助增量板液压成形(MSRAISHF)的开发,这是一种将多阶段增量板成形(MSISF)与液压成形相结合的创新工艺,可提高铝合金AA6061板的成形性、厚度均匀性和表面光洁度。将MSRAISHF与单段RAISHF进行比较,发现多段加工产生的固定壁角锥体(FWACF)成形深度提高,锥体壁厚均匀性增强。值得注意的是,MSRAISHF减少了60%的回弹,显著提高了成形零件的几何精度。表面质量也得到了显著改善,表面粗糙度降低,抑制了单级RAISHF中常见的不希望看到的波浪。为了进一步评估多个成形阶段对表面特性的影响,设计了变壁角阶梯式锥形锥台(VWASCF)。利用该样品分析了成形阶段对厚度分布和表面光洁度的影响。结果表明,MSRAISHF可以有效地生产出具有良好表面光洁度和尺寸稳定性的钣金件,适用于对精度和表面质量要求较高的应用。
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引用次数: 0
Investigation on the Augmentation of Corrosion Resistance in Zn-Al Coating via ZIF-8 Hydrophobic Films ZIF-8疏水膜增强Zn-Al涂层耐蚀性的研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-23 DOI: 10.1007/s11665-025-12034-3
Weiyi Zhang, Xinwei Zhang, Ti Zhang, Qingkun Meng, Yanwei Sui, Fuxiang Wei, Bin Xiao, Changjiang Zhang, Jiqiu Qi

This study investigates the enhancement of corrosion resistance in Zn-Al coatings by the application of novel ZIF-8 hydrophobic films, synthesized using a secondary growth method with varying molar ratios. The effectiveness of ZIF-8 films was assessed through electrochemical corrosion tests, scanning electron microscopy, atomic force microscopy, and electron probe microanalysis. Results indicate that ZIF-8 films prepared by the secondary growth method exhibit greater density and smoothness compared to those produced by traditional methods. The ZIF-8 hydrophobic films significantly improved the corrosion resistance of Zn-Al coating, with the ZIF-8 film at a molar ratio of 1:16 demonstrating the best corrosion protection performance. After 2 h of corrosion, ZIF-8 films with a molar ratio of 1:16 demonstrated the highest corrosion resistance, achieving a charge transfer resistance (Rct) of 13218 Ω/cm2, which is two orders of magnitude higher than that of uncoated Zn-Al coating. ZIF-8 films exhibited significant corrosion protection potential on Zn-Al coatings, providing important theoretical and experimental support for the development of high-performance corrosion-resistant coating. This has broad application prospects, particularly in corrosion protection for metal structures in bridges and transportation infrastructure, such as the main cables of offshore bridges and cross-sea bridges.

本文研究了采用二次生长方法合成的新型ZIF-8疏水薄膜对Zn-Al涂层耐腐蚀性能的增强。通过电化学腐蚀试验、扫描电镜、原子力显微镜和电子探针显微分析来评估ZIF-8薄膜的有效性。结果表明,与传统方法制备的ZIF-8薄膜相比,二次生长法制备的ZIF-8薄膜具有更高的密度和光滑度。ZIF-8疏水膜显著提高了Zn-Al涂层的耐蚀性,其中摩尔比为1:16的ZIF-8膜的防腐性能最好。腐蚀2h后,摩尔比为1:16的ZIF-8膜的耐蚀性最高,电荷转移电阻(Rct)为13218 Ω/cm2,比未涂覆Zn-Al膜提高了2个数量级。ZIF-8薄膜在Zn-Al涂层上表现出显著的防腐潜力,为高性能耐蚀涂层的发展提供了重要的理论和实验支持。这在桥梁和交通基础设施金属结构的防腐方面具有广阔的应用前景,如海上桥梁和跨海桥梁的主缆。
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引用次数: 0
Simultaneously Enhanced Strength and Plasticity of 2024 Aluminum Alloy Fusion Welds by Sc/Zr Microalloyed AlMg6 Filler Sc/Zr微合金化AlMg6填料同时提高2024铝合金熔焊焊缝的强度和塑性
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-23 DOI: 10.1007/s11665-025-11925-9
Renyao Qin, Guohui Zhang, Zhiqi Qu, Bingqing Chen, Bingbing Sun, Jian Zhang, Yipeng Wang, Hongbin Zhu, Jie Ren

The demand for high-strength and low-defect aluminum alloy welded structures has led to significant challenges in fusion welding technology, which is largely influenced by filler materials. This paper introduced a Sc/Zr microalloyed AlMg6 (AlMg6ScZr) filler wire for the welding of 2024 aluminum alloys. An AlCu4Mg1 filler wire was adopted for comparative analysis. Results demonstrate that the addition of AlMg6ScZr filler resulted in a better homogeneity of grain structure and a significant grain refinement in the weld zone, with a remarkable reduction in grain size of 59.3%. In contrast to the AlCu4Mg1 filler, no phases were continuously distributed along the grain boundaries in the weld zone. Nanoscale spherical Al3(Sc, Zr) phase formed on the surface of the α-Al matrix and together with the separately distributed bone-like α-Al + S-Al2CuMg + β-Al3Mg2 eutectics. The addition of AlMg6ScZr filler considerably improved the uniformity of hardness distribution, with a slight reduction of hardness values in the weld zone. The UTS and elongation were 318.0 MPa and 15.0%, respectively, showing an increase of 7.4% in UTS and 200% in elongation compared to the welds with AlCu4Mg1 filler. The results provide a valuable basis for obtaining high-performance fusion welds of high-strength aluminum alloys.

对高强度、低缺陷铝合金焊接结构的需求给熔焊技术带来了巨大的挑战,而熔焊技术在很大程度上受填充材料的影响。介绍了一种用于2024铝合金焊接的Sc/Zr微合金化AlMg6 (AlMg6ScZr)填充焊丝。采用AlCu4Mg1填充丝进行对比分析。结果表明:AlMg6ScZr钎料的加入使焊缝区晶粒组织均匀性更好,晶粒细化程度显著提高,晶粒尺寸减小幅度达59.3%;与AlCu4Mg1钎料相比,焊缝区没有沿晶界连续分布的相。α-Al基体表面形成了纳米级球形Al3(Sc, Zr)相,并形成了单独分布的骨状α-Al + S-Al2CuMg + β-Al3Mg2共晶。AlMg6ScZr填料的加入显著改善了硬度分布的均匀性,焊接区硬度值略有降低。与添加AlCu4Mg1钎料的焊缝相比,其焊接强度和伸长率分别为318.0 MPa和15.0%,焊接强度和伸长率分别提高7.4%和200%。研究结果为获得高性能高强度铝合金熔焊件提供了有价值的依据。
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引用次数: 0
Consequence of Rotating Arc GMAW Welding Parameters on Metallurgical and Mechanical Properties of Welded Joints of Low Carbon Steel 旋转电弧GMAW焊接参数对低碳钢焊接接头冶金性能和力学性能的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-21 DOI: 10.1007/s11665-025-12400-1
Anshika Gupta, N. Yuvraj,  Vipin

Conventional arc welding of low-carbon steel (LCS) often results in challenges such as extensive edge preparation, porosity, inadequate sidewall fusion, and a broad heat-affected zone, compromising joint integrity. To address these issues, this study explores the potential of rotating arc gas metal arc welding (RA-GMAW) as an advanced welding technique to enhance weld quality. The study investigates the RA-GMAW process on 6 mm thick AISI 1020 steel plates, focusing on the influence of arc rotation speed (ARS), arc rotating diameter (ARD), and gas flow rate (GFR). A face-centered central composite design (FCCCD) based on response surface methodology (RSM) is used to optimize process parameters. Analysis of variance (ANOVA) results reveal ARS as the most influential factor, followed by ARD and GFR. EBSD analysis demonstrates that increased ARS leads to finer grains and higher proportions of high-angle grain boundaries (HAGBs), enhancing mechanical properties. The EBSD results indicated that the welded sample 10 (1500 rpm, 5 mm, 14 l/min) shows a fine grain structure with an AGS of 5.09 ± 0.11 µm and a HAGB fraction of 54.12%. The optimized welding parameters, consisting of an ARS of 1500 rpm, ARD of 5 mm, and GFR of 14 l/min, yielded superior mechanical properties, including a maximum tensile strength of approximately 491 MPa, an elongation of around 15.4%, and a fusion zone hardness of about 208 HV. The RA-GMAW joint demonstrated an increase in tensile strength of 5.59% compared to the base metal and 26.1% compared to the non-rotating GMAW joint, highlighting the effectiveness of the RA-GMAW process in producing high-quality welds.

传统的低碳钢(LCS)电弧焊通常会带来一些挑战,如边缘准备不充分、气孔、侧壁熔合不充分、热影响区宽,从而影响接头的完整性。为了解决这些问题,本研究探讨了旋转电弧气体金属电弧焊(RA-GMAW)作为一种提高焊接质量的先进焊接技术的潜力。研究了6mm厚AISI 1020钢板的RA-GMAW工艺,重点研究了电弧转速(ARS)、电弧旋转直径(ARD)和气体流量(GFR)对RA-GMAW工艺的影响。采用基于响应面法(RSM)的面心中心复合设计(FCCCD)优化工艺参数。方差分析(ANOVA)结果显示ARS是最重要的影响因素,其次是ARD和GFR。EBSD分析表明,ARS的增加导致晶粒更细,高角晶界(HAGBs)的比例更高,从而提高了力学性能。EBSD结果表明,焊接样品10 (1500 rpm, 5 mm, 14 l/min)呈现出细晶粒结构,AGS为5.09±0.11µm, HAGB分数为54.12%。优化后的焊接参数为:ARS为1500 rpm, ARD为5 mm, GFR为14 l/min,获得了优异的机械性能,包括最大抗拉强度约为491 MPa,伸长率约为15.4%,熔合区硬度约为208 HV。与母材相比,RA-GMAW接头的抗拉强度提高了5.59%,与非旋转GMAW接头相比,抗拉强度提高了26.1%,凸显了RA-GMAW工艺在生产高质量焊缝方面的有效性。
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引用次数: 0
Deposition Rate–Microstructure-Property Relations for Additive Friction Stir Deposited 6061-T6 Al-Mg-Si Alloy 添加搅拌摩擦沉积6061-T6 Al-Mg-Si合金沉积速率-显微组织-性能关系
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-21 DOI: 10.1007/s11665-025-12373-1
Gang Chen, Leibo Wu, Jingyin Xu, Wei Jiang, Ze Liu, Zhixiong Zhu, Fengfeng Hu

Additive Friction Stir Deposition (AFSD) is an emerging solid-state additive manufacturing technology that can deposit metals without melting and solidification. This characteristic makes AFSD a potential alternative to traditional fusion-based additive manufacturing technologies. Although deposition rate is closely related to the additive efficiency of AFSD, its effects on microstructural and mechanical properties remain unclear. This study investigates the effects of deposition rate on microstructure and mechanical properties by conducting experiments at deposition rates of 0.2, 0.3, 0.4, 0.5, 0.6, and 1. AFSD multi-layer structures were fabricated at different deposition rates, and specimens for microstructure and mechanical property testing were extracted using wire-cut EDM. The relationship between deposition rate, microstructure, and mechanical properties was analyzed through electron backscatter diffraction (EBSD), tensile testing, and hardness testing. At deposition rates of 0.2, 0.4, and 0.6, the average grain sizes were 9.5, 11.8, and 13.8 μm, respectively, indicating a positive correlation between grain size and deposition rate. However, the ultimate tensile strength decreased with increasing deposition rate, reaching 215, 203, and 196 MPa at deposition rates of 0.2, 0.4, and 0.6, respectively. Combining test results for heat input, friction torque, and axial force, the study demonstrates that variations in deposition rate induce changes in thermal and force inputs during the AFSD process, subsequently driving the evolution of microstructure and mechanical properties. Specifically, increased deposition rate leads to higher plastic deformation heat input and greater axial force, ultimately resulting in grain growth and diminished mechanical performance. The results provide an important reference for optimizing AFSD and increasing additive manufacturing efficiency.

添加剂搅拌摩擦沉积(AFSD)是一种新兴的固体增材制造技术,可以在不熔化和凝固的情况下沉积金属。这一特点使AFSD成为传统基于融合的增材制造技术的潜在替代品。虽然沉积速率与AFSD的添加效率密切相关,但其对微观组织和力学性能的影响尚不清楚。研究了沉积速率为0.2、0.3、0.4、0.5、0.6和1时,沉积速率对合金微观组织和力学性能的影响。以不同的沉积速率制备了AFSD多层结构,并用电火花线切割提取了显微组织和力学性能测试试样。通过电子背散射衍射(EBSD)、拉伸测试和硬度测试分析了沉积速率、显微组织和力学性能之间的关系。在沉积速率为0.2、0.4和0.6时,平均晶粒尺寸分别为9.5、11.8和13.8 μm,晶粒尺寸与沉积速率呈正相关。随着沉积速率的增加,合金的抗拉强度逐渐降低,在沉积速率为0.2、0.4和0.6时,合金的抗拉强度分别达到215、203和196 MPa。结合热输入、摩擦扭矩和轴向力的测试结果,研究表明,在AFSD过程中,沉积速率的变化会引起热输入和力输入的变化,从而驱动微观结构和力学性能的演变。具体而言,沉积速率的增加导致塑性变形热输入增大,轴向力增大,最终导致晶粒长大,力学性能下降。研究结果为优化AFSD和提高增材制造效率提供了重要参考。
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引用次数: 0
Correction: Evolution Law of Plastic Damage in Circumferential Welded Joints of X80 Pipeline Steel 修正:X80管线钢环向焊接接头塑性损伤演化规律
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-21 DOI: 10.1007/s11665-025-12507-5
Wenhui Liu, Sen Wang, Jianjun Gou, Xueqi Sun, Lifeng Fan
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引用次数: 0
Microstructure and Mechanical Properties of 7136 Al Thick Plates at Different Locations in Homogenized, Hot-Rolled, and Aged Conditions 7136 Al厚板在均匀化、热轧和时效条件下不同位置的组织与力学性能
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-20 DOI: 10.1007/s11665-025-12391-z
Jiale Man, Yizhe Wu, Fengchun Wang, Lei Wang, Baoxia Ma, Yicheng Feng

In this study, the microstructure and mechanical properties of 7136 aluminum alloy thick plates (with a final thickness of 80 mm) at different position in homogenized, hot-rolled, and aged conditions were studied. The results demonstrate that the volume fraction of the second phase in homogenized ingots and hot-rolled thick plate exhibits the highest value at position 1/4 H, followed by surface, and the lowest value at position 1/2 H. Hot-rolled thick plate was more prone to dynamic recrystallization near the surface, and the volume fraction of recrystallization gradually decreases along the surface toward the center, resulting in uneven texture and mechanical properties. The maximum difference in tensile strength among the alloy samples taken at the different thickness positions in the TD and RD directions was 14.2%. Via aging, the alloy uniformly precipitates a large number of nano-scale η′ precipitates in different thicknesses position, and the size and volume fraction of the η′ phase exhibit negligible variations. Consequently, the mechanical properties demonstrate minimal variation, with a maximum tensile strength of 618.9 MPa and differences across various orientations and thicknesses position remaining below 6%.

研究了7136铝合金厚板(终厚为80 mm)在均匀化、热轧和时效条件下不同位置的组织和力学性能。结果表明:均匀化钢锭和热轧厚板中第二相体积分数在1/4 H处最高,表面次之,在1/2 H处最低,热轧厚板在靠近表面处更容易发生动态再结晶,再结晶体积分数沿表面向中心逐渐减小,导致织构和力学性能不均匀;在TD和RD方向不同厚度位置的合金试样抗拉强度最大差异为14.2%。时效过程中,合金在不同厚度位置均匀析出大量纳米级η′相,η′相的尺寸和体积分数变化可以忽略不计。因此,力学性能变化最小,最大抗拉强度为618.9 MPa,不同取向和厚度位置的差异保持在6%以下。
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引用次数: 0
Effect of Printing Parameters on Microstructure and Properties of Fe-3 wt.% Si Prepared by Metal Fused Filament Fabrication 打印参数对金属熔丝法制备fe - 3wt .% Si微结构和性能的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-20 DOI: 10.1007/s11665-025-12385-x
Qingqing Pan, Bingchen He, Wei Mai, Chenyu Wang, Chen Ou, Ziyang Zhang, Haiying Zhang, Shuangfei Yan, Jingguang Peng

Metal fused filament fabrication (MFFF), a type of additive manufacturing technology, involves heating and extruding metal filament materials to build objects layer by layer. This paper investigates the influence of printing parameters, including fill flow rate, raster angle, and building direction, on the microstructural characteristics, tensile properties, and magnetic properties of Fe-3 wt.% Si prepared by MFFF. Results indicate that porosity initially decreases and then increases with increasing infill flowrate, reaching a minimum at 108%. Different raster angles exhibit anisotropy, and the print direction significantly impacts porosity and properties. Specimens printed at an infill flowrate of 108%, with a raster angle of 45°/− 45°, and in a horizontal direction exhibit the lowest porosity, the anisotropy is not obvious, with a tensile strength of 505 MPa and yield strength of 355 MPa, maximum permeability is 11.37 mH/m, the saturation magnetic induction intensity is 1637 mT, and the initial permeability is 0.8541 mH/m.

金属熔丝制造(MFFF)是一种增材制造技术,涉及加热和挤压金属丝材料,逐层构建物体。本文研究了填充流量、栅格角度和构筑方向等印刷参数对MFFF法制备的fe - 3wt .% Si材料的显微组织特征、拉伸性能和磁性能的影响。结果表明:随着充填流量的增加,孔隙度先减小后增大,在108%时达到最小值;不同的光栅角度表现出各向异性,打印方向对孔隙度和性能影响显著。在填充流量为108%、栅格角为45°/−45°、水平方向上打印的试样孔隙率最低,各向异性不明显,拉伸强度为505 MPa,屈服强度为355 MPa,最大渗透率为11.37 mH/m,饱和磁感应强度为1637 mT,初始渗透率为0.8541 mH/m。
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引用次数: 0
Investigating the Welding Limit of Copper Foils to a Tab for Battery Applications with a Green Laser 用绿色激光研究铜箔在电池片上的焊接极限
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-20 DOI: 10.1007/s11665-025-11438-5
Teresa J. Rinker, Masoud M. Pour, Weiling Wen, Megan E. McGovern, Sen Xiang, Wayne Cai

The lithium-ion battery cells in electric vehicles are created in part by welding many layers of electrode foils to a tab to create the cell lead. While this process has conventionally involved an ultrasonic welding process, there is a desire to replace this process with laser welding to address certain limitations and remove a process step. The literature surrounding laser welding of multilayer thin foils to tabs is limited. This research aims to address this gap by developing a process window for green laser welding of multilayer foil-to-tab copper welds. Multiple copper foil layers, from 30 layers to 90 layers, were joined to a copper tab using a green laser with varying power and speed. The welds were analyzed based on micrographs, x-ray, failure load, and fracture mode. Process windows were developed for the various stack-ups. It was observed that very low heat input results in a narrow weld width and hence interfacial fracture under lap-shear loading. With suitable power and speed parameters, a process window exists where the welds have a minimum interface width greater than 180 µm, leading to fracture at the foil-weld fusion boundary. It was observed that excessive weld energy results in a weld with high porosity. Foil cut-through associated with excessive surface variation occurred under high speed and high-power conditions. As the number of foil layers increased, the process window is reduced due to the increasing number of defects present.

电动汽车中的锂离子电池部分是通过将多层电极箔焊接到一个标签上来制造电池引线的。虽然该工艺传统上涉及超声波焊接工艺,但人们希望用激光焊接取代该工艺,以解决某些限制并去除工艺步骤。关于激光焊接多层薄箔片的研究文献有限。本研究旨在通过开发多层箔片铜焊缝的绿色激光焊接工艺窗口来解决这一空白。多个铜箔层,从30层到90层,使用不同功率和速度的绿色激光连接到铜标签上。根据显微照片、x射线、失效载荷和断裂模式对焊缝进行了分析。为不同的堆栈开发了进程窗口。结果表明,极低的热输入导致焊缝宽度窄,从而导致界面在搭接剪切载荷下断裂。在适当的功率和速度参数下,存在焊缝最小界面宽度大于180µm的工艺窗口,导致箔焊融合边界处发生断裂。结果表明,过高的焊缝能量导致焊缝气孔率高。在高速和高功率条件下,与表面变化过大有关的箔穿断。随着箔层数的增加,由于缺陷数量的增加,工艺窗口减少。
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引用次数: 0
Enhancement of Mechanical and Oxidation Resistance in S390 High-Speed Steel via Graphene Nano-sheet Addition and Heat Treatment 通过添加纳米石墨烯片和热处理增强S390高速钢的机械和抗氧化性
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-10-20 DOI: 10.1007/s11665-025-12292-1
H. M. Zidan, Omayma A. El-Kady, A. Abd-Elwahed, Hossam M. Yehia

This study investigates the effects of incorporating surface-metallized graphene nano-sheets (GNS), specifically silver-coated GNS, into S390 high-speed steel (HSS) produced via powder metallurgy. The research focuses on evaluating the influence of GNS addition and post-sintering heat treatment on density, microstructure, hardness, wear resistance, and oxidation resistance. The silver coating on GNS improves interfacial bonding with the steel matrix, enhancing load transfer and dispersion. Results revealed that although the addition of GNS slightly decreased the density of sintered samples due to their low mass and increased porosity, heat treatment mitigated this effect by promoting densification. An optimal improvement was observed with 1 wt.% GNS, which resulted in a significant increase in hardness up to 957.8 HV after heat treatment compared to 215 HV for the untreated matrix. Wear resistance improved progressively with increasing GNS content, with heat treatment further reducing wear rates by 80% for the base matrix and 20% for the 1 wt.% GNS sample. Oxidation resistance was also enhanced due to the barrier effect of graphene and the formation of protective oxide films during heat treatment. These synergistic effects make silver-coated GNS a promising reinforcement for improving the mechanical and chemical performance of S390 HSS in high-temperature and high-wear applications.

本文研究了将表面金属化石墨烯纳米片(GNS),特别是镀银石墨烯纳米片(GNS)掺入粉末冶金生产的S390高速钢(HSS)中的效果。研究重点是评价GNS添加和烧结后热处理对合金密度、显微组织、硬度、耐磨性和抗氧化性的影响。银涂层改善了GNS与钢基体的界面结合,增强了载荷传递和分散。结果表明,虽然GNS的加入使烧结样品的密度略有降低,但由于其质量低,孔隙率增加,热处理通过促进致密化来减轻这种影响。当GNS添加量为1 wt.%时,硬度得到了最佳改善,与未处理基体的215 HV相比,热处理后硬度显著提高至957.8 HV。随着GNS含量的增加,耐磨性逐渐提高,热处理进一步降低了基体80%的磨损率,1 wt.% GNS样品的磨损率降低了20%。由于石墨烯的阻隔作用和热处理过程中形成的氧化保护膜,抗氧化性也得到了增强。这些协同效应使镀银GNS成为一种有希望改善S390 HSS在高温和高磨损应用中的机械和化学性能的增强剂。
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引用次数: 0
期刊
Journal of Materials Engineering and Performance
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