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Effect of Change in Strain Path by Cold Rolling on the Microstructure and Texture of Nb-10Hf-1Ti Refractory Alloy 冷轧应变路径变化对Nb-10Hf-1Ti耐火合金组织和织构的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-07-01 DOI: 10.1007/s11665-025-11637-0
Yogesh Singh, S. Manojkumar, Arka Ghosh, Kumud Kant Mehta

This study investigated the effect of the strain path followed during the unidirectional and two-step cross-rolling on the microstructure, texture, and mechanical properties of Nb-10Hf-1Ti refractory alloy (1 mm thick sheet). It has been demonstrated for the first time that the refractory alloy Nb-10Hf-1Ti can be smoothly cross-rolled like unidirectional rolling. The cross-rolling results in a stronger texture as compared to the unidirectional rolling. The development of a strong texture during cross-rolling as a result of a change in strain path is due to a partial texture transition from the γ-fiber to the α-fiber and strengthening of the texture components (left{001right}langle 110rangle). The grains are observed to be significantly finer after unidirectional rolling as compared to cross-rolling. A mixture of fine and coarse grains is observed after cross-rolling. The finer grains are related to the γ-fiber (〈111〉IIND)) while the coarser grains are associated with α-fiber (〈110〉IIRD). The visco-plastic self-consistent (VPSC) model establishes that the average number of active slip systems is significantly higher for cross-rolled samples than the unidirectional rolled. The presence of a higher number of active slip systems in cross-rolled relaxes the deformation constraints, resists grain fragmentation, and results in coarse as well as fine grains. The unidirectional rolling shows less deformation constraint and a higher extent of grain fragmentation which results in overall finer grains. The higher dislocation density, higher number of slip systems, and formation of cellular dislocation network results in higher work hardening of the cross-rolled sample. The highly work-hardened cross-rolled sample displays early attainment of saturation stress and results in moderately higher tensile strength compared to the unidirectional rolled sample.

研究了单向和两步交叉轧制过程中应变路径对Nb-10Hf-1Ti耐火合金(1mm厚板材)显微组织、织构和力学性能的影响。首次证明了Nb-10Hf-1Ti耐火合金可以像单向轧制一样进行平滑的交叉轧制。与单向轧制相比,交叉轧制产生更强的织构。由于应变路径的改变,在交叉轧制过程中形成了强织构,这是由于织构从γ-纤维向α-纤维的部分转变和织构成分的增强(left{001right}langle 110rangle)。与交叉轧制相比,单向轧制后的晶粒明显更细。在交叉轧制后,观察到细晶粒和粗晶粒的混合。细颗粒与γ-纤维(< 111 > IIRD)有关,粗颗粒与α-纤维(< 110 > IIRD)有关。粘塑性自一致(VPSC)模型表明,横向轧制样品的主动滑移系统的平均数量明显高于单向轧制样品。交叉轧制中大量主动滑移系统的存在使变形约束松弛,抑制了晶粒破碎,导致粗晶和细晶同时存在。单向轧制的变形约束较小,晶粒碎裂程度较高,整体晶粒较细。较高的位错密度、较多的滑移体系和胞状位错网络的形成导致了较高的加工硬化。与单向轧制样品相比,高度加工硬化的交叉轧制样品显示出较早达到饱和应力并具有较高的抗拉强度。
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引用次数: 0
The Low-Velocity Impact Behavior and Energy Absorption Characteristics of Aluminum Foam Sandwich Structures 泡沫铝夹层结构低速冲击性能及吸能特性研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11622-7
Baixing Deng, Junshan Zhang, Daoyuan Li, Yukun An, Youdong Xing, Hongtao Wang

In this paper, closed-cell aluminum foam sandwich structures with metallurgically bonded interfaces were fabricated utilizing a compression-powder metallurgical foaming technique. The aluminum foam sandwich structure was subjected to low-velocity impact tests with single and repetitive impact energy using a drop hammer testing machine. The mechanical responses, impact damage processes, and energy absorption characteristics with different impact energies and sandwich structure thicknesses were investigated through experimental testing. Based on the energy absorption index, the influence of specimen thickness on the energy absorption performance of the aluminum foam sandwich structure was quantitatively assessed. The results of the study can provide an important reference for the design of collision-resistant and energy-absorbing aluminum foam sandwich structures under low-velocity impact. To provide a theoretical basis for developing new lightweight aluminum foam sandwich structures with high impact resistance.

本文采用压缩粉末冶金发泡技术制备了具有冶金粘结界面的闭孔泡沫铝夹层结构。利用落锤试验机对泡沫铝夹层结构进行了单次和多次低速冲击试验。通过试验研究了不同冲击能量和夹层结构厚度下的力学响应、冲击损伤过程和能量吸收特性。基于吸能指数,定量评价了试样厚度对泡沫铝夹层结构吸能性能的影响。研究结果可为低速冲击下泡沫铝夹层结构的抗碰撞吸能设计提供重要参考。为开发新型轻质高抗冲击泡沫铝夹层结构提供理论依据。
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引用次数: 0
Resin-Bonded Discontinuous Grinding Tools for MO40 Steel Manufactured by Vat Photopolymerization 还原光聚合MO40钢用树脂结合不连续磨具
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11613-8
Babak Houshmand, Seyed Mohsen Safavi

Grinding remains a critical finishing process in manufacturing, yet it is often constrained by excessive friction, thermal damage, and inefficient coolant delivery—especially when machining hard-to-grind materials like MO40 steel. This study explores the design and evaluation of five innovative grinding tools, fabricated using vat photopolymerization-based 3D printing, each featuring distinct geometric modifications to enhance grinding performance. The tested designs included: a Standard Tool (ST), a Cylindrical Cooling Channel Tool (CCT), a Venturi Cooling Tool (VCT), and two V-grooved tools (T100 and T200) tailored for improved chip evacuation and thermal regulation. Experimental assessments revealed that structured geometries significantly influence tool behavior. Among them, the T100 tool exhibited the highest grinding ratio, lowest wear rate, and finest surface finish, attributed to enhanced coolant flow and reduced thermal load. These findings demonstrate the potential of geometrically engineered, 3D-printed tools to overcome conventional grinding limitations, paving the way for more efficient and sustainable machining of advanced alloys.

磨削仍然是制造业中一个关键的精加工过程,但它经常受到过度摩擦、热损伤和冷却剂输送效率低下的限制,尤其是在加工难磨削的材料(如MO40钢)时。本研究探索了五种创新研磨工具的设计和评估,这些工具采用基于还原光聚合的3D打印技术制造,每个工具都具有不同的几何修改以提高研磨性能。测试设计包括:一个标准工具(ST)、一个圆柱形冷却通道工具(CCT)、一个文丘里冷却工具(VCT)和两个v形槽工具(T100和T200),这些工具是为改进芯片排出和热调节而定制的。实验评估表明,结构几何形状显著影响工具的性能。其中,T100刀具的磨削率最高,磨损率最低,表面光洁度最好,这归功于冷却剂流量的增加和热负荷的降低。这些发现证明了几何工程3d打印工具克服传统磨削限制的潜力,为更高效和可持续的高级合金加工铺平了道路。
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引用次数: 0
Experimental Study on Response Characteristics of Detonation Mode to Strain Field Containing Heterogeneous Interfacial Elements 爆轰模式对含非均质界面元应变场响应特性的实验研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11573-z
Yong Zhao, Renshu Yang, Yu Wang, Dayang Yan, Songlin He, Zhongjian Ma

As a common structure in the material medium, the heterogeneous interfacial structure redistributes the stress field after the explosion stress wave acts on the material, which is easy to cause damage or even fracture of the material. In order to study the evolution process and distribution characteristics of strain field in media with heterogeneous interfaces under different initiation modes, an ultra-high-speed digital image correlation experimental system was established. Chloroform bonded polycarbonate (PC) board and polymethylmethacrylate (PMMA) board were used to construct heterogeneous interface structure. By changing the position of initiation point in PC board, the initiation point near the interface end was defined as hole bottom initiation. When the interface is far away from the end of the hole, the dynamic response characteristics of the explosion stress wave through the heterogeneous interface media are studied. The experimental results show that the interface has different hindering ability to stress waves under different initiation modes. The cracking phenomenon of the interface is macroscopic when only the opening is used, which is mainly due to the stress concentration area formed at the interface due to the action of reflected transverse tension waves. The contribution of detonation mode to the tensile and compressive strain field of PMMA medium is different. The influence on the transverse compressive strain field is mainly reflected in the strain field strength, while the influence on the longitudinal tensile strain field is mainly reflected in the strain field strength and strain zone morphology distribution. Under different initiation modes, the absolute value of the attenuation index in PC medium is greater than that of PMMA when it is close to the end of the gun hole, and the PMMA is larger when it is far away from the end. The difference is shown in the distribution of strain attenuation index in different media.

非均质界面结构作为材料介质中的一种常见结构,在爆炸应力波作用于材料后,会使应力场重新分布,容易造成材料的损伤甚至断裂。为了研究不同起爆模式下非均质界面介质中应变场的演化过程和分布特征,建立了超高速数字图像相关实验系统。采用氯仿键合聚碳酸酯(PC)板和聚甲基丙烯酸甲酯(PMMA)板构建非均相界面结构。通过改变PC板中起爆点的位置,将靠近接口端的起爆点定义为孔底起爆点。当界面距离孔端较远时,研究了爆炸应力波在非均质界面介质中的动态响应特性。实验结果表明,在不同起爆模式下,界面对应力波的抑制能力不同。仅使用开口时,界面的开裂现象是宏观的,这主要是由于反射的横向张力波在界面处形成应力集中区。爆轰方式对PMMA介质拉伸应变场和压缩应变场的贡献不同。对横向压缩应变场的影响主要体现在应变场强度上,而对纵向拉伸应变场的影响主要体现在应变场强度和应变区形貌分布上。在不同起爆方式下,PC介质中衰减指数的绝对值在接近炮孔端部时大于PMMA,远离炮孔端部时PMMA衰减指数的绝对值更大。应变衰减指数在不同介质中的分布存在差异。
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引用次数: 0
Role of Microstructural Modification in the Slurry Erosion Behavior of Friction Stir Processed AZ31 Magnesium Alloy 显微组织改性对搅拌摩擦处理AZ31镁合金浆液侵蚀行为的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11636-1
S. Annamalai, Md Saad Patel, B. Anand Ronald, Ariful Rahaman, R. Jose Immanuel

Material degradation due to slurry erosive wear affects components exposed to particle-entrained slurries. This study investigates the slurry erosion behavior of AZ31 Magnesium alloy processed through friction stir processing. The base and processed materials were subjected to slurry jet erosion test under various impingement angles. Alumina abrasive particles of 700 µm nominal size were used as the erodent. Experimental results indicated that the base and processed materials exhibit ductile erosion behavior, with maximum mass loss occurring at an oblique angle of 30°. With increase in impact angle, mass loss is found to be decreased. Compared to the unprocessed alloy, material processed through friction stir processing at 1500 rpm tool rotation speed and 60 mm/min traverse speed showed minor mass loss at all impingement angles. Surface profile analysis revealed a ‘U’-shaped scar profile, regardless of the impingement angle. Furthermore, surface roughness decreased with increasing impact angle. Scanning electron microscopy confirmed that micro-cutting and ploughing mechanisms dominated at shallow angles, while indentation and plastic deformation were more prevalent at higher impingement angles.

由于浆料侵蚀磨损导致的材料退化影响暴露于颗粒夹带浆料中的部件。研究了搅拌摩擦加工AZ31镁合金的料浆侵蚀行为。对基材和加工材料进行了不同冲击角下的料浆射流冲蚀试验。采用公称尺寸为700µm的氧化铝磨料颗粒作为侵蚀剂。试验结果表明,基材和加工材料均表现出韧性侵蚀行为,最大质量损失发生在30°斜角处。随着冲击角的增大,质量损失减小。与未加工的合金相比,在1500转/分钟的刀具转速和60毫米/分钟的横移速度下进行搅拌摩擦加工的材料在所有撞击角下的质量损失都很小。表面轮廓分析显示,无论撞击角度如何,疤痕轮廓都呈“U”型。表面粗糙度随冲击角的增大而减小。扫描电镜证实,微切削和犁耕机制在浅角度下占主导地位,而在高角度下,压痕和塑性变形更为普遍。
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引用次数: 0
Study on Strain Field and Damage Characteristics Caused by the Distribution of Detonation Point 爆震点分布引起的应变场及损伤特性研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11607-6
Yong Zhao, Renshu Yang, Jinjing Zuo, Zhen Liu, Shulin Chen

Due to the transient nature of the blasting process and the complexity of the blasting effect, the number and spatial distribution of detonation points significantly affect the intensity and damage distribution of the strain field in the medium. Based on this, this paper studies the time-varying effect of the spatial position of the detonation point on the strain field and the damage distribution using the digital image correlation method and LS-DYNA numerical simulation. The results indicate that the influence of the number of initiation points along the gun hole on the strain field primarily manifests in the characteristics of strain history and the intensity distribution of the strain field. The axial strain and radial strain exhibit a single peak distribution pattern at a single-point initiation, with the strain intensity gradually increasing in the direction of detonation. In contrast, the strain intensity at two-point initiation exhibits a double peak distribution pattern and presents a symmetrical distribution along the center of the gun hole, significantly enhancing the strain field intensity at the center of the two initiation points. The experimental results of the two-point initiation model are corroborated through the numerical simulation. In general, the damage length can be divided into four expansion stages based on the distance between initiation points. When the distance between the initiation points reaches a certain extent, the damage length at the central position peaks and is no longer influenced by the distance between the initiation points. The damage degree in the center area of the gun hole accurately represents the total energy of the area, and the two physical quantities demonstrate a positive correlation.

由于爆破过程的瞬态性和爆破效果的复杂性,爆震点的数量和空间分布显著影响介质中应变场的强度和损伤分布。基于此,本文采用数字图像相关法和LS-DYNA数值模拟研究了爆点空间位置对应变场和损伤分布的时变影响。结果表明,炮孔起始点数量对应变场的影响主要表现在应变历史特征和应变场强度分布上。轴向应变和径向应变在单点起爆处呈单峰分布,应变强度沿爆轰方向逐渐增大。而两点起爆处的应变强度呈双峰分布,且沿炮孔中心呈对称分布,显著增强了两个起爆点中心的应变场强度。通过数值模拟验证了两点起爆模型的实验结果。一般情况下,根据起爆点之间的距离,损伤长度可分为四个扩展阶段。当起爆点之间的距离达到一定程度时,中心位置的损伤长度达到峰值,不再受起爆点之间距离的影响。炮孔中心区域的损伤程度准确地代表了该区域的总能量,两个物理量呈正相关关系。
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引用次数: 0
Influence of Radio Frequency Magnetron Sputtering on the Microstructure, Mechanical Properties, and Wear Performance of NiTi Alloy Coating on Bearing Steel 射频磁控溅射对轴承钢表面NiTi合金涂层组织、力学性能和磨损性能的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11649-w
Tajamul Ashraf, Pavan Kumar Vangara, Turali Narayana, Deepak Kumar Naik, Shahid Saleem, Koppala Venu Gopal

NiTi thin coatings are increasingly explored to enhance the performance of bearing steel (AISI 52100) components in engineering applications due to their superior mechanical and tribological properties. In this research, NiTi thin coatings were deposited on bearing steel substrates using radio frequency magnetron sputtering. The deposition process was conducted with power densities of 1.72 W/cm2 for Ni and 2.96 W/cm2 for Ti, at a working pressure of 0.4 Pa. The microstructure, mechanical, and tribological properties of the coating were characterized using a range of techniques, including GI-XRD, FESEM, EDS, nanoindentation, scratch testing, 3D surface analysis, and ball-on-disk tribological testing. The composite interlayer developed columnar dendrites extending toward the NiTi coating layer, with a gradient distribution of Ni and Ti elements observed in the elemental spectra. The NiTi coating demonstrated a hardness of 7.57 GPa, marking a 33.9% improvement compared to the AISI 52100 substrate. The tribological performance of the coating was evaluated against a Si3N4 ball using a reciprocating ball-on-disk tribometer under varying loads. The NiTi-coated specimens exhibited superior wear resistance compared to the uncoated AISI 52100 substrate under identical conditions. The NiTi coating achieved the lowest coefficient of friction (0.036) at a 1.5 N sliding load and the minimum wear rate (3.39 × 10−6 mm3/N m) at a 1.25 N sliding load.

NiTi薄涂层由于其优异的机械和摩擦学性能,在工程应用中越来越多地用于提高轴承钢(AISI 52100)部件的性能。在本研究中,采用射频磁控溅射技术在轴承钢基体上沉积了NiTi薄涂层。在0.4 Pa的工作压力下,Ni的功率密度为1.72 W/cm2, Ti的功率密度为2.96 W/cm2。采用GI-XRD、FESEM、EDS、纳米压痕、划痕测试、3D表面分析和球盘摩擦学测试等一系列技术对涂层的微观结构、力学和摩擦学性能进行了表征。复合层间形成向NiTi涂层延伸的柱状枝晶,元素谱显示Ni和Ti元素呈梯度分布。NiTi涂层的硬度为7.57 GPa,比AISI 52100基体提高了33.9%。在不同载荷下,使用往复式球盘摩擦计对涂层的摩擦学性能进行了评估。在相同的条件下,与未涂覆的AISI 52100基体相比,涂覆niti的试样具有更好的耐磨性。在1.5 N滑动载荷下,NiTi涂层的摩擦系数最低(0.036),在1.25 N滑动载荷下,涂层的磨损率最低(3.39 × 10−6 mm3/N m)。
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引用次数: 0
Investigation of Residual Stress in Ice-Covered Milling of Ti-6Al-4V Alloy Thin-Walled Parts with Experimental and Finite Element Simulations Ti-6Al-4V合金薄壁件冰敷铣削残余应力的实验与有限元模拟
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11621-8
Yongquan Jin, Xiaoqiang Wu, Feng Gao, Taiyan Gong, Xiaofan Deng, Rui Xue

Ti-6Al-4 V titanium alloy thin-walled parts are susceptible to fatigue and plastic deformation due to the distribution of machining residual stresses. To reasonably regulate the distribution of residual stress inside the workpiece, this study investigates the influence of freezing temperature, tool coating, tool path, processing temperature, and feed speed on the distribution of residual stress in Ti-6Al-4 V titanium alloy thin-walled parts by combining an ice-covered milling experiment with low-temperature cutting simulation. The results indicate that ice-covered milling significantly enhances residual compressive stress by a range of 46% to 57.14%, with maximum improvement observed at a processing temperature of −15 °C. The AlTiN tool coating, with low friction and hardness, significantly improves the residual compressive stress of titanium alloy thin-walled parts, reaching −483.3 MPa. Compared with annular feeding, lateral and longitudinal feeding can increase the residual compressive stress value by 18.87 and 23.22%, respectively. The error between simulation and experiment can be minimized to 1.69%. Decreasing processing temperature increases residual compressive stress on the workpiece surface. Increasing the feed rate initially increases and then decreases residual tensile stress on the surface. The low-temperature two-dimensional cutting finite element model accurately predicts residual stress distribution in ice-covered milling and provides an effective practical scheme for thin-walled parts with high quality and precision.

ti - 6al - 4v钛合金薄壁件由于加工残余应力的分布,容易产生疲劳和塑性变形。为了合理调节工件内部残余应力的分布,本研究通过冰敷铣削实验和低温切削模拟相结合,研究了冻结温度、刀具涂层、刀具轨迹、加工温度和进给速度对ti - 6al - 4v钛合金薄壁件残余应力分布的影响。结果表明,覆冰铣削可显著提高残余压应力,提高幅度为46% ~ 57.14%,在加工温度为- 15℃时改善最大。AlTiN刀具涂层具有低摩擦、低硬度的特点,可显著提高钛合金薄壁件的残余压应力,达到−483.3 MPa。与环形进给相比,横向和纵向进给可使残余压应力值分别提高18.87%和23.22%。仿真与实验误差可降至1.69%。加工温度降低,工件表面残余压应力增大。增加进给量先增大后减小表面残余拉伸应力。建立的低温二维切削有限元模型能够准确地预测覆冰铣削过程中的残余应力分布,为薄壁零件的高质量、高精度加工提供了有效的实用方案。
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引用次数: 0
Influence of Boron on the Hardenability of Low Carbon Alloy Platform Steel 硼对低碳合金平台钢淬透性的影响
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11633-4
Guangdi Zhao, Ximin Zang, Bo Wang, Jie Yang, Lingzhong Kong, Xue Li, Xiaoyu Yao, Zhenming Yu

Rack steel is a key material for constructing self-elevating offshore platforms, and as the thickness of steel plates continues to increase, increased requirements are placed on the steel’s hardenability. Boron is a key element in improving the hardenability of steels, but there are currently few reports on its role in rack steels. In this paper the influential mechanism of boron on the hardenability of A514Q Modified rack steel was investigated by conducting end quenching tests, establishing continuous cooling transformation (CCT) curves, and analyzing the grain boundary segregation behavior of boron. The results indicate that the 0.006 wt.% boron addition significantly improves the hardenability, reducing the critical cooling rate for martensitic transformation from 2 to 0.5 °C·s-1. The boron is mainly enriched in the MA islands, especially those along prior austenite grain boundaries (PAGBs). Besides, the boron atoms are slightly segregated at matrix / MA islands interfaces. The PAGBs segregation of boron can be explained through non-equilibrium segregation mechanism. Analysis suggests that boron addition improves the hardenability of rack steels mainly because the segregation of boron at PAGBs decreases the grain boundary energy.

机架钢是建设自升式海上平台的关键材料,随着钢板厚度的不断增加,对钢材的淬透性提出了更高的要求。硼是提高钢淬透性的关键元素,但目前关于硼在齿条钢中的作用的报道很少。通过端淬试验、建立连续冷却转变(CCT)曲线和分析硼的晶界偏析行为,研究硼对A514Q改性齿条钢淬透性的影响机理。结果表明:0.006 wt.%的硼含量显著提高了合金的淬透性,使马氏体相变的临界冷却速率从2℃·s-1降低到0.5℃·s-1;硼主要富集于MA岛礁,特别是沿奥氏体晶界的岛礁。此外,硼原子在基体/ MA岛界面处有轻微的偏析。硼的PAGBs偏析可以用非平衡偏析机理来解释。分析表明,硼的加入提高了齿条钢的淬透性,主要是由于硼在pagb处的偏析降低了晶界能。
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引用次数: 0
Study of the Mechanical Properties and Metallurgical Behavior of Nickel-Based Coatings: Atmospheric Plasma Spraying and Plasma Spray Melting 镍基涂层力学性能和冶金行为的研究:大气等离子喷涂和等离子喷涂熔化
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-06-30 DOI: 10.1007/s11665-025-11566-y
Yuheng Li, Baodan Zhang, Ming Liu, Yuncai Zhao, Song Xiao, Rui Gao, Jie Zhang, Haidou Wang

To improve the bonding strength at the coating/substrate interface and increase the proportion of interfacial metallurgical bonding, plasma spray melting (PSM) technology for coating preparation was proposed. The coatings were prepared using PSM and air plasma spray (APS) on Q235 steel substrates in this paper, respectively. The micro-morphology of the coatings and the morphology of the molten droplet splat and melt pool were characterized by scanning electron microscopy (SEM) and energy-dispersive x-ray spectroscopy (EDS). The mechanical properties of the coatings were also investigated, including bond strength, microhardness, nanoindentation, and residual stress. The coating/substrate metallurgical bonding was analyzed by electron backscatter diffraction (EBSD) and micro-zone x-ray diffraction (XRD). The results showed that the plasma-sprayed coating exhibited distinct continuous metallurgical bonding characteristics with the substrate, and the elemental diffusion depth was approximately 4 μm. Compared to the APS coating, the porosity was reduced to 2.3%. The interfacial region was metallurgically bonded, and the internal bonding strength of the coating reached 53 MPa. Additionally, the coating was less prone to cracking due to the favorable elastic modulus matching between the coating and the substrate.

为了提高涂层与基体界面的结合强度,提高界面冶金结合的比例,提出了等离子体喷射熔融(PSM)涂层制备技术。本文分别采用PSM和空气等离子喷涂(APS)在Q235钢基体上制备了涂层。利用扫描电子显微镜(SEM)和能谱仪(EDS)对涂层的微观形貌、熔滴飞溅和熔池的形貌进行了表征。研究了涂层的力学性能,包括结合强度、显微硬度、纳米压痕和残余应力。采用电子背散射衍射(EBSD)和微区x射线衍射(XRD)分析了涂层与基体的冶金结合。结果表明:等离子喷涂涂层与基体表现出明显的连续冶金结合特征,元素扩散深度约为4 μm;与APS涂层相比,孔隙率降低至2.3%。界面区进行了冶金结合,镀层内部结合强度达到53 MPa。此外,由于涂层与基体之间良好的弹性模量匹配,涂层不易开裂。
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引用次数: 0
期刊
Journal of Materials Engineering and Performance
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