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Prediction of Flexural Strength with Fuzzy Logic Approach for Fused Deposition Modeling of Polyethylene Terephthalate Glycol Components 用模糊逻辑方法预测聚对苯二甲酸乙二醇酯成分熔融沉积模型的挠曲强度
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-29 DOI: 10.1007/s11665-024-09291-z
Osman Ulkir, Gazi Akgun

Additive manufacturing (AM) is a preferred industrial manufacturing method for modeling and rapid prototyping of physical systems. The final product in AM must have appropriate mechanical properties, such as flexural strength and be of good quality. The selection of printing parameters is essential for this reason. In this study, three critical printing parameters, such as layer thickness (100-200-300 µm), raster angle (0-30-60°), and infill density (40-60-80%) were examined. The analysis of variance method was used to look at the relationship between these parameters and the flexure strength of samples fabricated using the fused deposition modeling technique with polyethylene terephthalate glycol material. The experimental design process was performed using Taguchi L9 orthogonal design. Fuzzy logic-based modeling was applied to estimate the flexural strength. The results demonstrated that the infill density is the most important parameter affecting flexural strength compared to the other parameters. The highest strength of 57.76 MPa was achieved when the layer thickness, raster angle, and infill density were set to 100 µm, 60°, and 80%, respectively. The fuzzy logic provided a high-accuracy estimation of the flexural strength with a maximum percentage error of 2.65%. Consequently, it was determined that the model and experimental results were in agreement.

快速成型制造(AM)是物理系统建模和快速原型制作的首选工业制造方法。快速成型制造的最终产品必须具有适当的机械性能,如抗弯强度和良好的质量。因此,印刷参数的选择至关重要。在这项研究中,研究了三个关键的打印参数,如层厚度(100-200-300 µm)、光栅角度(0-30-60°)和填充密度(40-60-80%)。采用方差分析法研究了这些参数与使用聚对苯二甲酸乙二酯材料的熔融沉积建模技术制作的样品的抗弯强度之间的关系。实验设计过程采用田口 L9 正交设计。应用基于模糊逻辑的模型来估算抗弯强度。结果表明,与其他参数相比,填充密度是影响抗弯强度的最重要参数。当层厚、栅格角和填充密度分别设置为 100 µm、60° 和 80% 时,强度最高,达到 57.76 MPa。模糊逻辑对抗弯强度进行了高精度估算,最大误差为 2.65%。因此,可以确定模型和实验结果是一致的。
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引用次数: 0
Hydrogen Embrittlement Resistance of High Strength 9260 Bar Steel Heat Treated by Quenching and Partitioning 通过淬火和隔热处理的高强度 9260 棒材钢的抗氢脆性能
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-27 DOI: 10.1007/s11665-024-09242-8
E. Hoyt, M. Rupinen, E. De Moor, K. O. Findley

Hydrogen embrittlement (HE) continues to be a limiting factor in implementing high strength steel alloys in applications such as fasteners. In this work, 9260 bar steel was heat treated to produce quench and tempered (Q&T) martensite and quench and partitioned (Q&P) microstructures at hardness levels between 52 and 54 HRC. The Q&P microstructures consisted of lath martensite, retained austenite, martensite-austenite (M/A) constituents, and intercritical ferrite in some conditions. The Q&P process promoted higher strength and uniform elongation than the Q&T martensite, though also exhibited a relatively low degree of post-uniform elongation except in the lowest quench temperature condition. Slow strain rate tensile and circular notch tensile tests were performed on all conditions after electrochemical hydrogen charging at hydrogen levels of 1–1.5 ppm. The Q&T condition exhibited a better slow strain rate performance and notch tensile strength after hydrogen pre-charging than the Q&P conditions. In the Q&P conditions subjected to slow strain rate tensile tests, a higher HE susceptibility is correlated with higher quench temperatures, which had lower austenite stability and more fresh, non-tempered martensite in the initial microstructure. However, the HE susceptibility was comparable for all of the Q&P conditions in the notch tensile tests.

氢脆(HE)仍然是在紧固件等应用中使用高强度合金钢的一个限制因素。在这项研究中,对 9260 棒材进行了热处理,以产生淬火回火(Q&T)马氏体和淬火分层(Q&P)显微组织,硬度在 52 和 54 HRC 之间。Q&P显微组织由板条马氏体、残余奥氏体、马氏体-奥氏体(M/A)成分以及某些条件下的临界铁素体组成。与 Q&T 马氏体相比,Q&P 工艺能提高强度和均匀伸长率,但除了在最低淬火温度条件下,其后均匀伸长率也相对较低。在氢含量为 1-1.5 ppm 的电化学充氢后,对所有条件都进行了慢应变速率拉伸和圆形缺口拉伸试验。与 Q&P 条件相比,Q&T 条件在预充氢后表现出更好的慢应变速率性能和缺口拉伸强度。在进行慢应变速率拉伸试验的 Q&P 条件中,较高的高热敏感性与较高的淬火温度相关,淬火温度越高,奥氏体稳定性越低,初始微观结构中的新鲜非回火马氏体越多。不过,在缺口拉伸试验中,所有 Q&P 条件下的高热敏感性都相当。
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引用次数: 0
Optimizing Interfaces in Laser-Brazed Ceramic-Stainless Steel Joints for Hydrothermal Sensors through Finite-Element Modeling 通过有限元建模优化用于水热传感器的激光钎焊陶瓷-不锈钢接头界面
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-27 DOI: 10.1007/s11665-024-09285-x
Jian Feng, Marion Herrmann, Anne-Maria Reinecke, Antonio Hurtado

The development of reliable joining techniques for ceramics and metals is crucial for energy applications, such as fuel cells, nuclear reactors, and high-temperature sensors, most especially for the sealing of hydrothermal sensors to study multiphase flows. However, during one-step active laser brazing it is a serious problem that a high thermal stress concentration can occur at the joint interfaces or on the ceramic side of the joint due to mismatches between the CTEs (coefficients of thermal expansion) and/or elastic constants. The uncontrolled thermal residual stress can lead to cracks and defects in the brazement. In the present work, an elastoplastic finite element method/numerical model was formulated to study the thermal residual stresses developed in the brazement between ceramics and austenitic stainless steel during cooling in active laser brazing. Calculations and comparison experiments were conducted to validate the simulated stress distribution in un-patterned ceramics. Stress analyses were conducted for planar and cylindrical specimen geometries (lab joints) relevant for miniaturized energy sensors. Laser interface patterning was employed to create micro-scale features on ceramic interfaces that reduce thermal stress concentrations. The optimization of the interface designing parameters including hatch size, structure width, pattern depth and metal/ceramic thickness ratio was performed using the Taguchi method with orthogonal arrays. The study suggests that laser interface structuring can modify thermal residual stresses in ceramic-to-metal brazements, thereby increasing the reliability of active brazing joints.

为陶瓷和金属开发可靠的连接技术对于燃料电池、核反应堆和高温传感器等能源应用至关重要,尤其是对于密封研究多相流的水热传感器而言。然而,在一步法主动激光钎焊过程中,一个严重的问题是,由于热膨胀系数和/或弹性常数之间的不匹配,会在接合界面或接合处的陶瓷侧产生高热应力集中。失控的热残余应力会导致钎焊出现裂缝和缺陷。本研究采用弹塑性有限元方法/数值模型来研究主动激光钎焊中陶瓷和奥氏体不锈钢钎焊冷却过程中产生的热残余应力。通过计算和对比实验,验证了无图案陶瓷中的模拟应力分布。对与微型能量传感器相关的平面和圆柱形试样几何形状(实验室接头)进行了应力分析。采用激光界面图案化技术在陶瓷界面上创建微尺度特征,以减少热应力集中。采用正交阵列田口方法对界面设计参数进行了优化,包括舱口尺寸、结构宽度、图案深度和金属/陶瓷厚度比。研究表明,激光界面结构可改变陶瓷-金属钎焊中的热残余应力,从而提高活性钎焊接头的可靠性。
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引用次数: 0
Residual Stress Induced by Phase Transformation and its Role in the Delayed Cracking Performance of 22MnB5 Hot Roll Bending Pipes 相变引起的残余应力及其在 22MnB5 热轧弯管延迟开裂性能中的作用
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-26 DOI: 10.1007/s11665-023-08959-2
Kai Ding, Ping Zhu, Tianhan Hu, Wufeng Dong, Yu Sun, Jiayi Zhou, Bingge Zhao, Lei Shi, Yulai Gao

Residual stress plays an important role in the delayed cracking performance of the 22MnB5 hot roll bending pipe. In the present study, the residual stress distribution of the 22MnB5 hot roll bending pipes with different pipe thicknesses is compared. The results show that both the tensile and compressive residual stresses can be traced in the bending zone for the pipe with plate thickness around 1.5 mm. On the contrary, only tensile residual stress obtains in the residual stress measurement positions for the thicker one (~ 2.3 mm). In addition, the thicker 22MnB5 pipe exhibits poor delayed cracking behavior in the solution of 0.1 mol/L HCl for 300 h. Compared with thinner 22MnB5 pipe, high tensile residual stress occurs in the thicker one induced by phase transformation and deformation during the hot roll bending process, deteriorating its delayed cracking performance.

残余应力对 22MnB5 热轧弯管的延迟开裂性能起着重要作用。本研究比较了不同厚度 22MnB5 热轧弯管的残余应力分布。结果表明,对于板厚在 1.5 毫米左右的管材,在弯曲区域既可以追踪到拉伸残余应力,也可以追踪到压缩残余应力。相反,对于较厚的钢管(约 2.3 毫米),在残余应力测量位置只存在拉伸残余应力。此外,较厚的 22MnB5 管材在 0.1 mol/L HCl 溶液中 300 小时的延迟开裂性能较差。与较薄的 22MnB5 管材相比,较厚的管材在热轧弯曲过程中由于相变和变形而产生了较高的拉伸残余应力,从而降低了其延迟开裂性能。
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引用次数: 0
Effect of Travel Speed on the Properties of 5087 Aluminum Alloy Walls Produced by Wire and Arc Additive Manufacturing 行进速度对线材和电弧增材制造生产的 5087 铝合金壁性能的影响
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-26 DOI: 10.1007/s11665-024-09166-3
Miroslav Sahul, Marián Pavlík, Martin Sahul, Pavel Kovačócy, Maroš Martinkovič

An innovative Wire and Arc Additive Manufacturing combines the well-studied process of arc welding with direct energy deposition. Effect of travel speed 5.0 and 7.5 mm/s on the microstructure and mechanical properties of 5087 aluminum alloy was investigated. Five thousand eighty-three aluminum alloy was used as a substrate material and 5087 aluminum alloy was utilized as a filler material for the walls fabrication. The presence of pores reducing the strength of the overlay weld metal was detected on both overlay welds. The lower welding speed (5 mm/s) resulted in the smaller amount of porosity in comparison to higher welding speed (7.5 mm/s). Average pore area of wall No. 1 was 0.66% and wall No. 2 was 1.13%. It was found that higher welding speed affected the wall width and overlay weld bead geometry. Increase in welding speed led to a narrowing of wall width from 10.23 to 8.44 mm. The microstructure of weld metal matrix consisted of a α-Al substitution solid solution. The tensile strength of parallel to welding direction removed samples exceeded the tensile strength of perpendicular removed samples. It is a result of the cohesion of the layers in the overlay welding direction compared to the non-uniformity of the layers in the perpendicular direction. Furthermore, the tensile strength was higher in the case of travel speed of 5 mm/s in comparison to that of 7.5 mm/s.

一种创新的线弧增材制造技术结合了经过充分研究的电弧焊接和直接能量沉积工艺。研究了移动速度 5.0 和 7.5 mm/s 对 5087 铝合金微观结构和机械性能的影响。5,833 铝合金被用作基材,5087 铝合金被用作填充材料,用于壁厚制造。在两道堆焊焊缝中都发现了气孔,气孔的存在降低了堆焊焊缝金属的强度。与较高的焊接速度(7.5 毫米/秒)相比,较低的焊接速度(5 毫米/秒)产生的气孔较少。1 号焊缝的平均孔隙率为 0.66%,2 号焊缝的平均孔隙率为 1.13%。研究发现,较高的焊接速度会影响壁宽和堆焊焊缝的几何形状。焊接速度的提高导致壁宽从 10.23 毫米缩小到 8.44 毫米。焊接金属基体的微观结构由 α-Al 置换固溶体组成。与焊接方向平行的移除样品的抗拉强度超过了垂直移除样品的抗拉强度。这是由于堆焊方向的层间内聚力比垂直方向的层间不均匀性大。此外,与 7.5 mm/s 的移动速度相比,5 mm/s 移动速度下的拉伸强度更高。
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引用次数: 0
Electrical, Mechanical, and Electromechanical Properties of Screen-Printed Piezoresistive Polydimethylsiloxane with Multiwalled Carbon Nanotube Nanocomposites 丝网印刷压阻聚二甲基硅氧烷与多壁碳纳米管纳米复合材料的电气、机械和机电性能
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-23 DOI: 10.1007/s11665-024-09253-5
S. Riyaz Ali, A. L. G. N. Aditya, E. Megalai, R. Madhukaran, J. Kathirvelan, E. Rufus

Polydimethylsiloxane (PDMS) with multiwalled carbon nanotubes (MWCNT) fillers is a piezoresistive nanocomposite which is conformable, printable, and biocompatible. It is widely employed as a sensing layer in flexible pressure sensors, electronic skin (e-skin) of humanoid robots and as wearable sensors. Piezoresistive nanocomposites show significant increase in their electrical conductivity above a certain percolation threshold. In this work, PDMS + MWCNT-based sensing layers with different nanofiller MWCNT concentrations (2, 4 and 7 wt.%) are screen-printed and their electrical, mechanical, and percolation threshold responses are verified. The static I–V characteristics of the samples for a biasing DC voltage of 0-6 V are studied. The tensile test confirms maximum elongation of more than 50 mm. The change in resistance was minimal for 2 wt.% sample as the MWCNT’s are sparsely distributed and no conducting channels are formed; for the 7 wt.% sensing layer, negligible change in resistance was observed as the conducting channels are broken. The highest change in resistance of 2.4 MΩ was observed after the percolation threshold value of 4 wt.% of the nanofiller concentration was reached. Overall, the 4 wt.% screen-printed piezoresistive nanocomposite layer showed highest sensitivity with a gauge factor of 4.76 and a linear response suitable for industrial applications.

含有多壁碳纳米管(MWCNT)填料的聚二甲基硅氧烷(PDMS)是一种压阻纳米复合材料,具有保形性、可印刷性和生物相容性。它被广泛用作柔性压力传感器、仿人机器人电子皮肤(e-skin)和可穿戴传感器的传感层。压阻纳米复合材料的电导率在超过一定的渗流阈值时会显著增加。在这项工作中,丝网印刷了不同纳米填充物 MWCNT 浓度(2、4 和 7 wt.%)的 PDMS + MWCNT 传感层,并验证了它们的电气、机械和渗滤阈值响应。研究了样品在 0-6 V 偏置直流电压下的静态 I-V 特性。拉伸试验证实最大伸长率超过 50 毫米。2 wt.% 样品的电阻变化极小,因为 MWCNT 的分布稀疏,没有形成导电通道;7 wt.% 传感层的电阻变化可忽略不计,因为导电通道被破坏。在达到 4 wt.% 纳米填料浓度的渗流阈值后,观察到最高的电阻变化为 2.4 MΩ。总体而言,4 wt.%丝网印刷压阻纳米复合材料层的灵敏度最高,测量系数为 4.76,线性响应适合工业应用。
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引用次数: 0
Correction: On the Development of Computational Fluid Dynamics Quenching Simulation Methodology for Effective Thermal Residual Stress Control 更正:关于开发计算流体力学淬火模拟方法以实现有效的热残余应力控制
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-23 DOI: 10.1007/s11665-024-09266-0
James Jan, D. Scott MacKenzie
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引用次数: 0
Residual Stress Generation in Additive Manufacturing of Complex Lattice Geometries 复杂晶格几何体增材制造中的残余应力产生
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-21 DOI: 10.1007/s11665-024-09229-5
Katie Bruggeman, Nathan Klingbeil, Anthony Palazotto

Residual stresses developed during additive manufacturing (AM) can influence the mechanical performance of structural components in their intended applications. In this study, thermomechanical residual stress simulations of the laser powder bed fusion (LPBF) process are conducted for both simplified (plate and cube-shaped) geometries as well as five complex lattice geometries fabricated with Inconel 718. These simulations are conducted with the commercial software package Simufact Additive©, which uses a nonlinear finite element analysis and layer-by-layer averaging approach in determining residual stresses. To verify the efficacy of the Simufact Additive© simulations, numerical results for the plate and cube-shape geometries are analyzed for convergence and compared to experimental residual stress results available in the literature. Numerical residual stress results are subsequently compared for five complex lattice geometries. Results suggest that lattice geometry can play a significant role in the distribution and magnitude of residual stresses, which are significant in some applications.

摘要 在增材制造(AM)过程中产生的残余应力会影响结构部件在预期应用中的机械性能。本研究对激光粉末床熔融(LPBF)工艺进行了热机械残余应力模拟,模拟对象包括简化(板状和立方体状)几何形状以及用 Inconel 718 制造的五种复杂晶格几何形状。这些模拟使用 Simufact Additive© 商业软件包进行,该软件包使用非线性有限元分析和逐层平均法确定残余应力。为了验证 Simufact Additive© 模拟的有效性,对板材和立方体几何形状的数值结果进行了收敛分析,并与文献中的残余应力实验结果进行了比较。随后比较了五种复杂晶格几何形状的残余应力数值结果。结果表明,晶格几何形状对残余应力的分布和大小有重要影响,这在某些应用中非常重要。
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引用次数: 0
The Effect of Bonding Temperature on the Microstructural and Mechanical Properties of Transient Liquid Phase Bonded Commercially Pure Ti Joint 接合温度对瞬态液相接合商业纯钛接头微观结构和机械性能的影响
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-20 DOI: 10.1007/s11665-023-07813-9
Vahid Maleki, Sajad Shakerin, Seyyed Alireza Ziaei, Hamid Omidvar, Seyyed Ehsan Mirsalehi

Commercially pure Ti (AMS 4902) was joined using the transient liquid phase bonding technique. The joining process was implemented at various temperatures of 820, 860, 900, and 1000 °C for 90 min under a vacuum atmosphere of 7.99 Pa. The microstructural investigations were carried out comprehensively using scanning electron microscopy equipped with the EDS elemental detector. The mechanical properties were characterized using the microhardness and shear strength tests. Strength properties in terms of ultimate shear strength and ductility were presented as force-extension diagrams. The presence of eutectic intermetallics in the joint centerline indicated that isothermal solidification was not achieved at low bonding temperatures. However, the increase in temperature to 1000 °C resulted in a fully isothermal solidified joint. The elemental gradients between the bonding centerline and the base metal leveled off at high temperatures of 900 and 1000 °C, where the solubility of Ti increased in the Cu crystal structure. A higher hardness of 270 HV with a uniform gradient was also observed across the joint produced at high temperatures of 900 and 1000 °C. A combination of high strength and ductility was obtained for the samples fabricated at 900 and 1000 °C bonding temperatures.

使用瞬态液相键合技术连接了市售纯钛 (AMS 4902)。在 7.99 Pa 的真空环境下,在 820、860、900 和 1000 °C 的不同温度下进行了 90 分钟的接合过程。机械性能采用显微硬度和剪切强度测试进行表征。极限剪切强度和延展性方面的强度特性以力-拉伸图的形式呈现。接合中心线存在共晶金属间化合物,这表明在低接合温度下无法实现等温凝固。然而,温度升高到 1000 ℃ 时,接头完全等温凝固。接合中心线和基体金属之间的元素梯度在 900 和 1000 ℃ 高温时趋于平稳,此时钛在铜晶体结构中的溶解度增加。在 900 和 1000 °C 高温下生产的接头硬度更高,达到 270 HV,且梯度均匀。在 900 ℃ 和 1000 ℃ 焊接温度下制作的样品兼具高强度和延展性。
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引用次数: 0
Efficacy of Laser Shock Peening Post-milling: A Semi-numerical Study 激光冲击强化铣削后的功效:半数值研究
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-02-15 DOI: 10.1007/s11665-024-09241-9
Aryendra Singh, Viswanath Chinthapenta, Phani Mylavarapu

The role of the initial residual stresses (IRS) induced by the milling on the efficacy of laser shock peening (LSP) was investigated numerically on IN718 specimens. Three milling conditions exhibiting high (3.5 μm), medium (1.1 μm), and low (0.6 μm) surface roughness were considered for LSP. Experimentally measured (from XRD) milling-induced sub-surface (up to 60 μm depth) residual stresses were introduced into the simulations of LSP as predefined fields. The role of spot diameter with the IRS on the LSP-induced residual stress was studied systematically. For most cases, the tensile IRS from milling caused a significant decrease in the magnitude of maximum compressive residual stresses induced by LSP.

在 IN718 试样上对铣削引起的初始残余应力(IRS)对激光冲击强化(LSP)效果的作用进行了数值研究。LSP 考虑了三种铣削条件,分别表现出高(3.5 μm)、中(1.1 μm)和低(0.6 μm)表面粗糙度。在 LSP 模拟中引入了实验测量(来自 XRD)的铣削引起的次表面(深度达 60 μm)残余应力作为预定义场。系统研究了点直径与 IRS 对 LSP 诱导的残余应力的作用。在大多数情况下,铣削产生的拉伸 IRS 会显著降低 LSP 诱导的最大压缩残余应力的大小。
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引用次数: 0
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Journal of Materials Engineering and Performance
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