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Synergistic Tribological Enhancement of Bushings Via Topology-Optimized Bionic Textures and MAX Phase-Reinforced PTFE Composite Coatings 通过拓扑优化仿生织构和MAX相增强PTFE复合涂层增强衬套摩擦学性能
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-12 DOI: 10.1007/s11665-025-11986-w
Kunpeng Chen, Qipeng Huang, Xiaoliang Shi, Weijie Zheng, Haowen Qin, Yuxuan Chen, Haohui Li

To address boundary lubrication failure and surface fatigue wear in guide bushings under complex operating conditions, this study proposes a synergistic strategy combining topology-optimized bionic surface textures and MAX phase-reinforced PTFE coatings, leveraging multi-scale structural and material design to enhance interfacial tribological performance. Inspired by the micro-protrusion architecture of mosquito compound eyes, bionic textures were designed via topology optimization and fabricated on Cr12MoV steel surfaces using pulsed laser machining, while curing the PTFE-Mo2Ga2C composite coating on the surface. Reciprocating friction tests demonstrated that increasing the optimized aperture size of textures reduced the average friction coefficient by 13.5% and wear rate by 39.1%. Transient structural simulations validated the stress redistribution capability of topology-optimized textures on curved bushing surfaces, showing a 41% reduction in peak contact stress compared to non-optimized designs. Mechanistic analysis revealed a dual lubrication mechanism, PTFE extruded at texture edges forms lubricating films retained within grooves for cyclic replenishment, and MAX phase microparticle released from micro-pores dynamically reduce friction through lamellar shear. This synergy enhances lubricant retention, promotes uniform stress distribution, and delays coating wear.

为了解决复杂工况下导向衬套的边界润滑失效和表面疲劳磨损问题,本研究提出了一种结合拓扑优化仿生表面纹理和MAX相增强PTFE涂层的协同策略,利用多尺度结构和材料设计来提高界面摩擦学性能。受蚊子复眼微突出结构的启发,通过拓扑优化设计仿生纹理,并在Cr12MoV钢表面采用脉冲激光加工制备仿生纹理,同时在表面固化PTFE-Mo2Ga2C复合涂层。往复摩擦试验结果表明,增加织构优化孔径尺寸,平均摩擦系数降低13.5%,磨损率降低39.1%。瞬态结构模拟验证了拓扑优化纹理在弯曲衬套表面上的应力重新分布能力,与未优化设计相比,峰值接触应力降低了41%。力学分析揭示了双润滑机制,织体边缘的聚四氟乙烯形成润滑膜,保留在凹槽内循环补充,微孔释放的MAX相微粒通过片层剪切动态减少摩擦。这种协同作用增强了润滑剂的保留,促进均匀的应力分布,并延迟涂层磨损。
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引用次数: 0
Evaluation of Mechanical Properties and Fatigue Performance of L450 Pipeline Steel Base Metal and Welds L450管道钢母材及焊缝的力学性能和疲劳性能评价
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-11 DOI: 10.1007/s11665-025-11871-6
Jiao Wu, Guochun Zhong, Chen Zhang, Shichang Liu, Peng Li, Lihua Wan, Mujun Long

The mechanical properties of pipeline steel significantly influence the operational safety and service life of underground gas storage (UGS). This study follows results of tensile tests on the base metal (L450-BM) and welds (L450-WM) of L450 pipeline steel, evaluating their strength and ductility alongside analyzing their microstructure and fracture morphology. Using finite element software and based on experimentally measured mechanical properties, fatigue simulation models for the base metal and weld specimens were established to capture the evolution of fatigue life under different loading conditions. Results indicate that the ductility of L450-WM is significantly lower than that of L450-BM, with elongation at fracture being 17.2% for L450-BM and 14.6% for L450-WM. The fracture types are characterized as quasi-cleavage fracture and cleavage fracture, respectively. Both L450-BM and L450-WM exhibit reduced fatigue life with increasing average tensile force and load spectrum amplitude. Under a tensile force of 6.5 kN with an amplitude greater than 0.1, the fatigue cycles of L450-WM decreased by nearly two orders of magnitude, reaching only 1.8% of the L450-BM. These findings provide valuable data and theoretical support for material selection and pipeline failure prevention in UGS.

管道钢的力学性能对地下储气库的运行安全和使用寿命有重要影响。本研究对L450管线钢的母材(L450- bm)和焊缝(L450- wm)进行了拉伸试验,评估了它们的强度和延展性,同时分析了它们的显微组织和断裂形貌。利用有限元软件,在实验测量力学性能的基础上,建立了母材和焊缝试样的疲劳模拟模型,以捕捉不同加载条件下的疲劳寿命演变规律。结果表明,L450-WM的延展性明显低于L450-BM,断裂伸长率分别为17.2%和14.6%。断裂类型分别为准解理断裂和解理断裂。L450-BM和L450-WM的疲劳寿命随平均拉伸力和载荷谱幅值的增大而减小。在6.5 kN、振幅大于0.1的拉伸力作用下,L450-WM的疲劳循环次数减少了近两个数量级,仅为L450-BM的1.8%。这些发现为UGS的材料选择和管道故障预防提供了有价值的数据和理论支持。
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引用次数: 0
Selected Papers from the Fifth International Conference on Advances in Mechanical Engineering (ICAME 2024) 第五届国际机械工程进展会议(ICAME 2024)论文选集
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-10 DOI: 10.1007/s11665-025-12033-4
Junghyun Cho, Shubhabrata Datta, U. Mohammed Iqbal
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引用次数: 0
A Novel 3D Bioprinting Platform Integrating Coaxial Nozzle and Modified Rotating Bioreactor for Angiogenesis-Guided Vascular Tissue Engineering 结合同轴喷嘴和改良旋转生物反应器的新型生物3D打印平台用于血管生成引导的血管组织工程
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-09 DOI: 10.1007/s11665-025-11849-4
Khemraj Deshmukh, Jitendra Kumar, Nitesh Kumar Singh, Arindam Bit

3D bioprinting is a promptly developing biomedical alternative of 3D printing technology. It acts as a robotic device, which prints any tissue, organs, and blood vessels layer by layer according to our designed model on CAD System; further, it was cultured in a bioreactor. This procedure is not a replica of the generation of vascular structure in in vivo condition. The objective of the proposed design is to provide precise control on bioreactor-based 3D printer for blood vessel generation followed by the angiogenesis process. This proposed 3D printer design used extrusion-based coaxial nozzle for printing the entire structure layer by layer and simultaneously cultured layer by layer using a modified rotatory bioreactor. Control of each component is done by programmable logic controller PLC), and simulation of the electronics circuit was done by LabVIEW. In the proposed design of the 3D bioprinter, decision-based logic circuits were used to improve the utilization of media. The simulation result of the PLC shows that there is strong control on each parameter such as pH control, oxygen control, waste product control, rotational speed control, media stem rod, nozzle temperature, and pressure used for printing. Results indicated successful control of parameters pH (7.2-7.4), oxygen (~6%), and CO2 (~10%) which contributed to improved cell viability and angiogenesis throughout the culture process. Automation of waste media management was implemented using decision-based logic circuits, resulting in enhanced media utilization efficiency. The analysis conducted using Computational Fluid Dynamics (CFD) demonstrated a consistent flow distribution and effective shear stress management. Additionally, the uncertainty analysis confirmed the stability of the system, revealing minimal fluctuations in pressure (±7.90 mmHg) and shear stress (±179.36 N/m2). LabVIEW results verify that all electronic circuits work properly. The uncertainty analysis provided a strong framework for data reliability, measuring the variability in pressure, velocity, and strain rate on shear stress caused by sensor inaccuracies and system fluctuations. Overall, the proposed design provides a better environment for the printing of vascular structures by extrusion-based coaxial nozzle printing technology and modified rotatory bioreactor used for vascular cell culture.

3D生物打印是3D打印技术在生物医学领域的一种快速发展的替代技术。它是一个机器人装置,可以根据我们设计的模型在CAD系统上逐层打印任何组织、器官和血管;此外,它在生物反应器中培养。这个过程不是在体内条件下血管结构生成的复制品。提出的设计目标是为基于生物反应器的3D打印机提供血管生成和血管生成过程的精确控制。该3D打印机设计采用基于挤压的同轴喷嘴,一层一层地打印整个结构,并使用改进的旋转生物反应器一层一层地同时培养。各部件的控制由可编程控制器PLC完成,电子电路的仿真由LabVIEW完成。在提出的3D生物打印机设计中,采用基于决策的逻辑电路来提高介质的利用率。PLC的仿真结果表明,对印刷所用的pH值控制、氧气控制、废品控制、转速控制、介质杆杆、喷嘴温度、压力等各参数都有较强的控制。结果表明,成功控制pH(7.2-7.4)、氧气(~6%)和CO2(~10%)参数,有助于提高整个培养过程中细胞活力和血管生成。利用基于决策的逻辑电路实现废物介质管理的自动化,从而提高了介质的利用效率。使用计算流体动力学(CFD)进行的分析表明,流动分布一致,剪切应力管理有效。此外,不确定度分析证实了系统的稳定性,显示压力(±7.90 mmHg)和剪切应力(±179.36 N/m2)的最小波动。LabVIEW结果验证所有电子电路工作正常。不确定性分析为数据可靠性提供了一个强有力的框架,可以测量由传感器不准确和系统波动引起的剪切应力的压力、速度和应变率的变化。总体而言,该设计通过基于挤压的同轴喷嘴打印技术和用于血管细胞培养的改良旋转生物反应器,为血管结构的打印提供了更好的环境。
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引用次数: 0
Green Electronics Soldering by Application of Third Generation Lead-Free Solder Alloys: Studies on Their Wettability and Interface Microstructure Formed with Copper 应用第三代无铅钎料合金的绿色电子焊接:其与铜形成的润湿性和界面微观结构研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-09 DOI: 10.1007/s11665-025-12029-0
Maciej Sobolewski, Joanna Wojewoda-Budka, Natalia Sobczak, Marta Janusz-Skuza, Agnieszka Bigos, Sylwia Terlicka, Anna Korneva, Maciej Szlezynger, Zenon Adamek, Anna Wierzbicka-Miernik

Due to the regulations restricting the use of lead, the implementation of lead-free solders became a legal requirement more than 15 years ago. In addition to the well-known SAC305 solder, new alloys containing various concentrations of Bi, together with other additives improving the soldering process and reliability of joints, have appeared. The paper focuses on comparative study of wetting properties of SAC305 and commercially available third-generation lead-free solder alloys containing Bi: REL61, REL22, and HRL-1. The improved sessile drop method, was applied to measure the contact angle (θ) of the selected solders on a copper substrate. The highest contact angle value (36°) was observe for HRL-1 and the lowest (27°) for REL22. Initially the spreading phenomenon was very fast, below the resolution of the measurement method. In some cases of the wetting disturbance by the external factors, wetting has been inhibited and the intermetallic phases developed at the solder/substrate. The formation of a halo area at the substrate around the drop was also observed, most likely formed due to the surface diffusion of solder atoms. This phenomenon led to a further reduction of the contact angle, but the spreading of the drop was much slower. Comprehensive microstructure and chemical composition examination of the drop/substrate interfaces after wetting tests evidenced the presence of Cu6Sn5 phase for all samples. Moreover, it was proved that the alloy additives (e.g., Ag and Bi) influenced the achieved contact angle and reduced unfavorable intermetallic phases formation such as Cu3Sn (e.g., Ni, Sb, and Ti).

由于限制使用铅的法规,实施无铅焊料在15年前就成为一项法律要求。除了众所周知的SAC305焊料外,还出现了含有不同浓度Bi的新型合金,以及其他添加剂,改善了焊接工艺和接头的可靠性。本文重点对SAC305与市售的含Bi: REL61、REL22和HRL-1的第三代无铅钎料合金润湿性能进行了比较研究。采用改进的固滴法测量了铜衬底上焊料的接触角(θ)。HRL-1的接触角值最高(36°),REL22的接触角值最低(27°)。最初扩散现象非常快,低于测量方法的分辨率。在外部因素干扰润湿的某些情况下,润湿被抑制,在焊料/衬底处形成金属间相。还观察到在液滴周围的衬底上形成晕区,这很可能是由于焊料原子的表面扩散而形成的。这种现象导致接触角进一步减小,但液滴的扩散速度要慢得多。润湿试验后,对液滴/衬底界面进行了综合微观结构和化学成分检测,结果表明所有样品均存在Cu6Sn5相。此外,合金添加剂(如Ag和Bi)影响了所获得的接触角,并减少了不利的金属间相的形成,如Cu3Sn(如Ni, Sb和Ti)。
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引用次数: 0
Investigations on Flexural Performance of 3D-Printed Continuous Carbon Fiber-Reinforced Composites under Sub-ambient to Elevated Temperature 三维打印连续碳纤维增强复合材料亚环境至高温弯曲性能研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-08 DOI: 10.1007/s11665-025-11832-z
Vishista Kaushik, Kurra Suresh, Ramesh B. Adusumalli

The study aims to determine the optimal 3D-printed continuous fiber composite that performs effectively under varying temperature conditions. This is driven by the high design flexibility offered by 3D printers and the need to understand the performance parameters. The effect of fiber content and orientation on the flexural characteristics was analyzed through three-point bending tests at three temperatures. Four key attributes (environmental, mechanical, economic, social factors) were selected, which were further classified into nine decision criteria. A total of 12 models of multi-criteria decision-making (MCDM) approach were employed, incorporating four weighting and three ranking techniques. Detailed optical microscopic studies were conducted to analyze the fracture behavior of samples. The study found that the flexural performance of the 3D-printed composites improved with the addition of fiber content and change in orientation. Implementation of the hybrid MCDM approach provides a comprehensive and multi-faceted analysis, as each method offers a unique perspective on the optimal choice for reliable material selection. Overall, 0º unidirectional fiber composites showed superior performance among all MCDM models. This research is novel in applying a hybrid MCDM approach to identify the optimal 3D-printed continuous fiber composite under various environmental conditions ranging from sub-ambient to high temperature useful for industrial applications.

该研究旨在确定在不同温度条件下有效执行的最佳3d打印连续纤维复合材料。这是由3D打印机提供的高设计灵活性和需要了解性能参数驱动的。通过三种温度下的三点弯曲试验,分析了纤维含量和取向对弯曲特性的影响。选择了四个关键属性(环境、机械、经济、社会因素),并将其进一步划分为9个决策标准。采用了12个多准则决策模型,包括4个权重和3个排序技术。进行了详细的光学显微研究来分析样品的断裂行为。研究发现,3d打印复合材料的抗弯性能随着纤维含量的增加和取向的改变而提高。混合MCDM方法的实施提供了全面和多方面的分析,因为每种方法都提供了可靠材料选择的最佳选择的独特视角。总体而言,0º单向纤维复合材料在所有MCDM模型中表现出优越的性能。该研究新颖地应用了混合MCDM方法来确定各种环境条件下(从亚环境到高温)的最佳3d打印连续纤维复合材料,可用于工业应用。
{"title":"Investigations on Flexural Performance of 3D-Printed Continuous Carbon Fiber-Reinforced Composites under Sub-ambient to Elevated Temperature","authors":"Vishista Kaushik,&nbsp;Kurra Suresh,&nbsp;Ramesh B. Adusumalli","doi":"10.1007/s11665-025-11832-z","DOIUrl":"10.1007/s11665-025-11832-z","url":null,"abstract":"<p>The study aims to determine the optimal 3D-printed continuous fiber composite that performs effectively under varying temperature conditions. This is driven by the high design flexibility offered by 3D printers and the need to understand the performance parameters. The effect of fiber content and orientation on the flexural characteristics was analyzed through three-point bending tests at three temperatures. Four key attributes (environmental, mechanical, economic, social factors) were selected, which were further classified into nine decision criteria. A total of 12 models of multi-criteria decision-making (MCDM) approach were employed, incorporating four weighting and three ranking techniques. Detailed optical microscopic studies were conducted to analyze the fracture behavior of samples. The study found that the flexural performance of the 3D-printed composites improved with the addition of fiber content and change in orientation. Implementation of the hybrid MCDM approach provides a comprehensive and multi-faceted analysis, as each method offers a unique perspective on the optimal choice for reliable material selection. Overall, 0º unidirectional fiber composites showed superior performance among all MCDM models. This research is novel in applying a hybrid MCDM approach to identify the optimal 3D-printed continuous fiber composite under various environmental conditions ranging from sub-ambient to high temperature useful for industrial applications.</p>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"35 4","pages":"3248 - 3263"},"PeriodicalIF":2.0,"publicationDate":"2025-09-08","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146090984","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Study on Properties of FeCrCoMoCB Amorphous Coating Fabricated by Supersonic Plasma Spraying 超声速等离子喷涂制备FeCrCoMoCB非晶涂层的性能研究
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-05 DOI: 10.1007/s11665-025-11952-6
Yuncai Zhao, Mingchao Hu, Weiling Guo, Yanfei Huang, Zeling Hu, Longlong Zhou, Zhiguo Xing, Haidou Wang

Wear and corrosion are the main causes of structural failure of mechanical parts, using thermal spraying to fabricate raw materials into coating, which is a common method of protection of mechanical parts. In this work, FeCrCoMoCB amorphous coating was fabricated on the 45# steel substrate using supersonic plasma spraying (SPS). The microstructure, phase composition, mechanical, corrosion, and wear properties of FeCrCoMoCB amorphous coating were systematically investigated. The results show that FeCrCoMoCB amorphous coating had a relatively flat surface, low porosity with a dense structure, high hardness, and had an amorphous rate of more than 90%. The coating displays a passive region of about 500 mV, corrosion potential of − 1.01 V, and current density of 1.89 × 10-5 A/cm2. The wear mechanism of FeCrCoMoCB amorphous coating is dominated by oxidation wear, and with the increase of load, the abrasive wear transforms into delamination wear.

磨损和腐蚀是机械零件结构失效的主要原因,利用热喷涂将原材料加工成涂层,是机械零件保护的常用方法。采用超音速等离子喷涂(SPS)技术在45#钢基体上制备了FeCrCoMoCB非晶涂层。系统地研究了FeCrCoMoCB非晶涂层的显微组织、相组成、力学性能、腐蚀性能和磨损性能。结果表明:FeCrCoMoCB非晶涂层表面相对平坦,孔隙率低,组织致密,硬度高,非晶态率达90%以上;镀层的钝化区约为500 mV,腐蚀电位为- 1.01 V,电流密度为1.89 × 10-5 a /cm2。FeCrCoMoCB非晶涂层的磨损机制以氧化磨损为主,随着载荷的增加,磨粒磨损转变为分层磨损。
{"title":"Study on Properties of FeCrCoMoCB Amorphous Coating Fabricated by Supersonic Plasma Spraying","authors":"Yuncai Zhao,&nbsp;Mingchao Hu,&nbsp;Weiling Guo,&nbsp;Yanfei Huang,&nbsp;Zeling Hu,&nbsp;Longlong Zhou,&nbsp;Zhiguo Xing,&nbsp;Haidou Wang","doi":"10.1007/s11665-025-11952-6","DOIUrl":"10.1007/s11665-025-11952-6","url":null,"abstract":"<div><p>Wear and corrosion are the main causes of structural failure of mechanical parts, using thermal spraying to fabricate raw materials into coating, which is a common method of protection of mechanical parts. In this work, FeCrCoMoCB amorphous coating was fabricated on the 45# steel substrate using supersonic plasma spraying (SPS). The microstructure, phase composition, mechanical, corrosion, and wear properties of FeCrCoMoCB amorphous coating were systematically investigated. The results show that FeCrCoMoCB amorphous coating had a relatively flat surface, low porosity with a dense structure, high hardness, and had an amorphous rate of more than 90%. The coating displays a passive region of about 500 mV, corrosion potential of − 1.01 V, and current density of 1.89 × 10<sup>-5</sup> A/cm<sup>2</sup>. The wear mechanism of FeCrCoMoCB amorphous coating is dominated by oxidation wear, and with the increase of load, the abrasive wear transforms into delamination wear.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 Focus:","pages":"24680 - 24691"},"PeriodicalIF":2.0,"publicationDate":"2025-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145384791","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Synchronously Strengthening and Toughening the Binder Jet Additive Manufactured 17-4PH Stainless Steel Based on the Solution and Aging Heat Treatment 基于固溶时效热处理的粘结剂喷射增韧17-4PH不锈钢
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-05 DOI: 10.1007/s11665-025-11981-1
Xin Chen, Junming Liu, Yaoyao Feng, Tianyi Zhang

For developing the suitable heat treatment for binder jetting additive manufactured (BJAM) 17-4PH stainless steel (17-4PH SS) to improve the mechanical properties, the evolutions of microstructure and strengthening behavior of sintered samples were specifically studied after solution and solution-aging heat treatments. The obtained results indicated that the grain boundary distribution proportion and grain size presented unobvious differences among samples. While, the δ-Fe content decreased in samples after both solution and solution-aging heat treatments, and the activation of {110} < 110 > slip system increased after heat treatments, resulting in the increase in toughness, the elongation rates reached 14.1% and 14.4%, respectively, whereas the original sample exhibited an elongation of 13.4% under identical testing conditions. Relying on the hybrid strengthening mechanism composed of precipitation strengthening from Cu-rich precipitates and the dislocation strengthening, sample after solution-aging heat treatment presented the highest tensile strength. A significant strength enhancement to 1100 MPa was achieved, marking a ~ 39% improvement over the baseline(791 MPa), achieving toughening and strengthening synchronously.

为研究粘结剂喷射添加剂(BJAM) 17-4PH不锈钢(17-4PH SS)的热处理工艺,研究了烧结试样在固溶和固溶时效热处理后的显微组织和强化行为演变。结果表明,不同样品的晶界分布比例和晶粒尺寸差异不明显。固溶和固溶时效热处理后,试样的δ-Fe含量降低,{110}< 110 >;滑移体系活化增加,韧性提高,伸长率分别达到14.1%和14.4%,而在相同测试条件下,原始试样的伸长率为13.4%。基于富cu析出相析出强化和位错强化的复合强化机制,固溶时效热处理后试样的抗拉强度最高。强度显著提高到1100mpa,比基线(791 MPa)提高了39%,实现了增韧和强化同步。
{"title":"Synchronously Strengthening and Toughening the Binder Jet Additive Manufactured 17-4PH Stainless Steel Based on the Solution and Aging Heat Treatment","authors":"Xin Chen,&nbsp;Junming Liu,&nbsp;Yaoyao Feng,&nbsp;Tianyi Zhang","doi":"10.1007/s11665-025-11981-1","DOIUrl":"10.1007/s11665-025-11981-1","url":null,"abstract":"<div><p>For developing the suitable heat treatment for binder jetting additive manufactured (BJAM) 17-4PH stainless steel (17-4PH SS) to improve the mechanical properties, the evolutions of microstructure and strengthening behavior of sintered samples were specifically studied after solution and solution-aging heat treatments. The obtained results indicated that the grain boundary distribution proportion and grain size presented unobvious differences among samples. While, the δ-Fe content decreased in samples after both solution and solution-aging heat treatments, and the activation of {110} &lt; 110 &gt; slip system increased after heat treatments, resulting in the increase in toughness, the elongation rates reached 14.1% and 14.4%, respectively, whereas the original sample exhibited an elongation of 13.4% under identical testing conditions. Relying on the hybrid strengthening mechanism composed of precipitation strengthening from Cu-rich precipitates and the dislocation strengthening, sample after solution-aging heat treatment presented the highest tensile strength. A significant strength enhancement to 1100 MPa was achieved, marking a ~ 39% improvement over the baseline(791 MPa), achieving toughening and strengthening synchronously.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"35 3","pages":"2633 - 2644"},"PeriodicalIF":2.0,"publicationDate":"2025-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146007190","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Performance Evaluation of Various Tool Materials and Electrical Discharge Machining Parameters for Fabrication of Large-Area Micro-textured Surfaces 各种刀具材料及电火花加工参数在大面积微织构表面加工中的性能评价
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-05 DOI: 10.1007/s11665-025-11997-7
Ranajit Mahanti, Rahul Singh, Manas Das

The present research investigates the performance of mild steel (MS), copper (Cu), and tungsten copper (WCu) form tools in fabricating large-area micro-textured surfaces, alongside the optimization of EDM parameters for surface texturing. The WCu tool electrode achieved the highest form accuracy, producing uniform, sharp-edged micro-pillars, followed by Cu and MS electrodes. The lower form accuracy of the MS tool leads to a higher overcut in the MS-textured surface and reduced interspacing, resulting in increased textured density. The overcut in the cavities is (sim) 50 ± 15, (sim) 75 ± 20, and (sim) 110 ± 20 µm for WCu, Cu, and MS tools, respectively. MS-textured surfaces exhibited the roughest morphology, with uneven recast material deposition with high frequency, micro-cracks, pockmarks, and voids, further reducing the patterned surfaces' hydrophobicity. XRD analysis indicates tensile residual stress, microstrain, crystallite size reduction, stable oxide layer, and carbide formation on patterned surfaces. The MS-textured surface exhibited the highest corrosion resistance, with a corrosion rate (CR) of 0.00918 mm/year, compared to the Cu- and WCu-textured surfaces, which showed CR values of 0.01994 and 0.02773 mm/year, respectively. Additionally, the MS-textured surface demonstrated the lowest wear rate and coefficient of friction (COF), recording a wear rate of 0.001138 mm3/m and a COF of 0.433.

本研究研究了低碳钢(MS)、铜(Cu)和钨铜(WCu)成形工具在制造大面积微纹理表面中的性能,以及表面纹理的电火花加工参数的优化。WCu工具电极的形状精度最高,可以产生均匀、边缘锋利的微柱,其次是Cu和MS电极。MS刀具的较低形状精度导致MS纹理表面的过切率更高,间距减少,从而增加了纹理密度。WCu工具、Cu工具和MS工具的空腔过切量分别为(sim) 50±15、(sim) 75±20和(sim) 110±20µm。ms织构表面形貌最粗糙,重铸材料沉积不均匀,高频,微裂纹,麻坑和空洞,进一步降低了图案表面的疏水性。XRD分析表明,图案表面存在拉伸残余应力、微应变、晶粒尺寸减小、稳定的氧化层和碳化物形成。ms织构表面的耐蚀性最高,腐蚀速率(CR)为0.00918 mm/年,而Cu和wcu织构表面的CR分别为0.01994和0.02773 mm/年。此外,ms织构表面的磨损率和摩擦系数(COF)最低,磨损率为0.001138 mm3/m, COF为0.433。
{"title":"Performance Evaluation of Various Tool Materials and Electrical Discharge Machining Parameters for Fabrication of Large-Area Micro-textured Surfaces","authors":"Ranajit Mahanti,&nbsp;Rahul Singh,&nbsp;Manas Das","doi":"10.1007/s11665-025-11997-7","DOIUrl":"10.1007/s11665-025-11997-7","url":null,"abstract":"<div><p>The present research investigates the performance of mild steel (MS), copper (Cu), and tungsten copper (WCu) form tools in fabricating large-area micro-textured surfaces, alongside the optimization of EDM parameters for surface texturing. The WCu tool electrode achieved the highest form accuracy, producing uniform, sharp-edged micro-pillars, followed by Cu and MS electrodes. The lower form accuracy of the MS tool leads to a higher overcut in the MS-textured surface and reduced interspacing, resulting in increased textured density. The overcut in the cavities is <span>(sim)</span> 50 ± 15, <span>(sim)</span> 75 ± 20, and <span>(sim)</span> 110 ± 20 µm for WCu, Cu, and MS tools, respectively. MS-textured surfaces exhibited the roughest morphology, with uneven recast material deposition with high frequency, micro-cracks, pockmarks, and voids, further reducing the patterned surfaces' hydrophobicity. XRD analysis indicates tensile residual stress, microstrain, crystallite size reduction, stable oxide layer, and carbide formation on patterned surfaces. The MS-textured surface exhibited the highest corrosion resistance, with a corrosion rate (CR) of 0.00918 mm/year, compared to the Cu- and WCu-textured surfaces, which showed CR values of 0.01994 and 0.02773 mm/year, respectively. Additionally, the MS-textured surface demonstrated the lowest wear rate and coefficient of friction (COF), recording a wear rate of 0.001138 mm<sup>3</sup>/m and a COF of 0.433.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"34 Focus:","pages":"26232 - 26252"},"PeriodicalIF":2.0,"publicationDate":"2025-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"145533126","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
Surface Integrity and Fretting Wear Behavior of Modified 17Cr2Ni2MoVNb Steel by Gas Carburizing Combined with Ultrasonic Surface Rolling 气体渗碳结合超声表面轧制改性17Cr2Ni2MoVNb钢的表面完整性及微动磨损行为
IF 2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2025-09-04 DOI: 10.1007/s11665-025-11955-3
Yalong Zhang, Chenjia Jiao, Yuhan Hu, Dapeng Shi, Luji Wu, Le Liu, Vincent Ji, Yanfei Xia

In this study, ultrasonic surface rolling (USR) was introduced to reduce the coefficient of friction (COF) and wear volume of 17Cr2Ni2MoVNb carburized gear steel. Residual stress distribution, microstructure, microhardness, and fretting wear behaviors with different USR rolling loads (600 N, 800 N 1000 N, and 1200 N) based on the gas carburizing treatment were examined. Results showed that dislocation and grain refinement were formed after USR treatment, and the residual compressive stresses (−527 MPa) and microhardness (908 HV0.2) at the top surface were increased by 57.78 % and 14.21 % of the samples treated with 1200 N. In addition, fretting wear behavior tests verified that the reduced COF and wear volume were due to the formation of a compressive stress field and gradient ultrafine grain. Moreover, carburized samples exhibited adhesion and three-body abrasion wear mechanisms, and the USR-treated samples showed oxidative wear and lamination.

采用超声表面轧制(USR)技术降低了17Cr2Ni2MoVNb渗碳齿轮钢的摩擦系数(COF)和磨损量。研究了不同USR轧制载荷(600 N、800 N、1000 N和1200 N)下合金的残余应力分布、显微组织、显微硬度和微动磨损行为。结果表明:经USR处理后,合金表面出现位错和晶粒细化,表面残余压应力(- 527 MPa)和显微硬度(908 HV0.2)分别比1200 n处理后提高了57.78%和14.21%。微动磨损行为试验证实,COF的减小和磨损体积的减小是由于压应力场和梯度超细晶粒的形成。渗碳后的样品表现出粘附磨损和三体磨损机制,usr处理后的样品表现出氧化磨损和层合磨损。
{"title":"Surface Integrity and Fretting Wear Behavior of Modified 17Cr2Ni2MoVNb Steel by Gas Carburizing Combined with Ultrasonic Surface Rolling","authors":"Yalong Zhang,&nbsp;Chenjia Jiao,&nbsp;Yuhan Hu,&nbsp;Dapeng Shi,&nbsp;Luji Wu,&nbsp;Le Liu,&nbsp;Vincent Ji,&nbsp;Yanfei Xia","doi":"10.1007/s11665-025-11955-3","DOIUrl":"10.1007/s11665-025-11955-3","url":null,"abstract":"<div><p>In this study, ultrasonic surface rolling (USR) was introduced to reduce the coefficient of friction (COF) and wear volume of 17Cr2Ni2MoVNb carburized gear steel. Residual stress distribution, microstructure, microhardness, and fretting wear behaviors with different USR rolling loads (600 N, 800 N 1000 N, and 1200 N) based on the gas carburizing treatment were examined. Results showed that dislocation and grain refinement were formed after USR treatment, and the residual compressive stresses (−527 MPa) and microhardness (908 HV<sub>0.2</sub>) at the top surface were increased by 57.78 % and 14.21 % of the samples treated with 1200 N. In addition, fretting wear behavior tests verified that the reduced COF and wear volume were due to the formation of a compressive stress field and gradient ultrafine grain. Moreover, carburized samples exhibited adhesion and three-body abrasion wear mechanisms, and the USR-treated samples showed oxidative wear and lamination.</p></div>","PeriodicalId":644,"journal":{"name":"Journal of Materials Engineering and Performance","volume":"35 3","pages":"2740 - 2752"},"PeriodicalIF":2.0,"publicationDate":"2025-09-04","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"146007074","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":4,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
引用次数: 0
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