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Residual Stress Distribution in Sapphire/Ti6Al4V Alloy Joints Brazed with CuTi+B Composite Fillers 使用 CuTi+B 复合填料钎焊的蓝宝石/Ti6Al4V 合金接头中的残余应力分布
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-19 DOI: 10.1007/s11665-024-09437-z
H. S. Yuan, H. Li, Y. Y. Wang, M. Q. Li

Residual stress is a key factor affecting the properties of ceramic/metal brazed joints. In this work, the residual stress of sapphire/Ti6Al4V alloy joints brazed with CuTi+B composite filler after cooling and reheated to 400 °C was calculated by finite element numerical simulation method. The effect of the B content in the filler and the filler thickness on the residual stress distribution of brazed joints after cooling was studied. The results show that the residual stress is mainly concentrated in the area near the filler layer. The maximum von Mises stress is located in the filler layer and a large Z-axial (the direction perpendicular to the brazed surface) tensile stress is on the sapphire near the filler layer. The B content and the filler thickness have no significant effect on the distribution of residual stress, but they have a certain effect on the value of residual stress of the sapphire near the filler layer. The von Mises stress and the Z-axial stress of this area increase with the increase of B content, and they decrease first and then increases with the increase of filler thickness. When the sapphire/Ti6Al4V joint is reheated to 400 °C, its residual stress significantly reduces and the residual stress on the periphery of the filler layer changes from compressive stress to tensile stress. As the B content is 1 and 3 wt%, the sapphire/Ti6Al4V joint with a smaller residual stress can be obtained. The microstructure observation and shear tests of the joints show that cracks appear in the high stress concentration area and the fracture starts from the area with maximum axial tensile stress, which verifies the accuracy of the simulation results.

残余应力是影响陶瓷/金属钎焊接头性能的一个关键因素。在这项工作中,采用有限元数值模拟方法计算了使用 CuTi+B 复合填料钎焊的蓝宝石/Ti6Al4V 合金接头在冷却并重新加热至 400 °C 后的残余应力。研究了填料中的 B 含量和填料厚度对冷却后钎焊接头残余应力分布的影响。结果表明,残余应力主要集中在填充层附近区域。最大的 von Mises 应力位于填充层,填充层附近的蓝宝石上存在较大的 Z 轴(垂直于钎焊表面的方向)拉应力。B 含量和填料厚度对残余应力的分布没有明显影响,但对填料层附近蓝宝石的残余应力值有一定影响。该区域的 von Mises 应力和 Z 轴应力随 B 含量的增加而增大,随填料厚度的增加先减小后增大。当蓝宝石/Ti6Al4V 接头重新加热到 400 ℃ 时,其残余应力明显降低,填充层外围的残余应力由压应力变为拉应力。当 B 含量为 1 和 3 wt%时,可获得残余应力较小的蓝宝石/Ti6Al4V 接头。接头的微观结构观察和剪切试验表明,裂纹出现在高应力集中区域,断裂从轴向拉应力最大的区域开始,这验证了模拟结果的准确性。
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引用次数: 0
Selected Articles from the 29th and 31st Heat Treating Society Conferences 第 29 届和第 31 届热处理学会会议文章选编
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-18 DOI: 10.1007/s11665-024-09317-6
Robert Cryderman, John Tartaglia, Robert Goldstein, Collin Russell
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引用次数: 0
The Role of Microstructure in the Gradient of Tensile Properties through Thickness in 7449 Aluminium Alloy Thick Plate 微观结构在 7449 铝合金厚板拉伸性能厚度梯度中的作用
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-15 DOI: 10.1007/s11665-024-09445-z
J. A. Heredero, J. Medina, J. M. Antoranz, P. Adeva

In this article, the yield strength, tensile strength, and the microstructure of the wrought aluminium alloy 7449 rolled thick plate have been studied through thickness under different temper conditions. For all heat treatments, it has been proven that the yield strength and tensile strength values increase from the surface to the centre. The largest difference between the centre and the surface, in both properties, occurs in the case of a sample aged at room temperature for 120 h (TTA temper). The sample artificially aged at 120 °C for 24 h (TTB temper) shows the best strength-gradient relationship of the tensile properties through the thickness. Metallographic characterisation carried out by optical and scanning electron microscopy shows much finer elongated grains in the region near the surface of the plate than in the centre, with incipient recrystallisation in the area near the surface. In addition, electron backscattered diffraction technique, used for micro-texture analysis, has proven the presence of a gradient of crystallography texture in the plate. This explains the yield strength gradient, since the rate of change of the Taylor factor through thickness correlates with the rate of the change of yield strength in the longitudinal direction for the samples studied.

本文研究了锻造铝合金 7449 轧制厚板在不同回火条件下的屈服强度、抗拉强度和微观结构。事实证明,在所有热处理中,屈服强度和抗拉强度值都是从表面向中心递增的。在室温下老化 120 小时(TTA 回火)的试样,中心和表面在这两项性能上的差异最大。在 120 °C 下人工老化 24 小时的样品(TTB 回火)显示出拉伸性能在厚度上的最佳强度梯度关系。通过光学显微镜和扫描电子显微镜进行的金相表征显示,板材表面附近区域的细长晶粒比中心区域的细长晶粒要细得多,表面附近区域出现了初生再结晶现象。此外,用于微观纹理分析的电子反向散射衍射技术证明,板材中存在结晶纹理梯度。这就解释了屈服强度梯度,因为泰勒系数在厚度上的变化率与所研究样品在纵向上的屈服强度变化率相关。
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引用次数: 0
Austempering and Bainitic Transformation Kinetics of AISI 52100 AISI 52100 的奥氏体化和贝氏体转变动力学
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-12 DOI: 10.1007/s11665-024-09436-0
Haoxing You, Mei Yang, Yishu Zhang, Richard D. Sisson Jr.

AISI 52100 is a high carbon alloy steel typically used in bearings. One hardening heat treatment method for AISI 52100 is austempering, in which the steel is heated to above austenitizing temperature, cooled to just above martensite starting (Ms) temperature in quench media (typically molten salt), held at that temperature until the transformation to bainite is completed and then cooled further to room temperature. Different austempering temperatures and holding times will develop different bainite percentages in the steel and result in a variation in mechanical properties. In the present work, the bainitic transformation kinetics of AISI 52100 were investigated through experiments and simulation. Molten salt austempering trials of AISI 52100 were conducted at selected austempering temperatures and holding times. The microstructure of austempered samples were characterized with optical microscope and x-ray diffraction. The bainitic transformation kinetics were analyzed by Avrami equations using measured hardness data. The CHTE quench probe was used to measure the cooling curves in the molten salt from austenitizing temperature to the selected austempering temperatures. The heat transfer coefficient (HTC) was calculated with the measured cooling rates and used to calculate the bainitic transformation kinetics via DANTE software. The experimental results were compared with the calculated results and displayed good agreement.

AISI 52100 是一种高碳合金钢,通常用于轴承。奥氏体回火是 AISI 52100 的一种淬火热处理方法,将钢加热至奥氏体化温度以上,在淬火介质(通常为熔盐)中冷却至略高于马氏体起始(Ms)温度,在该温度下保温至贝氏体转变完成,然后进一步冷却至室温。不同的奥氏体回火温度和保温时间会在钢中形成不同比例的贝氏体,并导致机械性能的变化。本研究通过实验和模拟研究了 AISI 52100 的贝氏体转变动力学。在选定的奥氏体回火温度和保温时间下,对 AISI 52100 进行了熔盐奥氏体回火试验。用光学显微镜和 X 射线衍射法对奥氏体回火样品的微观结构进行了表征。利用测得的硬度数据,通过阿夫拉米方程分析了贝氏体转变动力学。使用 CHTE 淬火探头测量了熔盐从奥氏体化温度到选定奥氏体回火温度的冷却曲线。根据测量的冷却速率计算出传热系数 (HTC),并通过 DANTE 软件计算贝氏体转变动力学。实验结果与计算结果进行了比较,显示出良好的一致性。
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引用次数: 0
Correction: Microstructures and Mechanical Behaviors of Ni-Based Single-Crystal Superalloy DD90 Joints Brazed with a Co-Based Interlayer 更正:采用共基夹层钎焊的镍基单晶超合金 DD90 接头的微观结构和力学性能
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-11 DOI: 10.1007/s11665-024-09439-x
F. Gao, J. D. Liu, C. W. Zhu, H. Mei, Z. P. Zhang, J. L. Liu, X. M. Du, J. G. Li
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引用次数: 0
Regularization of Hole-Drilling Residual Stress Measurements with Eccentric Holes: An Approach with Influence Functions 偏心孔钻孔残余应力测量的正则化:利用影响函数的方法
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-10 DOI: 10.1007/s11665-024-09447-x
M. Beghini, L. Bertini, M. Cococcioni, T. Grossi, C. Santus, A. Benincasa

The hole-drilling method is one of the most widespread techniques to measure residual stresses. Since the introduction of the Integral Method to evaluate non-uniform stress distributions, there has been a considerable improvement in the instrumentation technology, as step increments of about 10 microns are now achievable. However, that spatial resolution makes the ill-posedness of the problem stand out among other sources of uncertainty. As the solution becomes totally dominated by noise, an additional regularization of the problem is needed to obtain meaningful results. Tikhonov regularization is the most common option, as it is also prescribed by the hole-drilling ASTM E837 standard, but it has only been studied in the reference case of a hole with no eccentricity with respect to the strain rosette. A recent work by Schajer addresses the eccentricity problem by defining a correction strategy that transforms strain measurements, allowing one to obtain the solution with the usual decoupled equations. In this work, Tikhonov regularization is applied to the eccentric hole case through the influence functions approach, in order to avoid the introduction of new error-compensating functions and bias-prone interpolations. Some useful general considerations for a practical implementation of the procedure and an experimental test case on an aluminum specimen are presented.

钻孔法是测量残余应力最广泛的技术之一。自从引入积分法来评估非均匀应力分布以来,仪器技术有了长足的进步,现在可以实现约 10 微米的步进增量。然而,这种空间分辨率使得问题的不确定性在其他不确定性来源中显得尤为突出。由于解法完全由噪声主导,因此需要对问题进行额外的正则化处理,以获得有意义的结果。Tikhonov 正则化是最常见的选择,因为它也是钻孔 ASTM E837 标准的规定,但它只在孔相对于应变罗盘没有偏心的参考情况下进行过研究。Schajer 最近的一项研究通过定义一种转换应变测量值的修正策略来解决偏心问题,从而使人们能够通过通常的解耦方程获得解决方案。在这项工作中,通过影响函数方法将 Tikhonov 正则化应用于偏心孔情况,以避免引入新的误差补偿函数和易产生偏差的插值。文中介绍了一些有用的一般考虑因素,以便实际应用该程序,并介绍了一个铝试样的实验测试案例。
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引用次数: 0
Residual Stress in Cold Spray SS304L Measured Via Neutron Diffraction and Comparison of Analytical Models to Predict the Residual Stress 通过中子衍射测量冷喷 SS304L 的残余应力并比较预测残余应力的分析模型
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-10 DOI: 10.1007/s11665-024-09422-6
Christopher M. Roper, Chris M. Fancher, Jeffrey R. Bunn, Luke N. Brewer

This study employs neutron diffraction to investigate the relationship between residual stress and coating thickness in cold sprayed 304L austenitic stainless steel. Results show that shot peening predominantly impacts the residual stress profile, leading to substantial in-plane compressive force. The impact of laser heating, a widely used method to alter cold spray's microstructural properties, on the coating's residual stress is also analyzed. The findings indicate that the maximum compressive residual stress in the in-plane component is mainly independent of coating thickness, which suggests that the material properties determine the maximum residual stress. The cold sprayed deposits possessed compressive, nearly biaxial strain and stresses. After laser heating, these stresses were replaced by tensile residual stresses. Two analytical models, the Tsui and Clyne and the Boruah models, for predicting residual stresses are also evaluated, and both models provide reasonable fits to the experimental data. At this point, the deviations between the experimental results and the models are principally caused by the inability of the current models to address plastic deformation and relaxation, and the residual stresses generated by thermal gradients.

本研究利用中子衍射法研究了冷喷 304L 奥氏体不锈钢中残余应力与涂层厚度之间的关系。结果表明,喷丸强化主要影响残余应力曲线,从而产生巨大的平面压缩力。此外,还分析了激光加热对涂层残余应力的影响,激光加热是改变冷喷微观结构特性的一种广泛使用的方法。研究结果表明,面内部分的最大压缩残余应力主要与涂层厚度无关,这表明材料特性决定了最大残余应力。冷喷沉积物具有近似双轴的压应变和应力。激光加热后,这些应力被拉伸残余应力所取代。我们还评估了预测残余应力的两个分析模型,即 Tsui 和 Clyne 模型以及 Boruah 模型,这两个模型都与实验数据进行了合理的拟合。目前,实验结果与模型之间的偏差主要是由于现有模型无法处理塑性变形和松弛以及热梯度产生的残余应力。
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引用次数: 0
Special Issue: Residual Stress Analysis—Measurement, Effects, and Control 特刊:残余应力分析--测量、影响和控制
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-10 DOI: 10.1007/s11665-024-09366-x
Rajan Bhambroo, Lesley Frame, Andrew Payzant, James Pineault
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引用次数: 0
Correlation Between Pressureless Sintering, Microstructure, and Properties of ZrB2-SiC-Y2O3 Composites ZrB2-SiC-Y2O3 复合材料的无压烧结、微观结构与性能之间的相关性
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-08 DOI: 10.1007/s11665-024-09417-3
S. Sarkar, M. K. Mondal, M. Mallik

The influence of Y2O3 addition on densification, physical, mechanical, thermal, and oxidation properties of ZrB2-20 vol.%SiC- (0-15 vol.%Y2O3) composites was investigated in the present study. Powders of ZrB2-SiC-Y2O3 were cold compacted uniaxially, and green compacts were densified by pressure-less sintering. Results indicate that Y2O3 addition improves the sinterability and mechanical properties, whereas it diminishes the electrical and thermal conductivities of the investigated composites. Removal of surface oxides by the additives and segregation of Y2O3 particles at the triple junction of the ZrB2 grains enhances densification. Reduction in porosity (9.5-4.2%) through Y2O3 addition (0-15 vol.%) improves hardness (up to 52%), relative elastic modulus (up to 9%), and fracture toughness (up to 26%) of the investigated composites. The electrical conductivity has been observed to vary in the range of 2.67-1.92 106 S/m, and thermal diffusivity values decrease with an increase in Y2O3 content and temperature. Oxidation studies indicate that the ZrB2-SiC composite shows better oxidation resistance than other investigated composites. Characterization of oxidized scales confirms the formation of a thicker oxide layer over the samples containing Y2O3.

本研究探讨了添加 Y2O3 对 ZrB2-20 vol.%SiC- (0-15 vol.%Y2O3) 复合材料的致密化、物理、机械、热和氧化性能的影响。对 ZrB2-SiC-Y2O3 粉末进行单轴冷压实,并通过无压烧结对绿色压实物进行致密化。结果表明,添加 Y2O3 可改善所研究复合材料的烧结性和机械性能,但会降低其导电性和导热性。添加剂对表面氧化物的去除以及 Y2O3 粒子在 ZrB2 晶粒三重交界处的偏析提高了致密性。通过添加 Y2O3(0-15 Vol.%)降低孔隙率(9.5-4.2%),提高了所研究复合材料的硬度(高达 52%)、相对弹性模量(高达 9%)和断裂韧性(高达 26%)。电导率的变化范围为 2.67-1.92 106 S/m,热扩散值随着 Y2O3 含量和温度的增加而降低。氧化研究表明,ZrB2-SiC 复合材料的抗氧化性优于其他已研究过的复合材料。氧化鳞片的表征证实,在含有 Y2O3 的样品上形成了较厚的氧化层。
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引用次数: 0
Residual Stress Distribution in Aluminum/Polypropylene/Aluminum Sandwich Laminates in U-Channel Draw Bending 铝/聚丙烯/铝夹层板在 U 型槽拉伸弯曲中的残余应力分布
IF 2.2 4区 材料科学 Q3 MATERIALS SCIENCE, MULTIDISCIPLINARY Pub Date : 2024-04-05 DOI: 10.1007/s11665-024-09421-7
Caroline Kella, Pankaj K. Mallick

Residual stresses in sheet metal parts are internal stresses that remain after the release of elastic strains at the end of metal forming operations. When the formed sheet metal part is removed from the forming tools, it not only springs back but also acquires a through-thickness residual stress distribution. Residual stresses for monolithic aluminum sheets and aluminum/polypropylene/aluminum sandwich laminates after springback of a U-channel formed by draw bending are presented in this paper. The forming stresses at the end of punch travel and residual stresses at the end of punch withdrawal are numerically determined using LS-DYNA, a well-established nonlinear finite element software. The through-thickness forming stress distribution is determined using an explicit forming simulation, following which the through-thickness residual stress distribution is determined using an implicit springback simulation. Stress distributions are studied at the die corner, punch corner and along the wall of the U-channel. Both forming and residual stresses in the sandwich laminate are found to be lower than those in monolithic aluminum of equivalent thickness. In sandwich laminates with the same skin thickness, higher residual stresses are observed in the skin layers as the core thickness is increased. The residual stresses at the punch corners of the formed U-channels are more influenced by changes in the die and punch corner radii than at the die corner.

钣金件中的残余应力是指在金属成型操作结束时释放弹性应变后残留的内应力。当成形的金属板材部件从成形工具中取出时,不仅会回弹,而且还会获得通厚的残余应力分布。本文介绍了整体铝板和铝/聚丙烯/铝夹层板在通过拉弯形成的 U 型槽回弹后的残余应力。本文使用成熟的非线性有限元软件 LS-DYNA 对冲头行程末端的成形应力和冲头撤回末端的残余应力进行了数值测定。通过显式成形模拟确定了通厚成形应力分布,然后通过隐式回弹模拟确定了通厚残余应力分布。对模具角、冲头角和 U 型槽壁的应力分布进行了研究。结果发现,夹层板的成形应力和残余应力均低于同等厚度的整体铝板。在表皮厚度相同的夹层板中,表皮层的残余应力随着芯材厚度的增加而增大。与模具角相比,成形 U 型槽冲孔角处的残余应力受模具和冲孔角半径变化的影响更大。
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引用次数: 0
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Journal of Materials Engineering and Performance
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