Pub Date : 2015-02-11DOI: 10.4236/WJNSE.2015.51001
Sabri M. Husssein, O. Shihab, S. S. Ibrahim, N. M. Ahmed
Interaction between kaolin (particle size 53 and 106 μm) and urea was studied by infrared spectroscopy and powder X-ray diffraction. Interaction was found to be dependent on the particle size of kaolin raw material. Nature of interaction achieved through the formation of hydrogen bonds between urea and both AlOH and Si-O surface of kaolinite. Effect of temperature on equilibrium adsorption of methylene blue (MB) from aqueous solution using kaolin also studied, the results were analyzed by Langmuir and frendlich isotherms. Thermodynamic parameters such as ΔG, ΔH and ΔS were calculated. Results suggested that the MB adsorption on kaolin was spontaneous and exothermic process.
{"title":"Interaction between Kaolin and Urea in Organoclay and Its Impact on Removing Methylene Blue from Aqueous Solution","authors":"Sabri M. Husssein, O. Shihab, S. S. Ibrahim, N. M. Ahmed","doi":"10.4236/WJNSE.2015.51001","DOIUrl":"https://doi.org/10.4236/WJNSE.2015.51001","url":null,"abstract":"Interaction between kaolin (particle size 53 and 106 μm) and urea was studied by infrared spectroscopy and powder X-ray diffraction. Interaction was found to be dependent on the particle size of kaolin raw material. Nature of interaction achieved through the formation of hydrogen bonds between urea and both AlOH and Si-O surface of kaolinite. Effect of temperature on equilibrium adsorption of methylene blue (MB) from aqueous solution using kaolin also studied, the results were analyzed by Langmuir and frendlich isotherms. Thermodynamic parameters such as ΔG, ΔH and ΔS were calculated. Results suggested that the MB adsorption on kaolin was spontaneous and exothermic process.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"176 2 1","pages":"1-9"},"PeriodicalIF":0.0,"publicationDate":"2015-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878966","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2015-02-11DOI: 10.4236/WJNSE.2015.51005
Ahmed H. Kurda, Y. M. Hassan, N. M. Ahmed
Zinc oxide (ZnO) nanorods have been synthesized by solution processing hydrothermal method in low temperature using the spin coating technique. Zinc acetate dehydrate, Zinc nitrate hexahydrate and hexamethylenetetramine were used as a starting material. The ZnO seed layer was first deposited by spin coated of ethanol zinc acetate dehydrate solution on a glass substrate. ZnO nanorods were grown on the ZnO seed layer from zinc nitrate hexahydrate and hexamethylene-tetramine solution, and their diameters, lengths were controlled by precursor concentration and development time. From UV-Visible spectrometry the optical band gap energy of ZnO nanorods was calculated to be 3.3 eV. The results of X-Ray Diffraction (XRD) showed the highly oriented nature of ZnO nanorods the hardest (002) peak reflects that c-axis elongated nanorods are oriented normal to the glass substrate. The Field Emission Scanning Electron Microscope (FESEM) was employed to measure both of average diameter of ZnO nanorods, Energy Dispersive X-Ray (EDX) is used to identify the elemental present and to determine the element composition in the samples.
{"title":"Controlling Diameter, Length and Characterization of ZnO Nanorods by Simple Hydrothermal Method for Solar Cells","authors":"Ahmed H. Kurda, Y. M. Hassan, N. M. Ahmed","doi":"10.4236/WJNSE.2015.51005","DOIUrl":"https://doi.org/10.4236/WJNSE.2015.51005","url":null,"abstract":"Zinc oxide (ZnO) nanorods have been synthesized by solution processing hydrothermal method in low temperature using the spin coating technique. Zinc acetate dehydrate, Zinc nitrate hexahydrate and hexamethylenetetramine were used as a starting material. The ZnO seed layer was first deposited by spin coated of ethanol zinc acetate dehydrate solution on a glass substrate. ZnO nanorods were grown on the ZnO seed layer from zinc nitrate hexahydrate and hexamethylene-tetramine solution, and their diameters, lengths were controlled by precursor concentration and development time. From UV-Visible spectrometry the optical band gap energy of ZnO nanorods was calculated to be 3.3 eV. The results of X-Ray Diffraction (XRD) showed the highly oriented nature of ZnO nanorods the hardest (002) peak reflects that c-axis elongated nanorods are oriented normal to the glass substrate. The Field Emission Scanning Electron Microscope (FESEM) was employed to measure both of average diameter of ZnO nanorods, Energy Dispersive X-Ray (EDX) is used to identify the elemental present and to determine the element composition in the samples.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"05 1","pages":"34-40"},"PeriodicalIF":0.0,"publicationDate":"2015-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70879052","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2015-02-11DOI: 10.4236/WJNSE.2015.51002
Eman Alzahrani
Green chemistry methods for production of nanoparticles have many advantages, such as ease of use, which makes the methods desirable and economically viable. The aim of the present work was to green synthesise silver nanoparticles (SNPs) using aqueous tangerine peel extract in different ratios (2:1, 1:1, 1:2). The formed SNPs were characterised using ultraviolet-visible (UV-Vis) spectrophotometry, and transmission electron microscopy (TEM). The UV-Vis spectra showed that the highest absorbance was observed when the ratio of peel tangerine extract to silver nitrate solution was 1:2. The transmission electron micrographs showed the formation of poly dispersed nanoparticles. It was found that the average diameter of the nanoparticles was 30.29 ± 5.1 nm, 16.68 ± 5.7 nm, and 25.85 ± 8.4 nm, using a tangerine peel solution and silver nitrate solution ratio of 2:1, 1:1, and 1:2, respectively. The formed SNPs were evaluated as catalysts for methyl orange dye degradation, and the results confirmed that SNPs can speed up the degradation of the dye.
{"title":"Eco-Friendly Production of Silver Nanoparticles from Peel of Tangerine for Degradation of Dye","authors":"Eman Alzahrani","doi":"10.4236/WJNSE.2015.51002","DOIUrl":"https://doi.org/10.4236/WJNSE.2015.51002","url":null,"abstract":"Green chemistry methods for production of nanoparticles have many advantages, such as ease of use, which makes the methods desirable and economically viable. The aim of the present work was to green synthesise silver nanoparticles (SNPs) using aqueous tangerine peel extract in different ratios (2:1, 1:1, 1:2). The formed SNPs were characterised using ultraviolet-visible (UV-Vis) spectrophotometry, and transmission electron microscopy (TEM). The UV-Vis spectra showed that the highest absorbance was observed when the ratio of peel tangerine extract to silver nitrate solution was 1:2. The transmission electron micrographs showed the formation of poly dispersed nanoparticles. It was found that the average diameter of the nanoparticles was 30.29 ± 5.1 nm, 16.68 ± 5.7 nm, and 25.85 ± 8.4 nm, using a tangerine peel solution and silver nitrate solution ratio of 2:1, 1:1, and 1:2, respectively. The formed SNPs were evaluated as catalysts for methyl orange dye degradation, and the results confirmed that SNPs can speed up the degradation of the dye.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"5 1","pages":"10-16"},"PeriodicalIF":0.0,"publicationDate":"2015-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878977","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2015-02-11DOI: 10.4236/WJNSE.2015.51004
M. Naschie
A basically topological interpretation of the Casimir effect is given as a natural intrinsic property of the geometrical topological structure of the quantum-Cantorian micro spacetime. This new interpretation compliments the earlier conventional interpretation as vacuum fluctuation or as a Schwinger source and links the Casimir energy to the so called missing dark energy density of the cosmos. We start with a general outline of the theoretical principle and basic design concepts of a proposed Casimir dark energy nano reactor. In a nutshell the theory and consequently the actual design depends crucially upon the equivalence between the dark energy density of the cosmos and the faint local Casimir effect produced by two sides boundary condition quantum waves. This Casimir effect is then colossally amplified as a one sided quantum wave pushing from the inside on the one sided M?bius-like boundary with nothing balancing it from the non-existent outside. In view of the present theory, this one sided M?bius-like boundary of the holographic boundary of the universe is essentially what leads to the observed accelerated expansion of the cosmos. Thus in principle we will restructure the local topology of space using material nanoscience technology to create an artificial local high dimensionality with a Dvoretzky theorem like volume measure concentration. Needless to say the entire design is based completely on the theory of quantum wave dark energy proposed by the present author. The quintessence of the present theory is easily explained as the intrinsic Casimir topological energy where produced from the zero set of the quantum particle when we extract the empty set quantum wave from it and find by restructuring space via plates similar to that of the classical Casimir experiments but with some modification.
{"title":"The Casimir Topological Effect and a Proposal for a Casimir-Dark Energy Nano Reactor *","authors":"M. Naschie","doi":"10.4236/WJNSE.2015.51004","DOIUrl":"https://doi.org/10.4236/WJNSE.2015.51004","url":null,"abstract":"A basically topological interpretation of the Casimir effect is given as a natural intrinsic property of the geometrical topological structure of the quantum-Cantorian micro spacetime. This new interpretation compliments the earlier conventional interpretation as vacuum fluctuation or as a Schwinger source and links the Casimir energy to the so called missing dark energy density of the cosmos. We start with a general outline of the theoretical principle and basic design concepts of a proposed Casimir dark energy nano reactor. In a nutshell the theory and consequently the actual design depends crucially upon the equivalence between the dark energy density of the cosmos and the faint local Casimir effect produced by two sides boundary condition quantum waves. This Casimir effect is then colossally amplified as a one sided quantum wave pushing from the inside on the one sided M?bius-like boundary with nothing balancing it from the non-existent outside. In view of the present theory, this one sided M?bius-like boundary of the holographic boundary of the universe is essentially what leads to the observed accelerated expansion of the cosmos. Thus in principle we will restructure the local topology of space using material nanoscience technology to create an artificial local high dimensionality with a Dvoretzky theorem like volume measure concentration. Needless to say the entire design is based completely on the theory of quantum wave dark energy proposed by the present author. The quintessence of the present theory is easily explained as the intrinsic Casimir topological energy where produced from the zero set of the quantum particle when we extract the empty set quantum wave from it and find by restructuring space via plates similar to that of the classical Casimir experiments but with some modification.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"36 1","pages":"26-33"},"PeriodicalIF":0.0,"publicationDate":"2015-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878658","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2015-02-11DOI: 10.4236/WJNSE.2015.51003
Chernet Amente, K. Dharamvir
Employing the arc discharge method we prepared carbon nanotubes, CNTs, in open air deionized water. Their morphology was studied varying the annealing temperature and characterizing by Raman Spectroscopy, Transmission Electron Microscopy (TEM), X-Ray Diffractogram (XRD) and Energy Dispersion X-Ray (EDX). According to the study, the CNTs are found self-assembled where the graphene sheets and/or defects are observed sort out themselves with enhancement of temperature.
{"title":"Thermally Agitated Self Assembled Carbon Nanotubes and the Scenario of Extrinsic Defects","authors":"Chernet Amente, K. Dharamvir","doi":"10.4236/WJNSE.2015.51003","DOIUrl":"https://doi.org/10.4236/WJNSE.2015.51003","url":null,"abstract":"Employing the arc discharge method we prepared carbon nanotubes, CNTs, in open air deionized water. Their morphology was studied varying the annealing temperature and characterizing by Raman Spectroscopy, Transmission Electron Microscopy (TEM), X-Ray Diffractogram (XRD) and Energy Dispersion X-Ray (EDX). According to the study, the CNTs are found self-assembled where the graphene sheets and/or defects are observed sort out themselves with enhancement of temperature.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"5 1","pages":"17-25"},"PeriodicalIF":0.0,"publicationDate":"2015-02-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878597","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2014-11-19DOI: 10.4236/WJNSE.2014.44015
Ting Tian, Jing Hu, Zuobing Xiao
Inorganic hollow spheres have shown their superiority in photocatalytic area due to the large specific surface area, controllable structure and their own special optical, electrical, magnetic properties. According to the classification of inorganic hollow spheres as photocatalysts, recent research progress and application status have been summarized in this paper. At last, the future developments of inorganic hollow spheres in photocatalytic field have been discussed.
{"title":"Research Advances in Photocatalysis of Inorganic Hollow Spheres","authors":"Ting Tian, Jing Hu, Zuobing Xiao","doi":"10.4236/WJNSE.2014.44015","DOIUrl":"https://doi.org/10.4236/WJNSE.2014.44015","url":null,"abstract":"Inorganic hollow spheres have shown their superiority in photocatalytic area due to the large specific surface area, controllable structure and their own special optical, electrical, magnetic properties. According to the classification of inorganic hollow spheres as photocatalysts, recent research progress and application status have been summarized in this paper. At last, the future developments of inorganic hollow spheres in photocatalytic field have been discussed.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"04 1","pages":"111-125"},"PeriodicalIF":0.0,"publicationDate":"2014-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878805","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2014-11-19DOI: 10.4236/WJNSE.2014.44018
P. Panda, S. Padhi, G. Dash
High frequency properties of 4H-SiC double drift region (DDR) Mixed Tunnelling Avalanche Transit Time (MITATT) diodes are studied through computer simulation method. It is interesting to observe that the efficiency of SiC (flat) DDR MITATT diode (16%) is more than 4 times that of Si (flat) DDR MITATT diode (3.59%). In addition, a power output of more than 15 times from the SiC MITATT diode compared to the Si MITATT diode is commendable. A reduced noise measure of 17.71 dB from a low-high-low (lo-hi-lo) structure compared to that of 21.5 dB from a flat structure of SiC is indicative of the favourable effect of tunnelling current on the MITATT diode performance.
{"title":"High Efficiency SiC Terahertz Source in Mixed Tunnelling Avalanche Transit Time Mode","authors":"P. Panda, S. Padhi, G. Dash","doi":"10.4236/WJNSE.2014.44018","DOIUrl":"https://doi.org/10.4236/WJNSE.2014.44018","url":null,"abstract":"High frequency properties of 4H-SiC double drift region (DDR) Mixed Tunnelling Avalanche Transit Time (MITATT) diodes are studied through computer simulation method. It is interesting to observe that the efficiency of SiC (flat) DDR MITATT diode (16%) is more than 4 times that of Si (flat) DDR MITATT diode (3.59%). In addition, a power output of more than 15 times from the SiC MITATT diode compared to the Si MITATT diode is commendable. A reduced noise measure of 17.71 dB from a low-high-low (lo-hi-lo) structure compared to that of 21.5 dB from a flat structure of SiC is indicative of the favourable effect of tunnelling current on the MITATT diode performance.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"04 1","pages":"143-150"},"PeriodicalIF":0.0,"publicationDate":"2014-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878920","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2014-11-19DOI: 10.4236/WJNSE.2014.44016
M. Ishihara, Ryuji Hirase, H. Yoshioka
Photoinduced spectral change can be utilized for various optical devices. The photoinduced spectral change due to an organic dye was demonstrated for the organic-inorganic hybrid film without the aid of photochromism with a simple preparation method for the first time. By the hybridization of a cyanine dye of 2-[5-(1,3-dihydro-3,3-dimethyl-1-octadecyl-2H-indol-2-ylidene)-1,3-pentadienyl]-3,3-dimethyl-1-octadecyl-3H-indolium perchlorate (NK3175) with an inorganic layered material of cation-exchangeable clay, smectite (SWN), a spectral change attributed to NK3175 was generated upon the irradiation of UV light. This result might serve as useful information on the methodology to produce optically controlled function for photoresponsive systems. Furthermore, the hybrid film of SWN and NK3175 was characterized by the use of XRD and FT-IR measurements. NK3175 molecules adsorbed onto external surfaces of SWN were confined by oriented SWN. It was suggested that the enhanced intermolecular interaction between NK3175 molecules caused by the hybridization with SWN resulted in the change of the aggregation state of NK3175 upon the UV light irradiation, which accounts for the spectral change of NK3175.
{"title":"Unusual Spectral Change Due to a Cyanine Dye Adsorbed on an Inorganic Layered Material upon Photoirradiation","authors":"M. Ishihara, Ryuji Hirase, H. Yoshioka","doi":"10.4236/WJNSE.2014.44016","DOIUrl":"https://doi.org/10.4236/WJNSE.2014.44016","url":null,"abstract":"Photoinduced spectral change can be utilized for various optical devices. The photoinduced spectral change due to an organic dye was demonstrated for the organic-inorganic hybrid film without the aid of photochromism with a simple preparation method for the first time. By the hybridization of a cyanine dye of 2-[5-(1,3-dihydro-3,3-dimethyl-1-octadecyl-2H-indol-2-ylidene)-1,3-pentadienyl]-3,3-dimethyl-1-octadecyl-3H-indolium perchlorate (NK3175) with an inorganic layered material of cation-exchangeable clay, smectite (SWN), a spectral change attributed to NK3175 was generated upon the irradiation of UV light. This result might serve as useful information on the methodology to produce optically controlled function for photoresponsive systems. Furthermore, the hybrid film of SWN and NK3175 was characterized by the use of XRD and FT-IR measurements. NK3175 molecules adsorbed onto external surfaces of SWN were confined by oriented SWN. It was suggested that the enhanced intermolecular interaction between NK3175 molecules caused by the hybridization with SWN resulted in the change of the aggregation state of NK3175 upon the UV light irradiation, which accounts for the spectral change of NK3175.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"04 1","pages":"126-133"},"PeriodicalIF":0.0,"publicationDate":"2014-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.4236/WJNSE.2014.44016","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878861","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2014-11-19DOI: 10.4236/WJNSE.2014.44017
B. Hafsi, Rabii Elmissaoui, A. Kalboussi
This paper presents a basic block for building large-scale single-electron neural networks. This macro block is completely composed of SET inverter circuits. We present and discuss the basic parts of this device. The full design and simulation results were done using MATLAB and SIMON, which are a single-electron tunnel device and circuit simulator based on a Monte Carlo method. Special measures had to be taken in order to simulate this circuit correctly in SIMON and compare results with those of SPICE simulation done before. Moreover, we study part of the network as a memory cell with the idea of combining the extremely low-power properties of the SET and the compact design.
{"title":"Neural Network Based on SET Inverter Structures: Neuro-Inspired Memory","authors":"B. Hafsi, Rabii Elmissaoui, A. Kalboussi","doi":"10.4236/WJNSE.2014.44017","DOIUrl":"https://doi.org/10.4236/WJNSE.2014.44017","url":null,"abstract":"This paper presents a basic block for building large-scale single-electron neural networks. This macro block is completely composed of SET inverter circuits. We present and discuss the basic parts of this device. The full design and simulation results were done using MATLAB and SIMON, which are a single-electron tunnel device and circuit simulator based on a Monte Carlo method. Special measures had to be taken in order to simulate this circuit correctly in SIMON and compare results with those of SPICE simulation done before. Moreover, we study part of the network as a memory cell with the idea of combining the extremely low-power properties of the SET and the compact design.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"4 1","pages":"134-142"},"PeriodicalIF":0.0,"publicationDate":"2014-11-19","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"https://sci-hub-pdf.com/10.4236/WJNSE.2014.44017","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878911","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2014-09-05DOI: 10.4236/WJNSE.2014.43014
M. Uonis, B. M. Mustafa, A. Ezzat
The research studies the effect of the distance between the sample and the plasma sputtering source on the properties of the junction (silicon wafer-carbon nanotubes). The silicon wafer is fixed at (near, medium and far distances from the plasma source which is in the form of high purity graphite rod heated electrically). For the three cases, thickness of the sample is constant (20 nm). The samples were studied by scanning electron (SEM) and atomic force microscopes (AFM), X-ray and Raman spectra. For optimum distances the carbon layer is in the form of multi wall carbon nanotube (MWCNT). SEM images shows no formation of CNT on the Si wafer for near distance, which is consistent with the AFM images, X-ray and Raman spectrograms and no existence of characteristics (002) peaks whereas it appears for medium and longer distances, and by experience the optimum distance was found. This means that at closer distance high energy and high intensity plasma particles prevent the formation of CNT. This effect decreases with increasing distance of substrate from the graphite rod.
{"title":"The Effect of Carbon Rod—Specimens Distance on the Structural and Electrical Properties of Carbon Nanotube","authors":"M. Uonis, B. M. Mustafa, A. Ezzat","doi":"10.4236/WJNSE.2014.43014","DOIUrl":"https://doi.org/10.4236/WJNSE.2014.43014","url":null,"abstract":"The research studies the effect of the distance between the sample and the plasma sputtering source on the properties of the junction (silicon wafer-carbon nanotubes). The silicon wafer is fixed at (near, medium and far distances from the plasma source which is in the form of high purity graphite rod heated electrically). For the three cases, thickness of the sample is constant (20 nm). The samples were studied by scanning electron (SEM) and atomic force microscopes (AFM), X-ray and Raman spectra. For optimum distances the carbon layer is in the form of multi wall carbon nanotube (MWCNT). SEM images shows no formation of CNT on the Si wafer for near distance, which is consistent with the AFM images, X-ray and Raman spectrograms and no existence of characteristics (002) peaks whereas it appears for medium and longer distances, and by experience the optimum distance was found. This means that at closer distance high energy and high intensity plasma particles prevent the formation of CNT. This effect decreases with increasing distance of substrate from the graphite rod.","PeriodicalId":66816,"journal":{"name":"纳米科学与工程(英文)","volume":"04 1","pages":"105-110"},"PeriodicalIF":0.0,"publicationDate":"2014-09-05","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"70878689","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":0,"RegionCategory":"","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}