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Experimental Study & Heat Transfer Analysis on Copper Spiral Heat Exchanger Using Water Based SiO2 Nanofluid as Coolant 以水基SiO2纳米流体为冷却剂的铜螺旋换热器的实验研究与传热分析
Pub Date : 2018-12-06 DOI: 10.4236/WJNSE.2018.84004
S. Shah, K. Kumar
Heat exchangers have its major application in automobile, air condition, refrigerator, power plants, and many others. Heat transfer characteristics and performance of Copper spiral heat exchanger are investigated and compared with pure water. Nanofluid can enhance thermos-physical properties. Experiment is carried out for water based SiO2 Nanofluid with 15 nm average sized nanoparticle at varying air velocity and mass flow rate of fluid to investigate its effect on heat transfer coefficient. From the experimental data, a closed form solution for Nusselt number has been calculated using ∈-NTU method. A new correlation has been proposed as a function of Reynolds number and Prandtl number. The heat transfer rate, effectiveness, has been significantly higher compared to pure water and with increasing volume fraction of nanoparticles.
热交换器在汽车、空调、冰箱、发电厂和许多其他领域有着重要的应用。研究了铜螺旋换热器的传热特性和性能,并与纯水进行了比较。纳米流体可以增强热物理性能。在不同的空气速度和流体质量流量下,对具有15nm平均尺寸纳米颗粒的水性SiO2纳米流体进行了实验,以研究其对传热系数的影响。根据实验数据,用∈-NTU方法计算了努塞尔数的闭式解。提出了一种新的雷诺数和普朗特数的函数关系。与纯水相比,随着纳米颗粒体积分数的增加,传热速率和有效性显著提高。
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引用次数: 5
Measurements of Pulsed 532 nm Laser Breakdown Spectroscopy of Synthesized Magnetite Nanoferrofluid 合成磁铁矿纳米流体的脉冲532 nm激光击穿光谱测量
Pub Date : 2018-09-28 DOI: 10.4236/WJNSE.2018.83003
M. E. Khosroshahi, M. Tajabadi
We describe the results of 532 nm pulse laser-induced breakdown spectroscopy (LIBS) of two samples of magnetite nanoparticles (SPIONs) nanoferrofluid synthesized at room (S1) and elevated temperatures (S2) and at three different laser energy levels and pulse frequency. The size of magnetite nanoparticles, size distribution, magnetic crystalline phase and magnetization were analyzed and measured using transmission electron microscopy (TEM), X-ray diffraction spectroscopy (XRD) and vibrating sample magnetometry (VSM). The SPIONs showed a distribution between 4 - 22 nm with a peak about 12 nm and saturation magnetization of about 65 emu/g. The Saha-Boltzmann analysis of spectra for medium energy level (1050 mJ) yields plasma temperatures of (3881 ± 200) K and (26,047 ± 200) K for Fe I and OV as the lowest and highest temperatures respectively. A range of corresponding electron density (Ne-) of (0.47 - 6.80) × 1020, (0.58 - 8.30) × 1020 and (0.69 - 9.96) × 1020 cm-3 were determined at 860, 1050 and 1260 mJ respectively using the estimated CCD pictures. The results confirmed a higher elements ratio for S1 than S2 and the signal intensity indicated a non-linear behaviour as a function of pulse frequency with the maximum ratio value at 3 Hz. At higher frequency of 6 Hz no such turning point was observed. The highest and lowest temperatures corresponded to Fe I and OV respectively. The LIBS technique can be utilized to study, characterize and determine the elements ratio required in most applications involving the synthesizing process.
我们描述了在室温(S1)和高温(S2)下以及在三种不同的激光能级和脉冲频率下合成的两种磁铁矿纳米颗粒(SPIONs)纳米铁磁流体样品的532nm脉冲激光诱导击穿光谱(LIBS)的结果。利用透射电子显微镜(TEM)、X射线衍射光谱(XRD)和振动样品磁强计(VSM)对磁铁矿纳米颗粒的尺寸、尺寸分布、磁性结晶相和磁化强度进行了分析和测量。SPION的分布在4-22nm之间,峰值约为12nm,饱和磁化强度约为65emu/g。中等能级(1050 mJ)的Saha Boltzmann光谱分析得出,Fe I和OV的等离子体温度分别为(3881±200)K和(26047±200)K。在860、1050和1260 mJ处分别测定了相应的电子密度(Ne-)范围为(0.47-6.80)×1020、(0.58-8.30)×1020和(0.69-9.96)×1020cm-3。结果证实S1的元素比高于S2,并且信号强度指示作为脉冲频率的函数的非线性行为,最大比值为3Hz。在6Hz的较高频率下,没有观察到这样的转折点。最高和最低温度分别对应于Fe I和OV。LIBS技术可用于研究、表征和确定涉及合成过程的大多数应用中所需的元素比例。
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引用次数: 1
Synthesis of SnO Nanopatricles—A Hydrothermal Approach SnO纳米颗粒的合成——水热法
Pub Date : 2018-06-29 DOI: 10.4236/WJNSE.2018.82002
E. Janardhan, M. M. Reddy, P. V. Reddy, M. Reddy
SnO nanoparticles were prepared by addition of HCl to tin oxide solution. The synthesis process is simplified for SnO nuclei. We herein report a better-defined and simple procedure for synthesis of SnO particles in a simple hydrothermal process.
通过向氧化锡溶液中加入HCl制备了SnO纳米颗粒。简化了SnO核的合成过程。我们在此报道了一种在简单的水热过程中合成SnO颗粒的更明确和简单的程序。
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引用次数: 12
Characterization of Polyvinyl Pyrollidone Coated Sodium Borohydride Stabilized Particle Colloidal Silver Fresh None Filtered and Nano Filtered Solution Made up of Magnetic Stirring and Cooling Method 聚乙烯软锰酸酯包被硼氢化钠稳定粒子胶体银新鲜无过滤和纳米过滤磁搅拌冷却溶液的表征
Pub Date : 2018-05-09 DOI: 10.4236/WJNSE.2018.81001
J. Pani, Royana Singh, S. Singh
Characterization is absolutely necessary and is a must in order to understand and estimate different silver nanoparticle (nm) size in specific group wise manner which corresponds to group wise in number & sizes, and their importance and effect on biological tissue and organs with agglomeration for nano toxicological studies in environments, the acute toxicity of colloidal silver nano particles (AgNps) were studied in fresh dissected tissues of Swiss Albino mice and their fetuses. In this manuscript, an attempt is made to demonstrate the synthesis and characterization of silver nano particles with a wide range of sizes (from 2.75 nm up to 1908.2 nm in radius) by reducing silver nitrate powder with polyvinyl pyrollidone in aqueous solutions in the presence of a sodium borohydride stabilizer. The resulting particles were found spherical aggregates with a rough surface and poly dispersity index below 18.26% (>0.783 PDI). The particle optical, cumulative, diluents and electrical conductivity properties were examined by dynamic light scattering and zeta potential but morphology was evaluated after examination by transmission electron microscopy & image-j. Silver nanoparticles were directly coated with polyvinyl pyrollidone with a sodium borohydride stabilizer. Optical properties on a single-particle level were studied by means of auto correlation function measurements. The effective poly dispersity index of the charged silver nanoparticles was low enough to form a colloidal crystal at low ionic strength. Colloidal form is found more toxic than suspended particles in 1.5 molar sodium chloride solution; this shows increase of silver nanoparticles size due to agglomeration, will reduce the toxicity but increase teratogenicity.
表征是绝对必要的,也是必须的,以便了解和估计不同的银纳米颗粒(nm)尺寸,以特定的分组方式,在数量和尺寸上与分组相对应,以及它们在环境中纳米毒理学研究中的重要性和对生物组织和器官的影响,研究了胶体银纳米粒子(AgNps)在瑞士白化小鼠及其胎儿新鲜解剖组织中的急性毒性。在这篇手稿中,试图证明在硼氢化钠稳定剂的存在下,通过在水溶液中用聚乙烯吡咯烷酮还原硝酸银粉末,合成和表征具有宽尺寸范围(半径从2.75nm到1908.2nm)的银纳米粒子。所得颗粒为球形聚集体,表面粗糙,多分散指数低于18.26%(>0.783PDI)。通过动态光散射和ζ电位检测颗粒的光学、累积、稀释剂和导电性能,但通过透射电子显微镜和图像喷墨检测后评估其形态。用硼氢化钠稳定剂将聚乙烯吡咯烷酮直接涂覆在银纳米颗粒上。通过自相关函数测量研究了单粒子水平上的光学性质。带电银纳米颗粒的有效多分散指数低到足以在低离子强度下形成胶体晶体。发现胶体形式比1.5摩尔氯化钠溶液中的悬浮颗粒毒性更大;这表明银纳米粒子由于团聚而增大尺寸,会降低毒性但增加致畸性。
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引用次数: 1
Remote Pyramid-Shaped Phosphor Coating for Phosphor-Converted White LEDs 用于磷光转换白光led的远端金字塔形磷光涂层
Pub Date : 2017-06-21 DOI: 10.4236/WJNSE.2017.72002
S. Abdullayeva, T. Orujov, N. Musayeva, R. Jabbarov, S. Orujov
Increasing light extraction efficiency is an important task when it comes to manufacturing a powerful white light emitting diode with high luminous flux per watt. In this paper the fabrication of a pyramid-shaped 3-dimensional phosphor coating is reported. It is represented by a phosphor cover, shaped into an array of pyramid like formations. It is proposed that such a structure can improve the light extraction efficiency and the color distribution characteristics of any phosphor-converted white LED. The luminous flux and luminous efficacy are being studied as a function of the forward current across the die. It was found out that with this kind of technique it was possible to achieve an 8% - 14% increase in the efficacy of the pc-LED. This increase of light output power is being attributed to the reduction of the phenomena of total internal reflection (TIR) inside the packaging module.
当涉及到制造具有高每瓦光通量的强大白光发光二极管时,提高光提取效率是一项重要任务。本文报道了一种金字塔形三维荧光粉涂层的制备。它由一个磷光体覆盖物来表示,该覆盖物成形为金字塔状的阵列。提出了这样的结构可以提高任何磷光体转换的白色LED的光提取效率和颜色分布特性。光通量和发光效率被研究为通过模具的正向电流的函数。研究发现,利用这种技术,可以使pc LED的功效提高8%-14%。光输出功率的这种增加归因于封装模块内部全内反射(TIR)现象的减少。
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引用次数: 1
Real Time Recrystallization Study of 1, 2 Dodecanediol on Highly Oriented Pyrolytic Graphite (HOPG) by Tapping Mode Atomic Force Microscopy 利用攻丝模式原子力显微镜研究1,2十二烷二醇在高取向热解石墨(HOPG)上的实时再结晶
Pub Date : 2017-03-31 DOI: 10.4236/WJNSE.2017.71001
S. K. Dora
Real-time atomic force microscopy (AFM) imaging revealed for the first time, the detailed growth/dissolution mechanism of Lauryl glycol (LG) or 1, 2 dodecanediol molecules on HOPG at the nano-level after recrystallizing them from chloroform solution. At the early stage of recrystallization, parallelogram-like-structures having lengths of several microns and distinct widths (between ~ 100 - 400 nm) were observed. Growth/dissolution behavior of these parallelogram-like-structures as a function of time was investigated. While dissolution occurred along all three dimensions, growth was found to be strictly two dimensional. Both the growth and dissolution process were found to be logarithmic in nature. The average growth rates along their length and width were found to be 11 nm/min and 1.5 nm/min respectively. Average dissolution rate in percentage on HOPG surface was found to be ~ 0.078%/min. Based upon the recrystallization of LG molecules schematics are drawn for a better understanding of the recrystallization process.
实时原子力显微镜(AFM)成像首次揭示了十二烷基乙二醇(LG)或1,2十二烷基二醇分子在氯仿溶液中重结晶后,在纳米水平上在HOPG上的生长/溶解机理。在再结晶初期,观察到长度为几微米,宽度在~ 100 ~ 400 nm之间的平行四边形结构。研究了这些平行四边形结构随时间的生长/溶解行为。虽然溶解发生在所有三个维度上,但生长被发现是严格的二维。发现生长和溶解过程本质上都是对数的。沿其长度和宽度的平均生长速率分别为11 nm/min和1.5 nm/min。在HOPG表面的平均溶出率为0.078%/min。根据LG分子的再结晶,绘制了再结晶示意图,以便更好地理解再结晶过程。
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引用次数: 2
Experimental Study of Filling Ratio Effect on the Thermal Performance in a Multi-Heat Pipe with Graphene Oxide/Water Nanofluids 填充率对氧化石墨烯/水纳米流体多热管热性能影响的实验研究
Pub Date : 2016-11-08 DOI: 10.4236/WJNSE.2016.64014
M. Salem, T. Meakhail, M. Bassily, S. Torii
This experimental study is performed to investigate heat transfer performance of a multi-heat pipe cooling device in the condition of different filling ratios (40%, 60%, 80% and 100%) and different constant heat fluxes (10 - 30 W). Here, pure water (distilled water) and graphene oxide (GO)/water nanofluids are employed respectively as working fluid. GO/water nanofluids were synthesized by the modified Hummers method with 0.05%, 0.10%, 0.15%, and 0.20% volume concentrations. Multi-heat pipe is fabricated from copper; the heating and cooling sections are the same size and both are connected by four circular parallel tubes. Temperature fields and thermal resistance are measured for different filling ratio, heat fluxes and volume concentrations. The results indicated that the thermal performance of heat pipe increased with increasing the concentration of GO nanoparticles in the base fluid, while the maximum heat transfer enhancement was observed at 0.20% volume concentration. GO/water nanofluids showed lower thermal resistance compared to pure water; the optimal thermal resistance was obtained at 100% filling charge ratio with 0.20% volume concentration. Studies were also demonstrated that heat transfer coefficient of the heat pipe significantly increases with increasing the input heat flux and GO nanoparticles concentration.
本文以纯净水(蒸馏水)和氧化石墨烯/水纳米流体为工质,研究了不同填充比(40%、60%、80%和100%)和不同恒定热流密度(10 ~ 30 W)条件下多热管冷却装置的换热性能。分别以0.05%、0.10%、0.15%和0.20%的体积浓度,采用改进Hummers法制备氧化石墨烯/水纳米流体。多热管由铜制成;加热和冷却部分的尺寸相同,并由四个圆形平行管连接。测量了不同填充比、热流密度和体积浓度下的温度场和热阻。结果表明:随着基液中氧化石墨烯纳米粒子浓度的增加,热管的传热性能有所提高,当体积浓度为0.20%时传热强化效果最大;与纯水相比,氧化石墨烯/水纳米流体的热阻更低;当填充率为100%、体积浓度为0.20%时,热阻最佳。研究还表明,热管的传热系数随着输入热流密度和氧化石墨烯纳米颗粒浓度的增加而显著增加。
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引用次数: 1
Development of Biofunctionalized Cellulose Acetate Nanoscaffolds for Heart Valve Tissue Engineering 用于心脏瓣膜组织工程的生物功能化醋酸纤维素纳米支架的研制
Pub Date : 2016-11-08 DOI: 10.4236/WJNSE.2016.64013
E. Chainoglou, V. Karagkiozaki, T. Choli-Papadopoulou, Charisios Mavromanolis, A. Laskarakis, S. Logothetidis
Currently-used mechanical and biological heart valve prostheses have a satisfactory short-term performance, but may exhibit several major drawbacks on the long-term. Mechanical prostheses, based on carbon, metallic and polymeric components, require permanent anticoagulation treatment, and their usage often leads to adverse reactions, e.g. thromboembolic complications and endocarditis. In recent years, there is a need for a heart valve prosthesis that can grow, repair and remodel. The concept of tissue engineering offers good prospects into the development of such a device. An ideal scaffold should mimic the structural and purposeful profile of materials found in the natural extracellular matrix (ECM) architecture. The goal of this study was to develop cellulose acetate scaffolds (CA) for valve tissue regeneration. After their thorough physicochemical and biological characterization, a biofunctionalization process was made to increase the cell proliferation. Especially, the surface of scaffolds was amplified with functional molecules, such as RGD peptides (Arg-Gly-Asp) and YIGSRG laminins (Tyrosine-Isoleucine-Glycine-Serine-Arginine-Glycine) which immobilized through biotin-streptavidin bond, the strongest non-covalent bond in nature. Last step was to successfully coat an aortic metallic valve with CA biofunctionallized nanoscaffolds and cultivate cells in order to create an anatomical structure comparable to the native valve. Promising results have been obtained with CA-based nanoscaffolds. We found that cells grown successfully on the biofunctionalized valve surface thereby scaffolds that resemble the native tissues, elaborated with bioactive factors such as RGD peptides and laminins not only make the valve’s surface biocompatible but also they could promote endothyliazation of cardiac valves causing an anti-coagulant effect
目前使用的机械和生物心脏瓣膜假体具有令人满意的短期性能,但可能在长期表现出几个主要的缺点。基于碳、金属和聚合物成分的机械假体需要永久性抗凝治疗,并且它们的使用经常导致不良反应,例如血栓栓塞并发症和心内膜炎。近年来,人们需要一种能够生长、修复和重塑的心脏瓣膜假体。组织工程的概念为这种装置的发展提供了良好的前景。理想的支架应该模仿天然细胞外基质(ECM)结构中发现的材料的结构和用途。本研究的目的是开发用于瓣膜组织再生的醋酸纤维素支架(CA)。在对其进行彻底的物理化学和生物学表征后,进行生物功能化处理以增加细胞增殖。特别是,支架表面被功能分子扩增,如RGD肽(Arg-Gly-Asp)和YIGSRG laminins(酪氨酸-异亮氨酸-甘氨酸-丝氨酸-精氨酸-甘氨酸),这些功能分子通过生物素-链亲和素键固定,这是自然界中最强的非共价键。最后一步是成功地用CA生物功能纳米支架覆盖主动脉金属瓣膜,并培养细胞,以创建与天然瓣膜相当的解剖结构。基于ca的纳米支架已经取得了令人满意的结果。我们发现,细胞在具有生物功能的瓣膜表面成功生长,从而形成类似于天然组织的支架,并与RGD肽和层粘连蛋白等生物活性因子相结合,不仅使瓣膜表面具有生物相容性,而且可以促进心脏瓣膜的内皮化,从而产生抗凝血作用
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引用次数: 12
Study of Timing Characteristics of NOT Gate Transistor Level Circuit Implemented Using Nano-MOSFET by Analyzing Sub-Band Potential Energy Profile and Current-Voltage Characteristic of Quasi-Ballistic Transport 基于准弹道输运子带势能分布和电流-电压特性的纳米mosfet非门晶体管电平电路时序特性研究
Pub Date : 2016-11-08 DOI: 10.4236/WJNSE.2016.64016
Chek Yee Ooi, S. Lim
This paper presents the quasi-ballistic electron transport of a symmetric double-gate (DG) nano-MOSFET with 10 nm gate length and implementation of logical NOT transistor circuit using this nano-MOSFET. Theoretical calculation and simulation using NanoMOS have been done to obtain parameters such as ballistic efficiency, backscattering mean free path, backscattering coefficient, critical length, thermal velocity, capacitances, resistance and drain current. NanoMOS is an on-line device simulator. Theoretical and simulated drain current per micro of width is closely matched. Transistor loaded NOT gate is simulated using WinSpice. Theoretical and simulated value of rise time, fall time, propagation delay and maximum signal frequency of logical NOT transistor level circuit is closely matched. Quasi-ballistic transport has been investigated in this paper since modern MOSFET devices operate between the drift-diffusion and ballistic regimes. This paper aims to enable modern semiconductor device engineers to become familiar with both approaches.
本文介绍了栅极长度为10nm的对称双栅极(DG)纳米mosfet的准弹道电子输运,并利用该纳米mosfet实现了逻辑非晶体管电路。利用NanoMOS进行了理论计算和仿真,得到了弹道效率、后向散射平均自由程、后向散射系数、临界长度、热速度、电容、电阻和漏极电流等参数。NanoMOS是一个在线设备模拟器。理论和模拟的每微宽度漏极电流是紧密匹配的。利用WinSpice对晶体管负载非栅极进行了仿真。逻辑非晶体管电平电路的上升时间、下降时间、传播延迟和最大信号频率的理论值与仿真值非常吻合。由于现代MOSFET器件工作在漂移扩散和弹道状态之间,本文研究了准弹道输运。本文旨在使现代半导体器件工程师熟悉这两种方法。
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引用次数: 1
Preparation of Electrode of Copper-Nickel Composite Material and Its Capacitance Performance 铜镍复合材料电极的制备及其电容性能
Pub Date : 2016-11-08 DOI: 10.4236/WJNSE.2016.64015
Xiuxia Zhang, Chaohui Li, Qianyu Ji
Nickel oxide/copper oxide composites are prepared. Then the composites were transferred into autoclave and thermal sinter under different temperature and different time. As-prepared composites were analyzed by XRD, and it was concluded that with the increase of hydrothermal time, content of NiO and Ni0.75Cu0.25O increases, but particles become smaller; it would improve the electrochemical activity. By SEM images directed lower crystallinity of composites, deeper porosity and rougher surface would have better electrochemical activity. The electrochemical performance was investigated by cyclic voltametry, AC impedance and galvanostatic charge-discharge. All results show that under the condition of 150°C 30 h, the electrochemical performance is the best. The specific capacitance was 225.67 F·g-1 at the charge-discharge current of 1 A·g-1.
制备了氧化镍/氧化铜复合材料。然后在不同温度和时间下将复合材料送入热压釜和热烧结。通过XRD对制备的复合材料进行了分析,结果表明:随着水热时间的延长,NiO和Ni0.75Cu0.25O的含量增加,但颗粒变小;它会提高电化学活性。SEM图像显示,结晶度越低、孔隙度越深、表面越粗糙的复合材料具有更好的电化学活性。采用循环伏安法、交流阻抗法和恒流充放电法对其电化学性能进行了研究。结果表明,在150℃30 h的条件下,电化学性能最好。充放电电流为1a· -1时,比电容为225.67 f· -1。
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引用次数: 2
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纳米科学与工程(英文)
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