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The Effect of Spray Distance on Porosity, Surface Roughness and Microhardness of WC-10Co-4Cr Coatings Deposited by HVOF 喷涂距离对HVOF沉积WC-10Co-4Cr涂层孔隙率、表面粗糙度和显微硬度的影响
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0028
M. Górnik, E. Jonda, M. Nowakowska, L. Łatka
Abstract The paper presents the computational studies on the microstructure of WC-Co-Cr coatings deposited by High Velocity Oxy Fuel spraying (HVOF). The study covers the porosity assessment according to ASTM E2109-01 standard, carried out in ImageJ software, in terms of volume porosity, size and shape of the pores. The evaluation was preceded by scanning electron microscope (SEM) observations at magnifications of 2000x and 5000x. Additionally, topography analysis has been performed by confocal laser scanning microscope (CLSM), and the surface roughness Ra was evaluated by the contact method with use of a stylus profilometer. Finally, the influence of porosity was observed for coatings microhardness HV0.3. According to the results, the total closed porosity was found to be in the range of 5.01 vol.% and 5.38 vol.%. The dominated pores in the coatings were of size 0.1-1.0 μm. Studies showed that HVOF process enabled deposition of dense coatings, characterized by homogenous distribution of pores and low roughness.
摘要:本文对高速氧燃料喷涂(HVOF)沉积WC-Co-Cr涂层的微观组织进行了计算研究。本研究根据ASTM E2109-01标准,在ImageJ软件中进行孔隙度评估,包括孔隙的体积孔隙度、大小和形状。在评估之前进行了2000倍和5000倍的扫描电子显微镜(SEM)观察。此外,用共聚焦激光扫描显微镜(CLSM)进行了形貌分析,并使用触笔轮廓仪用接触法评估了表面粗糙度Ra。最后,观察孔隙率对镀层显微硬度HV0.3的影响。结果表明,总封闭孔隙度在5.01 ~ 5.38 vol.%之间。涂层中孔隙主要分布在0.1 ~ 1.0 μm之间。研究表明,HVOF工艺可以沉积致密的涂层,其特点是孔隙分布均匀,粗糙度低。
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引用次数: 4
Assessment of Corrosive Behaviour and Microstructure Characterization of Hybrid Friction Stir Welded Martensitic Stainless Steel 马氏体不锈钢混合搅拌摩擦焊腐蚀性能评价及显微组织表征
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0025
Dhanesh G. Mohan, S. Gopi, J. Tomków, S. Memon
Abstract This study examined the effect of induction heating on the microstructure and corrosion characteristics of hybrid friction stir welded AISI 410 stainless steel. Five joints have been produced with different friction stir welding parameters like welding speed, spindle speed, plunge depth, and induction power. Their microstructures were evaluated using a scanning electron microscope, and chemical composition was examined using energy-dispersive X-ray spectroscopy (EDX). The rate of corrosion was found out via the weight loss method in a 1 M HCL solution. The hybrid friction stir welding method used for this work is induction assisted friction stir welding; the results show that this method could produce sound AISI 410 stainless steel Joints. The experiment results show that the joint made at a spindle speed of 1150 rpm, welding speed 40 mm/min, plunge depth 0.5 mm, and in-situ heat by induction 480°C show a better corrosion resistance property with a fine grain structure.
摘要:研究了感应加热对aisi410不锈钢混合搅拌摩擦焊接组织和腐蚀特性的影响。采用不同的搅拌摩擦焊接参数,如焊接速度、主轴转速、插入深度和感应功率,制作了5个接头。用扫描电子显微镜对其微观结构进行了评价,并用能量色散x射线光谱(EDX)检测了其化学成分。在1 M盐酸溶液中,通过失重法测定了腐蚀速率。本工作采用的混合搅拌摩擦焊方法为感应辅助搅拌摩擦焊;结果表明,该方法可获得良好的aisi410不锈钢接头。实验结果表明,在主轴转速为1150 rpm、焊接速度为40 mm/min、焊深为0.5 mm、原位感应加热温度为480℃条件下制备的接头具有较好的耐腐蚀性能和细小晶粒组织。
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引用次数: 7
Preparation and Evaluation of Conductive Polymeric Composite from Metals Alloys and Graphene to Be Future Flexible Antenna Device 金属合金与石墨烯导电聚合物复合材料未来柔性天线器件的制备与评价
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0023
Ameen Abdelrahman, F. Erchiqui, M. Nedil
Abstract Every year hundreds of serious accidents and catastrophic are accompanied by mining sector services as disaster, flooding, and demolition. To reduce the severity of the results such as high death numbers, lost communication inner and out mining, we have to find an easy way to improve communication means during that problems. In this paper, we reach out to fabricate durable, flexible, and wearable chaps, in addition to an easier carrier with highly efficient receiving and sending a signal at 2.4 GHz broad wide band. By doping a bunch of unique conductive metals (silver, copper, and gallium indium alloy) assembled on Graphene, its integration inside Polydimethylsiloxane to be future applicable antenna. Furthermore, we studied the physical and electric properties of a composite including Electrochemical Impedance properties (EIS), cyclic voltammetry (CV), and its thermal stability chip (DSC), as well as, using Transmission electron microscopy (TEM), and, scanning electron microscopy (SEM) techniques to clarify the surface morphology of fabricated materials. In addition to various measurements had been carried out such as Ultraviolet-visible, inductively coupled plasma (ICP) spectroscopy, and Energy-dispersive X-ray spectroscopy (EDX) to reinforce and elucidate the solid-state of ions inside fabricated Antenna. On the other hand, throughout stress-strain for the stretchability of fabricated is expanded to 30% of its original length, in addition to thermal stability reached to 485°C compared to pure PDMS substrate, with enhancing electric conductivity of composite ship.
矿业服务业每年都会发生数百起重大事故和灾难性事件,如灾害、洪水、拆迁等。为了减少严重的结果,如高死亡人数,失去内部和外部的通信,我们必须找到一个简单的方法来改善通信手段,在这些问题。在本文中,我们致力于制造耐用,灵活和可穿戴的chapp,以及更容易的载波,高效地接收和发送2.4 GHz宽带信号。通过在石墨烯上掺杂一堆独特的导电金属(银、铜和镓铟合金),将其集成在聚二甲基硅氧烷内,成为未来应用的天线。此外,我们研究了复合材料的物理和电学性能,包括电化学阻抗特性(EIS)、循环伏安(CV)和热稳定性芯片(DSC),并使用透射电子显微镜(TEM)和扫描电子显微镜(SEM)技术来阐明制备材料的表面形貌。此外,还进行了各种测量,如紫外-可见,电感耦合等离子体(ICP)光谱和能量色散x射线光谱(EDX)来加强和阐明天线内离子的固态。另一方面,对于整个应力应变制备的拉伸性被扩展到其原始长度的30%,此外与纯PDMS基材相比热稳定性达到485℃,具有增强复合材料船舶导电性的作用。
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引用次数: 0
Physico-Mechanical and Thermal Properties of Thermoplastic Poly(Vinyl Alcohol) Modified Thermosetting Urea Formaldehyde Resin 热塑性聚乙烯醇改性热固性脲醛树脂的物理力学和热性能
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0024
S. Sultana, Mehedi Mannan, Md. Jaynal Abedin, Z. Islam, H. Nur, P. R. Samaddar
Abstract Urea formaldehyde (UF) resins are brittle and to improve their tensile properties poly(vinyl alcohol) (PVA) has been used to modify the UF resin. An easy improved procedure was developed to make PVA modified UF resin on the basis of conventional synthesis of UF resin. Prepolymer of UF was mixed with different weight percentages of PVA (1-5%) to synthesize modified UF resin which can be used to make adhesive for forest products. Both UF and modified UF resins were characterized by FTIR, physico-mechanical and thermal properties analyses. Modified UF resin containing 2 wt. % PVA exhibited better results than the UF.
摘要脲醛树脂具有脆性,为改善其抗拉性能,采用聚乙烯醇(PVA)对脲醛树脂进行改性。在常规UF树脂合成方法的基础上,提出了一种简便的PVA改性UF树脂制备方法。将UF预聚物与不同重量百分比的PVA(1-5%)混合,合成改性UF树脂,用于林产品胶粘剂的制备。用红外光谱(FTIR)、物理力学和热性能分析对脲醛树脂和改性脲醛树脂进行了表征。含2 wt. % PVA的改性脲醛树脂比脲醛树脂效果更好。
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引用次数: 0
Microstructural Evaluation of the High-Frequency Induction Welded Joints of Low Carbon Steel Pipes 低碳钢管高频感应焊接接头的显微组织评价
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0022
A. Bunsch, J. Krawczyk, P. Matusiewicz
Abstract The work presents the results of research on the structure of welded joints in the area of heat affected zone (HAZ). Based on precisely performed metallographic tests, the contribution of individual structural components in the area of welds of pipes welded with the induction method was assessed. The volume fraction of individual structural components in various areas of the heat affected zone, the size of the grain formed in the welding process, as well as its shape coefficients were determined. On the basis of metallographic observations, an attempt was made to describe the course of the pressure induction welding process, taking into account the structural changes, phase changes and the recovering and recrystallization processes taking place in this process.
摘要本文介绍了热影响区焊接接头结构的研究成果。在精密金相试验的基础上,评估了感应焊管焊缝区域各结构构件的贡献。测定了热影响区各区域内各构件的体积分数、焊接过程中形成的晶粒尺寸及其形状系数。在金相观察的基础上,考虑到压力感应焊接过程中的组织变化、相变以及恢复和再结晶过程,对压力感应焊接过程进行了描述。
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引用次数: 0
Effect of Holes in Overlap on the Load Capacity of the Single-Lap Adhesive Joints Made of EN AW-2024-T3 Aluminium Alloy 重叠孔对EN AW-2024-T3铝合金单搭接粘接接头承载能力的影响
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0029
W. Zielecki, Katarzyna Burnat, A. Kubit, T. Katrňák
Abstract The paper presents the results of experimental research aimed at determining the possibilities of strengthening structural adhesive joints. Techniques to improve the strength of adhesive joints was to make holes in the front part of the adherends in order to make the joint locally more flexible in the area of stress concentration at the joint edges. The tests were carried out for the lap joints of EN AW-2024-T3 aluminum alloy sheets, which were bonded with Loctite EA3430 epoxy adhesive. Static tests were carried out on the basis of the tensile/shear test. It has been shown that the applied structural modifications allow for an increase in the strength of the joint, in the best variant, an increase in strength of 14.5% was obtained. In addition, it has been shown that making holes in the adherends allows to reduce the spread of strength results.
摘要本文介绍了旨在确定加强结构粘接接缝可能性的实验研究结果。提高粘接接头强度的方法是在粘接接头的前部打孔,使接头在接头边缘应力集中区域具有局部柔性。采用乐泰EA3430环氧胶粘剂对EN AW-2024-T3铝合金板材进行搭接试验。静态试验是在拉伸/剪切试验的基础上进行的。结果表明,所施加的结构修改可以提高接头的强度,在最佳变体中,强度提高了14.5%。此外,已经证明在附着物上打洞可以减少强度结果的传播。
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引用次数: 1
Microstructure and Mechanical Properties of Laser Surface-Treated Ti13Nb13Zr Alloy with MWCNTs Coatings 激光表面处理Ti13Nb13Zr合金MWCNTs涂层的组织和力学性能
IF 1.3 Pub Date : 2021-12-01 DOI: 10.2478/adms-2021-0021
B. Majkowska-Marzec, Joanna Sypniewska
Abstract Laser surface modification of titanium alloys is one of the main methods of improving the properties of titanium alloys used in implantology. This study investigates the microstructural morphology of a laser-modified surface layer on a Ti13Nb13Zr alloy with and without a carbon nanotube coating deposited by electrophoretic deposition. Laser modification was performed for samples with and without carbon nanotube coating for two different laser powers of 800 W and 900 W and for different scan rates: 3 mm/s or 6 mm/s at 25 Hz, and the pulse duration was 2.25 ms or 3.25 ms. A scanning electron microscope SEM was used to evaluate the surface structure of the modified samples. To observe the heat-affected zones of the individual samples, metallographic samples were taken and observed under an optical microscope. Surface wettability tests were performed using a goniometer. A surface roughness test using a profilograph and a nanoindentation test by NanoTest™ Vantage was also performed. Observations of the microstructure allowed to state that for higher laser powers the surfaces of the samples are more homogeneous without defects, while for lower laser powers the path of the laser beam is clearer and more regular. Examination of the microstructure of the cross-sections indicated that the samples on which the carbon nanotube coating was deposited are characterized by a wider heat affected zone, and for the samples modified at 800 W and a feed rate of 3 mm/s the widest heat affected zone is observed. The wettability tests revealed that all the samples exhibit hydrophilic surfaces and the samples with deposited carbon nanotube coating increase it further. Surface roughness testing showed a significant increase in Ra for the laser-modified samples, and the presence of carbon nanotubes further increased this value. Nanoindentation studies showed that the laser modification and the presence of carbon coating improved the mechanical properties of the samples due to their strength.
摘要钛合金激光表面改性是改善钛合金种植体性能的主要方法之一。研究了电泳沉积碳纳米管涂层前后Ti13Nb13Zr合金表面激光修饰层的微观组织形态。在激光功率分别为800 W和900 W、扫描速率分别为3 mm/s和6 mm/s、25 Hz、脉冲持续时间分别为2.25 ms和3.25 ms的条件下,对未涂覆碳纳米管的样品进行激光修饰。利用扫描电子显微镜(SEM)对改性后样品的表面结构进行了表征。为了观察单个样品的热影响区,取金相样品并在光学显微镜下观察。表面润湿性测试使用角计进行。使用轮廓仪进行表面粗糙度测试,并使用NanoTest™Vantage进行纳米压痕测试。对微观结构的观察表明,在较高的激光功率下,样品的表面更均匀,没有缺陷,而在较低的激光功率下,激光束的路径更清晰,更有规则。结果表明,碳纳米管涂层的热影响区较宽,在800 W、3 mm/s的进料速率下改性后,热影响区最宽。润湿性测试表明,所有样品表面均表现出亲水性,而碳纳米管涂层进一步增强了样品的亲水性。表面粗糙度测试表明,激光修饰样品的Ra含量显著增加,碳纳米管的存在进一步增加了该值。纳米压痕研究表明,激光改性和碳涂层的存在改善了样品的力学性能,这是由于它们的强度。
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引用次数: 5
Vacuum-arc Nitriding of Carbon Steels Having Low Tempering Temperature 低回火温度碳钢的真空电弧氮化
IF 1.3 Pub Date : 2021-10-29 DOI: 10.11648/J.AM.20211004.11
V. Stolbovyi, A. Andreev, I. Serdiuk, I. Kolodii, A. Shepelev
Studies have been made into a new possibility of modifying the surface of steels having a low tempering temperature by nitriding them in a vacuum-arc gas discharge followed by heat treatment (heating, quenching and tempering). Generally, nitriding of hardened steels takes place at a temperature of about 500°C, and thus this process appears impossible for steels with tempering temperatures of the order of 200... 300°C. It is demonstrated here that a single ion-plasma nitriding of high-carbon steel with the composition of 0.9% C, 1% Cr, 1% Si, followed by heat treatment, provides the nitrided layer of 2.5 mm in depth, with the hardness between 9 and 11 GPa. Within the range of X-rays penetration, the nitride-hardened layer of the surface is defined as the nitrogen austenite-alpha ferrite mixture, which shows high wear resistance and impact toughness. This layer contributes, in particular, to three-/four-foldin crease in the operational life of cutting punches (made of this steel and used in the manufacture of metal sieves) as opposed to the punches that have undergone conventional heat treatment. After repeated nitriding of the same steel and its subsequent heat treatment according to standard technologies the nitrided layer thickness becomes nearly twice as large, and that allows for multiple regrinding of steel tools. A computer analysis of related publications entered into three International Databases (INIS, MSCI, SCOPUS) has been carried out.
研究了一种新的可能性,即在真空电弧气体放电中氮化,然后进行热处理(加热、淬火和回火),以改性具有低回火温度的钢表面。一般来说,淬硬钢的氮化发生在500℃左右,因此对于回火温度为200℃的钢来说,这一过程似乎是不可能的。300°C。结果表明,对成分为0.9% C、1% Cr、1% Si的高碳钢进行单次离子等离子体渗氮,再进行热处理,可获得深度为2.5 mm、硬度在9 ~ 11gpa之间的氮化层。在x射线穿透范围内,表面的氮化硬化层定义为氮奥氏体- α铁素体混合物,具有较高的耐磨性和冲击韧性。与经过传统热处理的冲头相比,这一层特别有助于将切割冲头(由这种钢制成并用于制造金属筛子)的使用寿命延长三/四倍。同一种钢经过多次氮化处理和随后按照标准技术进行热处理后,氮化层厚度几乎增加了一倍,这就允许对钢工具进行多次再磨削。已对输入三个国际数据库(国际数据库、MSCI、SCOPUS)的有关出版物进行了计算机分析。
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引用次数: 0
Prediction and Optimization of Internal Return Fines Generation in Iron Ore Sintering Using Machine Learning 基于机器学习的铁矿石烧结内部返粉生成预测与优化
IF 1.3 Pub Date : 2021-10-28 DOI: 10.11648/J.AM.20211003.12
S. Mohanan, P. Mohapatra, C. Kumar, Ramakrishna Adepu, V. M. Koranne, Y. S. Prasad, A. S. Reddy, R. Ramna
Prior to dispatch of sinter to the blast furnace for hot metal production, the sinter product from the sinter cooler is screened to remove smaller/finer particles. The undersize so generated is called internal return fines, which are generally recirculated into the sintering machine. A very high level of internal return fines generation limits the use of virgin ore for sintering which may hamper sinter productivity. Recently, the sinter plant at Tata Steel’s Kalinganagar works has faced issues of high internal return fines generation. As the sinter plant begins to increase its productivity levels, it becomes critical to control the generation of internal return fines to allow fresh material consumption. Limited literature is available on factors affecting the internal return fines generation in sinter plant. Given the current computational capabilities, a machine learning model was developed to ascertain the factors affecting the internal return fines generation. The development of the machine learning model and the optimization carried out based on model output is described in this work. The key parameters affecting the internal return fines generation were the sintering rate, sinter basicity, charge density and temperature in the ignition hood. In Kalinganagar, the increase in ignition hood temperature was limited by the furnace refractory condition. Further, the sinter basicity is determined by the percentage of sinter in blast furnace burden. Incorporating these constraints, the model was used to optimize the process parameters to generate the lowest possible return fines. The understanding generated from this machine learning framework has resulted in a reduction of 2-3% in internal return fines generation, which implied higher net sinter production.
在将烧结矿送到高炉进行铁水生产之前,从烧结冷却器中取出的烧结矿产品要经过筛选,以去除更小/更细的颗粒。这样产生的过细粒被称为内回细粒,通常会再循环到烧结机中。高水平的内部回粉产生限制了原矿烧结的使用,这可能会妨碍烧结生产率。最近,塔塔钢铁公司Kalinganagar工厂的烧结厂面临着内部回报过高的问题。随着烧结厂开始提高其生产力水平,控制内部返粉的产生以允许新鲜材料的消耗变得至关重要。关于影响烧结厂内部返粉产生的因素的文献有限。考虑到目前的计算能力,开发了一个机器学习模型来确定影响内部回报产生的因素。本工作描述了机器学习模型的开发和基于模型输出的优化。影响内回粉生成的关键参数是烧结速率、烧结碱度、电荷密度和引火罩温度。在Kalinganagar,引火罩温度的升高受到炉膛耐火条件的限制。此外,烧结矿的碱度是由烧结矿在高炉炉料中的百分比决定的。结合这些约束,该模型用于优化工艺参数,以产生尽可能低的回报罚款。从这个机器学习框架中产生的理解导致内部回粉产生减少了2-3%,这意味着更高的净烧结矿产量。
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引用次数: 0
Computer Simulation of Continuous Casting Processes: A Review 连铸过程的计算机模拟:综述
IF 1.3 Pub Date : 2021-09-29 DOI: 10.11648/J.AM.20211003.11
Nitin Amratav, K. K. Kumar, M. Pillai
Steelmaking is the second step in producing steel from iron ore. In this stage, impurities such as sulfur, phosphorus, and excess carbon are removed from the raw iron, and alloying elements such as manganese, nickel, chromium, and vanadium are added to produce the exact steel required. Modern steelmaking processes are broken into two categories: primary and secondary steelmaking. Primary steelmaking uses mostly new iron as the feedstock, usually from a blast furnace. Secondary steelmaking uses scrap steel as the primary raw material. Gases created during the production of steel can be used as a power source. Steelmaking is presently a grounded innovation driven by plant, exploratory and computational examination. The continuous casting process comprises many complicated phenomena in terms of fluid flow, heat transfer, and structural deformation. The important numerical modeling method of the continuous casting process has been discussed in reference in this work. With the recent advancement in metallurgical methods, the continuous casting process now becomes the main method for steel production. To achieve efficient and effective production, the manufacturers of steel keep on searching for new methods which increase productivity. The present work describes molten steel flow, heat transfer, solidification, electromagnetic applications, formation of the shell by solidification and coupling, etc.
炼钢是用铁矿石炼钢的第二步。在这一阶段,从原铁中除去硫、磷和多余的碳等杂质,并加入锰、镍、铬和钒等合金元素,以生产所需的钢。现代炼钢过程分为两类:一次炼钢和二次炼钢。初级炼钢主要使用新铁作为原料,通常来自高炉。二次炼钢以废钢为主要原料。钢铁生产过程中产生的气体可用作电源。炼钢目前是一种由工厂、探索和计算驱动的接地式创新。连铸过程包含了流体流动、传热和组织变形等多种复杂现象。本文对连铸过程的重要数值模拟方法进行了探讨。随着冶金技术的进步,连铸法已成为炼钢的主要方法。为了实现高效率的生产,钢铁制造商不断寻求提高生产率的新方法。本文介绍了钢水的流动、传热、凝固、电磁应用、凝固和耦合形成壳等。
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引用次数: 1
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