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Analysis of quantitative and qualitative extractive components extracted from hornbeam (Carpinus betulus L.) and yakal (Shorea astylosa Foxw.) wood 牛角木(Carpinus betulus L.)和牦牛木(Shorea astylosa Foxw.)中提取成分的定量和定性分析
Pub Date : 2022-04-30 DOI: 10.5604/01.3001.0015.8937
Dominik Sierant, Dominka Szadkowska
The aim of the study was analysis of quantitative and qualitative extractive components extracted from hornbeam (Carpinus betulus L.) and yakal (Shorea astylosa Foxw.) wood. Two wood species similar to each other in terms of microscopic structure and physical properties, the native wood of Hornbeam (Carpinus betulus L.) and the yakal wood (Shorea astylosa Foxw.) endemic to the Philippines, which is still little understood, were investigated. Wood is a material composed mainly of polymers called lignocellulose which includes: (cellulose, lignin and hemicelluloses), but also contains many extractive and mineral substances. . The extractive content of wood in temperate climates is approximately for up to 5% by weight of wood. Their identification is difficult because of the wide variety and multiplicity of compounds present. However, extractive compounds are important for the resistance of trees and wood to biological agents such as fungal infestation or insect infestation. Usually the zones of dead wood (heartwood or cored wood) are characterized by a higher content of extractives. The understanding of the chemical composition of extractives in wood can contribute to the development of wood preservative products and environmentally friendly and would be part of the green chemistry policy.
对角木(Carpinus betulus L.)和牦牛木(Shorea astylosa Foxw.)的提取成分进行了定量和定性分析。本文研究了两种微观结构和物理性质相似的木材,即菲律宾特有的角木(Carpinus betulus L.)和对其了解甚少的雅卡尔木(Shorea astylosa Foxw.)。木材是一种主要由称为木质素纤维素的聚合物组成的材料,其中包括:(纤维素、木质素和半纤维素),但也含有许多提取物和矿物质。在温带气候下,木材的萃取物含量约为木材重量的5%。它们的鉴定是困难的,因为存在的化合物种类繁多。然而,提取物化合物对于树木和木材抵抗生物制剂如真菌侵染或昆虫侵染是重要的。通常,枯木区(心材或芯材)的特征是提取物含量较高。了解木材中萃取物的化学成分有助于木材防腐产品的开发和环境友好,将成为绿色化学政策的一部分。
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引用次数: 0
The study of selected properties of pine wood (Pinus sylvestris L.) subjected to acetylation 乙酰化处理对松材(Pinus sylvestris L.)若干特性的影响
Pub Date : 2022-04-30 DOI: 10.5604/01.3001.0015.8667
Tomasz Gliszczyński, A. Antczak
The study of selected properties of pine wood (Pinus sylvestris L.) subjected to acetylation. In the paper pine wood was subjected to acetylation with acetic anhydride and mixture of acetic anhydride and glacial acetic acid (50:50)v/v. After modification process density, WPG index, water absorbability, volume swelling and colour of wood were carried out and compared with results obtained for unmodified pine wood. Based on the obtained results the density of acetylated pine wood was increased for each group of samples. The highest WPG index was obtained for previously dried wood modified with acetic anhydride (15.6%) or mixture of acetic anhydride and glacial acetic acid (10.5%). Acetylation process with acetic anhydride or mixture of acetic anhydride and glacial acetic acid of samples, which were extracted (in chloroform-ethanol 93:7w/w mixture) and dried before modification, had beneficial effect on water absorbability of pine wood. These samples after 1001h (about 42 days) of soaking in water reached the lowest values of water absorbability (about 94%). Moreover, the volume swelling were significantly reduced for samples after double impregnation cycle (both in case of modification with acetic anhydride or mixture of acetic anhydride and glacial acetic acid). Wood after acetylation process was slightly darker than unmodified pine wood. Acetylation of samples, which were dried and soaked in DMF before modification, caused significant darkening of pine wood. The obtained colour was similar to colour of furfurylated wood (Kebony wood) or some of exotic species.
乙酰化处理对松材(Pinus sylvestris L.)若干特性的影响。在造纸中,用乙酸酐和乙酸酐与冰醋酸的混合物(50:50)进行乙酰化反应。对改性后木材的密度、WPG指数、吸水率、体积膨胀率和颜色进行了测定,并与未改性的松木进行了比较。根据得到的结果,每组样品的乙酰化松木密度都有所增加。经乙酸酐和冰醋酸混合改性的干燥木材WPG指数最高(15.6%)。用乙酸酐或乙酸酐与冰醋酸的混合物对样品进行乙酰化处理,提取样品(氯仿-乙醇93:7w/w混合物),干燥后再进行改性,对松材的吸水性能有良好的影响。这些样品在水中浸泡1001h(约42天)后,吸水率达到最低点(约94%)。两次浸渍(用乙酸酐或醋酸酐与冰醋酸混合)后,试样的体积膨胀明显减小。乙酰化处理后的木材比未改性的松木颜色略深。改性前在DMF中干燥和浸泡的样品乙酰化导致松木显着变暗。得到的颜色类似于糠醛化木材(克乌木)或一些外来物种的颜色。
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引用次数: 0
Influence of the glue joint on the speed of propagation of sound waves in wood 胶缝对声波在木材中传播速度的影响
Pub Date : 2022-04-30 DOI: 10.5604/01.3001.0015.9057
Alicja Banaś, Zbigniew Karwat
Influence of the glue joint on the speed of propagation of sound waves in wood. The aim of this study is to demonstrate differences in the propagation of sound waves in wood depending on the type of glue used to form the joint. Samples of tree species considered as resonant wood, i.e. Norway spruce (Picea abies) and sycamore (Acer pseudoplatanus), and for comparison, wood of European beech (Fagus sylvatica) were used. The fractured samples were glued together using glutinous fish glue, polyurethane glue (Titebond Liquid Glue) and cyanoacrylate glue (BONDOLOC B415). All types of glue are used in instrument repair, of which glutinous glue is regarded to be the correct one used in gluing technique. The test was carried out using a non-destructive ultrasonic method. It has been shown that the highest decreases in speed of propagation of sound waves are in wood glued with glutinous glue and the lowest in wood glued with cyanoacrylate glue.
胶缝对声波在木材中传播速度的影响。这项研究的目的是证明声波在木材中传播的差异,这取决于用于形成接头的胶水的类型。被认为是共振木材的树种样本,即挪威云杉(Picea abies)和梧桐(Acer pseudoplatanus),为了比较,使用了欧洲山毛榉(Fagus sylvatica)的木材。将断裂的样品用粘性鱼胶、聚氨酯胶(Titebond Liquid glue)和氰基丙烯酸酯胶(BONDOLOC B415)粘合在一起。仪器维修中使用各种类型的胶水,其中粘胶被认为是正确的粘胶技术。试验采用无损超声法进行。结果表明,用粘性胶粘接的木材对声波传播速度的衰减最大,而用氰基丙烯酸酯胶粘接的木材对声波传播速度的衰减最小。
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引用次数: 0
Giganten-wechsel in Europäische Sägeindustrie 握手
Pub Date : 2022-04-30 DOI: 10.5604/01.3001.0015.9278
T. Kłosińska, S. Krzosek
Giganten-wechsel in der Europäischen Sägeindustrie. In diesem Artikel werden die aktuelle Situation und die wichtigsten Änderungen in der Sägeindustrie in Europa vorgestellt: Die Großen werden noch größer. Sowohl die Einschnittskapazität von Rundholz als auch die Schnittholzproduktion in Europa wachsen kontinuierlich. Die Autoren schildern in diesem Artikel die Geschichte des ehemaligen Symbols für Expansion und dynamische Entwicklung in der europäischen Sägebranche: Klausner, so wie auch den heutigen Zustand der Firma Klausner. Darüber hinaus wird auch der Entwicklungsweg des neuen Erfolgssymbols in der Branche – der Firma Binderholz aufgezeichnet. Darüber hinaus wird über die wichtigsten Übernahmen in der Branche berichtet. Die größten Akteure sind heute nicht nur reine Sägewerksfirmen, sondern Konzerne, die Schnittholz produzieren und das Schnittholz sofort zu Endprodukten z.B. KVH, BSH, BBS verarbeiten, sich aber auch mit der Papierherstellung, mit Biomassekraftwerken oder der Pelletproduktion beschäftigen.
打破了欧洲的伐木工业在这一文章中概述了欧洲植树造林的当前形势和重大改变:太大了横切面的木板空间和欧洲的木头产量都有持续增长。本文的作者描述了曾经是欧洲锯木业蓬勃发展和发展的符号的故事:克劳斯内尔,就像他今天所在的德国公司一样。上面还记录了先进技术的发展路径它也记录了这个行业最主要的收购活动。今天最大行动者不仅是锯木厂,也是生产切木和立即生产切木的企业," k世代"、BSH、BBS和从事纸生产、生物发电厂或裘皮生产的企业。
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引用次数: 0
The influence of microbiological medium composition on the efficiency of bacterial cellulose synthesis 微生物培养基组成对细菌纤维素合成效率的影响
Pub Date : 2022-04-30 DOI: 10.5604/01.3001.0015.8701
K. Chlebiej, I. Betlej
The influence of the composition of microbiological medium on the efficiency of bacterial cellulose synthesis. The main objective was to investigate the effect of culture medium composition on the process of bacterial cellulose synthesis. Five different nutrients were used as carbon sources for cellulose synthesising microorganisms: glucose, fructose, erythrol, inulin and lactose, added to the medium at three different concentrations (1%, 2.5%, and 4.5%). It was observed that the type and amount of nutrients included in the culture medium significantly affected the cellulose synthesis efficiency. It was observed that the best results of polymer synthesis were obtained on medium containing 1% fructose. Furthermore, the results obtained clearly confirm that the composition of the culture medium has a significant effect on the water retention of the polymer during its synthesis on the culture media.
微生物培养基组成对细菌纤维素合成效率的影响。主要目的是研究培养基组成对细菌纤维素合成过程的影响。五种不同的营养物质被用作纤维素合成微生物的碳源:葡萄糖、果糖、红细胞、菊粉和乳糖,以三种不同的浓度(1%、2.5%和4.5%)添加到培养基中。结果表明,培养基中营养物质的种类和添加量对纤维素合成效率有显著影响。结果表明,在含1%果糖的培养基上,聚合物的合成效果最好。此外,所获得的结果清楚地证实了培养基的组成对聚合物在培养基上合成时的保水性有显著影响。
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引用次数: 0
Classics of Polish Design. Polish avant-garde Bauhaus style furniture from the interwar period 波兰设计经典。两次世界大战期间的波兰前卫包豪斯风格家具
Pub Date : 2022-04-30 DOI: 10.5604/01.3001.0015.8689
A. Różańska, Karolina Bodych
Classics of Polish Design. Polish avant-garde Bauhaus style furniture from the interwar period presents a review of the best Polish furniture designs from the 1920s and 1930s. In spite of the inspirations with historicism popular in the interwar period and the references to folk culture (e.g., the "Ład" Artists' Cooperative), Polish designers also drew inspiration from the works of the following artists: Le Corbusier, Marcel Breuer, Mies van der Rohe and Mart Stam, who designed avant-garde furniture made of metal pipes. The paper presents little known works of Polish artists from the groups "Praesens", "Atelier wnętrz i architektury" (The Atelier of Interiors and Architecture), "Studium wnętrz i sprzętu" (Studio of Interiors and Equipment), as well as furniture designs referring to the Bauhaus style for private and public interiors (including designs for transatlantics or the President's Castle in Wisła), among others, manufactured by the Thonet-Mundus company. The paper continues the series devoted to the "Classics of Polish Design", presenting the results of research on Polish furniture, carried out within the framework of dissertations in the Department of Wood Technology in the Warsaw University of Life Sciences (SGGW).
波兰设计经典。波兰前卫的包豪斯风格的家具从两次世界大战之间的时期呈现了最好的波兰家具设计从20世纪20年代和30年代的回顾。除了受到两次世界大战期间流行的历史主义和民间文化的启发(例如“Ład”艺术家合作社)之外,波兰设计师还从以下艺术家的作品中汲取灵感:勒·柯布西耶、马塞尔·布鲁耶、密斯·凡·德罗和玛特·斯塔姆,他们设计了由金属管制成的前卫家具。本文介绍了来自“Praesens”,“Atelier wnętrz i architekarchitecture”(室内和建筑工作室),“Studium wnętrz i sprzętu”(室内和设备工作室)的波兰艺术家的鲜为人知的作品,以及指私人和公共室内包豪斯风格的家具设计(包括跨大西洋或总统城堡的设计Wisła),等等,由Thonet-Mundus公司制造。该论文延续了“波兰设计经典”系列,展示了华沙生命科学大学(SGGW)木材技术系在论文框架内进行的波兰家具研究成果。
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引用次数: 0
Compression strength-focused properties of wood composites induced by structure 木结构复合材料抗压强度聚焦性能研究
Pub Date : 2021-12-30 DOI: 10.5604/01.3001.0015.6879
G. Kowaluk, Aleksandra Jeżo
Compression strength-focused properties of wood composites induced by structure. The aim of the following study was to examine the contractual compression strength and modulus of elasticity when compressing (MOEC) of three different wood composites with various structure types: softwood (coniferous) plywood, OSB and laminated particleboard 24 mm thick. The biggest MOEC value was performed by the particleboard laminated 24 mm MOEC equalling 70.00 N/mm2. The second was found by the OSB panels, equalling 63.03 N/mm2. Last, but with MOEC value close to OSB, was softwood plywood with MOEC of 62.44 N/mm2. The lowest compression strength was observed by OSB samples, with a value of 2.75 N/mm2. The second lowest value has been performed by coniferous plywood (2.80 N/mm2). The highest compression strength occurred by the particleboard laminated 24 mm, equalling 3.31 N/mm2. Density shares and density profiles of the samples were also analysed, all of the examined composites performed U-shaped density profile The results of the study showed that there is no significant correlation between density and obtained parameters under compression. Observation of density share let the Authors conclude conversely than the results showed. It is supposed that the key factor affecting the compression performance of samples was the adhesive area and solid glue content within the composites. It is assumed that the bigger total contact surface of wood particles coated with adhesive resin, so the sum of the effective (gluing particles) surfaces of the adhesive joint is the better mechanical properties can be performed. This is why the laminated particleboard gave the best mechanical properties, while the worst were observed by the softwood plywood.
木结构复合材料抗压强度聚焦性能研究。以下研究的目的是检查三种不同结构类型的木材复合材料的压缩压缩强度和弹性模量(MOEC):软木(针叶)胶合板,OSB和24毫米厚的层压刨花板。刨花板层压的24 mm MOEC值最大,为70.00 N/mm2。第二个是由OSB面板发现的,等于63.03 N/mm2。最后是MOEC值接近OSB的软木胶合板,MOEC值为62.44 N/mm2。OSB样品的抗压强度最低,为2.75 N/mm2。第二低值是针叶胶合板(2.80 N/mm2)。刨花板层压24mm时抗压强度最高,为3.31 N/mm2。分析了试样的密度份额和密度分布,所有检测的复合材料都表现为u型密度分布。研究结果表明,在压缩条件下,密度与得到的参数之间没有显著的相关性。对密度份额的观察使作者得出了与结果相反的结论。认为影响试样压缩性能的关键因素是复合材料的粘接面积和固体胶含量。假设涂覆胶合树脂的木颗粒的总接触面越大,则胶合接头的有效(胶合颗粒)面之和越好,则胶合接头的力学性能越好。这就是为什么层压刨花板的机械性能最好,而软木胶合板的机械性能最差。
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引用次数: 0
Investigation of selected properties of the black elder wood (Sambucus nigra L.) 黑接骨木(Sambucus nigra L.)部分特性的研究
Pub Date : 2021-12-30 DOI: 10.5604/01.3001.0015.6640
P. Kozakiewicz, Marcin Dadon, M. Marchwicka
Investigation of selected properties of the black elder wood (Sambucus nigra L.). The work has defined the selected chemical, physical and mechanical properties of the black elder wood, such as content of non-structural substances, shrinkage and density, speed of sound propagation, dynamic modulus of elasticity, acoustic resistance and sound attenuation, modulus of elasticity, bending strength, compressive strength, Brinell hardness, cold and hot-water extractives content and pH of hot-water extract. The black elder wood is hard and moderately shrinking. Mechanical properties are reduced by going from the pith to the perimeter, which is most likely affected by the increasing twist of the fibres. The distance from the pith also affects the acoustic properties and the size of the shrinkage, while the density remains constant.
黑接骨木(Sambucus nigra L.)若干特性的研究。本工作确定了黑接骨木的选定化学、物理和机械性能,如非结构物质含量、收缩率和密度、声音传播速度、动态弹性模量、声学阻力和声学衰减、弹性模量、弯曲强度、抗压强度、布氏硬度、冷水和热水浸出物含量和热水浸出物pH值。黑接骨木坚硬,适度收缩。从髓到周长,机械性能会降低,这很可能受到纤维捻度增加的影响。在密度保持不变的情况下,距髓的距离也会影响材料的声学性能和收缩率。
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引用次数: 2
Preparation of nanocellulose by hydrolysis with ionic liquids and two-step hydrolysis with ionic liquids and enzymes 离子液体水解及离子液体与酶两步水解制备纳米纤维素
Pub Date : 2021-12-30 DOI: 10.5604/01.3001.0015.6636
M. Babicka, M. Woźniak, K. Szentner, S. Borysiak, K. Dwiecki, I. Ratajczak
The aim of this study was to compare parameters of nanocellulose obtained by two different procedures:hydrolysis with ionic liquids (1-allyl-3-methylimidazolium chloride and 1-ethyl-3-methylimidazolium acetate) and hydrolysis with ionic liquids in combination with hydrolysis using a cellulolytic enzyme from Trichoderma reesei.Avicel cellulose was treated with two ionic liquids: 1-allyl-3-methylimidazolium chloride (AmimCl) and 1-ethyl 3-methylimidazolium acetate (EmimOAc). In the two-step hydrolysis cellulose after treatment with ionic liquids was additionally hydrolyzed with a solution of enzymes. In order to characterize the obtained material, the following analyses were used: infrared spectroscopy, X-ray diffraction and dynamic light scattering. The results indicated that cellulose obtained by two-step nanocellulose production methods (first hydrolysis with ionic liquids and then with enzymes) showed similar parameters (particle size, XRD patterns and degree of crystallinity) as the material after the one-step process, i.e. hydrolysis with ionic liquids.
本研究的目的是比较离子液体(1-烯丙基-3-甲基咪唑氯和1-乙基-3-甲基咪唑醋酸酯)水解和离子液体与里氏木霉纤维素水解酶联合水解两种不同方法获得的纳米纤维素的参数。用2种离子液体:1-烯丙基-3-甲基咪唑氯(AmimCl)和1-乙基-3-甲基咪唑乙酸(EmimOAc)处理Avicel纤维素。在两步水解中,纤维素经离子液体处理后,再用酶溶液水解。为了表征所获得的材料,使用了以下分析:红外光谱,x射线衍射和动态光散射。结果表明,两步法制备的纳米纤维素(先用离子液体水解,再用酶水解)与一步法制备的纳米纤维素具有相似的参数(粒度、XRD图谱和结晶度)。
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引用次数: 1
Measurement of tool wear using a non-contact method, using a laser measuring system 使用非接触方法测量刀具磨损,使用激光测量系统
Pub Date : 2021-12-30 DOI: 10.5604/01.3001.0015.6637
Bartłomiej Grzegorzewski, P. Król
Measurement of tool wear using a non-contact method, using a laser measuring system. This article examined the tools - straight cutters with a contactless method using a laser sensor. The first aspect of the research was to determine the influence of the spindle rotational speed on the accuracy of laser measurement. The second aspect of the research was to establish the correlation between the diameter of the tool measured with a laser micrometer and the wear of the tool measured with the microscope. A good (R2> 0.8) Pearson's correlation was found between the measured tool diameter and it’s wear.
使用非接触方法测量刀具磨损,使用激光测量系统。这篇文章检查了工具-直切割机与非接触方法使用激光传感器。研究的第一方面是确定主轴转速对激光测量精度的影响。研究的第二个方面是建立用激光测微计测量的刀具直径与用显微镜测量的刀具磨损之间的关系。在测量的刀具直径和磨损之间发现了良好的Pearson相关性(R2> 0.8)。
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引用次数: 0
期刊
Annals of WULS, Forestry and Wood Technology
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