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Wear behavior of crown restoration materials and bovine tooth enamel opposed by pure titanium. 纯钛对冠修复材料与牛牙釉质磨损行为的影响。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-04-01 Epub Date: 2025-02-14 DOI: 10.4012/dmj.2024-078
Hiroki Kagoura, Rika Munakata, Masaaki Kasahara, Tomoko Someya, Masayuki Hattori

The purpose of this study was to investigate the wear behavior of pure titanium when opposed to six different crown restorative materials. Abrader specimens were prepared by casting pure titanium and these were paired with substrates including pure titanium, resin composite, lithium disilicate, zirconia, silver-palladium-copper (Ag-Pd-Cu) alloy, and bovine enamel. The wear volume of each abrader and substrate specimen was measured using the two-body wear test, and factors affecting wear behavior, such as microstructures and hardness, were evaluated. Results indicated that titanium-to-titanium abrasion caused significant wear in both the abrader and the substrate. In contrast, no significant wear was observed for the zirconia and Ag-Pd-Cu alloy against titanium. SEM images showed linear wear marks in most specimens other than zirconia and resin composite, microcracks in enamel, and filler fall in resin composite. A strong correlation between the wear volume and Vickers hardness was found for ceramics, resin composites, and enamel. However, due to the small slope of the approximate straight line in this correlation suggests that the wear behavior of materials when abraded by titanium is only partially influenced by the microstructure and hardness of the material.

本研究的目的是研究纯钛与六种不同冠修复材料的磨损行为。通过铸造纯钛制备磨具样品,并将其与纯钛、树脂复合材料、二硅酸锂、氧化锆、银钯铜(Ag-Pd-Cu)合金和牛搪瓷等衬底配对。采用双体磨损试验测量了各磨具和基体试样的磨损量,并评估了影响磨损行为的因素,如显微组织和硬度。结果表明,钛对钛的磨损对研磨器和基体都产生了明显的磨损。相比之下,氧化锆和Ag-Pd-Cu合金对钛没有明显的磨损。扫描电镜图像显示,除氧化锆和树脂复合材料外,大部分样品呈线性磨损痕迹,牙釉质微裂纹,树脂复合材料中填料脱落。陶瓷、树脂复合材料和搪瓷的磨损量与维氏硬度之间存在很强的相关性。然而,由于该相关性中近似直线的斜率较小,这表明材料被钛磨损时的磨损行为仅部分受材料的显微组织和硬度的影响。
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引用次数: 0
Effects of PEEK surface treatment using alumina blasting or concentrated sulfuric acid etching in combination with functional monomers on shear bond strength to adhesive cement after artificial aging. 氧化铝喷砂或浓硫酸蚀刻复合功能单体表面处理对人工老化后与胶粘剂水泥剪切结合强度的影响。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-04-01 Epub Date: 2025-02-08 DOI: 10.4012/dmj.2024-233
Maowei Zhong, Ryuhei Kanda, Susumu Tsuda, Yoshiya Hashimoto, Ruonan Zhang, Takamasa Fujii, Kosuke Kashiwagi

The purpose of this study is to investigate the effects of surface treatment methods using polyetheretherketone (PEEK) (with or without a functional monomer-containing primer following treatment with alumina blasting or concentrated sulfuric acid) on the shear bond strength (SBS) of resin luting material after artificial aging. The PEEK specimens were classified into five groups according to their treatment methods: untreated, alumina blasting (AB), concentrated sulfuric acid (SA), alumina blasting+primer (ABP), and concentrated SA+primer (SAP). The SBS score of each group was determined experimentally using a universal testing machine. The SBS tests revealed that the initial bond strengths of ABP and SAP were significantly higher than those of AB and SA. In addition, both SBS after 20,000 thermal cycles remained high (>15 MPa). These results suggest that the ABP and SAP groups are the best predictive methods for evaluating SBS with PEEK and resin cement.

本研究的目的是探讨聚醚醚酮(PEEK)表面处理方法(氧化铝喷射或浓硫酸处理后使用或不使用含功能单体的底漆)对人工老化后树脂敷层材料剪切结合强度(SBS)的影响。根据处理方法将 PEEK 试样分为五组:未处理组、氧化铝喷射组(AB)、浓硫酸组(SA)、氧化铝喷射+底漆组(ABP)和浓硫酸组+底漆组(SAP)。各组的 SBS 评分是通过万能试验机进行实验测定的。SBS 测试表明,ABP 和 SAP 的初始粘接强度明显高于 AB 和 SA。此外,经过 20,000 次热循环后,这两种材料的 SBS 仍保持较高水平(大于 15 兆帕)。这些结果表明,ABP 和 SAP 组是评估 PEEK 和树脂水泥 SBS 的最佳预测方法。
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引用次数: 0
Network integrity of bulk-fill composites: Thermal stability, post-curing hardness development and acidic softening. 块体填充复合材料的网络完整性:热稳定性、固化后硬度发展和酸性软化。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-04-01 Epub Date: 2025-02-14 DOI: 10.4012/dmj.2024-247
Mohammed Aldhafyan, Abdel-Basit Al-Odayni, Waseem Sharaf Saeed, Rawaiz Khan, Ali Alrahlah

This study investigated the thermal stability and top-to-bottom hardness ratio of six bulk-fill composites (STARK® Bulk Fill Composite, Filtek™ One Bulk Fill Restorative, SDR® Plus Bulk Fill Flowable, Tetric® N-Ceram Bulk Fill, X-tra fil, and Beautifil-Bulk Restorative) following acidic softening. Discs-shaped specimens were fabricated and photo-cured for 20 s. Vickers hardness was sequentially measured, immediately after irradiation (VH0), after 24 h of dry storage (VHdry) and after 24 h of acidic storage (VHacidic) at 37°C. Network integrity was assessed by comparing the relative hardness decrease (VHRD) after acidic softening with the initial maximum rate temperature (IRT) of mass loss. Compared to VH0, VHdry significantly increased, whereas VHacidic significantly decreased. The VHRD of top surface ranged from 16.62% for FBF to 62.84% for SDR. IRT primarily reflects resin composition and residue is a filler-based value. Relative network integrity estimated by IRT revealed a negative correlation with VHRD. Consequently, acidic erosion hardness development can be indirectly employed to assess network integrity in bulk-fill composites.

本研究研究了六种散装填充复合材料(STARK®散装填充复合材料、Filtek™One散装填充修复材料、SDR®Plus可流动散装填充材料、Tetric®N-Ceram散装填充材料、X-tra fil和beautifil -散装修复材料)在酸性软化后的热稳定性和上下硬度比。制作盘状标本,光固化20 s。在37℃条件下,分别测定辐照后(VH0)、干贮存24 h (VHdry)和酸贮存24 h (vhacid)后的维氏硬度。通过比较酸软化后的相对硬度降低(VHRD)与初始最大失重速率温度(IRT)来评估网络完整性。与VH0相比,VHdry显著升高,vhacid显著降低。顶面VHRD为FBF的16.62% ~ SDR的62.84%。IRT主要反映树脂成分和残渣是一个以填料为主的值。IRT估计的相对网络完整性与VHRD呈负相关。因此,酸性侵蚀硬度发展可以间接用于评估块体填充复合材料的网络完整性。
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引用次数: 0
Effect of vacuum plasma treatment on the shear bond strength of 3D-printed resin and self-adhesive resin cement. 真空等离子体处理对3d打印树脂与自粘树脂水泥剪切粘结强度的影响。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-04-01 Epub Date: 2025-02-14 DOI: 10.4012/dmj.2024-128
Mintae Lee, You-Jung Kang, Yeseul Park, Hyun Jeong Jeon, Jee-Hwan Kim

This study investigated the effect of vacuum plasma treatment on the shear bond strength (SBS) of three-dimensional (3D)-printed resin and resin cement. Specimens were categorized based on airborne-particle abrasion (APA), plasma, and bonding agent treatments. Long-term adhesive stability was examined by comparing their SBSs before and after thermocycling. The group with the bonding agent applied after plasma treatment and before thermocycling exhibited the highest SBS of 23.9±2.2 MPa. No significant SBS difference was observed among the remaining groups, except for that subjected only to plasma treatment after thermocycling. The wettability of distilled water improved in the groups treated with plasma, whereas that of the bonding agent decreased in the group treated only with APA. Surface analysis revealed a roughened surface on the plasma-treated 3D-printed resin. Therefore, vacuum-plasma treatment before thermocycling can enhance the SBS of 3D-printed resin without compromising its properties.

研究了真空等离子体处理对三维(3D)打印树脂和树脂水泥剪切粘结强度(SBS)的影响。根据空气颗粒磨损(APA)、等离子体和粘结剂处理对标本进行分类。通过比较热循环前后的sbs,考察其长期粘接稳定性。在等离子体处理后和热循环前使用粘合剂的组SBS最高,为23.9±2.2 MPa。除热循环后仅接受等离子体处理的各组外,其余各组间SBS无显著差异。等离子体处理组蒸馏水的润湿性得到改善,而仅用APA处理组黏合剂的润湿性下降。表面分析显示,等离子体处理的3d打印树脂表面粗糙。因此,热循环前的真空等离子体处理可以在不影响其性能的情况下提高3d打印树脂的SBS。
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引用次数: 0
Dentin cavity pretreatments to improve the bond strength of direct and CAD/CAM restorations using resin composite. 牙本质腔预处理提高树脂复合材料直接修复体和CAD/CAM修复体的结合强度。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-04-01 Epub Date: 2025-03-05 DOI: 10.4012/dmj.2024-220
Reo Sugiyama, Toshio Maseki

Dentin cavity wall pretreatments to improve the bond strength of direct and computer-aided design/computer-aided manufacturing (CAD/CAM) restorations using resin composite were examined. Experiment 1 divided 18 standardized MOD cavities into three conditions: no pretreatment (Group N, control); chemical pretreatment with EDTA solution (Group C); and mechanical pretreatment with glycine air-powder polishing (Group M). Specimens were restored using direct resin composites. Micro-tensile bond strength (μ-TBS) was measured after cyclic loading. The μ-TBS was significantly higher for Groups C and M than for Group N. Group M showed the best bonding reliability. In Experiment 2, cavity preparation, dentin pretreatment, cyclic loading, and μ-TBS testing were performed using the same methods applied in Experiment 1. Specimens were restored using CAD/CAM resin composite inlays. The μ-TBS was significantly higher for Groups C and M than for Group N. No significant difference in bonding reliability was apparent among all groups.

采用树脂复合材料对牙本质腔壁进行预处理以提高直接修复体和计算机辅助设计/计算机辅助制造(CAD/CAM)修复体的粘结强度。实验1将18个标准化MOD空腔分为3组:未预处理(N组,对照组);EDTA溶液化学预处理(C组);采用甘氨酸空气粉末抛光(M组)进行机械预处理。循环加载后测定微拉伸粘结强度(μ-TBS)。C组和M组的μ-TBS显著高于n组。实验2采用与实验1相同的方法进行空腔制备、牙本质预处理、循环加载和μ-TBS测试。采用CAD/CAM树脂复合嵌体修复标本。C组和M组的μ-TBS显著高于n组,各组间的粘接可靠性无显著差异。
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引用次数: 0
PEEK stress-shielding with artificial bone for dental implants. 牙种植体用聚醚醚酮人工骨应力屏蔽材料。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-01-31 Epub Date: 2025-01-11 DOI: 10.4012/dmj.2024-203
Eiji Yoshida, Rie Nomoto, Yasuharu Amitani, Tohru Hayakawa

Dental titanium implants and their surface modifications markedly improve implant biocompatibility. However, studies evaluating the mechanical biocompatibility of implants are scarce. In particular, the analysis of mechanical biocompatibility deficiencies leading to stress shield-induced bone resorption. Recently, we focused on using PEEK as a dental material. This study explored the hypothesis that PEEK implants improve the stress shielding of titanium. In this study, artificial bone surfaces were examined to measure strains on the artificial bone surface under compressive loading with the implants in place. Additionally, 3D image analysis of the fracture state inside the bone tissue was performed using micro-CT (µCT). This hypothesis was supported by µCT imaging analysis of bone tissue changes under stress, which revealed that PEEK implants transfer greater loads than titanium implants. µCT imaging and statistical analysis showed that bone porosity had little effect on stress shielding.

牙钛种植体及其表面修饰可显著提高种植体的生物相容性。然而,评估种植体机械生物相容性的研究很少。特别是,机械生物相容性缺陷导致应力屏蔽诱导骨吸收的分析。最近,我们专注于使用PEEK作为牙科材料。本研究探讨了PEEK植入物改善钛的应力屏蔽的假设。在本研究中,我们检测了人工骨表面,以测量植入物在压缩载荷下人工骨表面的应变。此外,使用micro-CT(µCT)对骨组织内部的骨折状态进行3D图像分析。这一假设得到了应力作用下骨组织变化的微CT成像分析的支持,结果显示PEEK植入物比钛植入物转移的载荷更大。微CT成像和统计分析显示,骨孔隙度对应力屏蔽的影响很小。
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引用次数: 0
Effects of repetitive insertion/removal and occlusal load on the retentive force of rest plate-I bar clasps made by selective laser melting. 选择性激光熔化法制作的托板 I 型杆卡扣的重复插入/拔出和咬合负荷对其固位力的影响。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-01-31 Epub Date: 2024-11-09 DOI: 10.4012/dmj.2024-271
Yuki Uekubo, Yoshimitsu Kato, Keita Tomono, Mitsuo Kato, Juro Wadachi, Shinji Takemoto, Shuichiro Yamashita

The objective of this study was to investigate the effects of repetitive removal/insertion and a load equivalent to the occlusal force on the retentive force of rest plate-I bar (RPI) clasps fabricated by selective laser melting (SLM) on powder bed fusion. RPI clasp fabricated by SLM and casting were evaluated to the retentive force by repetitive removal/insertion (SLM-RI and Cast-RI), and the retentive force of RPI clasp by SLM was also evaluated by repetitive removal/insertion under load (SLM-L). SLM-RI group was kept superior retentive force during repetitive removal/insertion than Cast-RI group. SLM-L group showed the decrease of retentive force, and all specimens fractured during less than 7,000 repetitive removal/insertion. In SLM-L, the fracture of RPI clasp occurred at minor connector due to stress concentration. In conclusion, the RPI clasp by SLM demonstrated the superior retentive force and fitting for repetitive removal/insertion, yet improvements were necessary to withstand a load equivalent to occlusal force.

本研究的目的是探讨重复去除/插入和相当于咬合力的载荷对粉末床熔融上选择性激光熔化(SLM)制造的托板-I杆(RPI)扣的保持力的影响。采用 SLM 和铸造法制造的 RPI 扣通过重复取出/插入(SLM-RI 和 Cast-RI)对固位力进行了评估,采用 SLM 制造的 RPI 扣还通过在负载下重复取出/插入(SLM-L)对固位力进行了评估。与 Cast-RI 组相比,SLM-RI 组在重复取出/插入过程中保持了更高的牵引力。SLM-L 组的保持力有所下降,所有试样在少于 7000 次重复取出/插入过程中均发生断裂。在 SLM-L 组中,由于应力集中,RPI 扣的断裂发生在次要接头处。总之,采用 SLM 技术的 RPI 扣在重复摘戴/插入时表现出更优越的固位力和贴合性,但要承受与咬合力相当的负荷,还需要进行改进。
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引用次数: 0
Detecting the articular disk in magnetic resonance images of the temporomandibular joint using YOLO series. 应用YOLO系列在颞下颌关节磁共振图像中检测关节盘。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-01-31 Epub Date: 2024-12-28 DOI: 10.4012/dmj.2024-186
Yuki Yoshimi, Yuichi Mine, Kohei Yamamoto, Shota Okazaki, Shota Ito, Mizuho Sano, Tzu-Yu Peng, Takashi Nakamoto, Toshikazu Nagasaki, Naoya Kakimoto, Takeshi Murayama, Kotaro Tanimoto

The purpose of this study was to construct an artificial intelligence object detection model to detect the articular disk from temporomandibular joint (TMJ) magnetic resonance (MR) images using YOLO series. The study included two experiments using datasets from different MR imaging machines. A total of 536 MR images were retrospectively examined. The performance of YOLOv5 and YOLOv8 in detecting the TMJ articular disk in both normal and displaced conditions was evaluated. The impact of image-processing techniques, such as histogram equalization (HE) and contrast-limited adaptive HE (CLAHE) on model performance, was also examined. The results showed that the YOLO series could detect the articular disk regardless of displacement, with superior performance on images of normal disk position. The results suggest the applicability of object detection models in improving the diagnosis of TMJ disorders.

本研究的目的是利用YOLO序列构建人工智能目标检测模型,从颞下颌关节(TMJ)磁共振(MR)图像中检测关节盘。该研究包括两个实验,使用来自不同核磁共振成像仪的数据集。回顾性检查共536张MR图像。评估YOLOv5和YOLOv8在正常和移位情况下检测TMJ关节盘的性能。图像处理技术,如直方图均衡化(HE)和对比度限制自适应HE (CLAHE)对模型性能的影响也进行了研究。结果表明,YOLO系列可以检测关节盘,而不受关节盘位移的影响,在正常关节盘位置的图像上表现优异。结果表明,目标检测模型在提高颞下颌关节疾病诊断中的适用性。
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引用次数: 0
Enamel microcrack inspection using near-infrared light transillumination with fluorescence staining. 近红外光透照荧光染色法检测牙釉质微裂纹。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-01-31 Epub Date: 2024-12-03 DOI: 10.4012/dmj.2023-336
Toshio Maseki, Kensuke Furuki, Reo Sugiyama, Miwa Nakazawa, Mei Komoto, Masahiko Maeno

Enamel microcracks are often apparent in the teeth of elderly individuals. However, accurate clinical diagnosis of enamel microcracks is very difficult. The purpose of this study was to examine the utility of inspections for enamel microcracks using a near-infrared light transillumination device with fluorescence staining. Human upper incisors with typical enamel microcracks were selected. Grayscale pictures of each tooth specimen were then taken by digital camera under visible light as control. Every tooth specimen was stained using indocyanine green solutions, then examined, and photographed under visible light. All digital images were compared with the background enamel surface and measured using image analysis software. Inspection using near-infrared light transillumination with indocyanine green solution was effective for detecting the presence of enamel microcracks. This method offers a non-invasive method of chair-side diagnosis and appears effective for detecting the presence of enamel microcracks.

老年人牙齿上的牙釉质微裂纹经常很明显。然而,牙釉质微裂的临床诊断非常困难。本研究的目的是探讨近红外光透射荧光染色装置在牙釉质微裂纹检测中的应用。选择具有典型牙釉质微裂的人上切牙。然后用数码相机在可见光下拍摄每个牙齿标本的灰度图像作为对照。每个牙齿标本用吲哚菁绿溶液染色,然后检查,在可见光下拍照。所有数字图像与背景牙釉质表面进行比较,并使用图像分析软件进行测量。近红外光透射吲哚菁绿溶液检测牙釉质微裂纹的存在是有效的。这种方法提供了一种非侵入性的椅子侧诊断方法,对检测牙釉质微裂纹的存在是有效的。
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引用次数: 0
Evaluation of torque moment in self-ligation lingual brackets. 自结扎舌托槽力矩的评价。
IF 1.9 4区 医学 Q2 DENTISTRY, ORAL SURGERY & MEDICINE Pub Date : 2025-01-31 Epub Date: 2024-12-03 DOI: 10.4012/dmj.2024-187
Shingo Mineta, Akira Nakajima, Eiji Tanaka, Shigeki Hanawa, Shinya Horiuchi, Kazumitsu Sekine, Tsuyoshi Sasagawa, Yasuhiro Namura, Takayuki Yoneyama, Mitsuru Motoyoshi

This study investigates the moments generated when applying third-order bends to lingual brackets with different slot shapes and wires made of different materials. Three types of lingual brackets with different slot shapes: 0.018×0.018-inch square slot self-ligation bracket (AL-bracket); 0.018×0.025-inch slot self-ligation bracket (CL-bracket); 0.018×0.025-inch slot self-ligation bracket (ST-bracket). Wires of three different materials were measured. The torque value generated during torque application was measured using a torque gauge. The AL-bracket had a significantly larger torque moment than the CL- and ST-brackets at the same angles. The CL-bracket had the smallest torque moment of the three for the square wire; however, the CL-bracket revealed a larger torque moment than the ST-bracket for the rectangular wire. The torque moment of Ti-Ni wires was observed the smallest. In lingual orthodontic treatment, the results suggested the shape of the lingual bracket slot and the wire material should be considered when adjusting and applying third-order bends.

本研究考察了三阶弯矩对不同槽形舌托和不同材质舌托的作用。三种不同槽形舌托:0.018×0.018-inch方槽自结扎托(al -托);0.018×0.025-inch槽型自结扎支架(cl -支架:);0.018×0.025-inch槽型自结扎支架(st型支架)。测量了三种不同材料的导线。使用扭矩计测量扭矩施加过程中产生的扭矩值。在相同角度下,al型支架的扭矩明显大于CL型和st型支架。对于方线,cl -支架的力矩最小;然而,对于矩形导线,cl -支架显示出比st -支架更大的扭矩力矩。钛镍丝的转矩最小。结果提示在舌正畸治疗中,调整和应用三阶弯管时应考虑舌托槽的形状和丝线的材料。
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引用次数: 0
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Dental materials journal
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