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A new model to determine the shear modulus and Poisson's ratio of shock-compressed metals up to the melting point 一种确定熔点以下冲击压缩金属剪切模量和泊松比的新模型
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-09-13 DOI: 10.1080/08957959.2021.1976775
E. I. Kraus, I. Shabalin
ABSTRACT In this paper, using the few-parametric equation of state, an approach is implemented to the calculation of the longitudinal and bulk sound speeds, as well as the elastic moduli of a number of isotropic metals behind the front of a strong shock wave. The results of theoretical calculations for aluminum are compared with the available shock impact experimental data. A new analytical approximation of the dependence of the Poisson's ratio on the pressure is proposed for metals. Non-monotonic dependence of the shear modulus for uranium on the pressure and temperature in view of the melting behind the shock front is determined.
本文利用少参数状态方程,实现了强激波后各向同性金属的纵向声速、体声速以及弹性模量的计算方法。将理论计算结果与已有的冲击冲击实验数据进行了比较。提出了金属泊松比与压力关系的一种新的解析近似。考虑到激波后的熔化,确定了铀的剪切模量与压力和温度的非单调关系。
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引用次数: 2
Optimisation of toroidal ZTA anvils and gaskets; towards improved load and pressure performance 环形ZTA砧座和垫圈的优化;提高负载和压力性能
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1971214
N. Funnell, C. Bull, C. Ridley
ABSTRACT We have modified zirconia-toughened alumina anvil geometry and systematically varied single-toroidal, encapsulated, Ti–Zr gasket dimensions, exploring the resulting effects on pressure and maximum load performance, which have been measured using a Paris–Edinburgh press. Reducing the curvature and depth of the recess at the rear of the anvil appears to permit repeated use of the anvils to higher loads, and a general trend indicates that thinner Ti–Zr gaskets may achieve higher pressures than thicker alternatives.
摘要:我们修改了氧化锆增韧氧化铝砧座的几何形状,并系统地改变了单个环形、封装的Ti–Zr垫圈的尺寸,探索了由此对压力和最大负载性能的影响,这些影响已使用巴黎-爱丁堡压机进行了测量。减少砧座后部凹陷的曲率和深度似乎允许在更高的载荷下重复使用砧座,总体趋势表明,较薄的Ti–Zr垫圈可能比较厚的替代品获得更高的压力。
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引用次数: 0
Elastic properties of Mg-phase D at high pressure mg相D在高压下的弹性性能
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1954177
Chaowen Xu, Ying Li, T. Inoue, S. Gréaux, Qingze Li, Jing Gao, F. Sun, Leiming Fang
ABSTRACT The sound velocities of polycrystalline Mg-phase D were investigated at the pressure up to 13.6 GPa and room temperature, using ultrasonic interferometry in a multi-anvil apparatus. The P (VP ) and S (VS ) wave velocities obtained at ambient conditions produced the results of VP  = 9.26(3) km/s and VS  = 5.46(1) km/s. The results are in accordance with the values for Mg-phase D by Brillouin scattering (VP  = 9.25 km/s and VS  = 5.51km/s). The results, i.e. Ks0 = 153.8(13) GPa and G0 = 99.8(5) GPa obtained through two-dimensional linear fitting analysis are self-consistent with Ks0 = 153.3(16) GPa and G0 = 99.5(10) GPa derived by third-order Eulerian finite strain equations. We also find that Vp of phase D is 1.8–2.2% lower than Fe-ringwoodite, but Vs is higher than Fe-ringwoodite at the bottom of the mantle transition zone by up to 1.3%.
摘要在高达13.6的压力下,研究了多晶Mg相D的声速 GPa和室温,在多砧装置中使用超声波干涉测量法。在环境条件下获得的P(VP)和S(VS)波速度产生了VP的结果 = 9.26(3)km/s和VS  = 5.46(1)公里/秒。结果与通过布里渊散射得到的Mg相D的值(VP = 9.25公里/秒和VS  = 5.51km/s)。结果,即Ks0 = 153.8(13)GPa和G0 = 通过二维线性拟合分析获得的99.8(5)GPa与Ks0自洽 = 153.3(16)GPa和G0 = 由三阶欧拉有限应变方程导出的99.5(10)GPa。我们还发现,在地幔过渡带底部,D相的Vp比铁环木矿低1.8–2.2%,但Vs比铁环木矿高出1.3%。
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引用次数: 1
Continuous measurement of ultrasonic elastic wave velocities, X-ray radiography and X-ray diffraction of Zr50Cu40Al10 metallic glass at high pressure and high temperature conditions Zr50Cu40Al10金属玻璃在高压和高温条件下超声弹性波速度的连续测量、X射线照相和X射线衍射
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1941000
Y. Kono, Y. Higo, S. Gréaux, Y. Shibazaki, R. Yamada, H. Kuwahara, N. Kondo
ABSTRACT A new experimental setup to continuously and automatically measure ultrasonic elastic wave velocities, X-ray radiography, and X-ray diffraction in large volume press is developed to explore structural change of amorphous materials at in situ high pressure and high temperature conditions. A continuous measurement for Zr50Cu40Al10 metallic glass is carried out during the heating process from 304 to 1102 K under high pressure conditions of 6.8–8.6 GPa. The sample length, elastic wave velocities, and Poisson’s ratio show marked changes at 611, 745, 825, and 874 K, which are interpreted as glass transition temperature (Tg ) at 611 K, two polyamorphic structural changes at 745 and 825 K, and crystallization above 874 K, respectively. We find that the 1.2Tg temperature (733 K at ∼8 GPa), where simulations study predicted occurrence of thermal rejuvenation, corresponds to the temperature of the polyamorphic structural change (745 K) in Zr50Cu40Al10 metallic glass.
摘要开发了一种新的实验装置,用于在大体积压力机中连续自动测量超声弹性波速、X射线照相和X射线衍射,以探索非晶材料在原位高压和高温条件下的结构变化。在304到1102的加热过程中,对Zr50Cu40Al10金属玻璃进行了连续测量 K在6.8–8.6的高压条件下 GPa。样本长度、弹性波速和泊松比在611745825和874处显示出显著变化 K、 其被解释为611的玻璃化转变温度(Tg) K、 745和825的两次多晶结构变化 K、 结晶度高于874 K、 分别。我们发现1.2Tg的温度(733 K在~8 GPa),其中模拟研究预测了热再生的发生,对应于多晶结构变化的温度(745 K) 在Zr50Cu40Al10金属玻璃中。
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引用次数: 2
Pressure-induced structural phase transition in corundum-related class Cu3TeO6 刚玉相关类Cu3TeO6的压力诱导结构相变
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1975699
Jia Qu, Limin Yan, Hetian Liu, Q. Tao, P. Zhu, Zhihui Li, Xin Wang
ABSTRACT The high pressure structural changes of Cu3TeO6 have been investigated by using synchrotron radiation X-ray diffraction and Raman spectroscopy up to 23.2(4) and 45.9(7) GPa, respectively. It was found that Cu3TeO6 transformed from the cubic (Ia-3) structure to the orthorhombic (Ibca) structure around 8.6(1) GPa, and the phase transition was reversible. The phase transformation was subtle because of the similarity between two crystal structures. A large internal lattice strain could be the cause to the pressure-induced structural phase transition.
摘要利用同步辐射X射线衍射和拉曼光谱研究了Cu3TeO6的高压结构变化,分别高达23.2(4)和45.9(7)GPa。研究发现,Cu3TeO6在8.6(1)GPa左右从立方(Ia-3)结构转变为正交(Ibca)结构,并且相变是可逆的。由于两种晶体结构之间的相似性,相变是微妙的。大的内部晶格应变可能是压力诱导结构相变的原因。
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引用次数: 0
Phase transitions of ScOOH under high pressure 高压下ScOOH的相变
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1964495
Yoshiaki Ito, O. Ikeda, Rintaro Ban, T. Kubota, T. Sakamaki, T. Kuribayashi, A. Suzuki
ABSTRACT In-situ X-ray diffraction measurements of ScOOH were conducted under high pressure and temperature conditions up to 11 GPa and 900 K to understand its phase transitions. As the pressure increased, α-ScOOH, InOOH-type ScOOH, and YbOOH-type ScOOH were observed. The experimental results indicate that the boundaries between α-ScOOH and InOOH-type ScOOH, and between InOOH-type and YbOOH-type ScOOH are represented by the following linear equations: P(GPa) = (0.0009 ± 0.0015) × [T(K) – 700] + 4.33 ± 0.04 and P(GPa) = (–0.0029 ± 0.0002) × [T(K) – 800] + 8.1 ± 0.3, respectively. By using a least-squares fit of the second-order Birch–Murnaghan equation of state (EoS) to the experimental compression data, the EoS parameters of the three phases of ScOOH at 400 K were obtained. The volume change of the transition from α-ScOOH to InOOH-type ScOOH is ∼3.9% at 4 GPa and 400 K, while the volume change of the transition from InOOH-type to YbOOH-type ScOOH is ∼7.6% at 9 GPa and 400 K.
在高达11 GPa和900 K的高压和高温条件下,对ScOOH进行了原位x射线衍射测量,以了解其相变。随着压力的增加,出现α-ScOOH、inooh型ScOOH和yboo型ScOOH。实验结果表明,α-ScOOH与inooh型ScOOH、inooh型ScOOH与ybooh型ScOOH之间的边界分别为:P(GPa) =(0.0009±0.0015)× [T(K) - 700] + 4.33±0.04和P(GPa) =(- 0.0029±0.0002)× [T(K) - 800] + 8.1±0.3。利用二阶Birch-Murnaghan状态方程(EoS)对实验压缩数据进行最小二乘拟合,得到了400 K时ScOOH三相的EoS参数。在4 GPa和400 K条件下,α-ScOOH向inoh型ScOOH转变的体积变化为~ 3.9%,而在9 GPa和400 K条件下,inoh型ScOOH向yboo型ScOOH转变的体积变化为~ 7.6%。
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引用次数: 2
Inhibitory effect of high hydrostatic pressure, nisin, and moderate heating on the inactivation of Paenibacillus sp. and Terribacillus aidingensis spores isolated from UHT milk 高静水压、乳酸链球菌肽和适度加热对超高温灭菌乳中分离的Paenibacillus sp.和Terrillus aidingensis孢子灭活的抑制作用
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1946054
S. Kmiha, C. Modugno, C. Aouadhi, H. Simonin, S. Méjri, J. Perrier-Cornet, A. Maaroufi
ABSTRACT The sensitivity of Paenibacillus sp. and Terribacillus aidingensis spores to combined action of HP, nisin and moderate heating were investigated for the first time. The results showed that the effect of HP on spores varies with pressure level, treatment temperature, spore species and presence of nisin. T. aidingensis spores were more resistant than Paenibacillus sp., whatever the treatment applied. The inactivation rates of both spore species did not exceed 2.7log (CFU/mL) after HP treatment at 600 MPa/50°C/10 min. However, a high synergistic effect of nisin and HP was observed after a treatment at 500 MPa/10 min/50°C with addition of nisin during HP and into the recovery medium, leading to 6log (CFU/mL) and 4log (CFU/mL) reduction for Paenibacillus and Terribacillus spores, respectively. Finally, the fraction of germinated spores by HP was measured and the results showed that germination induction is not the only underlying mechanisms of nisin sensitization by HP.
首次研究了Paenibacillus sp.和Terribacillus aidingensis孢子对HP、nisin和温和加热联合作用的敏感性。结果表明,HP对孢子的影响随压力水平、处理温度、孢子种类和nisin的存在而变化。无论施用何种处理,辅助芽孢杆菌孢子的抗性都强于芽孢杆菌。HP在600 MPa/50℃/10 min下处理后,两种孢子的失活率均不超过2.7log (CFU/mL)。然而,在500 MPa/10 min/50℃条件下,在HP和恢复培养基中添加nisin后,观察到nisin和HP的高度协同效应,导致Paenibacillus和Terribacillus孢子分别减少6log (CFU/mL)和4log (CFU/mL)。最后,我们测量了HP的萌发孢子的比例,结果表明萌发诱导并不是HP致敏nisin的唯一潜在机制。
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引用次数: 5
Refractive index of MgAl2O4 transparent ceramic under quasi-isentropic compression loading 准等熵压缩载荷下MgAl2O4透明陶瓷的折射率
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1940999
K. Bao, Xianfeng Zhang, Guiji Wang, T. Chong, Jia-jie Deng, D. Han, M. Tan
ABSTRACT The indirect method of obtaining in situ particle velocity of sample, under dynamic high-pressure loading experiments, generates an error due to the influence of rarefaction wave from the sample-window interface. Using the spinel as a window is an attractive method to reduce the error due to the total impedance matching of sample and window in the loading experiments of the spinel. To explore the possibility of the spinel as a window, ramp wave compression experiments were conducted to determine the refractive index of loading longitudinal stress range below 15.9 GPa. The result showed smooth particle velocity curve and linear relationship between refractive index and density. The effect of temperature on refractive index can be negligible, proved by analyzing the effect of temperature on polarizability. It is indicated that the spinel can be used as a window for loading experiments of the spinel and similar impedance materials.
摘要:在动态高压加载实验中,间接获取样品原位颗粒速度的方法由于样品-窗口界面的稀薄波的影响而产生误差。在尖晶石加载实验中,采用尖晶石作为窗口是一种很有吸引力的减小样品与窗口总阻抗匹配误差的方法。为了探索尖晶石作为窗口的可能性,进行了斜波压缩实验,确定了加载纵向应力范围在15.9 GPa以下的折射率。结果表明,粒子速度曲线平滑,折射率与密度呈线性关系。通过分析温度对偏振率的影响,证明了温度对折射率的影响可以忽略不计。结果表明,尖晶石可作为尖晶石及类似阻抗材料加载实验的窗口。
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引用次数: 1
High pressure stability of β-Zr: no evidence for isostructural phase transitions β-Zr的高压稳定性:没有证据表明存在同构相变
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1957863
E. O’Bannon, P. Söderlind, D. Sneed, M. Lipp, H. Cynn, J. S. Smith, C. Park, Z. Jenei
ABSTRACT Isostructural transitions have been reported to occur in several pure elements; however, most of these have been disproven. Zr is one of those elements which remains controversial with two reports of an isostructural bcc-to-bcc transition at ∼56–60 GPa at an ambient temperature and a more recent report proposing a second bcc-to-bcc transition at 110 GPa. Here, we report a detailed experimental and theoretical study of zirconium in the pressure region of the proposed isostructural transition(s). We conducted three room temperature static compression experiments using Ne as a pressure transmitting medium up to 80 GPa. We see no evidence for an isostructural transition finding a smooth compression curve for β-Zr. We determined the theoretical volume, elastic parameters, and Poisson’s ratio for β-Zr up to 717 GPa and no obvious anomalies are identified. Our new results join the growing body of evidence that does not find evidence of isostructural transitions in β-Zr.
据报道,在几种纯元素中发生了等结构跃迁;然而,这些观点大多已被推翻。Zr是那些仍然存在争议的元素之一,有两份报告称,在~56–60时发生了同构bcc到bcc的转变 环境温度下的GPa和最近的一份报告提出了110时的第二次bcc到bcc转变 GPa。在这里,我们报道了锆在所提出的同构转变的压力区的详细实验和理论研究。我们进行了三次室温静态压缩实验,使用Ne作为压力传递介质,压力高达80 GPa。我们没有发现任何证据表明β-Zr存在一条光滑的压缩曲线。我们确定了高达717的β-Zr的理论体积、弹性参数和泊松比 GPa,未发现明显异常。我们的新结果加入了越来越多的证据,这些证据没有发现β-Zr中同构转变的证据。
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引用次数: 2
Chilled storage stability of spice marinated and high pressure processed Indian white prawns (Fenneropenaeus indicus) 香料腌制和高压加工印度白对虾的冷藏稳定性
IF 2 4区 物理与天体物理 Q3 PHYSICS, MULTIDISCIPLINARY Pub Date : 2021-07-03 DOI: 10.1080/08957959.2021.1957864
G. Joseph, C. K. Kamalakanth, K. R. Remya Kumari, J. Bindu, K. K. Asha
ABSTRACT Chilled storage stability of marinated and high pressure treated peeled and undeveined Indian white prawns (Fenneropenaeus indicus) were studied. The prawns were marinated with condiments viz. chilli powder, salt and turmeric, and - vacuum packed in ethylene-vinyl alcohol copolymer pouches. Marinated unpressurized prawn samples were kept as control. The products were stored at 2 ± 1°C for evaluating - shelf life by analysing biochemical, microbiological and organoleptic parameters. Pressurization significantly altered the quality indices such as pH, total volatile basic nitrogen, free fatty acid, thiobarbituric acid, total plate count and overall acceptability of samples. The control and 200  MPa treated sample were rejected on 20th and 25th day of storage respectively, whereas 250 and 300  MPa treated samples achieved a shelf life of 35 days. Among the samples, the prawns treated at 250  MPa were found to be organoleptically superior with respect to its biochemical and microbiological quality parameters.
摘要对印度对虾(Fenneropenaeus indicus)腌制和高压处理后去皮和未去皮的冷藏稳定性进行了研究。虾用辣椒粉、盐和姜黄等调味料腌制,真空包装在乙烯-乙烯醇共聚物袋中。以未加压腌制的对虾为对照。产品在2±1℃下保存,通过分析生化、微生物和感官参数来评估保质期。加压显著改变了样品的pH、总挥发性碱氮、游离脂肪酸、硫代巴比妥酸、总板数和总体可接受度等质量指标。对照和200 MPa处理的样品分别在第20天和第25天被拒收,而250和300 MPa处理的样品的保质期为35天。结果表明,在250 MPa条件下处理的对虾在生化和微生物质量指标上具有较好的感官优势。
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引用次数: 1
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High Pressure Research
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