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Electrolyte-based on-demand and disposable microbattery 基于电解的按需和一次性微电池
Pub Date : 2003-12-01 DOI: 10.1109/JMEMS.2003.820272
K. Lee, Liwei Lin
A micromachined battery based on liquid electrolyte and metal electrodes for on-demand and disposable usages has been successfully demonstrated. The microbattery uses gold as the positive electrode and zinc as the negative electrode and is fabricated by using the standard surface micromachining technology. Two kinds of electrolytes have been tested, including the combination of sulfuric acid/hydrogen peroxide and potassium hydroxide. The operation of the battery can be on-demand by putting a droplet of electrolyte to activate the operation. Theoretical voltage and capacity of the microbattery are formulated and compared with experimental results. The experimental study shows that a maximum voltage of 1.5 V and maximum capacity of 122.2 /spl mu/W-min have been achieved by using a single droplet of about 0.5 /spl mu/l of sulfuric acid/hydrogen peroxide.
一种基于液体电解质和金属电极的微机械电池已成功演示,用于按需使用和一次性使用。该微电池以金为正极,锌为负极,采用标准的表面微加工工艺制作而成。已经测试了两种电解质,包括硫酸/过氧化氢和氢氧化钾的组合。电池的运行可以按需输入一滴电解液来激活运行。推导了微电池的理论电压和容量,并与实验结果进行了比较。实验研究表明,硫酸/双氧水单滴用量约0.5 /spl mu/l时,最高电压可达1.5 V,最大容量可达122.2 /spl mu/W-min。
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引用次数: 31
Vertical-actuated electrostatic comb drive with in situ capacitive position correction for application in phase shifting diffraction interferometry 带原位电容位置校正的垂直驱动静电梳状驱动器在移相衍射干涉测量中的应用
Pub Date : 2003-12-01 DOI: 10.1109/JMEMS.2003.820262
A. Lee, C. McConaghy, G. Sommargren, P. Krulevitch, E. Campbell
This research utilizes the levitation effect of electrostatic comb fingers to design vertical-to-the-substrate actuation for optical phase shifting interferometry applications. For typical polysilicon comb drives with 2 /spl mu/m gaps between the stationary and moving fingers, as well as between the microstructures and the substrate, the equilibrium position is nominally 1-2 /spl mu/m above the stationary comb fingers. This distance is ideal for most phase shifting interferometric applications. A parallel plate capacitor between the suspended mass and the substrate provides in situ position sensing to control the vertical movement, providing a total feedback-controlled system. The travel range of the designed vertical microactuator is 1.2 /spl mu/m. Since the levitation force is not linear to the input voltage, a lock-in amplifier capacitive sensing circuit combined with a digital signal processor enables a linearized travel trajectory with 1.5 nm position control accuracy. A completely packaged micro phase shifter is described in this paper. One application for this microactuator is to provide linear phase shifting in the phase shifting diffraction interferometer (PSDI) developed at LLNL which can perform optical metrology down to 2 /spl Aring/ accuracy.
本研究利用静电梳指的悬浮效应设计了用于光学移相干涉测量的垂直于衬底的驱动装置。对于典型的多晶硅梳状驱动器,在固定和移动手指之间以及微结构和衬底之间具有2 /spl mu/m的间隙,通常平衡位置在固定梳子手指上方1-2 /spl mu/m。这个距离对于大多数相移干涉测量应用是理想的。悬浮质量和衬底之间的平行板电容器提供原位位置传感以控制垂直运动,从而提供一个完全反馈控制的系统。所设计的立式微动器行程范围为1.2 /spl mu/m。由于悬浮力与输入电压不是线性关系,锁相放大器电容传感电路与数字信号处理器相结合,使线性化的行程轨迹具有1.5 nm的位置控制精度。本文介绍了一种完全封装的微型移相器。该微致动器的一个应用是在LLNL开发的相移衍射干涉仪(PSDI)中提供线性相移,该干涉仪可以执行低至2 /spl / Aring/精度的光学测量。
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引用次数: 82
New low-stress PECVD poly-SiGe Layers for MEMS 用于MEMS的新型低应力PECVD聚sige层
Pub Date : 2003-01-01 DOI: 10.1109/JMEMS.2003.820304
C. Rusu, S. Sedky, B. Parmentier, A. Verbist, O. Richard, B. Brijs, L. Geenen, A. Witvrouw, F. Lärmer, F. Fischer, S. Kronmüller, V. Leca, B. Otter
Thick poly-SiGe layers, deposited by plasma-enhanced chemical vapor deposition (PECVD), are very promising structural layers for use in microaccelerometers, microgyroscopes or for thin-film encapsulation, especially for applications where the thermal budget is limited. In this work it is shown for the first time that these layers are an attractive alternative to low-pressure CVD (LPCVD) poly-Si or poly-SiGe because of their high growth rate (100-200 nm/min) and low deposition temperature (520/spl deg/C-590/spl deg/C). The combination of both of these features is impossible to achieve with either LPCVD SiGe (2-30 nm/min growth rate) or LPCVD poly-Si (annealing temperature higher than 900/spl deg/C to achieve structural layer having low tensile stress). Additional advantages are that no nucleation layer is needed (deposition directly on SiO/sub 2/ is possible) and that the as-deposited layers are polycrystalline. No stress or dopant activation anneal of the structural layer is needed since in situ phosphorus doping gives an as-deposited tensile stress down to 20 MPa, and a resistivity of 10 m/spl Omega/-cm to 30 m/spl Omega/-cm. With in situ boron doping, resistivities down to 0.6 m/spl Omega/-cm are possible. The use of these films as an encapsulation layer above an accelerometer is shown.
通过等离子体增强化学气相沉积(PECVD)沉积的厚聚sige层是非常有前途的结构层,可用于微加速度计,微陀螺仪或薄膜封装,特别是在热预算有限的应用中。在这项工作中,首次表明这些层是低压CVD (LPCVD)多晶硅或多晶硅的有吸引力的替代品,因为它们具有高生长速率(100-200 nm/min)和低沉积温度(520/spl°/C-590/spl°/C)。LPCVD SiGe (2- 30nm /min生长速率)或LPCVD多晶硅(退火温度高于900/spl度/C以获得具有低拉伸应力的结构层)都无法实现这两种特性的结合。其他优点是不需要成核层(直接沉积在SiO/sub 2/上是可能的),而且沉积层是多晶的。不需要对结构层进行应力或掺杂激活退火,因为原位磷掺杂使沉积时的拉伸应力降至20 MPa,电阻率为10 m/spl ω /-cm至30 m/spl ω /-cm。原位硼掺杂,电阻率可低至0.6 m/spl ω /-cm。使用这些薄膜作为一个封装层上面的加速度计显示。
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引用次数: 39
Fabrication of high-density electrical feed-throughs by deep-reactive-ion etching of Pyrex glass 高温玻璃深反应蚀刻制备高密度电馈通
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.805211
X. Li, T. Abe, Y. Liu, M. Esashi
This paper describes the fabrication technology for high-density electrical feed-throughs in Pyrex glass wafers. Small through holes (40-80 /spl mu/m in diameter) in Pyrex glass wafers have been fabricated using deep-reactive-ion etching (DRIE) in a sulfur hexafluoride (SF/sub 6/) plasma. The maximum aspect ratios obtained were between 5 and 7 for a hole pattern and 10 for a trench pattern. Through the wafer etching of a hole pattern of 50 /spl mu/m diameter was carried out using 150-/spl mu/m-thick Pyrex glass wafers. The electrical feed-throughs in the wafers were fabricated by filling the through-holes with electroplated nickel. We were able to successfully bond the glass wafer to silicon by anodic bonding after removing the electroplated nickel on the surface of the wafer by chemical-mechanical polishing (CMP). The electric resistance of the feed-through was estimated by a 4 point wire sensing method to be about 40 m/spl Omega/ per hole. The heat cycles test shows that the resistance changes were within 3% after 100 cycles. The fabrication of high density electrical feed-throughs is one of the key processes in the field of MEMS. Probable applications of this technology are in electrical feed-throughs between logic elements and microprobe arrays for high-density data storage and for packaged devices.
本文介绍了高温玻璃晶圆中高密度电馈线的制造工艺。在六氟化硫(SF/sub 6/)等离子体中,采用深度反应蚀刻(DRIE)技术在Pyrex玻璃晶圆上制备了直径为40-80 μ l μ m的小通孔。所获得的最大纵横比在孔型和沟槽型之间分别为5 ~ 7和10。采用厚度为150 μ m /spl μ m的Pyrex玻璃晶圆,通过晶圆刻蚀,实现了直径为50 μ m /spl μ m的孔洞图案。通过在晶圆的通孔中填充电镀镍来制造晶圆上的电馈线。通过化学机械抛光(CMP)去除硅片表面的电镀镍后,通过阳极键合成功地将硅片与硅结合在一起。通过4点导线传感方法估计馈线的电阻约为40 m/spl ω /每个孔。热循环试验表明,经过100次循环后,电阻变化在3%以内。高密度电馈通的制备是MEMS领域的关键工艺之一。该技术的可能应用是在高密度数据存储和封装设备的逻辑元件和微探针阵列之间的电馈线。
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引用次数: 125
Investigation of strain in microstructures by a novel moire method 用一种新的云纹法研究微结构中的应变
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.805044
Biao Li, H. Xie, Bai Xu, R. Geer, J. Castracane
A focused ion beam (FIB) moire method is proposed and demonstrated to measure the strain in microstructures. This technique is based on the advantages of the FIB system in nanofabrication, imaging, selective deposition, and fine adjustment. A nanograting is directly written on the top of the microstructures by ion milling without the requirement of an etch mask. The FIB moire pattern is formed by the interference between a prepared specimen grating and FIB raster scan lines. The strain of the microstructures is derived by calculating the average spacing of moire fringes. The sensitivity and accuracy of FIB moire in strain measurement is subsequently discussed. Since the local strain of a microstructure itself can be monitored during the process, the FIB moire technique has many potential applications in the mechanical metrology of microelectromechanical systems (MEMS). As an example, the strain distribution along the sticking microstructures and the contribution of surface oxidization and mass loading to the cantilever strain is determined by this FIB moire technique.
提出并演示了聚焦离子束云纹法测量微结构应变的方法。该技术是基于FIB系统在纳米加工、成像、选择性沉积和精细调节等方面的优势。在不需要蚀刻掩膜的情况下,通过离子铣削直接将纳米光栅写入微结构的顶部。FIB云纹图案是由制备的试样光栅与FIB光栅扫描线之间的干涉形成的。通过计算云纹条纹的平均间距,得到了微结构的应变。讨论了FIB云纹在应变测量中的灵敏度和精度。由于在测量过程中可以监测微结构本身的局部应变,因此FIB云纹技术在微机电系统(MEMS)的机械测量中具有许多潜在的应用前景。作为一个例子,用FIB云纹技术确定了沿粘接微结构的应变分布以及表面氧化和质量载荷对悬臂应变的贡献。
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引用次数: 15
Parylene gas chromatographic column for rapid thermal cycling 用于快速热循环的聚对二甲苯气相色谱柱
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.805052
H. Noh, P. Hesketh, G. Frye-Mason
This paper presents a parylene gas chromatographic column with an embedded heating element. The parylene coating on a silicon microchannel and parylene/parylene thermal bonding technique were employed to fabricate a parylene column. The heating element is a thin gold film evaporated on the corrugated surface of the parylene column having long and rectangular geometry. Joule heating via the thin gold film is a very effective heating system for a parylene column. ANSYS heat transfer analysis was performed to investigate the thermal cycling and temperature uniformity of the parylene column. The parylene column showed much faster heating and cooling rates as well as lower power consumption compared to a silicon/glass column. The temperature difference between the top and the bottom of a parylene column that is due to the low thermal conductivity of parylene could be reduced to less than 0.1 K by inserting a thin metal layer between two parylene layers, forming a triple layer structure (parylene/platinum/parylene).
本文介绍了一种内置加热元件的聚对二甲苯气相色谱柱。采用硅微通道上的聚对二甲苯涂层和聚对二甲苯/聚对二甲苯热键合技术制备了聚对二甲苯柱。加热元件是蒸发在具有长矩形几何形状的聚对二甲苯柱的波纹表面上的薄金膜。通过金薄膜进行焦耳加热是一种非常有效的聚对二甲苯柱加热系统。采用ANSYS进行传热分析,研究聚对二甲苯塔的热循环和温度均匀性。与硅/玻璃柱相比,聚对二甲苯柱显示出更快的加热和冷却速度以及更低的功耗。通过在两层聚对二甲苯之间插入一层薄薄的金属层,形成聚对二甲苯/铂/聚对二甲苯三层结构,可以将聚对二甲苯热导率低所导致的柱顶与柱底温差降低到0.1 K以下。
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引用次数: 141
Tunable optical filter of porous silicon as key component for a MEMS spectrometer 多孔硅可调谐滤光片是MEMS光谱仪的关键元件
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.803278
G. Lammel, S. Schweizer, S. Schiesser, P. Renaud
We present a microspectrometer based on a tunable interference filter for infrared or visible light that scans the desired part of the spectrum within milliseconds. A single pixel detector measures serially the intensity at selected wavelengths. This concept avoids expensive linear detectors as used for grating spectrometers. The tunable filter is fabricated by a new porous silicon technology using only two photolithography steps. A Bragg mirror or a Fabry-Perot bandpass filter for transmission wavelengths between 400 nm and 8 /spl mu/m at normal incidence is created by modulations of the refractive index in the filter plate. Two thermal bimorph micro-actuators tilt the plate by up to 90/spl deg/, changing the incidence angle of the beam to be analyzed. This tunes the wavelength transmitted to the detector by a factor of 1.16. The filter area can be chosen between 0.27 /spl times/ 0.70 mm/sup 2/ and 2.50 /spl times/ 3.00 mm/sup 2/, the filter thickness is typically 30 /spl mu/m. The spectral resolution of /spl Delta//spl lambda///spl lambda/ = 1/25 is sufficient for most sensor applications, e.g., measurement of CO/sub 2/ and CO in combustion processes by their IR absorption bands as will be presented.
我们提出了一种基于可调干涉滤光器的微光谱仪,用于红外或可见光,可以在几毫秒内扫描所需的光谱部分。单像素探测器在选定波长处连续测量强度。这个概念避免了昂贵的线性探测器用于光栅光谱仪。该可调谐滤波器是由一种新的多孔硅技术制造的,仅使用两个光刻步骤。通过调制滤光片的折射率,可以制造出传输波长在400 nm ~ 8 /spl mu/m之间的布拉格反射镜或法布里-珀罗带通滤波器。两个热双晶片微致动器将板倾斜90/spl度,改变待分析光束的入射角。这使得传输到探测器的波长以1.16的倍数调谐。过滤面积可在0.27 /spl倍/ 0.70 mm/sup 2/至2.50 /spl倍/ 3.00 mm/sup 2/之间选择,过滤厚度一般为30 /spl mu/m。光谱分辨率/spl Delta//spl lambda/// /spl lambda/ = 1/25对于大多数传感器应用来说是足够的,例如,燃烧过程中CO/sub 2/和CO的红外吸收带测量。
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引用次数: 81
The piezoelectric valve-less pump - improved dynamic model 改进的压电无阀泵动力学模型
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.805048
A. Ullmann, I. Fono
The piezoelectric valve-less pump is an attractive device to be used as a micro pump for low flow rates. The pump converts the reciprocating motion of a diaphragm, activated by a piezoelectric disk, into a pumping action. Instead of conventional valves, which have moving parts, nozzle/diffuser elements that have a preferential flow direction are used to direct the flow from the inlet to the outlet. In this paper, an improved dynamic model for the simulation of valve-less piezoelectric pumps is presented. The model is capable of accurate simulation of the pump performance including the natural frequency, flow rate, and pressure drop. The model is utilized here to study the effect of the driving frequency and the inlet/outlet length and diameter of the leading pipes on the pump performance. Comparison with experiments shows good agreement with a minimal number of adjusting parameters.
压电无阀泵是一种有吸引力的小流量微泵装置。泵将由压电片激活的隔膜的往复运动转化为泵送动作。传统的阀门具有运动部件,而喷嘴/扩散器元件具有优先的流动方向,用于将流量从入口引导到出口。本文提出了一种改进的无阀压电泵仿真动力学模型。该模型能够准确地模拟泵的固有频率、流量和压降等性能。利用该模型研究了驱动频率、进出口管道长度和管道直径对泵性能的影响。与实验结果的比较表明,在最小的调整参数下,该方法具有较好的一致性。
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引用次数: 89
A fast method for particulate microflows 一种快速测定微粒微流的方法
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.805209
Dong Liu, M. Maxey, G. E. Kamiadakis
Modeling of active control of microparticles is important in a number of different microfluidic applications, including bioflows and self-assembled structures. We present here a fast method for simulating the dynamics of many particles in complex microgeometries. The method is based on a spatial distribution of finite force multipoles and requires much less resolution than full direct numerical simulations. The numerical formulation is summarized, and examples are given for Stokes flow and low Reynolds number flow in smooth and rough microchannels. Comparisons made with full direct numerical simulations and experiments validate the accuracy and efficiency of the proposed approach.
微颗粒主动控制的建模在许多不同的微流体应用中是重要的,包括生物流和自组装结构。本文提出了一种快速模拟复杂微观几何中许多粒子动力学的方法。该方法基于有限力多极的空间分布,比完全直接数值模拟所需的分辨率要低得多。总结了数值计算公式,并给出了光滑微通道和粗糙微通道中斯托克斯流和低雷诺数流的算例。通过与全直接数值模拟和实验的比较,验证了该方法的准确性和有效性。
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引用次数: 40
Fabrication, modeling, and testing of micro-cross-flow heat exchangers 微型交叉流热交换器的制造、建模和测试
Pub Date : 2002-12-16 DOI: 10.1109/JMEMS.2002.806025
C. Harris, K. Kelly, Tao Wang, A. McCandless, S. Motakef
Planar micro-cross-flow heat exchangers, similar in concept to most automobile radiators, have been fabricated using two different processes. A process that was previously reported (Harris et al., 2000) to fabricate a polymer heat exchanger involved embossing two identical polymer parts using the LIGA process. Then the two parts were aligned and bonded together. In this paper, a process is described to fabricate a nickel micro-cross-flow heat exchanger by embossing a sacrificial polymer mandrel using a LIGA-fabricated mold insert. The mandrel is coated with nickel (using either electroplating or electroless plating), then the sacrificial mandrel is dissolved. Experimental results are reported for both the polymer and nickel heat exchangers to determine the rates of heat transfer between the in-plane liquid (water) and the through-plane gas (air). Pressure drops of both fluid streams were also measured. The experimental results compare favorably with a modified version of the analytical model that was described previously. The fabricated heat exchangers have values of heat transfer/volume that are more than five times higher than conventional scale counterparts (with characteristic dimensions at least one order of magnitude larger than those reported here) and values of heat transfer/mass that are 50% greater than their conventional scale counterparts.
平面微交叉流热交换器,在概念上类似于大多数汽车散热器,已经采用两种不同的工艺制造。先前报道的一种工艺(Harris et al., 2000)制造聚合物热交换器涉及使用LIGA工艺压印两个相同的聚合物部件。然后这两部分被对齐并粘合在一起。本文介绍了一种利用liga制造的模具镶件在牺牲聚合物芯轴上压纹的方法来制造镍微交叉流换热器的工艺。在芯轴上涂上镍(电镀或化学镀),然后溶解牺牲芯轴。本文报道了聚合物热交换器和镍热交换器的实验结果,以确定平面内液体(水)和平面内气体(空气)之间的传热速率。还测量了两种流体流的压降。实验结果与先前描述的分析模型的修正版本相吻合。制造的热交换器的传热/体积值比传统规模的热交换器高五倍以上(特征尺寸至少比这里报道的大一个数量级),传热/质量值比传统规模的热交换器大50%。
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引用次数: 74
期刊
IEEE\/ASME Journal of Microelectromechanical Systems
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