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Compressive Strength and Elastic Modulus of a 3D Woven Glass/Polyester Fire-Retardant Sandwich Composite 三维编织玻璃/聚酯防火夹层复合材料的压缩强度和弹性模量
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.1.2024.03.0849
R. Hidayanto, D. I. Taufiq, H. Judawisastra, R. Wirawan
A 3D woven sandwich composite structure has been widely used in various fields due to its advantages in terms of its strength-to-weight ratio. The adoption of lightweight materials in the railway industry for train carriages is aligned with United Nations Sustainable Development Goal 11, as this fosters the development of sustainable transportation by reducing carriage weight, enhancing fuel efficiency, minimizing component wear, and mitigating air pollution. This study explores the effect of the addition of aluminum trioxide (ATH) filler on the core structure, density, compressive strength, elastic modulus, and the number of added layers of 3D woven core fabric with 2D woven face sheets. Sandwich composites were produced with varying ATH loads of 30%, 40%, and 50%. We also varied the number of 3D woven core fabric layers in the composite sandwich (one, two, three, and four layers) and the 2D preform (one on the upper side, two on the upper side, and one on the upper + two on the lower sides) used as a face sheet thickener. The results showed that the addition of ATH filler increased the composite density. The addition of up to 40% ATH improved the strength and elastic modulus of the composite, while excessive loading led to a decrease in both properties. Variation of the 3D and 2D preform layers also improved the compressive strength and elastic modulus. We conclude that 3D woven sandwich composites incorporating 40% ATH, multilayered 3D woven core fabric, and 2D woven fabric face sheet thickener represent promising materials for use in the railway industry.
三维编织三明治复合材料结构因其强度重量比方面的优势,已被广泛应用于各个领域。在铁路行业的列车车厢中采用轻质材料符合联合国可持续发展目标 11,因为这可以减轻车厢重量、提高燃油效率、减少部件磨损和减轻空气污染,从而促进可持续交通的发展。本研究探讨了添加三氧化二铝(ATH)填料对带有二维编织面片的三维编织芯材结构、密度、抗压强度、弹性模量以及添加层数的影响。三明治复合材料的 ATH 负荷分别为 30%、40% 和 50%。我们还改变了复合材料夹层中三维编织芯材的层数(一层、两层、三层和四层),以及作为面片增厚剂的二维预成型(上侧一层、上侧两层、上侧一层+下侧两层)。结果表明,添加 ATH 填料可提高复合材料的密度。添加多达 40% 的 ATH 可提高复合材料的强度和弹性模量,而过量添加则会导致这两项性能下降。三维和二维预成型层的变化也提高了抗压强度和弹性模量。我们的结论是,含有 40% ATH、多层三维编织芯材和二维编织面材增稠剂的三维编织夹层复合材料是铁路工业中很有前途的材料。
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引用次数: 0
A Comparative Study and Improved Bearing Fault Classifier Using Raw Vibration Data Under Limited Training Samples 在有限的训练样本下使用原始振动数据进行比较研究和改进轴承故障分类器
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.1.2024.11.0857
J.S. Yap, M. Lim, M. S. Leong
Artificial intelligence is gaining traction in bearing fault detection and diagnosis. Generally, signal processing and feature selection are carried out to facilitate the fault classification process; however, classification accuracy tends to degrade under limited training data. In this paper, various artificial intelligence (AI) classification models are studied and compared using raw vibration data without signal processing and feature engineering. A Cosine k-Nearest Neighbours (CosKNN)-based classification model is optimized by integrating a Segmentive Mechanism, resulting in an overall classification F1-score improvement to 90.8% compared to the original classifier's 76.9%. The comparative findings show that the proposed model is suitable for circumstances with limited availability of training data, signal processing tools, and feature engineering tuning.
人工智能在轴承故障检测和诊断中的应用越来越广泛。一般来说,进行信号处理和特征选择是为了促进故障分类过程;然而,在有限的训练数据下,分类精度往往会降低。本文使用原始振动数据,在不进行信号处理和特征工程的情况下,对各种人工智能(AI)分类模型进行了研究和比较。通过整合分段机制,优化了基于余弦 k 最近邻域(CosKNN)的分类模型,与原始分类器的 76.9% 相比,整体分类 F1 分数提高到 90.8%。比较结果表明,建议的模型适用于训练数据、信号处理工具和特征工程调整有限的情况。
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引用次数: 0
Dynamic Contact Characteristics Analysis of Heavy-duty Track Rollers 重型滚轮的动态接触特性分析
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.1.2024.16.0862
Bijuan Yan, Zhiheng Zhang, HaiJing Zhang, WenJun Zhang, Zhangda Zhao, Tao Yang
As an important component of the crawler walking device, the track roller needs to withstand strong impact and is prone to failure, which can lead to serious economic losses. This paper focuses on the track roller of the spreader as the research subject and investigates the dynamic contact characteristics between the track roller and the track plate. Using RecurDyn software, a virtual prototype model of the crawler walking device is established to analyze the variation in a vertical dynamic load of the track roller under different working conditions. Simultaneously, a finite element model of the contact between the track roller and the track plate is developed using Ansys Workbench, and its accuracy is verified using Hertz contact theory. Finally, the study discusses various influencing factors on the contact characteristics, including load, curvature of the contacting bodies, and material yield strength. The results indicate that the track rollers experience the highest dynamic load when climbing a slope, reaching a maximum load of 1191.44 kN. Moreover, the maximum contact stress is 1750.4 MPa, and the maximum Mises stress is 921.34 MPa during this operation.  Importantly, when the load reaches 1218 kN, the maximum Mises stress of the track roller is 930.2 MPa, which may lead to roller failure after prolonged use. These findings provide valuable insights for the design and optimization of heavy-duty track rollers and offer significant assistance for various tracked vehicles.
滚轮作为履带行走装置的重要部件,需要承受强大的冲击力,容易发生故障,造成严重的经济损失。本文以吊具的履带滚轮为研究对象,研究履带滚轮与履带板的动态接触特性。利用 RecurDyn 软件,建立了履带行走装置的虚拟原型模型,分析了不同工况下滚轮垂直动载荷的变化。同时,使用 Ansys Workbench 建立了滚轮和履带板之间接触的有限元模型,并使用赫兹接触理论验证了其准确性。最后,研究讨论了影响接触特性的各种因素,包括载荷、接触体曲率和材料屈服强度。结果表明,履带滚子在爬坡时承受的动载荷最大,达到 1191.44 kN。此外,在此操作过程中,最大接触应力为 1750.4 兆帕,最大米塞斯应力为 921.34 兆帕。 重要的是,当载荷达到 1218 kN 时,滚轮的最大米氏应力为 930.2 MPa,这可能导致滚轮在长时间使用后失效。这些发现为重型滚轮的设计和优化提供了有价值的见解,并为各种履带车辆提供了重要帮助。
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引用次数: 0
Initial Study on Rheological Behaviour of Hydroxyapatites / Polylactic Acid Composite for 3D Printing Filament 用于 3D 打印丝的羟基磷灰石/聚乳酸复合材料流变行为初步研究
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.1.2024.10.0856
Afeeqa Puteri Marzuki, Mohd Alfiqrie Mohd Nasir, Farrahshaida Mohd Salleh, Muhammad Hussain Ismail, B. Murat, Marzuki Ibrahim
The present fused deposition modeling (FDM) printing process has concentrated on combining metal or ceramic filled with polymer because it could provide a strong composite in layered manufacturing technology in comparison to a single polymer material. However, the ability of the composite material to flow into the extruder becomes an obstacle because of the changes in the polymer concentration and dispersion of filler particles in producing the printed part. Hence, the rheological behavior of Hydroxyapatites (HAp) / Polylactic Acid (PLA) composite with different contents of HAp was studied to assess its ability to flow through the extruder during the 3D printing process. Measurements such as pycnometer density, thermal analysis (DSC) and FT-IR were performed on the composite feedstock containing a variation of 10% to 30% HAp powder. The feedstocks behavior then were characterized by rheological tests at three different temperatures (140 oC, 150 oC, and 160 oC). The composition of PLA/20HAp has produced optimum rheological behavior with effective flow behavior index (n) and activation energy (E) of 0.396 and 89.03 kJ/mol, respectively which is suitable for extruding out the HAp/PLA composite to become a 3D printing filament material.
目前的熔融沉积建模(FDM)打印工艺主要是将金属或陶瓷填充到聚合物中,因为与单一聚合物材料相比,这种材料可以在分层制造技术中提供一种坚固的复合材料。然而,在生产打印部件时,由于聚合物浓度和填料颗粒分散性的变化,复合材料在挤出机中的流动能力成为一个障碍。因此,我们研究了不同HAp含量的羟基磷灰石(HAp)/聚乳酸(PLA)复合材料的流变行为,以评估其在三维打印过程中流经挤出机的能力。对含有 10%-30%HAp粉末的复合原料进行了密度计密度、热分析(DSC)和傅立叶变换红外光谱等测量。然后在三种不同温度(140 摄氏度、150 摄氏度和 160 摄氏度)下进行流变测试,对原料的行为进行表征。聚乳酸/20HAp 成分产生了最佳流变行为,其有效流动行为指数(n)和活化能(E)分别为 0.396 和 89.03 kJ/mol,适合将 HAp/PLA 复合材料挤出成为 3D 打印丝材料。
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引用次数: 0
Evaluation and Performance Improvement of Environmentally Friendly Sustainable Turning of 6063 Aluminum Alloy in Dry Conditions Using Grey Relational Analysis 利用灰色关系分析法评估和改进在干燥条件下对 6063 铝合金进行环保型可持续车削的性能
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.1.2024.12.0858
A. Kannan, N.M.Sivaram
Sustainable machining has gained importance in recent years due to its environmental, economic, and societal implications. Aluminium (Al) 6063 alloy involves turning operation to make it suitable for various applications. The work's novelty is assessing the machining characteristics along with sustainability indicators. This study aims to find the best-turning parameters for machining Al 6063 alloy. The turning parameters considered were cutting speed, feed rate, and depth of cut. A cutting speed of 200 m/min, feed rate of 0.05 mm/rev, and depth of cut of 0.25 mm were the best parameter combinations for achieving a good machining response. From the response value of mean grey relational grade (GRG) and analysis of variance (ANOVA), the depth of cut ranks one with 34.38%, which is the most dominating parameter in achieving the sustainable machining of Al 6063 alloy. Through grey relational analysis, optimized machining parameters resulted in a 72.84 percent reduction in carbon emissions, 72.82 percent reduction in energy consumption, 18.58 percent reduction in cutting power, and 6.83 percent reduction in surface roughness considering the initial parameter settings and best machining parameters. The enhancement in total GRG was 0.1702, indicating improvement in the desired responses. As a result of this study, it is clear that appropriate machining parameter selection aids sustainable machining of Al 6063 alloy.
近年来,可持续加工因其对环境、经济和社会的影响而变得越来越重要。铝 (Al) 6063 合金涉及车削操作,使其适用于各种应用。这项工作的新颖之处在于在评估加工特性的同时评估可持续发展指标。本研究旨在找到加工铝 6063 合金的最佳车削参数。考虑的车削参数包括切削速度、进给量和切削深度。切削速度为 200 m/min、进给量为 0.05 mm/rev、切削深度为 0.25 mm 是实现良好加工响应的最佳参数组合。从平均灰色关系等级(GRG)和方差分析(ANOVA)的响应值来看,切削深度以 34.38% 的比例位居第一,是实现 Al 6063 合金可持续加工的最主要参数。通过灰色关系分析,考虑到初始参数设置和最佳加工参数,优化后的加工参数使碳排放量减少了 72.84%,能耗减少了 72.82%,切削功率减少了 18.58%,表面粗糙度减少了 6.83%。总 GRG 增强值为 0.1702,表明预期响应有所改善。研究结果表明,选择适当的加工参数有助于铝 6063 合金的可持续加工。
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引用次数: 0
Sustenance Strategies for Lean Manufacturing Implementation in Malaysian Manufacturing Industries 马来西亚制造业实施精益生产的维持策略
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.1.2024.06.0852
Norhana Mohd Aripin, G. Nawanir, Suhaidah Hussain, F. Mahmud, Khai Loon Lee
This study aims to investigate the relationship between sustaining factors and lean manufacturing implementation. This survey-based study was a cross-sectional study and the samples were drawn by using cluster sampling procedure from medium and large manufacturing companies based on the Federation of Manufacturers Malaysia (FMM) with the final number of 151 respondents. In total, four hypotheses were developed and tested statically using PLS-SEM through SmartPLS software. The result provided evidence that lean culture, lean leadership, and lean knowledge management have a positive relationship on lean manufacturing implementation. However, lean supplier management does not have a positive relationship on lean manufacturing implementation. The survey was responded by middle and top-level management from the discrete manufacturing industries. Although there is growing interest in empirical shreds of evidence in favor of sustaining lean, this study provides a comprehensive view of sustaining factors for lean manufacturing implementation. Hence, this study contributes to expanding the boundary of the existing literature and contributes to the body of knowledge while providing insights to practitioners in tailoring strategies to sustain lean manufacturing implementation and leverage their performance.
本研究旨在探讨持续因素与精益生产实施之间的关系。这项基于调查的研究是一项横断面研究,样本通过聚类抽样程序从马来西亚制造商联合会(FMM)的大中型制造企业中抽取,最终受访者人数为 151 人。研究共提出了四个假设,并通过 SmartPLS 软件使用 PLS-SEM 进行了统计检验。结果证明,精益文化、精益领导力和精益知识管理对精益生产的实施有积极影响。但是,精益供应商管理与精益生产的实施没有正相关关系。调查对象为离散制造业的中高层管理人员。尽管人们对有利于精益持续发展的经验证据越来越感兴趣,但本研究对精益生产实施的持续因素提供了一个全面的视角。因此,本研究有助于扩大现有文献的范围,为知识体系做出贡献,同时也为从业人员定制精益生产持续实施战略和提高绩效提供了见解。
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引用次数: 0
Effects of Pre-Injection and Antioxidants in a Diesel Engine Fuelled with Methyl Esters of Waste Cooking Oil Biodiesel 预喷射和抗氧化剂对使用废弃烹调油生物柴油的柴油发动机的影响
IF 1 Q2 Engineering Pub Date : 2024-03-20 DOI: 10.15282/ijame.21.4.2024.14.0860
R. Anbalagan, S. Sendilvelan, K. Bhaskar
Diesel engines are significant contributors to air pollution, particularly through emissions of nitrogen oxides (NOx), smoke, and carbon monoxide (CO). Finding sustainable fuel alternatives and additives to reduce emissions without compromising engine performance is imperative for environmental and public health concerns. This study investigates the impact of adding tert-butylhydroquinone (TBHQ) antioxidants to blends containing 20% Methyl Esters of Waste Cooking Oil (20MEOWCO) and 80% diesel fuel in Modified Common Rail Diesel (MCRD) engines. The experiment involves adjusting the pilot fuel injection timing to 36°CA bTDC (before Top Dead Centre) and the main injection timing to 15°CA bTDC, with a Nozzle Opening Pressure (NOP) of 500 bar. Biodiesel is produced from used cooking oil using standard procedures and then mixed with diesel fuel. Various concentrations of TBHQ are added to the 20MEOWCO fuel blend for the experiment. The findings indicate that introducing TBHQ in concentrations of 250 ppm and 500 ppm to the 20MEOWCO fuel blend results in a notable reduction of Oxides of Nitrogen (NOx) emission by 13% in MCRD engines. However, this reduction in emissions comes at the expense of increased specific fuel consumption, which is observed to rise by 2.1%. Furthermore, the study highlights a rise in smoke and carbon monoxide (CO) emissions by approximately 7–10% and 5-8%, respectively, under the experimental conditions. The results of this study suggest that the addition of TBHQ to 20MEOWCO blends holds promise for mitigating NOx emissions in MCRD engines.
柴油发动机是造成空气污染的重要因素,尤其是氮氧化物(NOx)、烟雾和一氧化碳(CO)的排放。寻找可持续的燃料替代品和添加剂,在不影响发动机性能的前提下减少排放,是环境和公共健康问题的当务之急。本研究调查了在改良型高压共轨柴油机 (MCRD) 发动机中,向含 20% 废食用油甲酯 (20MEOWCO) 和 80% 柴油的混合燃料中添加叔丁基对苯二酚 (TBHQ) 抗氧化剂的影响。实验包括将先导燃油喷射时间调整为 36°CA bTDC(顶死中心之前),将主喷射时间调整为 15°CA bTDC,喷嘴开启压力(NOP)为 500 巴。使用标准程序从废食用油中提取生物柴油,然后与柴油混合。实验中,在 20MEOWCO 混合燃料中添加了不同浓度的 TBHQ。实验结果表明,在 20MEOWCO 混合燃料中分别加入 250ppm 和 500ppm 浓度的 TBHQ 后,MCRD 发动机的氮氧化物(NOx)排放量显著减少了 13%。然而,排放量的减少是以特定燃料消耗量的增加为代价的,据观察,燃料消耗量增加了 2.1%。此外,研究还强调,在实验条件下,烟雾和一氧化碳(CO)排放量分别增加了约 7-10% 和 5-8%。研究结果表明,在 20MEOWCO 混合物中添加 TBHQ 有望减少 MCRD 发动机的氮氧化物排放。
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引用次数: 0
Evaluation of Automotive Bio-Composites Crash Box Performance 汽车生物复合材料碰撞箱性能评估
IF 1 Q2 Engineering Pub Date : 2024-01-02 DOI: 10.15282/ijame.20.4.2023.11.0846
Xin Yi Ang, C.S. Hassan, S.Y. Soh, E.U. Olugu, N.F. Abdullah, L.J. Yu, N. Abdul Aziz
In the automotive industry, sustainable materials, such as bio-composites, are progressively being adopted due to their lightweight feature, which reduces vehicle weight, fuel consumption and pollutants emissions. Bio-composites are renewable and biodegradable, making them more environmental-friendly. However, limited investigations into the use of bio-composites in crash box applications have indicated that they lack the impact strength to fully absorb collision energy. This study aims to compare the crashworthiness performance of crash boxes made from OPEFB fiber/epoxy and kenaf fiber/epoxy composites, with conventional steel and carbon fiber/epoxy using LS-DYNA quasi-static simulations. Six different crash box designs are proposed: square, hexagonal, decagonal, hexagonal 3-cell, hexagonal 6-cell, and decagonal 10-cell structure, to evaluate the effect of these designs on crash box performance. The results show that bio-composite crash boxes are inferior to traditional materials in terms of energy absorption and specific energy absorption, but they yield better performance in crush force efficiency. In terms of design, decagonal 10-cell structure produces the highest specific energy absorption and energy absorption for bio-composites. Hence, optimization is performed on the OPEFB fibre/epoxy decagonal 10-cell crash box, aiming to increase energy absorption capability by varying the thickness, perimeter, and length of the crash box. The design is optimized by increasing thickness and maintaining length and perimeter. Compared to the original design, the optimized design improves energy absorption by 59% and specific energy absorption by 19%. The optimized design is then subjected to both quasi-static and impact loading tests, revealing that the optimized OPEFB fibre/epoxy crash box design exhibits 44% lower energy absorption than steel under quasi-static load, but it demonstrates a 56% increase in crush force efficiency and a 6 % increase in specific energy absorption. Under impact load, it shows a 91% increase in specific energy absorption compared to the traditional square steel crash box.
在汽车行业,生物复合材料等可持续材料因其轻量化的特点,可减轻汽车重量、降低油耗和污染物排放,正逐步被采用。生物复合材料可再生、可生物降解,因此更加环保。然而,对生物复合材料在碰撞箱中应用的有限调查表明,它们缺乏完全吸收碰撞能量的冲击强度。本研究旨在利用 LS-DYNA 准静态模拟,比较 OPEFB 纤维/环氧树脂和 kenaf 纤维/环氧树脂复合材料制成的防撞箱与传统钢材和碳纤维/环氧树脂的防撞性能。提出了六种不同的碰撞箱设计:正方形、六边形、十边形、六边形 3 单元、六边形 6 单元和十边形 10 单元结构,以评估这些设计对碰撞箱性能的影响。结果表明,生物复合材料防撞箱在能量吸收和比能量吸收方面不如传统材料,但在挤压力效率方面却有更好的表现。在设计方面,十边形 10 单元结构能产生最高的生物复合材料比能量吸收和能量吸收。因此,对 OPEFB 纤维/环氧树脂十边形 10 单元碰撞箱进行了优化,旨在通过改变碰撞箱的厚度、周长和长度来提高能量吸收能力。通过增加厚度、保持长度和周长对设计进行了优化。与原始设计相比,优化设计的能量吸收能力提高了 59%,比能量吸收能力提高了 19%。然后,对优化设计进行了准静态和冲击载荷测试,结果表明,在准静态载荷下,优化的 OPEFB 纤维/环氧树脂防撞箱设计的能量吸收率比钢材低 44%,但挤压力效率提高了 56%,比能量吸收率提高了 6%。在冲击载荷下,与传统的方形钢制防撞箱相比,它的比能量吸收率提高了 91%。
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引用次数: 0
Motion Sickness Susceptibility Among Malaysians When Travelling in a Moving Vehicle 马来西亚人在行驶中的车辆中晕车的易感性
Q2 Engineering Pub Date : 2023-10-25 DOI: 10.15282/ijame.20.3.2023.18.0832
None D. Mohamad Ruse, Nidzamuddin Md. Yusof, None N. Sanusi, None J. Karjanto, None M.Z. Hassan, None S. Sulaiman, None Z. Mohd Jawi, None K.A. Abu Kassim
Motion sickness is a common problem when travelling in a moving vehicle, especially on land transportation. This occurrence would signify when users are exposed to unexpected movement in an obstructed view. Each user can experience a different level of motion sickness, depending on their susceptibility. This paper aims to study the motion sickness susceptibility among Malaysians using Motion Sickness Susceptibility Questionnaires (MSSQ-Short). A total of 252 Malaysians (146 males and 106 females) completed a set of questionnaires. The questionnaire was distributed through electronic means such as Facebook, WhatsApp, Twitter, and email and consisted of demographic, MSSQ-Short, travel experience as a driver and passenger, and seating position. This study provides a correlation between experiencing motion sickness between childhood and adulthood (r = 0.124, p < 0.05) for the Malaysian sample. This study concludes that Malaysian susceptibility is higher compared to other countries.
晕车是一种常见的问题,尤其是在移动的车辆上,尤其是在陆地上。这种情况意味着当用户在受阻的视图中遇到意外移动时。每个用户都可以根据他们的易感性体验到不同程度的晕动病。本文旨在利用运动病易感性问卷(MSSQ-Short)研究马来西亚人的运动病易感性。共有252名马来西亚人(146名男性和106名女性)完成了一套调查问卷。问卷通过Facebook、WhatsApp、Twitter和电子邮件等电子手段分发,包括人口统计、MSSQ-Short、作为司机和乘客的旅行体验以及座位位置。这项研究提供了儿童期和成年期晕车的相关性(r = 0.124, p <0.05)。这项研究的结论是,与其他国家相比,马来西亚的易感性更高。
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引用次数: 0
Effect of Bilayer Nano-Micro Hydroxyapatite on the Surface Characteristics of Implanted Ti-6Al-4V ELI 双层纳米微羟基磷灰石对植入Ti-6Al-4V ELI表面特性的影响
Q2 Engineering Pub Date : 2023-10-24 DOI: 10.15282/ijame.20.3.2023.19.0833
None Ilhamdi, None Gunawarman, None J. Affi, None O. Susanti, None D. Juliadmi, None D. Oktaviana, None M. Tauhid
Ti-6Al-4V ELI is a well-known, popular medical-grade titanium alloy due to its biocompatibility and excellent mechanical properties. However, like other metal implants, it is less bioactive that affects tissue regeneration around the implant, and may lead to implant failure. So, a bioactive substance such as hydroxyapatite (HA) has usually been coated on metal implants to improve its bioactive properties. However, a single layer of HA was reported to be dissolved into body fluid after a long time of exposure in the human body. In this study, bilayer HA was deposited on the surface of screw-type implants made of Ti-6Al-4V ELI through electrophoretic deposition (EPD method. The bottom layer consists of micro-size of HA, and the second layer contains nano-size HA. The suspension contains each micro and nano size of HA powder was homogenized for 1 h followed by sonication for 2 h using a magnetic stirrer. The coating layer was subsequently sintered at 700oC for 1 h. The bilayer-coated screw implant was then implanted into the proximal tibia of health rattus novergicus under proper surgical procedures. Some screws without HA deposition were also implanted into rattus novergicus for comparison. The implanted screws were then taken out via surgery after 2, 3 and 4 weeks, and they were subsequently observed by optical microscope, SEM and XRF. The results showed that organic material is found on each coated specimen, and few HA layer is disintegrated from the surface of the screw. The disintegrated HA remained in the surface of the screw, and the amount of HA increased with increasing implantation time, which indicates the increase of osseointegration between the bone and HA layer. XRF showed a significant difference in Ti and titanium oxide contents on the surface of the coated samples and the non-coted ones, where it is only 0.66%Ti (0.39% TiO2) on the surface of the screw with HA layer and 70%Ti (67% TiO2) for without HA. When TiO2 is formed as a fast self-healing reaction while the screw is exposed to body fluid, the HA acts as an interface against body fluid that may contain aggressive ions. So, HA layer is not only effective against corrosion attack but also inhibits the formation of TiO2 on the implant surface. The coated screws also revealed a strong bonding between the HA layer and the surface of the implant screw. Besides, the ratio between Ca and P elements on the screw surface is in the range of 0.58 – 2.04, which is in the range of bone characteristics.
Ti-6Al-4V ELI是一种众所周知的、流行的医用级钛合金,因为它具有生物相容性和优异的机械性能。然而,像其他金属种植体一样,它的生物活性较低,影响种植体周围的组织再生,并可能导致种植体失败。因此,生物活性物质如羟基磷灰石(HA)通常被涂覆在金属植入物上以提高其生物活性。然而,据报道,单层透明质酸在人体内长期暴露后会溶解到体液中。本研究采用电泳沉积(EPD)方法,将双层HA沉积在Ti-6Al-4V ELI螺旋型植入体表面。底层是微尺寸的HA,第二层是纳米尺寸的HA。将含有各种微纳米级HA粉末的悬浮液均质1 h,然后用磁力搅拌器超声2 h。涂层层在700℃下烧结1 h,按照适当的手术步骤将双层涂层螺钉植入健康大鼠胫骨近端。一些没有HA沉积的螺钉也被植入黑家鼠体内进行比较。2、3、4周后手术取出植入螺钉,进行光学显微镜、扫描电镜、x射线荧光观察。结果表明:各涂层试样表面均有有机物质存在,螺杆表面有少量HA层崩解;崩解的HA残留在螺钉表面,且随着植入时间的增加,HA的数量增加,说明骨与HA层的骨结合增强。XRF分析表明,涂覆后的螺杆表面Ti和氧化钛含量与未涂覆的螺杆表面Ti和氧化钛含量有显著差异,有HA层的螺杆表面Ti含量仅为0.66% (TiO2含量0.39%),未涂覆的螺杆表面Ti含量为70% (TiO2含量67%)。当螺丝钉暴露在体液中时,TiO2作为一种快速的自愈反应形成,透明质酸作为一个界面来对抗可能含有侵略性离子的体液。因此,HA层不仅可以有效地抵抗腐蚀,还可以抑制种植体表面TiO2的形成。涂覆的螺钉也显示了HA层与种植螺钉表面之间的牢固结合。此外,螺钉表面Ca和P元素的比值在0.58 ~ 2.04之间,在骨特性范围内。
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引用次数: 1
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International Journal of Automotive and Mechanical Engineering
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