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Instantaneous formation of covalently bonded diamond–graphite–graphene with synergistic properties 瞬间形成具有协同性能的共价键金刚石-石墨-石墨烯
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-12-01 DOI: 10.1016/j.ijmachtools.2023.104087
Bo Yan , Ni Chen , Yan Zhu , Yinfei Yang , Guolong Zhao , Wei Zhao , Xiuqing Hao , Liang Li , Lei Wang , Eberhard Abele , Ning He

Diamond and graphene are the most widely used carbon allotropes and offer great potential for developing mechanical, electronic, energy-storage, and sensor applications. Their combination, especially interfacial covalent bonding, can impart excellent properties. However, achieving interfacial covalent bonding with superior performance using flexible and low-power strategies remains challenging. This study developed a novel instantaneous transformation method from diamond to graphene to prepare a new covalent structure of diamond–nano-graphite–graphene (CDGG). That is, a nanosecond-pulse laser induces sp3-to-sp2 instantaneous transformations from diamond to graphite in air, and the subsequent mechanical cleavage overcomes the weak van der Waals forces to achieve the final transformation of graphite to graphene. First, the key factors influencing laser-induced graphitization and mechanical cleavage were investigated, and a covalent carbon structure with multidirectional graphene was obtained. Furthermore, the mechanisms encompassing the lattice transformation, interface relationships, transformation time, and interface bonding were elucidated. The obtained new structure synergized the excellent properties of diamond, nano-graphite, and graphene, exhibiting superior lubrication, mechanochemical wear resistance, durability, and load-capacity. Compared to polished diamond, the obtained structure exhibited a significant decrease in the stable coefficient of friction by 49–59 % and a reduction of more than one order of magnitude in the relative wear rate under high friction against ferrous metals with a normal load of 1–9 N. Even under a heavy load of 100 N, it still exhibited superior lubrication and mechanochemical wear resistance. Finally, the preparation and patterning of covalent carbon structures were achieved on various diamond surfaces with high efficiency, environmental friendliness, and low power. This study is expected to broaden the scope of developing and applying diamond, diamond films, and graphene devices.

金刚石和石墨烯是应用最广泛的碳同素异形体,在机械、电子、储能和传感器应用方面具有巨大的潜力。它们的结合,特别是界面共价键,可以赋予优异的性能。然而,使用灵活和低功耗的策略实现具有优异性能的界面共价键仍然具有挑战性。本研究提出了一种新的从金刚石到石墨烯的瞬时转化方法,制备了一种新的共价结构金刚石-纳米石墨-石墨烯(CDGG)。即纳秒脉冲激光诱导金刚石在空气中sp3到sp2的瞬时转变为石墨,随后的机械解理克服了微弱的范德华力,最终实现了石墨向石墨烯的转变。首先,研究了影响激光诱导石墨化和机械解理的关键因素,获得了具有多向石墨烯的共价碳结构。在此基础上,对晶格转换、界面关系、转换时间和界面键合等机理进行了探讨。所获得的新结构协同了金刚石、纳米石墨和石墨烯的优异性能,具有优异的润滑性能、机械化学耐磨性、耐久性和承载能力。与抛光后的金刚石相比,在1-9 N的正常载荷下,与黑色金属的高摩擦下,所得结构的稳定摩擦系数显著降低了49% - 59%,相对磨损率降低了一个数量级以上。即使在100 N的重载荷下,它仍然表现出优异的润滑和机械化学耐磨性。最后,在各种金刚石表面实现了高效、环保、低功耗的共价碳结构的制备和图像化。这项研究有望拓宽金刚石、金刚石薄膜、石墨烯器件的开发和应用范围。
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引用次数: 0
Efficient post-processing of additive manufactured maraging steel enhanced by the mechanochemical effect 机械化学效应提高了添加剂制造马氏体时效钢的后处理效率
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-12-01 DOI: 10.1016/j.ijmachtools.2023.104086
Yuchao Bai , Yan Jin Lee , Yunfa Guo , Qi Yan , Cuiling Zhao , A. Senthil Kumar , Jun Min Xue , Hao Wang

Additive manufacturing technologies are beginning to shift toward hybridization with subtractive processes and it is vital to identify techniques that can enhance the machinability of the difficult-to-cut additively manufactured metals and offer easy integration. The mechanochemical effect, which can be induced by surfactant, is a feasible solution for hybrid integration due to the beneficial enhancements to the cutting performance, online integrability, and negligible impact on the AM process as compared to cutting fluids, cryogenic cutting, etc. To realize the successful integration of the mechanochemical effect and hybrid additive/subtractive manufacturing, micro-cutting of AMed high-strength maraging steel was performed to study the relationship between microstructural features, mechanical properties, cutting performance and effectiveness of the mechanochemical effect. The results show that the mechanochemical effect was successfully induced in the as-built and solution-treated steels by inhibiting dislocation movement to induce the embrittlement of chip surface and strain localization within the chip, thereby leading to substantial reductions in cutting forces of up to 35.24 % and 53.09 %, respectively, with significant improvement in the machined surface quality. However, the presence of 7.7 nm nanoparticles in the age-treated steels renders the mechanochemical effect ineffective in improving machinability. The nanoparticles sharply increased the strength, hardness, and brittleness of the AMed maraging steel where the brittleness replaced the role of surfactant that suppressed plasticity in the chip free surface. The notion was affirmed by the similarities between the cutting chips of the brittle aged steel without surfactant and the as-built steel with surfactant. This study systematically revealed the underlying mechanism of inducing the mechanochemical effect during the micro-cutting of AMed high-strength materials with different microstructures and mechanical properties. More importantly, it is evident that the mechanochemical effect is a highly feasible solution for enhanced hybrid manufacturing, especially for robot-based fabrication works that involve high degrees of freedom and large working ranges but are limited by low mechanical stiffness.

增材制造技术正开始向减法工艺的杂交转变,确定能够提高难以切割的增材制造金属的可加工性并提供易于集成的技术至关重要。表面活性剂可以诱导的机械化学效应是混合集成的可行解决方案,因为与切削液、低温切削等相比,它可以有益地提高切削性能、在线可积性,并且对AM工艺的影响可以忽略不计。为了实现机械化学效应与混合加减法制造的成功结合,对AMed高强度马氏体时效钢进行了显微切削,研究了显微组织特征、力学性能、切削性能与机械化学效应有效性之间的关系。结果表明,通过抑制位错运动来诱导芯片表面的脆化和芯片内的应变局部化,机械化学效应在制造钢和固溶处理钢中成功地诱导了,从而使切削力分别大幅降低35.24%和53.09%,机械加工表面质量显著提高。然而,在时效处理的钢中存在7.7nm纳米颗粒使得机械化学效应在提高可加工性方面无效。纳米颗粒显著提高了AM马氏体时效钢的强度、硬度和脆性,其中脆性取代了表面活性剂抑制无芯片表面塑性的作用。不含表面活性剂的脆性时效钢和含表面活性素的竣工钢的切削屑之间的相似性证实了这一概念。本研究系统地揭示了在具有不同微观结构和力学性能的AMed高强度材料的微切削过程中诱导机械化学效应的潜在机制。更重要的是,很明显,机械化学效应是增强混合制造的一种非常可行的解决方案,特别是对于涉及高自由度和大工作范围但受低机械刚度限制的基于机器人的制造工作。
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引用次数: 0
Towards understanding the crack suppression mechanism in brittle materials with high grinding speed at different temperatures 探讨不同温度下高磨削速度脆性材料的裂纹抑制机理
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-12-01 DOI: 10.1016/j.ijmachtools.2023.104088
Jianqiu Zhang , Xuekun Shang , BinBin He , Bi Zhang

Ductile-regime grinding has been used to eliminate the formation of subsurface cracks by setting an extremely small depth of cut (DOC). The critical DOC is affected by multiple factors, including the grinding speed and material temperature. The underlying mechanism of DOC affected by the grinding speed is still unclear. To reveal the role of grinding speed and material temperature during the formation of cracks, we conducted a series of single-point grinding experiments with the different grinding speeds (26.7–192.3 m/s) and the initial material temperatures (25–200 °C). The experimental results showed that cracks were suppressed with an increase in the grinding speed and initial material temperature even when the DOC was much deeper than the critical DOC determined by the ductile-regime grinding. To understand the mechanisms underlying crack nucleation and suppression, we conducted systematic molecular dynamics simulations. Both simulation and experimental results showed that a crack can be formed by a single slip band. The crack nucleates from a microvoid within the slip band. With the aid of the local tensile stress on one side of the slip band tip, the crack nucleation forms an opening crack. The crack suppression is primarily caused by the high‐pressure field during high‐speed grinding, where the high‐pressure field superposes the local tensile stress to forming a compressive stress state that prevents crack nucleation. In addition, the brittle‐ductile transition is induced by the high temperature on the surface during high‐speed grinding. This study provides insights into building the DOC criterion for different grinding speeds and temperatures based on a ‘bottom-up’ approach.

延性磨削通过设置极小的切削深度(DOC)来消除次表面裂纹的形成。临界DOC受磨削速度和材料温度等多种因素的影响。磨削速度对DOC影响的潜在机制尚不清楚。为了揭示磨削速度和材料温度在裂纹形成过程中的作用,我们在不同的磨削速度(26.7 ~ 192.3 m/s)和材料初始温度(25 ~ 200℃)下进行了一系列单点磨削实验。实验结果表明,随着磨削速度的增加和材料初始温度的升高,裂纹得到抑制,即使裂纹深度远高于塑性磨削所确定的临界裂纹深度。为了了解裂纹成核和抑制的机制,我们进行了系统的分子动力学模拟。模拟和实验结果均表明,单条滑移带可以形成裂纹。裂纹由滑移带内的微孔洞成核。在滑移带尖端一侧的局部拉应力作用下,裂纹形核形成开口裂纹。裂纹抑制主要是由于高速磨削过程中的高压场引起的,高压场与局部拉应力叠加形成压应力状态,从而阻止裂纹成核。此外,高速磨削过程中表面的高温诱发了脆性-韧性转变。该研究提供了基于“自下而上”方法构建不同磨削速度和温度的DOC标准的见解。
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引用次数: 0
In-situ experimental and high-fidelity modeling tools to advance understanding of metal additive manufacturing 现场实验和高保真建模工具,促进对金属增材制造的理解
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-12-01 DOI: 10.1016/j.ijmachtools.2023.104077
Lu Wang , Qilin Guo , Lianyi Chen , Wentao Yan

Metal additive manufacturing has seen extensive research and rapidly growing applications for its high precision, efficiency, flexibility, etc. However, the appealing advantages are still far from being fully exploited, and the bottleneck problems essentially originate from the incomplete understanding of the complex physical mechanisms spanning from the manufacturing processes, microstructure evolutions, to mechanical properties. Specifically, for powder-fusion-based additive manufacturing such as laser powder bed fusion, the manufacturing process involves powder dynamics, heat transfer, phase transitions (melting, solidification, evaporation, and condensation), fluid flow (gas, vapor, and molten metal liquid), and their interactions. These interactions induce not only various defects but also complex thermal-mechanical-compositional conditions. These transient conditions lead to highly non-equilibrium microstructure evolutions, and the resultant microstructures, together with those defects, can significantly alter the mechanical properties of the as-built parts, including strength, ductility and residual stress. We believe that the most efficient approach to advance the fundamental understanding is integrating in-situ experimentation and high-fidelity modeling. In this review, we summarize the state of the art of these two powerful tools: in-situ synchrotron experimentation and high-fidelity modeling, and provide an outlook for potential research directions.

金属增材制造以其高精度、高效率、灵活性等优点得到了广泛的研究和快速增长的应用。然而,其吸引人的优势仍远未得到充分利用,瓶颈问题本质上源于对制造过程中复杂物理机制的不完全理解,微观结构演变到机械性能。具体而言,对于基于粉末融合的增材制造,如激光粉末床融合,制造过程涉及粉末动力学、传热、相变(熔化、固化、蒸发和冷凝)、流体流动(气体、蒸汽和熔融金属液体)及其相互作用。这些相互作用不仅引起各种缺陷,而且引起复杂的热机械组成条件。这些瞬态条件导致高度不平衡的微观结构演变,由此产生的微观结构以及这些缺陷可以显著改变竣工零件的机械性能,包括强度、延展性和残余应力。我们认为,推进基本理解的最有效方法是将现场实验和高保真建模相结合。在这篇综述中,我们总结了这两种强大工具的技术现状:原位同步加速器实验和高保真度建模,并对潜在的研究方向进行了展望。
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引用次数: 0
Achieving material diversity in wire arc additive manufacturing: Leaping from alloys to composites via wire innovation 实现线材电弧增材制造的材料多样性:通过线材创新实现从合金到复合材料的跨越
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-11-28 DOI: 10.1016/j.ijmachtools.2023.104103
Hao Yi , Le Jia , Jialuo Ding , Huijun Li

Multi-material components featuring high performance and design flexibility have attracted considerable attention, providing solutions to meet the performance demands of high-end equipment components. Achieving material diversity in additive manufacturing (AM) is a fundamental step towards manufacturing multi-material components. Wire arc additive manufacturing (WAAM), an important branch of AM technology, boasts notable advantages in the efficient and customized preparation of large-scale parts due to its high deposition efficiency and unrestricted forming size. However, achieving material diversity in WAAM, constrained by its reliance on wire-form raw materials, has emerged as a compelling challenge. Wire innovation, including multiple, stranded, and cored wires, have furnished solutions to this challenge. To this end, this review provides an overview of the current developments in WAAM via wire innovation and suggests future research directions, aiming to serve as a reference for the further advancement of WAAM. Initially, the article introduces several WAAM printing forms, their manufacturing features, printable materials and inherent manufacturing limitations, and the intermixing of metal constituents of WAAM, prior to highlighting the advantages and necessity of achieving material diversity. Subsequently, the exposition of multi-wire-arc AM demonstrates its utility in the preparation of binary or ternary alloys, inclusive of intermetallic compounds and functionally graded materials, responding adeptly to the deficiencies of conventional WAAM, which is limited to single-material printing. The merits and progression of stranded-wire-arc AM for high-entropy alloy production are synthesized and debated, especially given that creating components with multiple metal elements via multi-wire-arc AM customarily confronts the constraint of necessitating more intricate manufacturing equipment and processes. Further, the review explores the recently developed cored-wire-arc AM technology, which actualizes the manufacturing of composite materials, amalgamating metals and non-metals, to remedy the issues encountered with standard WAAM, incapable of realizing non-metallic material printing. Considering machine tools as an important means to achieve material diversity in WAAM, we expand on the current machine tool architecture and its corresponding design tools. Finally, the current research status on WAAM via wire innovation is summarized and potential future research directions are proposed.

高性能、设计灵活的多材料组件备受关注,为满足高端设备组件的性能需求提供了解决方案。在增材制造(AM)中实现材料多样性是制造多材料部件的基本步骤。电弧增材制造(WAAM)是增材制造技术的一个重要分支,由于其沉积效率高,成形尺寸不受限制,在大型零件的高效定制制备方面具有显著的优势。然而,由于WAAM对线状原材料的依赖,实现WAAM材料的多样性已经成为一项引人注目的挑战。电线创新,包括多线、绞线和芯线,为这一挑战提供了解决方案。为此,本文综述了目前WAAM在导线创新方面的研究进展,并提出了未来的研究方向,旨在为WAAM的进一步发展提供参考。本文首先介绍了几种WAAM打印形式及其制造特点,可打印材料和固有的制造限制,以及WAAM金属成分的混合,然后强调了实现材料多样性的优势和必要性。随后,多线弧增材制造展示了其在制备二元或三元合金(包括金属间化合物和功能梯度材料)方面的实用性,巧妙地弥补了传统WAAM仅限于单材料打印的不足。本文对高熵合金用电弧增材制造技术的优点和发展进行了综合和讨论,特别是考虑到利用电弧增材制造由多个金属元素组成的零件通常需要更复杂的制造设备和工艺的限制。此外,本文还探讨了最近开发的芯线电弧增材制造技术,该技术实现了金属和非金属混合复合材料的制造,以弥补标准WAAM无法实现非金属材料打印的问题。考虑到机床是WAAM中实现材料多样性的重要手段,对现有的机床体系结构及其相应的设计工具进行了扩展。最后,总结了通过导线创新实现WAAM的研究现状,并提出了未来可能的研究方向。
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引用次数: 0
Integrating reversion ageing and forming of high-strength Al alloys: Principles and theoretical basis 高强铝合金可逆时效与成形一体化:原理与理论基础
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-11-24 DOI: 10.1016/j.ijmachtools.2023.104091
Chunhui Liu , Jun He , Zhuangzhuang Feng , Peipei Ma , Lihua Zhan

Simultaneously improving the formability and post-formed strength of high-strength aluminum (Al) alloys, such as Al–Zn–Mg–Cu alloys, is essential in manufacturing complex-shaped panel components. The strict requirements on heat-treatment condition and high tooling costs limit the applications of current forming methods. A novel process called integrated reversion ageing and forming (IRAF) is proposed to form naturally aged (NA or T4 tempered) Al alloys. A principle-based concept analysis and systematic thermo-mechanical-metallurgical study of the IRAF process were performed. Additionally, tensile tests were conducted to evaluate the effects of parameters including heating rate, holding time, and forming temperature on formability and baked strength. The deformability of the AA7075-T4 alloy can be significantly enhanced through rapid heating to the reversion ageing temperature (150–300 °C), followed by short-term holding, as evidenced by the reduced yield strength of 200 MPa and increased uniform ductility. An instant strength increase to a value close to that of the T6 state was obtained after a short bake hardening (BH) treatment. Further, temperature-time-property (TTP) diagrams were established based on the correlation between the measured mechanical properties and through-process microstructure evolution to explain the mechanism underlying the optimised processing window of IRAF. The results indicate that fast-heating rate (>300 °C/min) promotes the reversion of NA clusters and inhibits re-precipitation of solutes, thereby improving the warm formability. Reversion ageing above 240 °C could induce the formation of coarse η'/η phases, leading to a considerably declined BH response. To accurately predict the strength evolution and deformation behavior during IRAF, a physical-based unified constitutive model was constructed by considering the reversion of NA clusters and solute re-precipitation. The bending and drawing tests on the AA7075-T4 alloy sheets verified that IRAF in the most-reverted state enabled optimum formability. The findings inspire promoting the reversion of pre-existing metastable particles to improve warm formability and post-formed age hardening.

同时提高高强度铝(Al)合金(如Al - zn - mg - cu合金)的成形性和成形后强度是制造复杂形状面板部件的必要条件。对热处理条件的严格要求和高昂的模具成本限制了现有成形方法的应用。提出了一种称为综合回火时效和成形(IRAF)的新工艺来形成自然时效(NA或T4回火)铝合金。对该工艺进行了基于原理的概念分析和系统的热-机械-冶金研究。此外,还进行了拉伸试验,以评估加热速率、保温时间和成形温度等参数对成形性和烘烤强度的影响。快速加热至150 ~ 300 ℃后,再进行短期保温,可显著提高合金的变形能力,屈服强度降低200 MPa,塑性均匀性提高。经过短时间的烘烤硬化(BH)处理后,强度瞬间提高到接近T6状态的值。此外,基于测量的力学性能与整个工艺组织演变之间的相关性,建立了温度-时间-性能(TTP)图,以解释优化的IRAF加工窗口的机制。结果表明,快速升温(>300 °C/min)促进了NA团簇的逆转,抑制了溶质的再沉淀,从而提高了热成形性能。在240 °C以上的回火时效可以诱导粗η′/η相的形成,导致BH响应明显下降。考虑NA簇的反演和溶质的再沉淀,建立了基于物理的统一本构模型,以准确地预测raf过程中的强度演变和变形行为。通过对AA7075-T4合金板材的弯曲和拉伸试验,验证了在最大还原状态下的IRAF具有最佳的成形性能。这一发现启发了促进已有亚稳颗粒的逆转,以改善热成形性和成型后的时效硬化。
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引用次数: 0
Tailoring of residual stress by ultrasonic vibration-assisted abrasive peening in liquid cavitation of metallic alloys 超声振动辅助磨料强化在金属合金液体空化过程中的残余应力裁剪
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-11-23 DOI: 10.1016/j.ijmachtools.2023.104100
Rahul Yadav, Nilanjan Das Chakladar, Soumitra Paul

The present study proposes a novel method of ultrasonic vibration assisted-abrasive peening for the enhancement of residual stress on the surface of metals and their alloys. The system employs a vibrating sonotrode that drives the formation and collapse of bubbles within a fluid medium. The imploding bubbles produce pressure waves which transfer momentum to the abrasives which are uniformly distributed in the fluid medium. The abrasives bombard a targeted surface along with intense pressure waves. This induces compressive residual stress through local plastic deformation in a short period. The capability of the ultrasonic-assisted abrasive peening setup is analysed in terms of residual stress by altering the abrasive concentration, peening time, and stand-of-distance between the bottom of the sonotrode and the exposed surface to be treated. The process is able to induce significant residual stress at around 67 % of yield strength for hard material Ti–6Al–4V and more than 80 % of yield strength for ductile materials, Al-6061 and OFHC-Cu. A numerical method coupled with a finite element model is employed to predict the dynamics of the process from cavitation of the bubble to the plastic deformation of the work material. At first, the model estimates the magnitudes of high-pressure waves at the bubble implosion near the solid surface, micro-jet velocity, and abrasive velocity. This information is then fed to Abaqus for numerical modelling of the deformation of work material. The impact of high-speed abrasives in the range of 100 m/s, pressure waves and microjets at the material surface are simulated through the FE model. The simulated results are verified with experimental findings in terms of surface residual stress for different materials, deviating within 10 %.

提出了一种超声振动辅助磨粒强化金属及其合金表面残余应力的新方法。该系统采用振动声电极驱动流体介质中气泡的形成和破裂。内爆气泡产生压力波,将动量传递给均匀分布在流体介质中的磨料。磨料伴随着强烈的压力波轰击目标表面。这在短时间内通过局部塑性变形引起压缩残余应力。通过改变磨料浓度、强化时间和超声电极底部与待处理暴露表面之间的距离,分析了超声辅助磨料强化装置的残余应力性能。对于硬材料Ti-6Al-4V,该工艺能够产生显著的残余应力,其屈服强度约为67 %,而对于韧性材料Al-6061和OFHC-Cu,其屈服强度超过80 %。采用数值方法与有限元模型相结合的方法对气泡空化到工作材料塑性变形的动力学过程进行了预测。首先,该模型估计了固体表面附近气泡内爆时高压波的震级、微射流速度和磨粒速度。然后将这些信息输入Abaqus进行工作材料变形的数值模拟。通过有限元模型模拟了100 m/s范围内高速磨料、压力波和微射流对材料表面的影响。在不同材料的表面残余应力方面,模拟结果与实验结果相吻合,偏差在10 %以内。
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引用次数: 0
Ni–Ti multicell interlacing Gyroid lattice structures with ultra-high hyperelastic response fabricated by laser powder bed fusion 激光粉末床熔合制备具有超高超弹性响应的Ni-Ti多细胞交错陀螺晶格结构
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-11-20 DOI: 10.1016/j.ijmachtools.2023.104099
Jiulu Jin , Siqi Wu , Lei Yang , Cong Zhang , Yang Li , Chao Cai , Chunze Yan , Yusheng Shi

Ni–Ti alloys based on triple-periodic minimal surface lattice metamaterials have great application potential. In this work, the triply periodic minimal surface (TPMS) lattice structures with the same volume fraction from a normal Gyroid lattice to an octuple interlacing Gyroid lattice were prepared by the laser powder bed fusion (LPBF) technique. The influence of the interlacing-cell number on manufacturability, uniaxial compression mechanical behaviors, and hyperelastic responses of Ni–Ti lattice structures are analysed by experiments. The stress distributions and fracture mechanism of multicell interlacing lattice structures are illustrated by the finite element method. The obtained results reveal that when the volume fraction is the same, the specific surface area of the lattice structure increases with increasing interlacing-cell number, and the curvature radius of the single-cell strut reduces, which leads to the decrease in the manufacturability of the lattice structure. Meanwhile, the diameter of the single cell strut decreases, and the stress it can bear decreases, which leads to a decline in the compressive mechanical property of the lattice structure. However, the number of struts increases with the increase of interlacing cells, which makes the stress distribution of the lattice structure more uniform. The cyclic compression results indicate that with increasing interlacing-cell number, the proportion of the hyperelastic recoverable strain increases, and the residual strain in the cyclic compression test decreases. For the lattice structure with a chiral arrangement of single cells, the manufacturability, compressive mechanical properties, and hyperelasticity are comparable to those with a normal arrangement. Notably, the Ni–Ti Gyroid TPMS lattice structures have superior hyperelasticity properties (98.87–99.46 % recoverable strain).

基于三周期极小表面晶格的Ni-Ti合金具有很大的应用潜力。本文采用激光粉末床熔合(LPBF)技术制备了具有相同体积分数的三周期极小表面(TPMS)晶格结构,从正常的陀螺晶格到八元交错的陀螺晶格。通过实验分析了交织单元数对Ni-Ti晶格结构工艺性、单轴压缩力学性能和超弹性响应的影响。用有限元方法分析了多胞网格交错结构的应力分布和断裂机理。结果表明,在体积分数一定的情况下,晶格结构的比表面积随着交错单元数的增加而增大,单单元支撑的曲率半径减小,导致晶格结构的可制造性降低;同时,单胞支板直径减小,其所能承受的应力减小,导致晶格结构的压缩力学性能下降。但是,随着交错单元个数的增加,支板个数也随之增加,使得晶格结构的应力分布更加均匀。循环压缩结果表明,随着交织单元数的增加,循环压缩试验中超弹性可恢复应变所占比例增大,残余应变减小;对于单胞手性排列的晶格结构,其可制造性、压缩力学性能和超弹性与正常排列的晶格结构相当。值得注意的是,Ni-Ti Gyroid TPMS晶格结构具有优异的超弹性性能(98.87 ~ 99.46%的可恢复应变)。
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引用次数: 0
IJMTM & JMPT – Serving a wider and stronger community IJMTM,JMP -服务更广泛、更强大的社区
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-11-10 DOI: 10.1016/j.ijmachtools.2023.104090
Dragos Axinte
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引用次数: 0
An operando synchrotron study on the effect of wire melting state on solidification microstructures of Inconel 718 in wire-laser directed energy deposition 用同步加速器研究了熔丝状态对线激光定向能沉积中inconel 718凝固组织的影响
IF 14 1区 工程技术 Q1 Engineering Pub Date : 2023-11-09 DOI: 10.1016/j.ijmachtools.2023.104089
Lin Gao , Andrew C. Chuang , Peter Kenesei , Zhongshu Ren , Lilly Balderson , Tao Sun

Directed energy deposition (DED) with a coaxial wire-laser configuration has gained significant attention in recent years for the production of large-scale metallic components because of its low directional dependence, fast deposition rate, high feedstock efficiency, and low manufacturing costs. This work studies the coaxial wire-laser DED process of Inconel 718 alloy under a stable deposition condition with a relatively low input volumetric energy density (55.5 J/mm3). Post characterization reveals a cluster of refined grains at the center-bottom region of the as-printed track. Operando high-energy synchrotron X-ray experiments and multi-physics modeling are applied innovatively to study the fundamental mechanism responsible for the formation of this microstructure. The X-ray diffraction experiment provides direct evidence, which is supported by the simulation, that the feeding wire can reach the melt pool bottom and release solid particles (primarily carbides) near the mushy zone owing to insufficient melting. Consequently, these sub-micron sized particles suppress the growth of large columnar grains and cause the formation of unique microstructural heterogeneity. This discovery offers new opportunities for tailoring the solidification microstructure by controlling the melting state of the feedstock wire in DED process, in addition to commonly known factors such as the thermal gradient and solidification velocity.

近年来,同轴线-激光定向能沉积(DED)技术因其方向性依赖性低、沉积速度快、给料效率高、制造成本低等特点,在大型金属部件的生产中受到了广泛关注。本文研究了在较低的输入体积能量密度(55.5 J/mm3)和稳定的沉积条件下,同轴线激光对Inconel 718合金的DED工艺。后期表征显示,在打印轨迹的中心底部区域有一簇精细颗粒。创新地应用Operando高能同步加速器x射线实验和多物理场建模来研究这种微观结构形成的基本机制。x射线衍射实验提供了直接的证据,并得到了模拟的支持,即由于熔化不足,进料丝可以到达熔池底部,并在糊状区附近释放固体颗粒(主要是碳化物)。因此,这些亚微米大小的颗粒抑制了大柱状晶粒的生长,并导致独特的微观结构不均匀性的形成。除了众所周知的热梯度和凝固速度等因素外,这一发现为通过控制DED过程中原料丝的熔化状态来定制凝固微观结构提供了新的机会。
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引用次数: 0
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International Journal of Machine Tools & Manufacture
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