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Dry sliding friction and wear behaviour of developed copper metal matrix hybrid composites 开发的铜-金属基复合材料的干滑动摩擦磨损行为
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024006
Manvandra Kumar Singh, R. Gautam
In the present investigation, dry sliding friction and wear behaviour of developed copper-based hybrid composites were studied. Tungsten carbide (WC), zirconia (ZrO2), alumina (Al2O3) of grade A6 and chromium (Cr) hybrid reinforcements were utilised to develop various copper-based hybrid composites using liquid stir-casting technique. The developed hybrid composites were characterised by X-rays diffraction (XRD), high-resolution scanning electron microscope (HR-SEM), energy-dispersive analysis of X-rays (EDAX), relative density and Vickers hardness. Developed hybrid composites show improved Vickers hardness compared to its copper matrix while relative density was found lower. Dry sliding friction and wear behaviour of the developed hybrid composites were studied using pin-on-disc tribometer at variable normal load, constant sliding speed and sliding distance. Hybrid composites exhibited low wear compared to its copper matrix, particularly (WC + Al2O3 + Cr) hybrid reinforced composites revealed better wear resistance among all. Fluctuating nature of the coefficient of friction was observed in all the materials. However, developed hybrid composites revealed higher coefficient of friction compared with its matrix. The worn surfaces were analysed using scanning electron microscopy (SEM), EDAX and optical profilometer to discuss the friction and anti-wear mechanism involved in developed materials.
在本研究中,研究了所开发的铜基杂化复合材料的干滑动摩擦磨损行为。采用液体搅拌铸造技术,利用碳化钨(WC)、氧化锆(ZrO2)、A6级氧化铝(Al2O3)和铬(Cr)混杂增强材料开发了各种铜基混杂复合材料。通过X射线衍射(XRD)、高分辨率扫描电子显微镜(HR-SEM)、X射线能量色散分析(EDAX)、相对密度和维氏硬度对所开发的杂化复合材料进行了表征。与铜基体相比,所开发的杂化复合材料显示出更好的维氏硬度,同时发现相对密度更低。采用销盘式摩擦计研究了所研制的复合材料在变法向载荷、恒定滑动速度和滑动距离下的干滑动摩擦磨损行为。与铜基体相比,混杂复合材料表现出较低的耐磨性,特别是(WC+Al2O3+Cr)混杂增强复合材料在所有材料中表现出更好的耐磨性。在所有材料中都观察到摩擦系数的波动性。然而,与基体相比,所开发的杂化复合材料显示出更高的摩擦系数。利用扫描电子显微镜(SEM)、EDAX和光学轮廓仪对磨损表面进行了分析,探讨了所开发材料的摩擦和抗磨机理。
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引用次数: 5
SEM-based observations and analysis of the green silicon carbide grinding wheel active surfaces after the graphite and silicone impregnation process 基于sem的绿色碳化硅砂轮活性表面石墨与硅酮浸渍工艺的观察与分析
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024014
W. Kapłonek, K. Nadolny, M. Ungureanu, D. Pimenov, B. Zieliński
In the paper, initial studies focused on observations and analysis of the effects of the impregnation process of the grinding wheel active surface (GWAS) 1-35 × 20 × 10 99C46K8V made of green silicon carbide (SiCg) are presented. One of the allotropic varieties of carbon (graphite) and a synthetic organosilicon polymer (silicone) was introduced into the structure of the GWAS. For an assessment of the effects of impregnation, a JEOL JSM-550LV scanning electron microscope (SEM) was used. The data acquired by this instrument are presented in the form of a set of SEM micrographs subjected to visual and computer image analysis using Image Pro®-Premier software. This software allowed one to calculate the size of the area containing the impregnate in relation to the area without an impregnate, and to determine other useful geometrical parameters. The obtained results provided information about the effects of the impregnation process, its efficiency and influence on the characteristics of the GWAS.
本文对由绿色碳化硅(SiCg)制成的1-35×20×10 99C46K8V砂轮活性表面(GWAS)浸渍过程的影响进行了初步的观察和分析。在GWAS的结构中引入了碳(石墨)和合成有机硅聚合物(硅酮)的同素异形变体之一。为了评估浸渍的效果,使用JEOL JSM-550LV扫描电子显微镜(SEM)。该仪器采集的数据以一组SEM显微照片的形式呈现,并使用image Pro®-Premier软件进行视觉和计算机图像分析。该软件允许计算含有浸渍物的区域相对于没有浸渍物的面积的大小,并确定其他有用的几何参数。所获得的结果提供了关于浸渍过程的影响、其效率以及对GWAS特性的影响的信息。
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引用次数: 8
Microscopic analysis of the Sol-Gel alumina grinding wheel after the introduction of a synthetic organosilicon polymer-based impregnate dedicated for near dry grinding processes 溶胶-凝胶氧化铝砂轮在引入用于近干研磨工艺的合成有机硅聚合物浸渍剂后的微观分析
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024005
K. Nadolny, W. Kapłonek, M. Niemczewska-Wójcik, M. Ungureanu
In the paper, analysis of the surface condition of 1-35 × 10 × 10-SG/ F46G10VTO grinding wheels with microcrystalline sintered alumina abrasive grains and a glass-crystalline bond after the impregnation process using a synthetic organosilicon polymer (silicone) has been presented. The main goal was to compare the values of selected surface topography parameters obtained from the active surfaces of an impregnated set of grinding wheels with those same parameters obtained from a non-impregnated reference wheel. The analysis proved that an elaborated method of introducing the impregnating substance is effective and allowing to uniformly its distribution throughout the body of the grinding wheel. However, the introduction of impregnating substance caused a reduction (average from 13% to 50%) in the values of the selected 3D parameters of grinding wheel active surface (GWAS) roughness. An analysis described in this work is the basis of an objective evaluation of the experimental results of the grinding process conducted with use of that kind of wheels.
本文分析了1-35×10×10-SG/F46G10VTO微晶烧结氧化铝磨粒和玻璃晶结合剂砂轮经合成有机硅聚合物浸渍处理后的表面状况。主要目标是将从浸渍的一组砂轮的有效表面获得的选定表面形貌参数的值与从未浸渍的参考轮获得的相同参数进行比较。分析证明,引入浸渍物质的详细方法是有效的,并允许其均匀分布在砂轮的整个本体中。然而,浸渍物质的引入导致砂轮有效表面(GWAS)粗糙度的选定3D参数的值降低(平均从13%到50%)。这项工作中描述的分析是对使用这种轮子进行的研磨过程的实验结果进行客观评估的基础。
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引用次数: 3
Electrophoretic deposition of zinc-doped hydroxyapatite coatings on titanium: deposition kinetics and coating morphology 掺杂锌羟基磷灰石涂层在钛上的电泳沉积:沉积动力学和涂层形貌
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024018
C. Moseke, Yunis Alnazal Alramadan, E. Vorndran, P. Elter
A wet chemistry reaction route was utilised to fabricate hydroxyapatite (HA) coatings with the incorporation of different amounts of zinc by electrophoretic deposition on titanium. HA powders and coatings were characterised by X-ray diffraction, scanning electron microscopy, and energy dispersive X-ray analysis. The presence of Zn had only a small impact on the crystallinity and practically no effect on the crystallite morphology of the powders and coatings. High additions of Zn apparently led to a change of the migration direction of the HA particles in the coating electrolyte and also resulted in increased crack formation during the drying process of the deposited coatings. Zn was incorporated in the HA coatings by ionic substitution and by incorporation of a low-crystalline ZnO phase, which may be advantageous for the application as a long-term reservoir for Zn as an osteoclast-inhibiting agent on biomaterials for implantation in critical bone situations.
采用湿化学方法,在钛上电泳沉积不同锌含量的羟基磷灰石(HA)涂层。通过x射线衍射、扫描电子显微镜和能量色散x射线分析对HA粉末和涂层进行了表征。锌的存在对结晶度的影响很小,对粉末和涂层的结晶形态几乎没有影响。高Zn的添加明显改变了涂层电解质中HA颗粒的迁移方向,也导致涂层干燥过程中裂纹的形成增加。锌通过离子取代和低晶ZnO相的掺入到HA涂层中,这可能有利于作为锌的长期储存库,作为生物材料的破骨抑制剂,用于危急骨情况下的植入。
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引用次数: 3
Wet-chemical etching of GaAs(211)B wafers for controlling the surface properties 控制GaAs(211)B晶圆表面性质的湿化学蚀刻
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024001
S. Özden, M. M. Koç
Substrate surface plays an important role to achieve high performance infrared devices and high-quality film layers. GaAs (211)B wafers were intensively used in infrared detector applications. Despite 'epiready' wafers can easily be found on the market, most of them have defects and contaminations due to their fabrication processes. The defects and contaminations on wafers may have deleterious effects on thin film growth and detector applications. To overcome such problems, various chemical treatments should be implemented prior to thin film growth. In this study, to understand the effect of wet chemical cleaning process on epiready (211)B GaAs wafers, piranha solution-based wet chemical etching was performed. After these treatments, the surfaces of GaAs wafers were investigated by atomic force microscopy and scanning electron microscopy. Energy dispersive X-ray spectroscopy was used to assess the chemical composition of the surface. The vibrational modes and two-dimensional maps were observed by a Raman spectroscopy.
衬底表面对实现高性能红外器件和高质量薄膜层起着重要作用。GaAs (211)B晶片广泛应用于红外探测器。尽管在市场上可以很容易地找到“epiready”晶圆,但由于其制造过程,大多数晶圆都存在缺陷和污染。晶圆片上的缺陷和污染可能对薄膜生长和探测器的应用产生有害影响。为了克服这些问题,应在薄膜生长之前实施各种化学处理。为了了解湿法化学清洗工艺对epiready (211)B GaAs晶圆的影响,采用水虎鱼溶液进行了湿法化学刻蚀。通过原子力显微镜和扫描电镜对处理后的GaAs晶圆表面进行了研究。利用能量色散x射线光谱学对表面的化学成分进行了评估。用拉曼光谱观察了其振动模式和二维图。
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引用次数: 8
Effect of laser surface texturing on tribological behaviour of grey cast iron 激光表面织构对灰口铸铁摩擦学性能的影响
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024024
B. Kumar, P. D. Babu, P. Marimuthu, M. Duraiselvam
This work aims to study the effect of laser surface microtexture on the sliding behaviour of grey cast iron, which is used as a liner material in internal combustion engines. The sliding wear analysis was conducted at different sliding speeds (200 rpm, 400 rpm, and 600 rpm) and a normal load of 10 N. Laser machining system was used to create micro-dimples with texture densities of 13.45% and 6.37%. The dimple sizes were observed using a scanning electron microscope, and the surface roughness was measured using the white light interferometer. The sliding wear results show that the textured samples with 13.45% densities in higher viscosity 146 mPas oil show better wear resistance with 0.1828 mm3'm wear rate and reduced friction coefficient of 0.1973. The wear morphology of the textured samples confirms the abrasive wear mechanism with minimum material removal compared with the non-textured specimen for the given applied load and sliding speed.
本工作旨在研究激光表面微织构对灰口铸铁滑动行为的影响,灰口铸铁是内燃机内衬材料。在不同的滑动速度(200转、400转和600转)和10 n的正常载荷下进行滑动磨损分析,利用激光加工系统制造出纹理密度分别为13.45%和6.37%的微窝。用扫描电子显微镜观察微窝大小,用白光干涉仪测量表面粗糙度。摩擦磨损结果表明,在高粘度146 mpa油中,密度为13.45%的织构试样具有较好的耐磨性,磨损率为0.1828 mm3 m,摩擦系数降低0.1973。在给定的载荷和滑动速度下,与非织构试样相比,织构试样的磨损形貌证实了磨粒磨损机制,其材料去除量最小。
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引用次数: 1
Finite element-based contact analysis of a radially functionally graded hemisphere and a rigid flat 基于有限元的径向功能梯度半球与刚性平面接触分析
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-09-17 DOI: 10.1504/ijsurfse.2019.10024012
Tamonash Jana, A. Mitra, P. Sahoo
In the present work, a normally loaded contact between a radially functionally graded hemisphere and a rigid flat is analysed in perfect slip condition for different values of gradient/inhomogeneity parameter. The analysis was performed with an axisymmetric model in commercial finite element software ANSYS 18.2. The Young's modulus, yield strength and tangent modulus (for bilinear isotropic hardening) are varied according to an exponential function. The effect of the inhomogeneity parameter on different contact behaviours, e.g., contact area, contact pressure, contact stresses, etc., of the hemisphere are obtained. Stress and deformation behaviour of the contact interface as well as of the entire hemisphere has been analysed. It is observed that for negative inhomogeneity parameter, while being deformed by the rigid flat, the summit of the hemisphere loses contact with flat and sinks in to have a concave shape at the top of the hemisphere. This phenomenon has not been reported in established literature yet.
在本工作中,对于不同的梯度/不均匀性参数值,分析了在理想滑动条件下径向功能梯度半球和刚性平面之间的正载荷接触。利用商业有限元软件ANSYS 18.2中的轴对称模型进行分析。杨氏模量、屈服强度和切线模量(双线性各向同性硬化)根据指数函数变化。得到了不均匀性参数对半球不同接触行为的影响,如接触面积、接触压力、接触应力等。分析了接触界面以及整个半球的应力和变形行为。观察到,对于负的不均匀性参数,当被刚性平面变形时,半球的顶部失去与平面的接触,并在半球的顶部下沉为凹形。这一现象尚未在已有文献中报道。
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引用次数: 2
Mechanical and anti-wear properties of multi-module Cr/CrN coatings 多模态Cr/CrN涂层的力学性能和抗磨性能
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-02-25 DOI: 10.1504/IJSURFSE.2019.10019183
Ł. Szparaga, K. Mydłowska, A. Gilewicz, J. Ratajski
The objects of investigations were Cr/CrN multi-module coatings deposited using a cathodic arc evaporation method (CAPVD) on HS6-5-2C steel used as a substrates. Analysed coatings possesses seven Cr/CrN modules of fixed thickness each, with various thicknesses of Cr and CrN layers. Aiming for the evaluation of mechanical properties of tested multi-module Cr/CrN coatings, its hardness and Young's modulus were measured, on the basis of which were determined values of H/E and H3/E2 ratios. Coatings wear and friction coefficients were measured in so called ball-on-disc test. The adhesion of the coatings was evaluated using scratch tester and was shown that main mechanism of adhesive damage of all tested coatings at higher loads are buckle spallations. All tested coatings are also characterised by good adhesion to the substrate, which is evidenced by the fact that cracked coating remains inside the scratch track. Basing on the analysis of obtained experimental results it was confirmed and explicitly shown that the thickness of the individual layers of Cr and CrN in the multi-module coating significantly affects its critical loads (in scratch test), fracture toughness and wear rate.
研究对象是使用阴极电弧蒸发法(CAPVD)在用作基底的HS6-5-2C钢上沉积的Cr/CrN多模块涂层。所分析的涂层具有七个固定厚度的Cr/CrN模块,每个模块具有不同厚度的Cr和CrN层。为了评价所测试的多模块Cr/CrN涂层的力学性能,测量了其硬度和杨氏模量,并在此基础上确定了H/E和H3/E2比值。涂层的磨损和摩擦系数是在所谓的圆盘上球试验中测量的。使用划痕测试仪对涂层的附着力进行了评估,结果表明,在较高载荷下,所有测试涂层的附着力损伤的主要机制是屈曲剥落。所有测试的涂层都具有与基材的良好粘附性,这一点可以从裂纹涂层保留在划痕轨迹内的事实中得到证明。基于对所获得的实验结果的分析,证实并明确地表明,多模块涂层中Cr和CrN单层的厚度显著影响其临界载荷(在划痕试验中)、断裂韧性和磨损率。
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引用次数: 4
Solid particle erosion studies on fibre composite with egg shell as filler materials 蛋壳填充纤维复合材料的固体颗粒侵蚀研究
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-02-25 DOI: 10.1504/IJSURFSE.2019.10019179
M. A. Khan, S. Manikandan, G. Ebenezer, M. Uthayakumar, S. Kumaran
The development on composite materials has a tremendous role in the place of metals and alloys for different engineering applications. On the other hand, the material selected for specific applications are prone to fail in bulk with surface defect and shear based on working conditions. Hence, the challenges convince the researchers to modifying the materials with different reinforcement. In this paper, glass fibre composite material was developed with and without fillers to investigate on solid particle erosion test rig. From the experiments, the surface wear and parameter influencing air jet erosion are studied in detail. The parameters involve are jet pressure, volume of erodent and exposed time at constant angle of impingement. Based on mass change erosive wear rate are empirically calculated. The surface topography of the sample are observed with electron microscopic analysis for superficial studies. Influence of process parameter is evaluated using 2k factorial design. It is confirmed that erodent behaviour and composite with filler material are dominating the erosive wear rate. The sample with polyester resin has an affinity to hold the abrasive particle as inclusion during striking of solid particle. Therefore the proposed model with natural filler in fibre reinforced surface has resistance toward erosion.
复合材料的发展在不同的工程应用中取代了金属和合金,发挥了巨大的作用。另一方面,根据工作条件,为特定应用选择的材料容易因表面缺陷和剪切而导致整体失效。因此,这些挑战说服了研究人员用不同的增强剂对材料进行改性。本文研制了含填料和不含填料的玻璃纤维复合材料,在固体颗粒侵蚀试验台上进行了试验研究。通过实验,详细研究了表面磨损和影响空气射流侵蚀的参数。参数包括射流压力、侵蚀剂体积和恒定冲击角下的暴露时间。基于质量变化对冲蚀磨损率进行了经验计算。通过电子显微镜分析观察样品的表面形貌,进行表面研究。采用2k因子设计对工艺参数的影响进行了评价。结果表明,侵蚀行为和填料复合材料是侵蚀磨损率的主要因素。具有聚酯树脂的样品在固体颗粒的撞击过程中具有保持磨料颗粒作为夹杂物的亲和力。因此,所提出的纤维增强表面含有天然填料的模型具有抗侵蚀性。
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引用次数: 6
Pull-off strength and abrasion resistance of anti-corrosive polymer and composite coatings 抗腐蚀聚合物和复合涂层的脱拉强度和耐磨性
IF 0.8 4区 工程技术 Q4 ENGINEERING, MECHANICAL Pub Date : 2019-02-25 DOI: 10.1504/IJSURFSE.2019.10019184
A. Dmitruk, P. Mayer, J. Pach
The paper aims at presenting the results of pull-off strength and abrasion resistance tests for anti-corrosive coatings on steel substrates. It contains the measured data on the thickness of manufactured coatings in the function of the applied amount of abrasive material. Three polymeric coatings were subjected for testing: chlorinated rubber, oil-phthalic and alkyd. The analogous studies were repeated for composite coatings with alumina α-Al2O3 filler and subsequently also for the aged (72 h, -19°C) systems. For the pull-off tests, the damage analysis of samples after failure was performed. The highest pull-off strength's values for the produced coatings were obtained for the alkyd one. Concerning the abrasion resistance it can be stated that, the addition of a filler significantly improves the system's durability, while the aging process causes its deterioration.
本文旨在介绍钢基体防腐涂层的剥离强度和耐磨性试验结果。它包含了以磨料用量为函数的制造涂层厚度的测量数据。测试了三种聚合物涂层:氯化橡胶、油邻苯二甲酸和醇酸。对含有氧化铝α-Al2O3填料的复合涂层以及随后的老化(72小时,-19°C)系统重复了类似的研究。对于拉拔试验,进行了失效后样品的损伤分析。醇酸树脂涂层的剥离强度最高。关于耐磨性,可以说,添加填料显著提高了系统的耐久性,而老化过程会导致其劣化。
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引用次数: 2
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International Journal of Surface Science and Engineering
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