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Assessment of mechanical and physicochemical properties of palm fiber composites: Effect of alkaline treatment and volume alterations 评估棕榈纤维复合材料的机械和物理化学性能:碱性处理和体积改变的影响
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-10 DOI: 10.1177/00219983241246614
Hocine Heraiz, Chouki Farsi, Hocine Makri, Salah Amroune, Ahmed Belaadi, Khalissa Saada, Moussa Zaoui, Mohammed Ismail Beddiar
This study assesses the impact of alkaline treatments and volume fractions on biocomposites composed of a high-density polyethylene (HDPE) matrix reinforced with date palm tree fibers (FPDS). Tensile tests were conducted on both untreated and NaOH-treated biocomposites. Additionally, fiber analysis was performed using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results reveal higher strength and stiffness compared to HDPE, albeit with limited plasticity making the material brittle. The NaOH treatment enhances certain mechanical properties. Further assessments encompassed hardness, density, melt index, and Izod impact tests. Two volume fractions, 20% and 25%, of FPDS were tested. The study establishes a correlation between empirical predictions and artificial neural network (ANN) models. Notably, an ANN architecture consisting of two input factors, 10 hidden nodes, and one output provides the analysis of mechanical properties. This investigation highlights the potential of FPDS-reinforced HDPE biocomposites, emphasizing their mechanical performance under various treatments and fiber levels.
本研究评估了碱性处理和体积分数对由枣椰树纤维(FPDS)增强的高密度聚乙烯(HDPE)基体组成的生物复合材料的影响。对未经处理和经 NaOH 处理的生物复合材料进行了拉伸试验。此外,还使用扫描电子显微镜(SEM)和 X 射线衍射(XRD)对纤维进行了分析。结果表明,与高密度聚乙烯相比,该材料具有更高的强度和刚度,尽管有限的塑性使其变脆。NaOH 处理增强了某些机械性能。进一步的评估包括硬度、密度、熔融指数和伊佐德冲击试验。对两种体积分数(20% 和 25%)的 FPDS 进行了测试。该研究建立了经验预测与人工神经网络(ANN)模型之间的相关性。值得注意的是,由两个输入因子、10 个隐藏节点和一个输出组成的人工神经网络结构提供了机械性能分析。这项研究突出了 FPDS 增强高密度聚乙烯生物复合材料的潜力,强调了其在不同处理和纤维水平下的机械性能。
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引用次数: 0
Investigations on the development of impact-resistant thermoplastic fibre hybrid composites from glass and steel fibre 关于开发玻璃纤维和钢纤维抗冲击热塑性纤维混合复合材料的研究
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-09 DOI: 10.1177/00219983241246128
Matthias Overberg, Mir Mohammad Badrul Hasan, Anwar Abdkader, Jan Rehra, Sebastian Schmeer, Chokri Cherif
With the increased use of fibre reinforced composites (FRP), the design of new generation of composite structures with high stiffness and a ductile material behaviour is required to cope with complex load scenarios and high damage tolerances. This can be achieved, in particular, by a combination of conventional fibre-reinforced composites (FRP), which possess high stiffness and strength with metallic materials characterized by their high ductility and associated higher energy absorption capacity. Currently, there are no solutions for hybridisation of high performance filament yarns, metal filament yarns and thermoplastic filament yarns on micro level. Therefore, the main objective of this study is to develop a fibre hybrid composite based on hybrid yarn consisting of glass, steel and polypropylene filament yarns and to compare its tensile and impact properties with those of the composite reinforced only with glass filament yarn. The tensile and impact properties of the unidirectional hybrid composites produced from the developed multi-material hybrid yarn consisting of steel, glass and polypropylene filament yarns are compared with those of a non-hybrid composite reinforced exclusively with glass filament yarn. The results show that by hybridising with steel fibres a characteristic post-failure behaviour can be achieved, so that the developed multi-material hybrid yarns have a high potential for use in composites with high crash and impact performance requirements, where safety demands are essential.
随着纤维增强复合材料(FRP)使用的增加,需要设计出具有高刚度和延展性材料行为的新一代复合材料结构,以应对复杂的载荷情况和高损伤公差。传统的纤维增强复合材料(FRP)具有高刚度和高强度,而金属材料则具有高延展性和更高的能量吸收能力。目前,还没有在微观层面上将高性能长丝纱、金属长丝纱和热塑性长丝纱混合使用的解决方案。因此,本研究的主要目的是开发一种基于由玻璃丝、钢丝和丙纶长丝组成的混合纱线的纤维混合复合材料,并将其拉伸和冲击性能与仅用玻璃丝增强的复合材料进行比较。比较了由钢、玻璃和丙纶长丝组成的多材料混合纱制成的单向混合复合材料与只用玻璃长丝增强的非混合复合材料的拉伸和冲击性能。结果表明,通过与钢纤维的杂化,可以实现特征性的失效后行为,因此开发的多材料杂化纱在对碰撞和冲击性能有较高要求的复合材料中具有很大的应用潜力,因为在这种情况下,安全要求是至关重要的。
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引用次数: 0
Compression-compression fatigue performances of hybrid unidirectional/woven carbon-fiber reinforced composite laminates after LVI 单向/编织混合碳纤维增强复合材料层压板在 LVI 后的压缩-压缩疲劳性能
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-08 DOI: 10.1177/00219983241246108
Wenqian Wang, Hangchao Wang, Yu Feng, Binlin Ma, Zhe Li, Jinpeng Li
Compression-compression fatigue behavior of hybrid unidirectional/woven carbon-fiber reinforced composite laminates after low-velocity impact (LVI) was studied in this paper. The paper contains two parts. Firstly, different levels of impact energy were introduced on the specimens. Impact damage modes were obtained and characterized as fiber breakages, matrix cracks, indentation and delamination. The relationships between indentation depth/damage area and impact energy were established. Secondly, compression-compression fatigue tests were conducted on the impact damaged specimens. Fatigue life degradation trends were analyzed and fatigue limit for different types of specimens was determined. Delamination areas by depth mode and amplitude mode of C-scan showed an increasing trend with the fatigue life increasing. Stiffness decreased sharply in the early and ending stages of fatigue life. However, stiffness exhibited stable or slightly decreasing rates in the mid-stage of fatigue life. A line-shaped failure cracks going through the impact point were observed in the fatigue failure specimens.
本文研究了低速冲击(LVI)后混合单向/编织碳纤维增强复合材料层压板的压缩-压缩疲劳行为。本文包括两个部分。首先,在试样上引入了不同程度的冲击能量。得到的冲击破坏模式包括纤维断裂、基体裂纹、压痕和分层。建立了压痕深度/损伤面积与冲击能量之间的关系。其次,对受到冲击破坏的试样进行了压缩-压缩疲劳试验。分析了疲劳寿命退化趋势,并确定了不同类型试样的疲劳极限。C 扫描深度模式和振幅模式下的分层面积随着疲劳寿命的延长呈上升趋势。刚度在疲劳寿命的初期和末期急剧下降。然而,在疲劳寿命的中期阶段,刚度表现出稳定或略微下降的趋势。在疲劳失效试样中观察到穿过冲击点的线形失效裂纹。
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引用次数: 0
PAN-based fiber-reinforced carbon-carbon composites for improved fire retardancy and thermal and electrical conductivities for harsh environments 基于 PAN 纤维的碳-碳增强复合材料,可提高恶劣环境下的阻燃性、导热性和导电性
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-08 DOI: 10.1177/00219983241246610
TKS Murali, Md Shafinur Murad, Mete Bakir, Ramazan Asmatulu
Carbon-carbon (C-C) fiber composites are a new class of materials that are used in various industries due to their exceptional chemical, thermal and electrical conductivities properties. In this study, carbon-carbon fiber composites were manufactured where polyacrylonitrile (PAN) powder was dissolved in dimethylformamide (DMF) solution, and carbon fibers with desired concentrations (20–80 wt%) were immersed into this solution as reinforcement through evaporation and solidification. The PAN-fiber systems were then stabilized at 250–270°C for 120 min in the air and subsequently carbonized at 650, 750, and 850°C for 60 min in the presence of argon gas to obtain the desired C-C fiber composites. Thermogravimetric analysis (TGA) results showed that the carbonized samples had a small weight loss of 2.5%, while actual and oxidized samples had more weight loss. Moreover, the carbonized sample surface was more hydrophobic compared to other samples due to the carbon presence and surface texture changes. Fourier-Transform Infrared (FTIR) spectroscopy peaks showed the presence of different functional groups of PAN before oxidation and carbonization, but those peaks disappeared after oxidation and carbonization. The developed carbon-carbon composite passed the UL94 vertical flame retardancy testing with a V-0 rating. Surface smoothness, proper matrix and reinforcements bonding were confirmed by scanning electron microscopy (SEM) results and the manufactured composite properties changes were validated by the confocal microscopy images. The carbon-carbon fiber composite achieved an electrical conductivity value up to 4.75 × 103 S/m after the carbonization process. The excellent thermal, chemical, and electrical properties of these composites can be useful for numerous industrial applications in different extreme environments.
碳-碳(C-C)纤维复合材料是一类新型材料,因其优异的化学、热和导电特性而被广泛应用于各行各业。本研究制造了碳-碳纤维复合材料,将聚丙烯腈(PAN)粉末溶解在二甲基甲酰胺(DMF)溶液中,通过蒸发和凝固将所需浓度(20-80 wt%)的碳纤维浸入该溶液中作为增强材料。然后将 PAN 纤维体系在 250-270°C 的空气中稳定 120 分钟,随后在氩气存在下在 650、750 和 850°C 的温度下碳化 60 分钟,以获得所需的 C-C 纤维复合材料。热重分析(TGA)结果表明,碳化样品的重量损失较小,仅为 2.5%,而实际样品和氧化样品的重量损失较大。此外,由于碳的存在和表面纹理的变化,碳化样品表面比其他样品更疏水。傅立叶变换红外光谱峰显示,氧化和碳化前 PAN 存在不同的官能团,但氧化和碳化后这些峰消失了。开发的碳-碳复合材料通过了 UL94 垂直阻燃测试,阻燃等级为 V-0。扫描电子显微镜(SEM)结果证实了表面的平滑性、基体和增强体的适当结合,共聚焦显微镜图像也验证了所制造的复合材料性能的变化。碳-碳纤维复合材料在碳化过程后的电导率值高达 4.75 × 103 S/m。这些复合材料优异的热学、化学和电学特性可用于不同极端环境下的多种工业应用。
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引用次数: 0
Enhancement of the contact behavior of a quasi-isotropic carbon fiber/epoxy matrix laminate with an elastic body by modifying the fiber-matrix interphase using graphene nanoplatelets 通过使用石墨烯纳米片改变纤维-基体间相,增强准各向同性碳纤维/环氧基体层压板与弹性体的接触行为
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-08 DOI: 10.1177/00219983241245715
Abad Arcos-Alomía, Aarón Rivas-Menchi, Alex Valadez-González, Pedro J Herrera-Franco
This study analyzed the effect of incorporating graphene nanoplatelets in the fiber-matrix interphase on the behavior of a multiscale composite laminate based on carbon fibers and epoxy resin subjected to contact loads. The selected loading mode was the contact between an elastic surface and a cylinder. The multiscale composite material used was a quasi-isotropic laminate with graphene nanoplatelets (GnPs) added at the fiber-matrix interface. The specimens were prepared with 0.0%, 0.1%, and 0.25% by-weight GnPs. Laminate beams were used according to the ASTM D7264 standard, and contact was studied in two configurations, applying the load at the edge of the laminate and in the other, in the plane of the test pieces. The normal strains in the contact region were determined experimentally using the interferometric Moiré technique. These results were compared with estimations using the Hertz contact theory and the finite element method (FEM). The normal strains in the contact area of specimens with fibers modified with 0.1% GnPs were lower than those with 0.25% or fibers without surface modification. Excellent agreement between the experimental results along lines in the contact zone with those estimated with the FEM. The normal strains in a direction perpendicular to the applied load obtained by the Hertz theory for the maximum deformation were slightly higher than those obtained by FEM. Except for those calculated for the normal strain in εy for the load in the direction of the thickness, although the distribution was very similar to those obtained by FEM as well as the experimental one.
本研究分析了在纤维-基体相间加入石墨烯纳米颗粒对基于碳纤维和环氧树脂的多尺度复合材料层压板在接触载荷下的行为的影响。所选加载模式为弹性表面与圆柱体之间的接触。所使用的多尺度复合材料是一种准各向同性层压材料,在纤维-基质界面上添加了石墨烯纳米片(GnPs)。制备试样时,GnPs 的重量分别为 0.0%、0.1% 和 0.25%。根据 ASTM D7264 标准使用层压梁,研究了两种配置下的接触情况:一种是在层压梁边缘施加载荷,另一种是在试件平面上施加载荷。接触区域的法向应变是利用干涉莫伊里技术通过实验测定的。这些结果与使用赫兹接触理论和有限元法(FEM)估算的结果进行了比较。使用 0.1% GnPs 改性纤维的试样接触区域的法向应变低于使用 0.25% GnPs 或未进行表面改性的纤维。接触区沿线的实验结果与有限元估算的结果非常一致。用赫兹理论计算的最大变形时垂直于外加载荷方向的法向应变略高于有限元计算的结果。除了计算出的厚度方向载荷在 εy 处的法向应变,尽管其分布与有限元以及实验所得非常相似。
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引用次数: 0
Concurrent effect of shear flow and CNT presence on crystallization behavior and electrical properties of polypropylene based nanocomposites: A comprehensive structure-property investigation 剪切流动和碳纳米管的存在对聚丙烯基纳米复合材料的结晶行为和电性能的并发影响:结构-性能综合研究
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-06 DOI: 10.1177/00219983241245998
Younes Alimoradi, Maryam Nourisefat, Arman Farzaneh, Hossein Nazokdast
The loading of nanoparticle in the polymer matrix affects their response to shear flows applied during the fabrication process. With this in mind, in the present study, the concurrent effect of carbon nanotube (CNT) presence and shear application on the rheological and electrical properties as well as on the crystallization behavior of polypropylene (PP) based nanocomposites has been investigated. The results of rheological analyses showed that the solid-like behavior increases in proportion to the CNT content, and a remarkable increase in the solid-like behavior is obtained at a CNT content of 2 wt%. The isothermal crystallization results corroborated that crystallization temperature increases proportionally with the CNT content, however does not change with shearing. The non-isothermal crystallization findings confirmed that crystallization kinetics promotes with increasing CNT content, and this effect becomes more pronounced with shearing. The results of thermal analysis confirmed that the melting temperature decreases slightly, and the crystallinity remains almost unchanged with increasing CNT content up to 2%. However, when the CNT content rose up to 4%, the crystallinity decreased significantly due to confined crystallization. When this nanocomposite was subjected to shearing, the crystallinity increased. The results of electrical conductivity measurement revealed that the conductivity increases with increasing CNT content, while it decreases with shearing and the vulnerability of nanocomposites to shearing decreases with increasing CNT content.
聚合物基体中的纳米粒子含量会影响其对制造过程中施加的剪切流的响应。有鉴于此,本研究调查了碳纳米管(CNT)的存在和剪切应用对聚丙烯(PP)基纳米复合材料的流变性能、电性能和结晶行为的影响。流变分析结果表明,类固行为随 CNT 含量的增加而增加,当 CNT 含量为 2 wt% 时,类固行为显著增加。等温结晶结果证实,结晶温度随 CNT 含量的增加而成正比增加,但不随剪切而变化。非等温结晶结果证实,结晶动力学随着碳纳米管含量的增加而加快,这种效应在剪切时更为明显。热分析结果证实,随着碳纳米管含量的增加,熔化温度略有下降,结晶度几乎保持不变,最高可达 2%。然而,当碳纳米管的含量增加到 4% 时,结晶度却因限制结晶而显著下降。当这种纳米复合材料受到剪切时,结晶度增加了。电导率测量结果表明,电导率随碳纳米管含量的增加而增加,而随剪切力的增加而降低,并且纳米复合材料对剪切力的易损性随碳纳米管含量的增加而降低。
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引用次数: 0
Structural improvement of 3D woven honeycomb composite liner for enhanced energy absorption and impact performance in aircrew helmet 改进三维编织蜂窝复合材料衬垫的结构,提高空勤人员头盔的能量吸收和冲击性能
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-05 DOI: 10.1177/00219983241246058
Omender Singh, BK Behera
This study aims to enhance the performance of aircrew helmet liners made of 3D woven honeycomb composites through structural improvements. To achieve this, an optimization of the honeycomb design was carried out using a statistical tool by varying its geometrical parameters. A Box Behnken design was employed, using three independent factors: cell height, cell size, and cell wall thickness to assess its impact and their interactions on responses. The performance was evaluated using a multiobjective response to maximize impact energy absorption, achieve the target cushion factor, and balance relative density for lightweight design. Since the liner materials were subjected to flatwise compression and dynamic impact tests to assess the performance. Their behavior. The results revealed that the honeycomb core with a cell height of 15 mm, a cell size of 10 mm, and a cell wall thickness of 0.6 mm exhibited good behavior. The response surface analysis and contour plots were used to analyze the interactions and combined effects of variables on each response. It was observed that lesser cell size shows significant improvement in impact energy with higher wall thickness. However, the cushion factor implies inadequate energy mitigation. The analysis comparing desirability and confirmatory experiments highlighted the potential for the aircrew helmet liner to achieve its maximum performance. This study provides valuable insights into the structural design of 3D woven honeycomb composite liners for aircrew helmets and its findings signify the potential for applications in the aerospace and defense industries.
本研究旨在通过改进三维编织蜂窝复合材料提高空勤人员头盔衬里的性能。为此,我们使用统计工具,通过改变蜂窝的几何参数,对蜂窝设计进行了优化。采用盒式贝肯设计,使用三个独立因素:蜂窝高度、蜂窝尺寸和蜂窝壁厚度来评估其对响应的影响及其相互作用。性能评估采用了多目标响应,以最大限度地吸收冲击能量,达到目标缓冲系数,并平衡相对密度以实现轻量化设计。对衬垫材料进行了平向压缩和动态冲击试验,以评估其性能。它们的行为。结果显示,蜂窝芯的单元高度为 15 毫米,单元尺寸为 10 毫米,单元壁厚为 0.6 毫米,表现出良好的性能。响应面分析和等高线图用于分析变量对每个响应的相互作用和综合影响。结果表明,较小的电池尺寸与较高的壁厚能显著提高冲击能量。然而,缓冲系数意味着能量减缓不足。通过对可取性和确认性实验进行比较分析,突出了空勤人员头盔衬垫实现其最大性能的潜力。这项研究为空勤人员头盔的三维编织蜂窝复合材料衬垫的结构设计提供了宝贵的见解,其研究结果表明了在航空航天和国防工业中的应用潜力。
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引用次数: 0
Analysis of load-bearing characteristics of bi-modulus composite stiffened plates: Numerical simulation method and large-scale experimental verification 双模量复合加劲板的承载特性分析:数值模拟方法和大规模实验验证
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-04-01 DOI: 10.1177/00219983241244518
Zhenzhou Ye, Xiaobin Li, Lin Lv, Weimeng Xie, Wei Chen, Wei Shen
A large number of experiments show that composite materials usually show different modulus properties in tension and compression (bi-modulus). However, for actual composite engineering structures, especially complex models, the numerical simulation calculation is usually based on a single modulus. In order to consider the different modulus characteristics of composite materials in tension and compression, researchers put forward simplified constitutive models of dual-modulus materials. However, these constitutive models have not been verified by a large number of experiments, especially by complex models. In this paper, the GWFMM model is simplified and used to analyze complex structures with different modulus in tension and compression. The experimental results of stiffened plate show that the improved GWFMM model can be used to analyze different modulus of tension and compression of complex stiffened structures. In addition, the influence of elastic modulus ratio in tension and compression under different experimental load conditions is further explored, and the influence law of bending and torsion on structures with bi-modulus is discussed. The relevant conclusions provide reference for the design and optimization of full-scale composite structures in marine engineering.
大量实验表明,复合材料在拉伸和压缩时通常表现出不同的模量特性(双模量)。然而,对于实际的复合材料工程结构,尤其是复杂模型,数值模拟计算通常基于单一模量。为了考虑复合材料在拉伸和压缩时的不同模量特性,研究人员提出了简化的双模量材料构成模型。然而,这些构成模型并没有经过大量实验的验证,尤其是复杂模型。本文简化了 GWFMM 模型,并将其用于分析具有不同拉伸和压缩模量的复杂结构。加劲板的实验结果表明,改进后的 GWFMM 模型可用于分析复杂加劲结构的不同拉伸和压缩模量。此外,还进一步探讨了不同实验载荷条件下拉伸和压缩弹性模量比的影响,并讨论了弯曲和扭转对双模量结构的影响规律。相关结论为海洋工程中全尺寸复合材料结构的设计和优化提供了参考。
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引用次数: 0
Performance analysis of fiber-reinforced polypropylene composite laminates under quasi-static and super-sonic shock loading conditions for impact application 准静态和超音速冲击加载条件下纤维增强聚丙烯复合材料层压板在冲击应用中的性能分析
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-03-28 DOI: 10.1177/00219983241243070
Khushi Ram, Mohit Gupta, Kartikeya Kartikeya, Vikas Khatkar, Puneet Mahajan, Naresh Bhatnagar
In the present research, glass and basalt fiber-reinforced polypropylene composites’ behaviour in quasi-static and dynamic conditions is studied. Composites were fabricated by vacuum assisted Compression molding method. Composites failure under quasi-static tension and compressive conditions was studied along with its failure behaviour under low-velocity impact and super-sonic shock loading under dynamic conditions. The study results showed that basalt fiber-reinforced polypropylene (Basalt/PP) composite’s tensile and compressive strength is higher than glass fiber-reinforced polypropylene (Glass/PP). The Basalt/PP showed no penetration against low velocity impact (LVI) with negligible deformations till 50 J. However, the Glass/PP perforated at 50 J with various failure patterns occurring at back side. The fiber-matrix interface adhesion plays an important role in super-sonic shock loading by absorbing shock wave energy due to ductile nature of polypropylene and the two composites absorbed energy via matrix and fibers failure, no brittle failure of laminates occurred under shock loading.
本研究对玻璃纤维和玄武岩纤维增强聚丙烯复合材料在准静态和动态条件下的行为进行了研究。复合材料采用真空辅助压缩成型法制造。研究了复合材料在准静态拉伸和压缩条件下的失效情况,以及在动态条件下低速冲击和超音速冲击加载下的失效情况。研究结果表明,玄武岩纤维增强聚丙烯(Basalt/PP)复合材料的拉伸和压缩强度高于玻璃纤维增强聚丙烯(Glass/PP)。在低速冲击(LVI)下,玄武岩/聚丙烯没有穿透,50 J 的变形可以忽略不计,但玻璃/聚丙烯在 50 J 的冲击下穿孔,背面出现各种破坏形态。由于聚丙烯具有延展性,纤维与基体的界面粘附在超音速冲击载荷中起着吸收冲击波能量的重要作用,这两种复合材料通过基体和纤维的破坏吸收能量,在冲击载荷下,层压板没有发生脆性破坏。
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引用次数: 0
Expression of concern: “Effect of friction and shear strength enhancement on delamination prediction” 表达关切:"摩擦和剪切强度增强对分层预测的影响"
IF 2.9 3区 材料科学 Q3 MATERIALS SCIENCE, COMPOSITES Pub Date : 2024-03-26 DOI: 10.1177/00219983241242870
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引用次数: 0
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Journal of Composite Materials
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