Pub Date : 2024-04-24DOI: 10.1177/00219983241249707
Fatma Bakal Gumus, A. Yapici
Ballistic behaviours of hybrid composite armors were investigated through experiments. The effects of hexagonal boron nitride (h-BN) nanopowders and number of layers on ballistic performance were examined. Four types of armors were manufactured by hand lay-up and vacuum bagging technique: 60 layers of fabric (30 layers carbon and 30 layers basalt fabrics) with 0% h-BN (1-A) and 1% h-BN (1-B), also 100 layers of fabric (50 layers carbon and 50 layers basalt fabrics) with 0% h-BN (2-A) and 1% h-BN (2-B) with epoxy resin. Ballistic impact tests were performed on the armors using a 9 mm full metal jacket projectile. The densities of the ballistic plates are 1.53, 1.56, 1.61 and 1.65 respectively. After three shots to each plate, the average hole depths were 5.55 mm on the 1-A coded plate, 4.34 mm on the 1-B armor, 4.68 mm on the 2-A plate, and 4.69 mm on the 2-B armor. All of the armors were able to confront for the velocities between [Formula: see text] m/s successfully. However, the h-BN showed a significant influence on the overall ballistic performance of composite armors. It has been found that the penetration depth decreases with the addition of h-BN. Also SEM-EDS mapping and XRD analysis were used to characterize the hybrid composites.
{"title":"Ballistic behaviour of hybride carbon/basalt fiber reinforced epoxy-hBN composite","authors":"Fatma Bakal Gumus, A. Yapici","doi":"10.1177/00219983241249707","DOIUrl":"https://doi.org/10.1177/00219983241249707","url":null,"abstract":"Ballistic behaviours of hybrid composite armors were investigated through experiments. The effects of hexagonal boron nitride (h-BN) nanopowders and number of layers on ballistic performance were examined. Four types of armors were manufactured by hand lay-up and vacuum bagging technique: 60 layers of fabric (30 layers carbon and 30 layers basalt fabrics) with 0% h-BN (1-A) and 1% h-BN (1-B), also 100 layers of fabric (50 layers carbon and 50 layers basalt fabrics) with 0% h-BN (2-A) and 1% h-BN (2-B) with epoxy resin. Ballistic impact tests were performed on the armors using a 9 mm full metal jacket projectile. The densities of the ballistic plates are 1.53, 1.56, 1.61 and 1.65 respectively. After three shots to each plate, the average hole depths were 5.55 mm on the 1-A coded plate, 4.34 mm on the 1-B armor, 4.68 mm on the 2-A plate, and 4.69 mm on the 2-B armor. All of the armors were able to confront for the velocities between [Formula: see text] m/s successfully. However, the h-BN showed a significant influence on the overall ballistic performance of composite armors. It has been found that the penetration depth decreases with the addition of h-BN. Also SEM-EDS mapping and XRD analysis were used to characterize the hybrid composites.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140659470","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-23DOI: 10.1177/00219983241249238
Gen Li, Tianwei Wu, B. Sun, B. Gu
The effect of thermo-oxidative aging on mechanical properties is important to designing carbon fiber-reinforced composites serviced in long-term atmospheric environments. Here, we report the progressive bending damage behaviors of carbon fiber/epoxy 3D angle-interlock woven composites (3DAWCs) after thermo-oxidative aging. Three-point bending tests were conducted to characterize bending damage behaviors after different aging days. The electrical resistance change of 3DAWCs was also simultaneously measured with the two-probe method during three-point bending tests. Combining side image and digital image correlation (DIC) technology, we found that the bending strength and modulus deteriorated rapidly during thermo-oxidative aging. The strain distribution and progressive bending damage modes also changed significantly, i.e., a symmetrical strain distribution for the unaged specimens, while the existing interface cracks of the aged specimen changed this symmetry. The electrical resistance method (ERM) effectively identified the early-stage damages, and the first derivative of the rate of resistance change (FDC) revealed differences in the progressive damage modes of aged and unaged specimens.
{"title":"Effects of thermo-oxidative aging on progressive bending damages and electromechanical behaviors of carbon fiber/epoxy 3D woven composites","authors":"Gen Li, Tianwei Wu, B. Sun, B. Gu","doi":"10.1177/00219983241249238","DOIUrl":"https://doi.org/10.1177/00219983241249238","url":null,"abstract":"The effect of thermo-oxidative aging on mechanical properties is important to designing carbon fiber-reinforced composites serviced in long-term atmospheric environments. Here, we report the progressive bending damage behaviors of carbon fiber/epoxy 3D angle-interlock woven composites (3DAWCs) after thermo-oxidative aging. Three-point bending tests were conducted to characterize bending damage behaviors after different aging days. The electrical resistance change of 3DAWCs was also simultaneously measured with the two-probe method during three-point bending tests. Combining side image and digital image correlation (DIC) technology, we found that the bending strength and modulus deteriorated rapidly during thermo-oxidative aging. The strain distribution and progressive bending damage modes also changed significantly, i.e., a symmetrical strain distribution for the unaged specimens, while the existing interface cracks of the aged specimen changed this symmetry. The electrical resistance method (ERM) effectively identified the early-stage damages, and the first derivative of the rate of resistance change (FDC) revealed differences in the progressive damage modes of aged and unaged specimens.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-23","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140669979","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-21DOI: 10.1177/00219983241247910
Samet Ozyigit, Mostafa Mehdipour, A. Al-Nadhari, Arvin T Tabrizi, Semih Dogan, Kuray Dericiler, Bertan Beylergil, Mehmet Yildiz, B. S. Okan
Harnessing the potential of hexagonal boron nitride (h-BN) in epoxy composites for tailoring thermal conductivity is a promising avenue in materials science. However, achieving balanced enhancements in both in-plane and through-plane directions remains a challenge that requires innovative solutions. The primary objective of this research is to evaluate how thermal and mechanical characteristics of an epoxy matrix are affected by the size and amount of h-BN particles. To achieve this goal, h-BN particles with varying sizes (micro and nano) are incorporated into the epoxy matrix at different weight ratios spanning from 0.5 wt % to 20 wt % using a pre-dispersion technique. The epoxy composites reinforced with h-BN through a molding process exhibits enhanced mechanical and thermal performance in contrast to the pristine epoxy material. During the flexural test, acoustic emission data is collected to identify the initiation and progression of damage within the specimens under testing conditions. The most notable enhancement in thermal conductivity is observed when incorporating 20 wt% of micron-sized h-BN particles. This leads to a remarkable 107% increase in the in-plane direction and an impressive 112% increase in the through-plane direction. These results can be attributed to the formation of a three-dimensional thermally conductive network by the larger h-BN particles, which extends the path of phonon scattering. Furthermore, there are significant improvements in both flexural modulus and tensile modulus. Epoxy composites containing 10 wt% of micron-sized h-BN experiences an approximate 42% increase, while those with 20 wt% of the same particles displays a substantial 47% rise in these properties. This study effectively addresses the challenges associated with tailoring the thermal properties of epoxy composites, opening up new opportunities for applications in various industries, including electronics, aerospace and thermal management systems.
{"title":"A comprehensive experimental study on the effects of hexagonal boron nitride particle size and loading ratio on thermal and mechanical performance in epoxy composites","authors":"Samet Ozyigit, Mostafa Mehdipour, A. Al-Nadhari, Arvin T Tabrizi, Semih Dogan, Kuray Dericiler, Bertan Beylergil, Mehmet Yildiz, B. S. Okan","doi":"10.1177/00219983241247910","DOIUrl":"https://doi.org/10.1177/00219983241247910","url":null,"abstract":"Harnessing the potential of hexagonal boron nitride (h-BN) in epoxy composites for tailoring thermal conductivity is a promising avenue in materials science. However, achieving balanced enhancements in both in-plane and through-plane directions remains a challenge that requires innovative solutions. The primary objective of this research is to evaluate how thermal and mechanical characteristics of an epoxy matrix are affected by the size and amount of h-BN particles. To achieve this goal, h-BN particles with varying sizes (micro and nano) are incorporated into the epoxy matrix at different weight ratios spanning from 0.5 wt % to 20 wt % using a pre-dispersion technique. The epoxy composites reinforced with h-BN through a molding process exhibits enhanced mechanical and thermal performance in contrast to the pristine epoxy material. During the flexural test, acoustic emission data is collected to identify the initiation and progression of damage within the specimens under testing conditions. The most notable enhancement in thermal conductivity is observed when incorporating 20 wt% of micron-sized h-BN particles. This leads to a remarkable 107% increase in the in-plane direction and an impressive 112% increase in the through-plane direction. These results can be attributed to the formation of a three-dimensional thermally conductive network by the larger h-BN particles, which extends the path of phonon scattering. Furthermore, there are significant improvements in both flexural modulus and tensile modulus. Epoxy composites containing 10 wt% of micron-sized h-BN experiences an approximate 42% increase, while those with 20 wt% of the same particles displays a substantial 47% rise in these properties. This study effectively addresses the challenges associated with tailoring the thermal properties of epoxy composites, opening up new opportunities for applications in various industries, including electronics, aerospace and thermal management systems.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140678319","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-18DOI: 10.1177/00219983241247913
Daouda Nikiema, Pascale Balland, Alain Sergent
The 3D printing of continuous-fiber composites is currently relevant to engineers and researchers. This study aims to characterize and predict the mechanical properties of Onyx/glass fiber specimens printed using 3D printing. The work assesses the impact of glass fiber printing parameters on the mechanical behavior of printed parts and proposes analytical and numerical methods to predict mechanical properties. A physicochemical analysis was conducted on 3D printed continuous glass fibers. The study also investigated the impact of fiber printing parameters on composite parts. The results indicate that the 3D-printed glass fibers consist of nylon, continuous glass fibers, and voids (porosity), which range from 58% to 63%, 31% to 38%, and 5% to 8%, respectively. Mechanical characterizations indicate that printing fiber layers in blocks results in superior mechanical properties compared to printing alternating layers of glass fibers and Onyx. Additionally, the concentric mode of fiber printing can be challenging if the ‘start rotation’ parameter is not adjusted correctly. Premature specimen breakage occurred when fiber printing began within their useful length, resulting in a deformation at break that was approximately 34% less, depending on the starting position. The proposed analytical and numerical prediction methods had prediction errors of approximately 7% to 12% and 5% to 7%, respectively. Engineers can use these prediction approaches during the dimensioning phase of 3D printed composite parts.
{"title":"Study of 3D-printed onyx parts reinforced with continuous glass fibers: Focus on mechanical characterization, analytical prediction and numerical simulation","authors":"Daouda Nikiema, Pascale Balland, Alain Sergent","doi":"10.1177/00219983241247913","DOIUrl":"https://doi.org/10.1177/00219983241247913","url":null,"abstract":"The 3D printing of continuous-fiber composites is currently relevant to engineers and researchers. This study aims to characterize and predict the mechanical properties of Onyx/glass fiber specimens printed using 3D printing. The work assesses the impact of glass fiber printing parameters on the mechanical behavior of printed parts and proposes analytical and numerical methods to predict mechanical properties. A physicochemical analysis was conducted on 3D printed continuous glass fibers. The study also investigated the impact of fiber printing parameters on composite parts. The results indicate that the 3D-printed glass fibers consist of nylon, continuous glass fibers, and voids (porosity), which range from 58% to 63%, 31% to 38%, and 5% to 8%, respectively. Mechanical characterizations indicate that printing fiber layers in blocks results in superior mechanical properties compared to printing alternating layers of glass fibers and Onyx. Additionally, the concentric mode of fiber printing can be challenging if the ‘start rotation’ parameter is not adjusted correctly. Premature specimen breakage occurred when fiber printing began within their useful length, resulting in a deformation at break that was approximately 34% less, depending on the starting position. The proposed analytical and numerical prediction methods had prediction errors of approximately 7% to 12% and 5% to 7%, respectively. Engineers can use these prediction approaches during the dimensioning phase of 3D printed composite parts.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-18","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140630100","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-16DOI: 10.1177/00219983241248754
Benoit Vieille, Alexis Coppalle
This study investigates the influence of a combined thermal heat flux (imposed by a cone calorimeter) and a compressive loading on the deformation and damage mechanisms within quasi-isotropic carbon fibers reinforced PolyEtherEther Ketone laminates. Thermogravimetric Analyses conducted at increasing heating rates under nitrogen (from 5 to 500°C/min) provide valuable information on the thermal decomposition of C/PEEK that ranges from 550°C to 627°C, with a corresponding mass loss ranging from 20 to 26%. From the thermo-mechanical coupling standpoint, the softening and the thermal decomposition of the PEEK matrix under a 50 kW/m2 heat flux result in the micro-buckling of fibers bundles in matrix-rich areas at the ply scale. Ultimately, it leads to the formation and propagation in the transverse direction of plastic kink bands at the laminates scale. Post-failure observations show that this macroscopic kinking propagates specifically according to the PEEK matrix pyrolysis.
{"title":"In situ compressive behavior of carbon fibers reinforced PolyEtherEther Ketone laminates exposed to one-sided heat flux","authors":"Benoit Vieille, Alexis Coppalle","doi":"10.1177/00219983241248754","DOIUrl":"https://doi.org/10.1177/00219983241248754","url":null,"abstract":"This study investigates the influence of a combined thermal heat flux (imposed by a cone calorimeter) and a compressive loading on the deformation and damage mechanisms within quasi-isotropic carbon fibers reinforced PolyEtherEther Ketone laminates. Thermogravimetric Analyses conducted at increasing heating rates under nitrogen (from 5 to 500°C/min) provide valuable information on the thermal decomposition of C/PEEK that ranges from 550°C to 627°C, with a corresponding mass loss ranging from 20 to 26%. From the thermo-mechanical coupling standpoint, the softening and the thermal decomposition of the PEEK matrix under a 50 kW/m<jats:sup>2</jats:sup> heat flux result in the micro-buckling of fibers bundles in matrix-rich areas at the ply scale. Ultimately, it leads to the formation and propagation in the transverse direction of plastic kink bands at the laminates scale. Post-failure observations show that this macroscopic kinking propagates specifically according to the PEEK matrix pyrolysis.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-16","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140617704","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-15DOI: 10.1177/00219983241248216
Till Hermann, Dariusz Niedziela, Diyora Salimova, Timo Schweiger
The injection molding simulation of short fiber reinforced plastics (SFRP) is time consuming. However, until now it is necessary for predicting the local fiber orientation, to optimize the molding process and to predict the mechanical behavior of the material. This research presents the capabilities of artificial neural networks (NN) in predicting fiber orientation tensor (FOT) during injection molding processes, with a focus on enhancing computational efficiency compared to traditional simulation methods. Three NN architectures are compared based on simulated injection molded plates, with the goal of predicting the effect of the plate geometry on the local fiber orientation. Results indicate that NN outperform the baseline assumption of aligned fibers and demonstrate significant potential for accurate FOT prediction. The computational efficiency of NN, especially during the prediction phase, showcases a reduction in processing time by a factor of 104 compared to traditional simulation methods. This research lays a foundation for further exploration into the feasibility of NN in partly replacing time-consuming simulations for practical applications in injection molding processes.
短纤维增强塑料(SFRP)的注塑成型模拟非常耗时。然而,迄今为止,它对于预测局部纤维取向、优化成型工艺和预测材料的机械性能是非常必要的。本研究介绍了人工神经网络(NN)在注塑成型过程中预测纤维取向张量(FOT)的能力,重点是与传统模拟方法相比提高计算效率。以模拟注塑成型板为基础,比较了三种 NN 架构,目的是预测板的几何形状对局部纤维取向的影响。结果表明,NN 优于对齐纤维的基线假设,并展示了准确预测 FOT 的巨大潜力。NN 的计算效率,尤其是在预测阶段,与传统模拟方法相比,减少了 104 倍的处理时间。这项研究为进一步探索 NN 在注塑成型工艺实际应用中部分取代耗时模拟的可行性奠定了基础。
{"title":"Predicting the fiber orientation of injection molded components and the geometry influence with neural networks","authors":"Till Hermann, Dariusz Niedziela, Diyora Salimova, Timo Schweiger","doi":"10.1177/00219983241248216","DOIUrl":"https://doi.org/10.1177/00219983241248216","url":null,"abstract":"The injection molding simulation of short fiber reinforced plastics (SFRP) is time consuming. However, until now it is necessary for predicting the local fiber orientation, to optimize the molding process and to predict the mechanical behavior of the material. This research presents the capabilities of artificial neural networks (NN) in predicting fiber orientation tensor (FOT) during injection molding processes, with a focus on enhancing computational efficiency compared to traditional simulation methods. Three NN architectures are compared based on simulated injection molded plates, with the goal of predicting the effect of the plate geometry on the local fiber orientation. Results indicate that NN outperform the baseline assumption of aligned fibers and demonstrate significant potential for accurate FOT prediction. The computational efficiency of NN, especially during the prediction phase, showcases a reduction in processing time by a factor of 10<jats:sup>4</jats:sup> compared to traditional simulation methods. This research lays a foundation for further exploration into the feasibility of NN in partly replacing time-consuming simulations for practical applications in injection molding processes.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570111","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-15DOI: 10.1177/00219983241244882
Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick
This study presents an investigation into mechanical and thermal properties, as well as the microstructure of Automated Fiber Placement-manufactured laminates using a novel carbon fiber-reinforced low-melt polyaryl ether ketone polymer material. The material’s lower melting temperature and lower melt viscosity as compared to established high-temperature thermoplastic materials as PEEK, promises favourable characteristics for the Automated Fiber Placement process. This work aims at in-situ consolidation and the influence of a heated tooling and a post process tempering step, which both turned out to be promising in previous investigations. Laminates were manufactured using a cold tooling, a heated tooling configuration, a cold tooling with a subsequent tempering process step and a hot-pressed reference laminate. Differential Scanning Calorimetry showed that crystallinity values more than doubled for the heated tooling and post process tempering configurations, compared to the cold tooling, reaching 24% and 30%, respectively. Mechanical strength values showed an increase in interlaminar shear strength and compression strength but did not increase to the same extent as was expected from the increase in crystallinity. With Scanning Electron Microscopy differences in the microscopic structure of the polymer matrix could be detected. While the post process tempering step leads to a mostly lamellar crystalline structure, the heated tooling configuration and the post process hot pressing induce a predominance of crystalline spherulites, which might positively affect the mechanical performance. Computed Tomography scans revealed a high amount of porosity in the in-situ-manufactured samples and unprocessed tape material, which likely mitigated the positive effect of increased crystallinity.
{"title":"Characteristics of in-situ automated fiber placement carbon-fiber-reinforced low-melt polyaryl ether ketone laminates part 1: Manufacturing influences","authors":"Ines Mössinger, Lukas Raps, Daniel Fricke, Jonathan Freund, Miriam Löbbecke, Ashley R Chadwick","doi":"10.1177/00219983241244882","DOIUrl":"https://doi.org/10.1177/00219983241244882","url":null,"abstract":"This study presents an investigation into mechanical and thermal properties, as well as the microstructure of Automated Fiber Placement-manufactured laminates using a novel carbon fiber-reinforced low-melt polyaryl ether ketone polymer material. The material’s lower melting temperature and lower melt viscosity as compared to established high-temperature thermoplastic materials as PEEK, promises favourable characteristics for the Automated Fiber Placement process. This work aims at in-situ consolidation and the influence of a heated tooling and a post process tempering step, which both turned out to be promising in previous investigations. Laminates were manufactured using a cold tooling, a heated tooling configuration, a cold tooling with a subsequent tempering process step and a hot-pressed reference laminate. Differential Scanning Calorimetry showed that crystallinity values more than doubled for the heated tooling and post process tempering configurations, compared to the cold tooling, reaching 24% and 30%, respectively. Mechanical strength values showed an increase in interlaminar shear strength and compression strength but did not increase to the same extent as was expected from the increase in crystallinity. With Scanning Electron Microscopy differences in the microscopic structure of the polymer matrix could be detected. While the post process tempering step leads to a mostly lamellar crystalline structure, the heated tooling configuration and the post process hot pressing induce a predominance of crystalline spherulites, which might positively affect the mechanical performance. Computed Tomography scans revealed a high amount of porosity in the in-situ-manufactured samples and unprocessed tape material, which likely mitigated the positive effect of increased crystallinity.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-15","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570093","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-12DOI: 10.1177/00219983241246615
Renaud Metz, Sofiane Terzi, Barbara Fayard, Jean-Louis Bantignies, Mehrdad Hassanzadeh
The correlations between the electrical behavior and microstructural properties of samples consisting of particle composites fabricated from SiC particles embedded in a silicone matrix, were investigated using X-ray computed tomography. In the voltage field range 200-1000 V/mm, the measured conductivity as a function of SiC volume fraction exhibits two distinct gaps. Upon further investigations, we attribute these observations to percolation thresholds at the microscale. The first gap, corresponding to interconnections between SiC particles that were originally disconnected, is more significant at higher voltage; while the second one, resulting from shortening conductivity pathways between the external surfaces of the samples with the increase of SiC volume fraction, seems more sensitive to lower voltages and is correlated with a decrease of the tortuosity of the percolated SiC network.
利用 X 射线计算机断层扫描技术研究了由嵌入硅酮基质中的碳化硅颗粒制成的颗粒复合材料样品的电气行为与微观结构特性之间的相关性。在 200-1000 V/mm 的电压场范围内,测得的电导率与碳化硅体积分数的函数关系呈现出两种截然不同的差距。经过进一步研究,我们将这些观察结果归因于微尺度的渗流阈值。第一个间隙与原本断开的 SiC 颗粒之间的相互连接相对应,在电压较高时更为显著;而第二个间隙则是由于随着 SiC 体积分数的增加,样品外表面之间的导电路径缩短而产生的,似乎对较低的电压更为敏感,并与渗滤 SiC 网络的曲折性降低相关。
{"title":"Contribution to the percolation threshold study of Silicon carbide filled polydimethylsiloxane composites used for field grading application","authors":"Renaud Metz, Sofiane Terzi, Barbara Fayard, Jean-Louis Bantignies, Mehrdad Hassanzadeh","doi":"10.1177/00219983241246615","DOIUrl":"https://doi.org/10.1177/00219983241246615","url":null,"abstract":"The correlations between the electrical behavior and microstructural properties of samples consisting of particle composites fabricated from SiC particles embedded in a silicone matrix, were investigated using X-ray computed tomography. In the voltage field range 200-1000 V/mm, the measured conductivity as a function of SiC volume fraction exhibits two distinct gaps. Upon further investigations, we attribute these observations to percolation thresholds at the microscale. The first gap, corresponding to interconnections between SiC particles that were originally disconnected, is more significant at higher voltage; while the second one, resulting from shortening conductivity pathways between the external surfaces of the samples with the increase of SiC volume fraction, seems more sensitive to lower voltages and is correlated with a decrease of the tortuosity of the percolated SiC network.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-12","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140569999","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
A single-layer and double-layer corrugated core sandwich structure consisting of carbon fibre–reinforced polymer (CFRP) panels and aluminium alloy core layers was designed. Numerical simulations were carried out in HyperMesh/LsDyna, and the simulation results of single-layer and double-layer corrugated sandwich structure were compared with the experimental results to verify the reliability of the proposed numerical model. Compared with the results of single-layer and double-layer corrugated sandwich structure, the superiority of a double-layer corrugated sandwich structure in anti-collision performance is verified. Considering the effects of impact energy and impact position on impact force, energy absorption capacity, and failure mode, a series of low-velocity impact finite element simulations was carried out. It was found that the main failure mode of composite laminates included fibre damage, matrix damage and delamination, and core buckling. At the same impact position, the higher the impact energy, the greater the initial slopes of the contact force-time and absorbed energy-time curves, the higher the peak force, and the larger the energy absorption capacity. Under the same impact energy, when the impactor hit the wave crest of the sandwich structure, the damage to the structure was small; however, the maximum impact force on the structure was large (∼8 kN).
{"title":"Dynamic responses and interactive failure mechanisms of carbon fiber composite face sheets/double-layer corrugated core sandwich structures under low-velocity impacts loading","authors":"Hangyan Wang, Jiayou Guo, Guangguang Zhang, Shuiting Zhou, Liange Ouyang","doi":"10.1177/00219983241246109","DOIUrl":"https://doi.org/10.1177/00219983241246109","url":null,"abstract":"A single-layer and double-layer corrugated core sandwich structure consisting of carbon fibre–reinforced polymer (CFRP) panels and aluminium alloy core layers was designed. Numerical simulations were carried out in HyperMesh/LsDyna, and the simulation results of single-layer and double-layer corrugated sandwich structure were compared with the experimental results to verify the reliability of the proposed numerical model. Compared with the results of single-layer and double-layer corrugated sandwich structure, the superiority of a double-layer corrugated sandwich structure in anti-collision performance is verified. Considering the effects of impact energy and impact position on impact force, energy absorption capacity, and failure mode, a series of low-velocity impact finite element simulations was carried out. It was found that the main failure mode of composite laminates included fibre damage, matrix damage and delamination, and core buckling. At the same impact position, the higher the impact energy, the greater the initial slopes of the contact force-time and absorbed energy-time curves, the higher the peak force, and the larger the energy absorption capacity. Under the same impact energy, when the impactor hit the wave crest of the sandwich structure, the damage to the structure was small; however, the maximum impact force on the structure was large (∼8 kN).","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570264","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}
Pub Date : 2024-04-10DOI: 10.1177/00219983241246614
Hocine Heraiz, Chouki Farsi, Hocine Makri, Salah Amroune, Ahmed Belaadi, Khalissa Saada, Moussa Zaoui, Mohammed Ismail Beddiar
This study assesses the impact of alkaline treatments and volume fractions on biocomposites composed of a high-density polyethylene (HDPE) matrix reinforced with date palm tree fibers (FPDS). Tensile tests were conducted on both untreated and NaOH-treated biocomposites. Additionally, fiber analysis was performed using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results reveal higher strength and stiffness compared to HDPE, albeit with limited plasticity making the material brittle. The NaOH treatment enhances certain mechanical properties. Further assessments encompassed hardness, density, melt index, and Izod impact tests. Two volume fractions, 20% and 25%, of FPDS were tested. The study establishes a correlation between empirical predictions and artificial neural network (ANN) models. Notably, an ANN architecture consisting of two input factors, 10 hidden nodes, and one output provides the analysis of mechanical properties. This investigation highlights the potential of FPDS-reinforced HDPE biocomposites, emphasizing their mechanical performance under various treatments and fiber levels.
{"title":"Assessment of mechanical and physicochemical properties of palm fiber composites: Effect of alkaline treatment and volume alterations","authors":"Hocine Heraiz, Chouki Farsi, Hocine Makri, Salah Amroune, Ahmed Belaadi, Khalissa Saada, Moussa Zaoui, Mohammed Ismail Beddiar","doi":"10.1177/00219983241246614","DOIUrl":"https://doi.org/10.1177/00219983241246614","url":null,"abstract":"This study assesses the impact of alkaline treatments and volume fractions on biocomposites composed of a high-density polyethylene (HDPE) matrix reinforced with date palm tree fibers (FPDS). Tensile tests were conducted on both untreated and NaOH-treated biocomposites. Additionally, fiber analysis was performed using scanning electron microscopy (SEM) and X-ray diffraction (XRD). The results reveal higher strength and stiffness compared to HDPE, albeit with limited plasticity making the material brittle. The NaOH treatment enhances certain mechanical properties. Further assessments encompassed hardness, density, melt index, and Izod impact tests. Two volume fractions, 20% and 25%, of FPDS were tested. The study establishes a correlation between empirical predictions and artificial neural network (ANN) models. Notably, an ANN architecture consisting of two input factors, 10 hidden nodes, and one output provides the analysis of mechanical properties. This investigation highlights the potential of FPDS-reinforced HDPE biocomposites, emphasizing their mechanical performance under various treatments and fiber levels.","PeriodicalId":15489,"journal":{"name":"Journal of Composite Materials","volume":null,"pages":null},"PeriodicalIF":2.9,"publicationDate":"2024-04-10","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":null,"resultStr":null,"platform":"Semanticscholar","paperid":"140570002","PeriodicalName":null,"FirstCategoryId":null,"ListUrlMain":null,"RegionNum":3,"RegionCategory":"材料科学","ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":"","EPubDate":null,"PubModel":null,"JCR":null,"JCRName":null,"Score":null,"Total":0}