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Absorbable Organic Halide Reduction Research in Elemental Chlorine-Free Bleaching of Eucalyptus Kraft Pulp 桉木硫酸盐浆无氯漂白中可吸收有机卤化物的还原研究
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/S1/1
Shuangquan Yao, Huixia Zhu Lei Jiang Shuangxi Nie Chengrong Qin Cong Gao, Chen Liang
The parameters of elemental chlorine-free (ECF) bleaching (D0EpD1) of eucalyptus kraft pulp were optimized to reduce AOX formation. The optimal conditions were pulp concentration 10%, ClO2 dosage 2.8%, pH 3.5, temperature 60°C, time 60 min at D0; H2O2 dosage 1.25%, alkali dosage 2.0%, temperature 65°C, time 105 min at Ep; ClO2 dosage 0.2%, pH 4.5, temperature 60°C, time 55 min at D1. AOX formation was 0.553 kg.tp–1, each stage was 0.470 kg.tp–1, 0.060 kg.tp–1 and 0.023 kg.tp–1, respectively. Compared with un-optimized AOX formation decreased by 23.7%.The brightness and viscosity was 84.36% ISO, 834.6 mL.g–1. In fact, good quality of the pulp was obtained when AOX formation has fallen dramatically. These provide a theoretical basis for reducing the produce of AOX and realizing the clean bleaching.
对桉木硫酸盐浆进行无元素氯漂白(ECF)工艺参数优化,以减少AOX的生成。最佳条件为纸浆浓度10%,ClO2用量2.8%,pH 3.5,温度60℃,时间60 min, D0;H2O2用量1.25%,碱用量2.0%,温度65℃,时间105 min;ClO2投加量0.2%,pH值4.5,温度60℃,D1下时间55 min。AOX形成量为0.553 kg。Tp-1,每级0.470 kg。Tp-1, 0.060千克。Tp-1和0.023 kg。分别tp-1。与未优化的AOX地层相比,降低了23.7%。亮度和粘度为84.36% ISO, 834.6 mL.g-1。事实上,当AOX形成量急剧下降时,获得了良好的纸浆质量。为减少AOX的产生,实现清洁漂白提供了理论依据。
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引用次数: 2
Influence of Polymeric Sand Porous Material on the Aerodynamic Effect when a High-Speed Train is Entering into a Tunnel 聚合物砂多孔材料对高速列车入洞气动效应的影响
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/S1/13
Luo Jian-jun
In order to effectively reduce the compression wave in tunnel and the micro pressure wave at the exit of tunnel, improve the comfort of passengers, this study put forward laying polymeric sand porous material in tunnel by using the sound absorption properties of porous media, and give the numerical simulation calculation method of the aerodynamic effect of three-dimensional compressible, viscous and unsteady flow field when a high-speed train entering into a tunnel, furthermore, the influence of sound absorption board on the aerodynamic effect in tunnel was studied. Theoretical analysis and numerical results show the compression wave in tunnel and the micro pressure wave at the exit of tunnel can be decreased significantly when pasting porous materials in tunnel. The reason is mainly due to there are lots of micro-pores in the material and it could absorb the energy from compression wave, then the peak value of it and pressure gradient are decreased. Secondly, the method of laying polymeric sand sound absorption material has influence on the change of the pressure in the tunnel and the micro pressure wave at the exit of tunnel. When the length and height of sound absorption materials are same, calculation results show that the best pressure reduction effect is achieved when laying the material at the entrance of tunnel. However, when laying the material at different circumferential positions of tunnel, the pressure reduction effect at haunch is better than vault and spandrel. Based on that, considering the pressure noise reduction problem, material cost and height of construction in practical engineering, when laying the material at haunch, the relationship between the reduction effect of pressure gradient and the length of laying is summarized with 3 different speeds, which have certain reference value for the design of the method of laying sound absorption material in tunnel.
为了有效降低隧道内的压缩波和隧道出口处的微压力波,提高乘客的舒适度,本文利用多孔介质的吸声特性,提出了在隧道内铺设聚合物砂多孔材料,并给出了高速列车进入隧道时三维可压缩、粘性和非定常流场气动效应的数值模拟计算方法。研究了吸声板对隧道内气动效果的影响。理论分析和数值计算结果表明,在隧道内粘贴多孔材料可以显著降低隧道内的压缩波和隧道出口的微压力波。这主要是由于材料中存在大量的微孔,可以吸收压缩波的能量,从而降低压缩波的峰值和压力梯度。其次,聚合物砂吸声材料的铺设方式对隧道内压力和隧道出口微压力波的变化有影响。计算结果表明,在吸声材料长度和高度相同的情况下,在隧洞入口处敷设吸声材料降压效果最好。但在隧道不同周向位置敷设材料时,后腰处的降压效果优于拱顶和拱肩。在此基础上,考虑到实际工程中降压降噪问题、材料成本和施工高度,在尾部铺设材料时,以3种不同的速度,总结了压力梯度降压效果与铺设长度之间的关系,对隧道吸声材料铺设方法的设计具有一定的参考价值。
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引用次数: 1
3D Graphene/Cu2O Nanocomposite as a Highly Efficient Sorbent and Photocatalysis 三维石墨烯/Cu2O纳米复合材料作为高效吸附剂和光催化
Pub Date : 2017-01-01 DOI: 10.12783/issn.1544-8053/14/S1/18
Boye Zhou, Yan Wu
There-dimensional graphene (3DG)/Cu2O nanocomposites are prepared using one-pot template-free solvent-thermal synthesis route with (CH3COO)2Cu·H2O as a precursor. The cube Cu2O nanoparticles are deposited on the spongy nanosheets of 3DG. The adsorbent experiment reveals that the 3DG/Cu2O has a adsorption rate of 83.34% which is 14 times higher than that of pure Cu2O. Using photocatalytic degradation of methyl orange (MO) under visible-light illumination to investigate the photocatalytic activity of 3DG/Cu2O. The prepared 3DG/Cu2O particles exhibited a higher photo-degradation capability than Cu2O. The superior activity of 3DG/Cu2O for MO decomposition can be attributed to not only its nanoporous structure and large specific surface area, but also the strong interaction between 3DG and Cu2O from in-situ synthesis.
以(CH3COO)2Cu·H2O为前驱体,采用一锅无模板溶剂-热合成的方法制备了三维石墨烯(3DG)/Cu2O纳米复合材料。立方体Cu2O纳米颗粒沉积在海绵状的3DG纳米片上。吸附剂实验表明,3DG/Cu2O的吸附率为83.34%,是纯Cu2O的14倍。采用可见光下光催化降解甲基橙(MO)的方法研究了3DG/Cu2O的光催化活性。制备的3DG/Cu2O颗粒具有比Cu2O更高的光降解能力。3DG/Cu2O具有优异的MO分解活性,除了其纳米孔结构和较大的比表面积外,还与原位合成的3DG/Cu2O之间的强相互作用有关。
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引用次数: 1
Preparation, Microstructure and Properties of Environmentally Friendly Sn-58Bi Eutectic Solder Ribbon for Electronic Package 电子封装用环保Sn-58Bi共晶焊料带的制备、微观结构与性能
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/1/32
Lan‐Lan Zhu, Shengfa Liu, W. Xiong, J. Xiong, Zhebing Hu, Chen Chen
Sn-58Bi eutectic solder ribbon was successfully prepared using an improved single-roller rapid solidification device with the optimum process parameters. The microstructure, melting behavior and wettability of Sn-58Bi eutectic solder ribbon prepared by rapid solidification technology (RST) and conventional casting-rolling process (CRP) respectively were investigated by optical microscopy (OM), differential scanning calorimetry (DSC) and wettability tests. The results show that the forming effect of solder ribbons can be obviously improved by mainly optimizing roller line speed, nozzle-to-roller spacing and heating temperature. Sn-58Bi eutectic solder ribbon prepared by RST has finer microstructure, lower solidus temperature and more excellent wettability than that of the ribbon prepared by CRP. Therefore, the study of Sn-58Bi eutectic solder ribbon is conducive to cut cost, meet growing performance requirements, and reduce lead contamination for electronic package industry.
采用改进的单辊快速凝固装置,优化工艺参数,成功制备了Sn-58Bi共晶焊料带。采用光学显微镜(OM)、差示扫描量热法(DSC)和润湿性试验研究了快速凝固技术(RST)和常规铸轧工艺(CRP)制备的Sn-58Bi共晶焊料带的显微组织、熔化行为和润湿性。结果表明,通过优化辊速、喷嘴与辊间距和加热温度,可以明显改善焊带的成形效果。RST制备的Sn-58Bi共晶焊点带比CRP制备的焊点带具有更细的组织、更低的固相温度和更优异的润湿性。因此,研究Sn-58Bi共晶焊料带有利于电子封装行业降低成本,满足日益增长的性能要求,减少铅污染。
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引用次数: 0
Enhancement of Anti-inflammatory Activities of Aronia melanocarpa through High-pressure Homogenization Process 高压均质工艺增强黑檀抗炎活性
Pub Date : 2017-01-01 DOI: 10.12783/issn.1544-8053/14/1/23
H. Lee
It was first confirmed that the increase of anti-inflammatory activities of Aronia melanocarpa from high-pressure homogenization at 25,000 psi and 25°C was caused by the three times higher extraction of very heat-labile cyanidin-3-O-galactoside (C3G), a bioactive anthocyanin existing in A. melanocarpa, than that of conventional 70% ethanol extraction at 80°C. The extracts from this process showed better efficacies in suppressing the production of both nitric oxide and the cytokines, IL-6 and TNF-α, and resulted in high liver weight gain in mice. This result could be employed to extract other heat-sensitive components from various bioresources.
首先证实,在25000 psi和25°C高压均质条件下,黑果野莓抗炎活性的增强是由于在80°C条件下提取的非常热不稳定的花青素-3- o -半乳糖苷(C3G)比传统的70%乙醇提取高3倍。该工艺的提取物对一氧化氮和细胞因子IL-6、TNF-α的产生均有较好的抑制作用,并导致小鼠肝脏增重。该结果可用于从各种生物资源中提取其他热敏成分。
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引用次数: 0
Effect of Lithium Slag on Drying Shrinkage of Concrete with Manufactured-sand 锂渣对制砂混凝土干缩的影响
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/1/21
Zhi-hai He, Yanfei Wu, Yueqing Gao
In order to comprehensively grasp the effect of lithium slag on the properties of concrete and promote the application of lithium slag in concrete, the effect of lithium slag on drying shrinkage of concrete with manufactured-sand was studied by testing drying shrinkage of concrete with manufactured-sand at different ages. The corresponding effect mechanism was also analyzed by water retention of the corresponding mortar and the pore structure of concrete which was obtained by evaporable water test. The results indicate that 15% and 30% lithium slag decrease effectively the drying shrinkage of concrete with manufactured-sand, and with the increase of the content of lithium slag, the decrease effect is better. When the content of lithium slag is increased to be 45%, the drying shrinkage of the concrete is increased. The smaller pores correspond to the higher water retention to decrease the drying shrinkage of manufactured-sand concrete with the appropriate content of lithium slag.
为了全面掌握锂渣对混凝土性能的影响,促进锂渣在混凝土中的应用,通过对不同龄期的制砂混凝土的干缩试验,研究了锂渣对制砂混凝土干缩的影响。通过相应砂浆的保水性和可蒸发水试验得到的混凝土孔隙结构,分析了相应的作用机理。结果表明,15%和30%的锂渣能有效降低制砂混凝土的干缩,且随着锂渣掺量的增加,降低效果更好。当锂渣掺量增加到45%时,混凝土的干缩率增大。适当掺量的锂渣,孔隙越小,保水性越高,可降低成品砂混凝土的干燥收缩率。
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引用次数: 3
Solar Water Purification System Design: Application Study in Lake Taihu, China 太阳能净水系统设计:在太湖的应用研究
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/1/43
Zhenwei You, Jian Liu Shun Zhang Wei Sun Yi Zheng, W. Ho
Through investigation and comparison of the methods of water purification, salvage and aeration were confirmed to be the most effective methods in treating the pollution in Lake Taihu. A solar water purification system was designed to achieve the effects of salvage and aeration. To collect algae as “salvage,” this purification system employed a combination of a water pump and filter screen. To increase the dissolved oxygen, the water pump lifted water and sprayed it into the air, and an air pump was equipped to inject oxygen bubbles into the water. After a one-year test at Lake Taihu, the effectiveness of this purification system was confirmed. It could effectively lower the levels of permanganate, NH3 4 NH+ / , and chlorophyll a and increase the level of dissolved oxygen in the lake water.
通过对水质净化方法的调查和比较,确定了打捞和曝气是处理太湖污染最有效的方法。设计了一种太阳能水净化系统,以达到打捞和曝气的效果。为了收集藻类作为“回收物”,这个净化系统采用了水泵和过滤器的组合。为了增加溶解氧,水泵将水提起并喷射到空气中,并配备气泵向水中注入氧气气泡。经过为期一年的太湖试验,该净化系统的有效性得到了证实。它能有效降低高锰酸盐、nh34 NH+ /和叶绿素a的含量,提高湖水溶解氧的含量。
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引用次数: 2
Association of Carbon Emissions and Expressway Longitudinal Slope in Northern China 中国北方高速公路纵向坡度与碳排放的关系
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/1/22
Xingli Jia, Jinliang Xu, Xingliang Liu
In Northern China, heavy trucks are common on highways. Vehicles traveling on longitudinal sections of expressways produce higher carbon emissions. Current carbon emission models include the vehicular operating conditions, but do not reveal the influence of highway alignment conditions, such as the longitudinal gradient and slope length, on emissions. To address this problem, this study attempts to relate the design parameters of longitudinal roadway segments with carbon emissions, as derived from diesel fuel consumption data, using an iterative nonlinear multiple regression method. Diesel fuel consumption data were collected through field tests along two typical overloaded expressways in China’s coal-producing regions. The associated carbon emission data were calculated using the method defined by the Intergovernmental Panel on Climate Change. Using this data, a carbon emission prediction model was developed that related carbon emissions with roadway segment gradients, segment slope length, and initial vehicle speed. The proposed model was verified using the field test data. A relative error of 4.9% between predicted and observed data suggested high accuracy and applicability for the proposed prediction model.
在中国北方,重型卡车在高速公路上随处可见。在高速公路纵向路段行驶的车辆产生更高的碳排放。目前的碳排放模型包括车辆运行工况,但没有揭示公路线形条件(如纵向坡度和坡度长度)对排放的影响。为了解决这一问题,本研究尝试使用迭代非线性多元回归方法,将纵向路段的设计参数与柴油油耗数据的碳排放联系起来。柴油消耗数据是通过中国产煤地区两条典型超载高速公路的实地测试收集的。相关的碳排放数据是使用政府间气候变化专门委员会定义的方法计算的。利用该数据,建立了碳排放预测模型,将碳排放与路段坡度、路段坡度长度和初始车速相关联。利用现场试验数据对模型进行了验证。预测值与观测值的相对误差为4.9%,表明该预测模型具有较高的准确性和适用性。
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引用次数: 4
A New DGA Based Transformer Fault Diagnosis Scheme Suitable for Time-Series Fault Data 一种适用于时序故障数据的基于DGA的变压器故障诊断新方案
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/S1/21
Yongliang Liang, Kejun Li
The quality of original data is crucial to the performance of diagnosis model. To improve the performance of transformer diagnosis model based on Dissolved Gas Analysis (DGA), a new diagnosis scheme suitable for time-series dissolved gas data is proposed in this paper. After the analysis of traditional transformer diagnosis architecture, a fault data extraction step is added to the architecture to improve the quality of original fault data. The fault data extraction step is mainly composed of two parts, invalid data correction and determination of possible initial fault time based on fault early warning. Finally, the numerical results validate that the accuracy and sensitivity of DGA based fault diagnosis for the transformer are improved by extracting fault feature of time-series data.
原始数据的质量对诊断模型的性能至关重要。为了提高基于溶解气体分析(DGA)的变压器诊断模型的性能,提出了一种适用于时间序列溶解气体数据的变压器诊断方案。在分析传统变压器诊断体系结构的基础上,增加故障数据提取步骤,提高原始故障数据的质量。故障数据提取步骤主要由无效数据的校正和基于故障预警的可能初始故障时间的确定两部分组成。最后,通过对时序数据进行故障特征提取,提高了基于DGA的变压器故障诊断的精度和灵敏度。
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引用次数: 0
Effects of Different Land Use on Soil Bacterial Functional Diversity in Sanjiang Plain, Northeast China 三江平原不同土地利用方式对土壤细菌功能多样性的影响
Pub Date : 2017-01-01 DOI: 10.12783/ISSN.1544-8053/14/1/12
Wang Jifen
To investigate the bacterial functional diversity regarding soil carbon metabolism in Sanjiang Plain wetlands, the top soils (0–20 cm) of three different land use types were collected in Sanjiang Plain, China. The distribution and variation of carbon source utilization was assessed by the Biolog microplate method. The results showed that the physicochemical properties of the soil were significantly different between the three land use types, wetland, farmland and forest (P 0.05). Principal component analysis (PCA) indicated that soil bacterial carbon utilization revealed obvious spatial variation, suggesting the bacterial metabolism diversity could be reflected in the use of carbohydrates, amino acids and carboxylic acids, particularly carbohydrates. In addition, soil physicochemical properties and vegetation composition were important factors modifying soil bacterial composition and functional activity in different land use types.
为研究三江平原湿地土壤碳代谢的细菌功能多样性,以三江平原3种不同土地利用类型的表层土壤(0 ~ 20 cm)为研究对象。采用Biolog微孔板法评价碳源利用的分布和变化。结果表明:湿地、农田和森林3种土地利用类型土壤理化性质差异显著(P < 0.05);主成分分析(PCA)表明,土壤细菌对碳的利用存在明显的空间差异,表明细菌对碳水化合物、氨基酸和羧酸的利用具有多样性,尤其是碳水化合物。土壤理化性质和植被组成是影响不同土地利用类型土壤细菌组成和功能活性的重要因素。
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引用次数: 7
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Journal of Residuals Science & Technology
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