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Characterization of ceramics based on laser speckle photometry 基于激光散斑光度法的陶瓷表征
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-10-20 DOI: 10.5194/jsss-9-345-2020
Lili Chen, U. Cikalova, B. Bendjus, S. Muench, M. Roellig
Abstract. Advanced ceramic components are frequently used inindustrial applications. As a brittle material, ceramic reacts very suddenly to excessively high stresses. Existing defects lead to rapid crack growth followed by spontaneous destruction. This leads to a functional failure of the entire component. It is therefore important to develop innovative techniques to ensure a good quality condition of ceramic products. Laser speckle photometry (LSP) is an optical nondestructive testing method. It is based on the dynamic analysis of time-resolved speckle patterns that are generated by an external excitation. In this paper, we will present two investigations on ceramic components using the LSP technique. One is the nondestructive stress characterization on ceramic surfaces, and the other is the defect detection on ceramics components. The aim is to improve the quality and safety control of ceramic production in the challenging industrial field. Preliminary results have shown the potential of the LSP sensor system for the nondestructive characterization of ceramics in terms of stress monitoring and surface defect detection.
摘要先进的陶瓷元件经常用于工业应用。作为一种脆性材料,陶瓷对过高的应力反应非常突然。现有缺陷导致裂纹快速扩展,随后自发破坏。这将导致整个组件的功能故障。因此,开发创新技术以确保陶瓷产品的良好质量是非常重要的。激光散斑测光(LSP)是一种光学无损检测方法。它是基于外部激励产生的时间分辨散斑图案的动态分析。在本文中,我们将提出两个研究陶瓷组件使用LSP技术。一种是陶瓷表面的无损应力表征,另一种是陶瓷部件的缺陷检测。目的是在具有挑战性的工业领域提高陶瓷生产的质量和安全控制。初步结果表明,LSP传感器系统在应力监测和表面缺陷检测方面具有陶瓷无损表征的潜力。
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引用次数: 4
Multi-gas sensor to detect simultaneously nitrogen oxides and oxygen 可同时检测氮氧化物和氧气的多气体传感器
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-10-09 DOI: 10.5194/jsss-9-327-2020
J. Herrmann, G. Hagen, J. Kita, F. Noack, D. Bleicker, R. Moos
Abstract. Due to tightened emission limits, the efficiency of exhaust gas aftertreatment systems has to be further enhanced. Therefore, inexpensive and robust NOx sensors are required to be installed notonly in automotive exhausts, but also in any other kind of combustion-based application. In this contribution, an impedimetric NOx sensor is presented. The impedance of a functional thick film ( KMnO4 , manufactured in a screen-printing technique on planar alumina substrates) depends selectively on the NOx concentration in the exhaust but shows a dependency on the oxygen concentration. Therefore, an additional temperature-independent resistive oxygen sensor structure was integrated on the same sensor platform. BFAT ( BaFe0.74Al0.01Ta0.25O3−δ ( BaFe0.74Al0.01Ta0.25O3−δ ) was used for thispurpose, and the measurement was conducted in the dc resistance mode. It serves not only to determine the oxygen concentration in the exhaust, but also to correct the oxygen dependency of the NOx sensor.
摘要由于排放限制的收紧,废气后处理系统的效率必须进一步提高。因此,不仅需要在汽车排气中安装廉价且坚固的NOx传感器,还需要在任何其他类型的基于燃烧的应用中安装该传感器。在这一贡献中,提出了一种阻抗式NOx传感器。功能性厚膜(KMnO4,在平面氧化铝基板上以丝网印刷技术制造)的阻抗选择性地取决于排气中的NOx浓度,但显示出对氧浓度的依赖性。因此,在同一传感器平台上集成了额外的与温度无关的电阻式氧传感器结构。BFAT(BaFe0.74Al0.01Ta0.25O3-δ),并在直流电阻模式下进行测量。它不仅用于确定排气中的氧浓度,还用于校正NOx传感器的氧依赖性。
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引用次数: 5
A tactile sensor based on magneto-sensitive elastomer to determine the position of an indentation 一种基于磁敏弹性体的触觉传感器,用于确定压痕的位置
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-10-08 DOI: 10.5194/jsss-9-319-2020
S. Gast, K. Zimmermann
Abstract. In this paper, we investigate the capabilities of a tactile sensor based on magneto-sensitive elastomers (MSEs). The main feature of the sensor is the determination of the position of indentation. The principle is based on inductance measurements of multiple planar coils and a soft magneto-sensitive layer. The proposed prototype consists of a linear array of hexagonal coils with overlapping sections. First, the results of the experiments are presented, which include a sampling of a sensor region with indentations of constant depth. Subsequently, we introduce a mathematical model based on the bell-shaped flux density distribution of a planar coil. This model consists of ellipse equations with three parameters and a polynomial fit for each parameter. Finally, solving the system of equations results in the determination of the x coordinate of the indentation.
摘要在本文中,我们研究了基于磁敏弹性体(MSEs)的触觉传感器的性能。传感器的主要特点是确定压痕的位置。该原理是基于多个平面线圈和软磁敏感层的电感测量。提出的原型由六边形线圈的线性阵列组成,这些线圈具有重叠的部分。首先,给出了实验结果,其中包括具有恒定深度压痕的传感器区域的采样。在此基础上,建立了基于平面线圈钟形磁通密度分布的数学模型。该模型由三个参数的椭圆方程和每个参数的多项式拟合组成。最后,通过求解方程组来确定凹痕的x坐标。
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引用次数: 1
Development and test of a highly sensitive and selective hydrogen sensor system 高灵敏度选择性氢传感器系统的研制与测试
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-10-05 DOI: 10.5194/jsss-9-309-2020
P. Sood, J. Zosel, M. Mertig, W. Oelssner, O. Herrmann, M. Woratz
Abstract. A miniaturized field-applicable sensor system was developed for the measurement of hydrogen ( H2 ) in air in the concentration range 0.2–200 ppmv. The sensor system is based on the application of an yttria-stabilized zirconia (YSZ) solid electrolyte cell (SEC) as a coulometric detector with gas chromatographic (GC) pre-separation. The main system components for injection, chromatographic separation, and the oxygen pumping cell were significantly miniaturized and tested separately to characterize important measurement properties like selectivity, lower limit of detection, repeatability, and signal-to-noise ratio. Measurements were conducted under varying GC parameters and detector operating conditions. While changing the detector temperature influences the hydrogen peak significantly due to diffusion processes at the electrode–electrolyte interface; different oxygen-partial pressures at the measuring electrode have no visible effect. The combination of two packed columns with 1 m length, one filled with a molecular sieve (13 X ) and the other one with silica gel, enabled highly reproducible and selective H2 measurements with more than 90 % analyte turnover compared to Faraday's law. The resulting insights wereused to define appropriate system parameters, construction guidelines, andmaterial properties for the final test prototype.
摘要开发了一种小型化的现场适用传感器系统,用于测量0.2–200浓度范围内的空气中的氢气(H2) ppmv。该传感器系统基于钇稳定的氧化锆(YSZ)固体电解质电池(SEC)作为具有气相色谱(GC)预分离的库仑检测器的应用。注射、色谱分离和氧泵池的主要系统组件被显著小型化,并分别进行测试,以表征重要的测量特性,如选择性、检测下限、重复性和信噪比。在不同的GC参数和检测器操作条件下进行测量。而由于电极-电解质界面的扩散过程,改变检测器温度会显著影响氢峰;在测量电极处不同的氧分压没有可见的影响。两个填充柱与1 m长,一个用分子筛(13X)填充,另一个用硅胶填充,使H2测量具有高度可重复性和选择性,超过90 % 分析物周转率与法拉第定律相比。由此产生的见解被用于为最终测试原型定义适当的系统参数、施工指南和材料特性。
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引用次数: 0
Influence of Pt paste and the firing temperature of screen-printed electrodes on the NO detection by pulsed polarization Pt糊剂和丝网印刷电极焙烧温度对脉冲极化法检测NO的影响
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-09-17 DOI: 10.5194/JSSS-9-293-2020
N. Donker, A. Ruchets, D. Schönauer-Kamin, J. Zosel, U. Guth, R. Moos
Abstract. Symmetrical Pt | YSZ | Pt sensors wereproduced by screen printing with frit-containing and fritless Pt pastes andfired at 950, 1100, and 1300  ∘ C. Subsequently, the sensors wereoperated by pulsed polarization, and the NO sensitivity was investigated. Thesensitivity of the sensors with fritless pastes was found to besignificantly higher. The influence of the firing temperature was low incontrast to the influence of the paste. The low NO sensitivity of thefrit-containing electrodes was attributed to a blocking effect that probablyoccurs at the triple-phase boundaries. Therefore, the oxygen transportthrough the sensor is inhibited, which, however, seems to be necessary forthe sensor effect.
摘要用含玻璃料和无玻璃料的Pt浆通过丝网印刷制备了对称的Pt|YSZ|Pt传感器,并在950、1100和1300下烧制  ∘ C.随后,通过脉冲极化操作传感器,并研究NO的灵敏度。使用无玻璃料浆料的传感器的灵敏度显著更高。烧成温度的影响比浆料的影响小。含rit电极的低NO敏感性归因于可能发生在三相边界的阻断效应。因此,通过传感器的氧气传输被抑制,然而,这似乎是传感器效果所必需的。
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引用次数: 0
Siloxane treatment of metal oxide semiconductor gas sensors in temperature-cycled operation – sensitivity and selectivity 温度循环操作中金属氧化物半导体气体传感器的硅氧烷处理——灵敏度和选择性
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-08-28 DOI: 10.5194/jsss-9-283-2020
Caroline Schultealbert, Iklim Uzun, T. Baur, T. Sauerwald, A. Schütze
Abstract. The impact of a hexamethyldisiloxane (HMDSO) treatment on the response of doped SnO2 sensors is investigated for acetone, carbon monoxide and hydrogen. The sensor was operated in temperature cycles based on the DSR concept (differential surface reduction). According to this concept, the rate constants for the reduction and oxidation of the surface after fast temperature changes can be evaluated and used for quantification of reducing gases as well as quantification and compensation of sensor poisoning by siloxanes, which is shown in this work. Increasing HMDSO exposure reduces the rate constants and therefore the sensitivity of thesensor more and more for all processes. On the other hand, while the rateconstants for acetone and carbon monoxide are reduced nearly to zero alreadyfor short treatments, the hydrogen sensitivity remains fairly stable, which greatly increases the selectivity. During repeated HMDSO treatment thequasistatic sensitivity, i.e. equilibrium sensitivity at one point duringthe temperature cycle, rises at first for all gases but then drops rapidly for acetone and carbon monoxide, which can also be explained by reduced rateconstants for oxygen chemisorption on the sensor surface when consideringthe generation of surface charge.
摘要研究了六甲基二硅氧烷(HMDSO)处理对掺杂SnO2传感器对丙酮、一氧化碳和氢气的响应的影响。传感器在基于DSR概念(微分表面还原)的温度循环中运行。根据这一概念,可以评估快速温度变化后表面还原和氧化的速率常数,并将其用于还原气体的量化以及硅氧烷对传感器中毒的量化和补偿,如本工作所示。HMDSO暴露量的增加降低了速率常数,因此在所有过程中,传感器的灵敏度越来越低。另一方面,虽然丙酮和一氧化碳的速率常数已经在短时间内降低到几乎为零,但氢敏感性保持相当稳定,这大大提高了选择性。在重复HMDSO处理过程中,准静态灵敏度,即温度循环中某一点的平衡灵敏度,首先对所有气体都会上升,但对丙酮和一氧化碳会迅速下降,这也可以通过考虑表面电荷的产生时传感器表面上氧化学吸附的速率常数降低来解释。
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引用次数: 3
Determination of the mean base circle radius of gears by optical multi-distance measurements 用光学多距离测量法确定齿轮的平均基圆半径
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-08-20 DOI: 10.5194/jsss-9-273-2020
M. Pillarz, A. von Freyberg, A. Fischer
Abstract. The required reliability of wind turbine gearboxes increases the requirements for large gear measurements. Extensive measurements to reliably assess the geometry of large gears in the single micrometer range are necessary. Due to an individually fixed measuring volume, standard methods like coordinate and gear measuring instruments reach their limits for large gears with diameters  >  1 m. Therefore, a scalable optical measurement approach consisting of a single sensor in combination with a rotary table for multi-distance measurements with subsequent model-based evaluation of shape parameters of gears is presented. The scalable measurement approach is to be extended to a multisensory system in further work. As a fundamental shape parameter the mean base circle radius using the example of spur gears is determined. The base circle radius is used due to the geometric relationship to further shape parameters for example to the profile slope deviation. The theoretically achievable measurement uncertainty of the mean base circle radius due to sensor noise is estimated to less than 5  µ m ( k=2 ) for a small and a large gear, which verifies the scalability of the sensor system. In order to show a general proof of principle, two series of optical measurements on a gear with a diameter of 0.105 m are performed and referenced with a tactile measurement. As a result, random errors of 1.2  µ m for k=2 are determined. The remaining systematic deviations to the reference value amount to 4.3 and 1.6  µ m, respectively. Hence, the total measurement uncertainty is currently limited by systematic effects, and the defined aim of a total uncertainty of less than 5  µ m ( k=2 ) is narrowly missed by 1.5  µ m. The random errors of 1.2  µ m ( k=2 ) show, however, that an adequate measurement precision is achieved and that the multi-distance measurement approach has the potential to reach the aimed measurement uncertainty with appropriate strategies to compensate for the systematic influences. The experimental and theoretical results prove the principle applicability of the proposed single sensor multi-distance approach for the precise inspection of gears.
摘要风力涡轮机齿轮箱所需的可靠性增加了对大齿轮测量的要求。需要进行广泛的测量,以可靠地评估单个微米范围内的大齿轮的几何形状。由于测量体积单独固定,坐标和齿轮测量仪器等标准方法达到了直径较大齿轮的极限  >  1. m。因此,提出了一种可扩展的光学测量方法,该方法由单个传感器与旋转台相结合,用于多距离测量,并随后对齿轮的形状参数进行基于模型的评估。可扩展的测量方法将在进一步的工作中扩展到多传感器系统。以直齿轮为例,确定了平均基圆半径作为基本形状参数。基圆半径是由于与其他形状参数的几何关系而使用的,例如与轮廓斜率偏差的几何关系。传感器噪声导致的平均基圆半径理论上可实现的测量不确定度估计小于5  µm(k=2),这验证了传感器系统的可扩展性。为了显示原理的一般证明,对直径为0.105的齿轮进行了两系列光学测量 m被执行并且以触觉测量作为参考。结果,1.2的随机误差  对于k=2,确定µm。与参考值的剩余系统偏差分别为4.3和1.6  µm。因此,总测量不确定度目前受到系统效应的限制,总不确定度小于5的既定目标  µm(k=2)差1.5  µm。1.2的随机误差  µm(k=2)表明,实现了足够的测量精度,并且多距离测量方法有可能通过适当的策略来补偿系统影响,从而达到目标测量不确定性。实验和理论结果证明了所提出的单传感器多距离方法在齿轮精确检测中的原理适用性。
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引用次数: 3
Optimization of soot deposition by high-temperature prepolarization of a resistive particulate matter sensor 电阻式微粒传感器高温预极化优化烟尘沉积
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-08-20 DOI: 10.5194/jsss-9-263-2020
J. Ebel, Carolin Schilling, H. Fritze
Abstract. For the purposes of the onboard diagnosis (OBD) of diesel particulatefilters (DPFs) in diesel exhaust treatment systems, a particulate matter(PM) sensor is applied downstream from the DPFs to detect small amounts ofdiesel soot that passed through the filter. The state-of-the-art technology is a sensor based on the resistive measurement principle, i.e., charged soot particles are attracted by electrophoretic forces, deposited on an interdigital electrode (IDE) structure and conductive soot bridges that reduce the overall resistance are formed. This paper reportshow the response time of a resistively working particulate matter sensor can beshortened up to 30  % by the optimization of soot depositionthat is initiated by a change in the sensor operation strategy. Themeasurement voltage is applied for prepolarization during the sensor regeneration phase rather than during the cooling phase before themeasurement is commonly done. Experiments were performed at dieselengine test benches to examine this context and simulations ofthe electric field above and below the IDE structure. The data are usedto deduct a model, including the solid state chemistry of the sensor'sceramic materials, the effect of impurities on the electric fieldproperties and the interconnection with the soot deposition, whichdefines the sensor's response.
摘要为了对柴油废气处理系统中的柴油微粒过滤器(dpf)进行车载诊断(OBD),在dpf的下游安装了一个微粒物质(PM)传感器,以检测通过过滤器的少量柴油烟尘。最先进的技术是基于电阻测量原理的传感器,即带电烟尘颗粒被电泳力吸引,沉积在数字间电极(IDE)结构上,形成导电烟尘桥,降低总电阻。本文报告表明,通过改变传感器的工作策略,优化烟尘沉积,可使电阻式工作颗粒物传感器的响应时间缩短30%。测量电压在传感器再生阶段而不是在通常测量之前的冷却阶段应用于预极化。在柴油机试验台进行了实验,以检查这种情况,并模拟了IDE结构上下的电场。这些数据被用来推导一个模型,包括传感器陶瓷材料的固态化学,杂质对电场特性的影响以及与烟灰沉积的互连,这些模型定义了传感器的响应。
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引用次数: 2
In-line monitoring of electrolytes and urea during continuous renal replacement therapy 连续性肾脏替代治疗过程中电解质和尿素的在线监测
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-08-19 DOI: 10.5194/jsss-9-251-2020
M. Berger, M. Sehlmeyer, F. Sellering, H. Röhrich, T. Perl, H. Mansour, D. Baasner, S. Zimmermann
Abstract. The individualization of dialysis treatment using acustomized dialysate composition usually requires a continuous measurementof electrolytes and urea in blood. The current practices are spotmeasurements of blood samples either with blood gas analyzers or in thelaboratory, involving considerable personnel effort. Furthermore, themeasured values are time delayed and not available in a continuousfashion. In this paper we investigate an in-line concept for continuousmonitoring of important blood parameters such as sodium, potassium, calciumand urea concentrations in blood serum using ion-selective electrodes. Thisconcept is evaluated in a preclinical study with human packed red bloodcells as a test medium over a period of 7 h. It has been shown that theelectrolytes can be well monitored. In addition, we present firstmeasurements with ion-sensitive field-effect transistors in aminiaturized sensor assembly. Therefore, new low-cost electronics for suchion-sensitive field-effect transistors have been developed.
摘要使用超声透析液组合物的个性化透析治疗通常需要连续测量血液中的电解质和尿素。目前的做法是用血气分析仪或实验室对血液样本进行现场测量,需要大量的人员投入。此外,测量值是有时间延迟的,不能连续使用。在本文中,我们研究了一种在线概念,用于使用离子选择电极连续监测重要的血液参数,如血清中的钠、钾、钙和尿素浓度。这一概念在一项临床前研究中得到了评估,该研究将人红细胞作为试验介质,历时7年 h.已经证明,可以很好地监测电解质。此外,我们还首次在胺化传感器组件中使用离子敏感场效应晶体管进行测量。因此,已经开发出用于这种离子敏感场效应晶体管的新的低成本电子器件。
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引用次数: 1
Design study for a multicomponent transducer for wind turbine test benches 风力发电机试验台多部件换能器设计研究
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2020-08-17 DOI: 10.5194/jsss-9-239-2020
J. Gnauert, G. Jacobs, S. Kock, D. Bosse, B. Janik
Abstract. This paper covers the design study of a multicomponent transducer (MCT) for wind turbine test benches. The MCT will cover the characteristics of wind turbines in the power range of up to 6 MW. The motivation to develop a MCT such as this is to provide satisfying measurement accuracy of loads and moments for all 6 degrees of freedom in order to reduce the uncertainty in the traceability of the drive train behavior due to the applied loads. Therefore, the estimation of the measurement uncertainty is significant with respect to evaluating the design of the MCT. First, the design process of the MCT is briefly introduced. Second, the strain-gauge-based transducer design is investigated under operational conditions (e.g., torque and multiaxial loads) using finite element (FE) simulations to determine the crosstalk effects. Finally, the measurement uncertainties of all quantities are estimated based on these FE simulations according to the type B evaluation of the “Guide to the Expression of Uncertainty inMeasurement” (GUM; JCGM, 2010), including metrological aspects (e.g., linearity deviation and hysteresis) and the crosstalk. It can be shown that the MCT has great potential to significantly improve themeasurement uncertainty for the applied wind loads on a wind turbine testbench.
摘要本文介绍了一种用于风力涡轮机试验台的多分量换能器(MCT)的设计研究。MCT将涵盖功率范围高达6的风力涡轮机的特性 开发这样的MCT的动机是为所有6个自由度提供令人满意的载荷和力矩测量精度,以减少由于施加载荷而导致的传动系行为可追溯性的不确定性。因此,测量不确定度的估计对于评估MCT的设计具有重要意义。首先,简要介绍了MCT的设计过程。其次,在操作条件下(例如,扭矩和多轴负载),使用有限元(FE)模拟来研究基于应变仪的换能器设计,以确定串扰效应。最后,根据“测量不确定度表达指南”(GUM;JCGM,2010)的B类评估,包括计量方面(如线性偏差和滞后)和串扰,基于这些有限元模拟来估计所有量的测量不确定性。可以表明,MCT在显著提高风力涡轮机试验台上施加的风载荷的测量不确定性方面具有巨大的潜力。
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引用次数: 2
期刊
Journal of Sensors and Sensor Systems
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