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Creep adjustment of strain gauges based on granular NiCr-carbon thin films 基于NiCr颗粒碳薄膜的应变片蠕变调整
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-03-12 DOI: 10.5194/JSSS-10-53-2021
M. Mathis, Dennis Vollberg, M. Langosch, Dirk Göttel, A. Lellig, G. Schultes
Abstract. An important property of high-precision mechanical sensors such as force transducers or torque sensors is the so-called creep error. It is defined as the signal deviation over time at a constant load. Since this signal deviation results in a reduced accuracy of the sensor, it is beneficial to minimize the creep error. Many of these sensors consist of a metallic spring element and strain gauges. In order to realize a sensor with a creep error of almost zero, it is necessary to compensate for the creep behavior of the metallic spring element. This can be achieved by creep adjustment of the used strain gauges. Unlike standard metal foil strain gauges with a gauge factor of 2, a type of strain gauges based on sputter-deposited NiCr -carbon thin films on polymer substrates offers the advantage of an improved gauge factor of about 10. However, for this type of strain gauge, creep adjustment by customary methods is not possible. In order to remedy this disadvantage, a thorough creep analysis is carried out. Five major influences on the creep error of force transducers equipped with NiCr -carbon thin-film strain gauges are examined, namely, the material creep of the metallic spring element (1), the creep (relaxation) of the polymer substrate (2), the composition of the thin film (3), the strain transfer to the thin film (4), and the kind of strain field on the surface of the transducer (5). Consequently, we present two applicable methods for creep adjustment of NiCr -carbon thin- film strain gauges. The first method addresses the intrinsic creep behavior of the thin film by a modification of the film composition. With increasing Cr content (at the expense of Ni, the intrinsic negative creep error can be shifted towards zero. The second method is not based on the thin film itself but rather on a modification of the strain transfer from the polyimide carrier to the thin film. This is achieved by controlled cutting of well-defined deep trenches into the polymer substrate via a picosecond laser.
摘要诸如力传感器或扭矩传感器的高精度机械传感器的一个重要特性是所谓的蠕变误差。它被定义为在恒定负载下随时间的信号偏差。由于这种信号偏差导致传感器的精度降低,因此最小化蠕变误差是有益的。这些传感器中的许多传感器由金属弹簧元件和应变仪组成。为了实现蠕变误差几乎为零的传感器,需要补偿金属弹簧元件的蠕变行为。这可以通过对使用的应变仪进行蠕变调整来实现。与应变系数为2的标准金属箔应变仪不同,一种基于聚合物衬底上溅射沉积的NiCr-碳薄膜的应变仪具有改进的应变系数约为10的优点。然而,对于这种类型的应变计,通过常规方法进行蠕变调整是不可能的。为了弥补这一缺点,进行了全面的蠕变分析。研究了五个主要影响NiCr-碳薄膜应变仪力传感器蠕变误差的因素,即金属弹簧元件(1)的材料蠕变、聚合物衬底(2)的蠕变(弛豫)、薄膜的组成(3)、向薄膜的应变传递(4)和传感器表面的应力场类型(5)。因此,我们提出了两种适用于镍铬碳薄膜应变计蠕变调整的方法。第一种方法通过改变薄膜成分来解决薄膜的固有蠕变行为。随着Cr含量的增加(以Ni为代价),固有的负蠕变误差可以向零偏移。第二种方法不是基于薄膜本身,而是基于改变从聚酰亚胺载体到薄膜的应变传递。这是通过皮秒激光器在聚合物基片中控制切割明确的深沟来实现的。
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引用次数: 2
Impact of particle size and morphology of cobalt oxide on the thermal response to methane examined by thermal analysis 用热分析方法研究了氧化钴的粒度和形貌对甲烷热响应的影响
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-02-24 DOI: 10.5194/JSSS-10-37-2021
O. Yurchenko, H. Pernau, L. Engel, B. Bierer, M. Jägle, J. Wöllenstein
Abstract. Differential thermal analysis (DTA) was used to examine the effect of the particle size and morphology of cobalt (III/IV) oxide ( Co3O4 ) on its thermal response under exposure to methane (1 vol % in dry synthetic air), which is a relevant gas for the detection of combustible gases. The DTA response results from the catalytic oxidation of methane, and its characteristics should correlate with the pellistor response. Co3O4 samples differing in particle size and morphology were produced by ball milling (top-down technique) or were synthesized from precursor molecules by precipitation (bottom-up technique). The investigations carried out in dry air and a temperature range between 250 and 450  ∘ C reveal that both particle size and particle shape have a considerable effect on thermal response, since the resulting layer structures and the associated surface area available for gas interaction differ. The Co3O4 catalyst, with small particles and an irregular shape, exhibits significantly higher response than milled Co3O4 samples. Comparison of DTA with the mass spectroscopy signal of CO2 evolved by the reaction verified a certain analogy between DTA measurements and the response produced by a pellistor.
摘要采用差热分析(DTA)研究了钴(III/IV)氧化物(Co3O4)的粒度和形貌对其暴露于甲烷(干燥合成空气中1vol %)下热响应的影响,甲烷是检测可燃气体的相关气体。DTA反应是由甲烷的催化氧化引起的,其特征应该与造纸机反应相关。不同粒径和形态的Co3O4样品通过球磨(自上而下的技术)或前体分子通过沉淀(自下而上的技术)合成。在干燥空气和250至450°C的温度范围内进行的调查显示,颗粒大小和颗粒形状对热反应都有相当大的影响,因为产生的层结构和相关的气体相互作用表面积不同。颗粒小、形状不规则的Co3O4催化剂的响应率明显高于研磨后的Co3O4样品。将DTA与反应产生的CO2的质谱信号进行比较,证实了DTA测量结果与造粒器产生的响应具有一定的相似性。
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引用次数: 4
Characterization of sand and sand–binder systems from the foundry industry with electrical impedance spectroscopy 用电阻抗谱法表征铸造工业中的沙子和沙子-粘结剂系统
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-02-24 DOI: 10.5194/JSSS-10-43-2021
L. Bifano, A. Fischerauer, A. Liedtke, G. Fischerauer
Abstract. The global economy consumes an estimated 4×1010  t of sandper year, with only 2×1010  t of sand being reproduced by naturalsedimentation (Gotze and Gobbels, 2017; Peduzzi, 2014). Among other things, sandis also used as a basic material for the production of molds and cores inthe foundry industry. The consumption and the economic as well as ecologicalsavings' potential in this area of application can be appreciated by way ofan example: the environmental certificate of a single, albeit big Germanfoundry (5160 employees) can be consulted, which states that 39 820 t ofsand for casting molds had to be purchased in 2017 (Denes, 2018). In orderto avoid having to dispose of the used sand in landfills and to reduce the use of new sand,it is therefore advantageous to renew the used sand in a so-calledregeneration process and reuse it as a substitute for new sand in theproduction of molds and cores. It would be very advantageous if thecondition of molding materials (sand–binder systems) in regenerator unitscould be monitored in real time because of the economic and ecologicaladvantages of a monitored and optimized regeneration process. This workpresents the results of investigations in this direction. The objects ofinvestigation in this work are typical molding materials in the foundryindustry, e.g., quartz sand, chromite sand, and bentonite as a binder, whichare measured impedimetrically with the help of a plate capacitor measuringcell which is connected to an LCR meter (Agilent E4980A). The impedance ofthe filled capacitor is measured in a frequency range from 1.2 kHz to 1 MHz,containing 123 frequency points. The aim of this research is to work out ifthe mentioned substances can be measured with the presented measuring methodand classified on the basis of impedance characteristics and thus whether impedancespectroscopy can be considered for process monitoring in the moldingindustry. It is shown that the condition monitoring can possibly be based onimpedance spectroscopy because the resulting curves are characteristic ofthe material used. New and used sands as well as two-component mixtures ofsands and binders showed a systematic behavior, which allows the sand or thecomposition of the mixture to be identified (classified) in the future. Theexamination of the scatter of the measurement results shows that theimpedance data obtained with this method can be measured reproducibly. Adescriptive model for multi-component systems is developed in order to beable to interpret the impedance scatter results and their representation inNyquist plots. From this model, the filling density of the measurement celland the density of conduction paths can be extracted as essential influencequantities.
摘要据估计,全球经济每年消耗4×1010吨沙子,其中只有2×1010吨沙子是通过自然沉积再生的(格策和戈培尔,2017;Peduzzi, 2014)。除此之外,砂还被用作铸造工业中生产模具和芯的基本材料。可以通过一个例子来了解这一应用领域的消费、经济和生态节约潜力:可以咨询一家大型德国铸造厂(5160名员工)的环境证书,该证书指出,2017年必须购买39820吨用于铸造模具的沙子(Denes, 2018)。为了避免在垃圾填埋场处理用过的沙子并减少新沙子的使用,因此在所谓的再生过程中更新用过的沙子并将其作为模具和岩心生产中新沙子的替代品是有利的。由于监测和优化再生过程的经济和生态优势,因此对再生机组内成型材料(砂胶系统)的状况进行实时监测将是非常有利的。本文介绍了这一方向的研究结果。这项工作的研究对象是铸造工业中典型的成型材料,例如石英砂、铬铁矿砂和作为粘合剂的膨润土,这些材料在连接到LCR仪表(Agilent E4980A)的板电容测量单元的帮助下进行阻抗测量。填充电容器的阻抗在1.2 kHz至1 MHz的频率范围内测量,包含123个频率点。本研究的目的是研究上述物质是否可以用所提出的测量方法进行测量,并根据阻抗特性进行分类,从而是否可以考虑将阻抗光谱技术用于成型工业的过程监测。结果表明,基于阻抗谱的状态监测是可行的,因为所得到的曲线具有所用材料的特性。新砂和旧砂以及砂和粘合剂的双组分混合物表现出系统的行为,这使得将来可以识别(分类)砂或混合物的组成。对测量结果的散射性检验表明,用该方法测得的阻抗数据具有可重复性。为了能够解释阻抗散射结果及其在奈奎斯特图中的表示,建立了多组分系统的描述模型。从该模型中,可以提取出测量单元的填充密度和传导路径的密度作为重要的影响因素。
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引用次数: 5
Comparison of laser-based photoacoustic and optical detection of methane 基于激光的甲烷光声和光学检测方法的比较
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-02-22 DOI: 10.5194/JSSS-10-25-2021
T. Strahl, J. Herbst, Eric Maier, S. Rademacher, C. Weber, H. Pernau, A. Lambrecht, J. Wöllenstein
Abstract. The measurement of low methane ( CH4 ) concentrations is a key objective for safety of industrial and public infrastructures and in environmental research. Laser spectroscopy is best suited for this purpose because it offers high sensitivity, selectivity, dynamic range, and a fast measurement rate. The physical basis of this technique is infrared absorption of molecular gases. Two detection schemes – direct absorption spectroscopy (DAS) and photoacoustic spectroscopy (PAS) – are compared at three wavelength regions in the near-infrared (NIR), mid-wavelength (MWIR), and long-wavelength (LWIR) infrared ranges. For each spectral range a suitable semiconductor laser is selected and used for both detection techniques: a diode laser (DL), an interband cascade laser (ICL), and a quantum cascade laser (QCL) for NIR, MWIR and LWIR, respectively. For DAS short absorption path lengths comparable to the cell dimensions of the photoacoustic cell for PAS are employed. We show that for DAS the lowest detection limit can be achieved in the MWIR range with noise-equivalent concentrations (NECs) below 10 ppb. Using PAS, lower detection limits and higher system stabilities can be reached compared to DAS, especially for long integration times. The lowest detection limit for PAS is obtained in the LWIR with a NEC of 7 ppb. The different DAS and PAS configurations are discussed with respect to potential applications.
摘要低甲烷(CH4)浓度的测量是工业和公共基础设施安全以及环境研究的一个关键目标。激光光谱学最适合用于此目的,因为它具有高灵敏度、选择性、动态范围和快速测量速率。这项技术的物理基础是分子气体的红外吸收。在近红外(NIR)、中波(MWIR)和长波(LWIR)红外范围的三个波长区域,比较了两种检测方案——直接吸收光谱(DAS)和光声光谱(PAS)。对于每个光谱范围,选择合适的半导体激光器并用于两种检测技术:二极管激光器(DL)、带间级联激光器(ICL)和量子级联激光器(QCL),分别用于NIR、MWIR和LWIR。对于DAS,采用与PAS的光声池的池尺寸相当的短吸收路径长度。我们表明,对于DAS,在噪声当量浓度(NECs)低于10的MWIR范围内可以达到最低检测极限 ppb。与DAS相比,使用PAS可以达到更低的检测极限和更高的系统稳定性,尤其是在长集成时间的情况下。PAS的最低检测限在LWIR中获得,NEC为7 ppb。讨论了不同的DAS和PAS配置的潜在应用。
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引用次数: 5
Six-degree-of-freedom pose estimation with µm/µrad accuracy based on laser multilateration 基于激光多点定位的精度为µm/µrad的六自由度姿态估计
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-02-19 DOI: 10.5194/JSSS-10-19-2021
J. Nitsche, M. Franke, N. Haverkamp, D. Heißelmann
Abstract. The estimation of the six-degree-of-freedom position and orientation of an end effector is of high interest in industrial robotics. High precision and data rates are important requirements when choosing an adequate measurement system. In this work, a six-degree-of-freedom pose estimation setup based on laser multilateration is described together with the measurement principle and self-calibration strategies used in this setup. In an experimental setup, data rates of 200  Hz are achieved. During movement, deviations from a reference coordinate measuring machine of 20  µm are observed. During standstill, the deviations are reduced to 5  µm .
摘要末端执行器六自由度位置和姿态的估计是工业机器人研究的热点问题。在选择合适的测量系统时,高精度和数据速率是重要的要求。本文介绍了一种基于激光多倍体的六自由度姿态估计装置,以及该装置的测量原理和自校准策略。在实验装置中,数据速率达到200hz。在运动过程中,观察到与参考坐标测量机的偏差为20 μ m。在静止状态下,偏差减小到5µm。
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引用次数: 5
Measurements at laser materials processing machines: spectrum deconvolution including uncertainties and model selection 激光材料加工机的测量:光谱反褶积,包括不确定度和模型选择
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-02-18 DOI: 10.5194/JSSS-10-13-2021
R. Behrens, B. Pullner, M. Reginatto
Abstract. Laser materials processing of workpieces using ultra-short pulsed lasers can lead to unwanted X-ray emission. Their dose rate and spectral distribution have been precisely determined. The measurements werecarried out using a thermoluminescence detector (TLD)-based spectrometer in which 30 TLD planes are arranged one behind the other, the first 10 layersmade of polymethyl methacrylate, while the remaining 20 layers are interspaced by absorbers with, from the front to the back, increasing atomiccharge and thickness. The penetration depth of the radiation into thespectrometer depends on its energy, so that the energy-resolved spectrum ofthe radiation can be calculated from the TLD dose values by means ofmathematical methods (Bayesian deconvolution). The evaluation process alsotakes into account both the uncertainties of all input quantities and thepossibility of adopting different models for the spectrum form. This allowedthe resulting spectra to be associated with their realistic uncertainty. The measurements are traceable to the Systeme international d'unites (SI), i.e. the International System of Units. The results not only provide manufacturers and users of ultra-short pulsed lasers with important information on the design of the machines with regard to radiationprotection, but were also included in the recently concluded legislative procedure in the field of radiation protection in Germany.
摘要使用超短脉冲激光器加工工件的激光材料会导致不必要的x射线发射。它们的剂量率和光谱分布已被精确地测定。使用基于热释光探测器(TLD)的光谱仪进行测量,其中30个TLD平面一个接一个地排列,前10层由聚甲基丙烯酸甲酯制成,其余20层由吸收剂间隔,从前到后增加原子电荷和厚度。辐射进入光谱仪的穿透深度取决于它的能量,因此辐射的能量分辨光谱可以通过数学方法(贝叶斯反卷积)从TLD剂量值计算出来。评估过程还考虑了所有输入量的不确定性和对频谱形式采用不同模型的可能性。这使得得到的光谱与实际的不确定性相联系。这些测量可以追溯到国际单位制(SI),即国际单位制。研究结果不仅为超短脉冲激光器的制造商和用户提供了有关辐射防护机器设计的重要信息,而且还被纳入德国最近完成的辐射防护领域立法程序。
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引用次数: 2
Inline quality monitoring of diesel exhaust fluid (AdBlue) by using the 3ω method 使用3ω方法对柴油机排气液(AdBlue)进行在线质量监测
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-01-27 DOI: 10.5194/JSSS-10-5-2021
R. Bernhardsgrütter, C. Hepp, M. Jägle, H. Pernau, K. Schmitt, J. Wöllenstein
Abstract. Because diesel combustion processes produce harmful detrimental nitrous oxides, the selective catalytic reduction, an after-treatment method using diesel exhaust fluid (AdBlue) to reduce these emissions, is an important part in the cycle of the combustion process. Therefore, it is crucial to continuously monitor the quality of the diesel exhaust fluid to secure the ideal selective catalytic reduction. This article presents a platinum thin-film sensor using the 3 ω method which is able to characterize the diesel exhaust fluid. By means of the 3 ω method, information about the concentration of urea in water can be extracted. In this investigation, a digital lock-in amplification technique is used to execute the measurements. The results show that this sensor can determine the urea content within 1 % by weight. Moreover, besides the analysis of the 3 ω signal, the 1 ω signal is analyzed in depth to receive additional information about the temperature. Because the same structure can measure multiple parameters, such as concentration, temperature, and flow, the sensor might be a good alternative to the state-of-the-art diesel exhaust fluid sensor.
摘要由于柴油燃烧过程产生有害的有害氧化亚氮,选择性催化还原是一种利用柴油排气液(AdBlue)减少这些排放的后处理方法,是燃烧过程循环中的重要组成部分。因此,持续监测柴油机排气液的质量,以确保理想的选择性催化还原效果至关重要。本文介绍了一种采用3 ω法的铂薄膜传感器,该传感器能够对柴油机排气液进行表征。利用3 ω法可以提取水中尿素的浓度信息。在本研究中,使用了数字锁相放大技术来执行测量。结果表明,该传感器可测定尿素含量在重量比1%以内。此外,除了对3 ω信号进行分析外,还对1 ω信号进行深入分析,以接收有关温度的附加信息。由于相同的结构可以测量多个参数,如浓度、温度和流量,因此该传感器可能是最先进的柴油排气流体传感器的一个很好的替代品。
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引用次数: 2
Explaining to different audiences the new definition and experimental realizations of the kilogram 向不同的听众解释千克的新定义和实验实现
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-01-21 DOI: 10.5194/JSSS-10-1-2021
J. Valdés
Abstract. Different options were discussed before reaching the final agreement on the new definitions of the SI units, effective from 20 May 2019, especially with regard to the kilogram, now defined in terms of the numerical value of the Planck constant ( h ). Replacing the artefact definition of the kilogram with a new one based on the mass of a particle, or the atomic mass constant ( mu ), would have been preferable for ease of understanding, among other reasons. In this paper we discuss some limitations of teaching to different audiences what a kilogram is in the redefined International System of Units (SI), including realizations of the new definition.
摘要在就国际单位制的新定义达成最终协议之前,讨论了不同的选项,该定义自2019年5月20日起生效,特别是千克,现在根据普朗克常数(h)的数值定义。出于便于理解等原因,用基于粒子质量或原子质量常数(μ)的新定义取代公斤的人工制品定义是可取的。在本文中,我们讨论了在重新定义的国际单位制(SI)中向不同受众教授千克的一些局限性,包括新定义的实现。
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引用次数: 0
Methods and procedure of referenced in situ control of lateral contour displacements in additive manufacturing 增材制造中横向轮廓位移参考原位控制方法和程序
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-01-01 DOI: 10.5194/jsss-10-219-2021
Martin Lerchen, Jakob Hornung, Yu Zou, T. Hausotte
Abstract. Additive manufacturing technologies are further developing from prototype to serial production. This trend requires rising challenges to the process-accompanying quality assurance. Optical in situ quality control approaches show great potential to generate accurate measurement data, which are essential for feedback control. If a reliable referencing concept for the layer-by-layer measured data is guaranteed, contour information can be used during the manufacturing to correct occurring geometrical deviations. Within this scientific study, two methods of optical, referenced in situ control of lateral displacements of additive manufactured contours are presented. In the first approach the 2-D contour of the melting pool is analysed in relation to a position-stable reference system implemented in the powder bed. The second approach uses the translucent contour of deeper layers covered with powder as a reference. Within the image evaluation several pre-processing steps like calibration, undistortion, rectification, illumination correction and low-pass filtering are essential for reliable and correct geometric measurements. The following adapted contour detection and position determination of the referenced melting pool contours are based on an extended edge detection algorithm according to Canny (1986). With the evaluation of further manufacturing layers of already lowered powder bed levels, it is possible to specify the influence of powder application on geometrical displacements separately. This is done by a comparison of the position of the detected powder-covered melting pool contours with the previously applied melted region. Consequently a better understanding of lateral contour displacements within the additive manufacturing process is the goal, which is important for a process-accompanying correction of geometrical deviations.
摘要增材制造技术正从原型向批量生产进一步发展。这种趋势要求对伴随质量保证的过程提出越来越多的挑战。光学原位质量控制方法显示出产生精确测量数据的巨大潜力,这对反馈控制至关重要。如果保证了逐层测量数据的可靠参考概念,则可以在制造过程中使用轮廓信息来纠正发生的几何偏差。在这项科学研究中,提出了两种光学的、参考的增材制造轮廓横向位移的原位控制方法。在第一种方法中,分析了熔池的二维轮廓与在粉末床中实现的位置稳定参考系统的关系。第二种方法使用覆盖着粉末的深层半透明轮廓作为参考。在图像评估的几个预处理步骤,如校准,不失真,整流,照明校正和低通滤波是必不可少的可靠和正确的几何测量。根据Canny(1986)的一种扩展边缘检测算法,对参照熔池轮廓进行了以下调整轮廓检测和位置确定。通过对已经降低的粉末床水平的进一步制造层的评估,可以单独指定粉末应用对几何位移的影响。这是通过将检测到的粉末覆盖的熔池轮廓的位置与先前应用的熔化区域进行比较来完成的。因此,在增材制造过程中更好地理解横向轮廓位移是目标,这对于伴随过程的几何偏差校正非常重要。
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引用次数: 2
Characterization of specular freeform surfaces from reflected ray directions using experimental ray tracing 利用实验射线追踪从反射射线方向表征镜面自由曲面
IF 1 Q4 INSTRUMENTS & INSTRUMENTATION Pub Date : 2021-01-01 DOI: 10.5194/jsss-10-261-2021
T. Binkele, D. Hilbig, M. Essameldin, T. Henning, F. Fleischmann, W. Lang
Abstract. The applications of freeform surfaces in optical components and systems are increasing more and more. Therefore, appropriate measurement techniques are needed to measure these freeform surfaces for verification. This task is still a challenge for most measurement techniques. In this paper, we propose a measurement technique for optical and other specular freeform surfaces based on experimental ray tracing. This technique is able to measure form and mid-spatial-frequency deviations simultaneously. The focus will be set on the sensing technique and the measurement uncertainties in the setup. As the measurement technique is described, an estimation of the influence of different uncertainties based on simulations is given. The result from an experimental measurement is evaluated in relation to the influence of the uncertainties. A comparison measurement for evaluation is given.
摘要自由曲面在光学元件和系统中的应用越来越广泛。因此,需要适当的测量技术来测量这些自由曲面进行验证。这项任务对大多数测量技术来说仍然是一个挑战。在本文中,我们提出了一种基于实验光线追踪的光学和其他镜面自由曲面的测量技术。该技术能够同时测量形状和中空间频率偏差。重点将放在传感技术和测量不确定度的设置。在描述测量技术的同时,给出了基于仿真的不同不确定度影响的估计。根据不确定度的影响对实验测量的结果进行评价。给出了一种评价的比较方法。
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引用次数: 1
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Journal of Sensors and Sensor Systems
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