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Pyroelectric lithium niobate electron emission-based ion-pump 热释电铌酸锂电子发射离子泵
K. Vinayakumar, V. Gund, A. Lal
This work presents a compact ion-pump that utilizes pyroelectricity for ionization of ambient molecules. The pyroelectric ionization is realized by heating a lithium niobate (LiNbO3) crystal with low voltage resistive heating (10 V drive voltage, 0.5 W Joule heating) to generate a high voltage across the poled surface of the crystal. Pyroelectrically generated electrons from the polarized surface of the crystal are accelerated using an electric field generated by both the crystal and external titanium (Ti) electrodes biased at ±300 V, which results in the ionization of molecules in the chamber. The low collector current in the pA range ensures that the power consumed due to ionization current is lower than the LiNbO3 heating power. The ionized gas molecules are accelerated toward the Ti collector electrodes where they are implanted owing to large acceleration produced by the collector electrodes. The system is configured as a sputter pump for gettering ions to reduce chamber pressure from the baseline value of 1.4 μTorr with just the external pump to 1.1 μTorr by incorporating the LiNbO3 pump. The proof-of-concept of the pyroelectric pumping mechanism is demonstrated using a 140 cm3 stainless steel vacuum chamber, with supplementary turbomolecular and diaphragm pumps and demonstrates that a 50 s thermal cycling of the crystal is optimal for the ion-pump. Pumping action was measured with a Pirani gauge and a hot cathode ion gauge. Analytical modeling and experimental results for pumping speed calculations showed a good match during high-pressure pumping.
这项工作提出了一个紧凑的离子泵,利用热释电电离周围的分子。热释电电离是通过用低压电阻加热(10v驱动电压,0.5 W焦耳加热)加热铌酸锂(LiNbO3)晶体,在晶体的极表面产生高电压来实现的。晶体和外部钛(Ti)电极产生的电场在±300 V的偏置下加速晶体极化表面产生的热释电电子,导致腔内分子电离。集电极电流在pA范围内,保证了电离电流消耗的功率低于LiNbO3加热功率。电离的气体分子被加速到钛收集器电极,在那里它们被植入,由于大的加速度由收集器电极产生。该系统配置为一个溅射泵,用于离子的吸收,通过加入LiNbO3泵,将腔室压力从仅使用外部泵时的基线值1.4 μTorr降低到1.1 μTorr。热释电抽运机制的概念验证是使用一个140 cm3的不锈钢真空室,与补充的涡轮分子泵和隔膜泵进行演示,并证明了50 s的晶体热循环是离子泵的最佳选择。泵送作用用皮拉尼计和热阴极离子计测量。分析模型与实验结果吻合良好。
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引用次数: 2
High sensitivity x-ray detectors based on 4H-SiC p-i-n structure with 80 μm thick intrinsic layer 基于80 μm厚本征层4H-SiC p-i-n结构的高灵敏度x射线探测器
Qing Liu, Dong Zhou, Weizong Xu, Dunjun Chen, F. Ren, Rong Zhang, Youdou Zheng, Hai Lu
In this work, a large size x-ray detector with a 25 mm2 active area is demonstrated based on a thick 4H-SiC p-i-n structure. The detector exhibits obvious merits of high photon sensitivity over 4 × 104 μC Gy−1 cm−2, good photon-response linearity, and high-temperature operation compatibility. Meanwhile, due to the ultralow leakage current level achieved, single photon detection performance for x-ray photons is further realized with energy resolutions of 1.1 and 4.9 keV at 5.9 and 59.5 keV, respectively. This work thus suggests the significant potentials of wide-bandgap SiC semiconductor for photon-resolved x-ray detection in a harsh environment.
在这项工作中,基于厚的4H-SiC p-i-n结构,展示了具有25 mm2活性面积的大尺寸x射线探测器。该探测器具有4 × 104 μC Gy−1 cm−2以上的高光子灵敏度、良好的光子响应线性度和高温工作兼容性等优点。同时,由于实现了超低泄漏电流水平,进一步实现了对x射线光子的单光子探测性能,在5.9 keV和59.5 keV下能量分辨率分别为1.1和4.9 keV。因此,这项工作表明了宽带隙SiC半导体在恶劣环境下用于光子分辨x射线探测的巨大潜力。
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引用次数: 2
Theoretical model for fast calculations of the electrical resistivity of thin metallic films with rough surfaces 具有粗糙表面的金属薄膜电阻率快速计算的理论模型
A. A. Pribylov
A model of electron gas scattering at surface inhomogeneities was developed and applied to describe a surface roughness influence on the electrical resistivity of thin metallic films. The model is developed to be simple enough for fast calculations without detailed investigation of surface topology. The film’s shape is assumed to be described by the average thickness, the surface rms, and the correlation length. The scattering mechanism corresponds to electrical potential changes caused by inhomogeneities. It was found that the electrical resistivity of thin films increases with the increase of the roughness of surface for films of any thickness, whereas the law of this effect depends on film’s thickness. Basing on the developed model, formulas for the electrical resistivity as a function of the roughness rms and the correlation length in cases of thick enough, thin, and extremely thin films have been obtained and discussed with comparison to other models already in literature and experimental data.
建立了一个表面不均匀的电子气体散射模型,并应用该模型来描述表面粗糙度对金属薄膜电阻率的影响。该模型开发得足够简单,无需详细研究表面拓扑结构即可进行快速计算。假定薄膜的形状由平均厚度、表面均方根和相关长度来描述。散射机制与不均匀性引起的电势变化相对应。对任意厚度的薄膜,其电阻率随表面粗糙度的增加而增大,但其规律与薄膜的厚度有关。基于所建立的模型,得到了足够厚、较薄和极薄薄膜情况下电阻率随粗糙度rms和相关长度的函数表达式,并与文献中已有的模型和实验数据进行了比较。
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引用次数: 1
Intrinsic excitation-dependent room-temperature internal quantum efficiency of AlGaN nanowires with varying Al contents 不同Al含量的AlGaN纳米线的本征激发相关室温内量子效率
Jiaying Lu, Y. Zhong, Songrui Zhao
Aluminum gallium nitride (AlGaN) nanowires have become an emerging approach for semiconductor deep ultraviolet light-emitting devices. To further improve the device performance, it is critical to understand the optical quality of AlGaN nanowires. However, today, the room-temperature internal quantum efficiency (IQE) of AlGaN nanowires is predominantly analyzed by the temperature-dependent photoluminescence (PL) approach under one excitation power or taking the PL intensity ratio at the room temperature and low temperature with different excitation powers. In both cases, one needs to assume the low temperature IQE to be 100%, which is not always valid, in particular when the excitation power changes at the low temperature. In this work, we study the room-temperature IQE of AlGaN nanowires through the detailed excitation power-dependent PL experiments and theoretical analysis. This allows us to derive the intrinsic room-temperature IQE of AlGaN nanowires as a function of the excitation power. It is found that for an Al content in the range of 22%–54%, the IQE of all samples increases as the excitation increases, followed by an efficiency droop. Moreover, comparing different samples, the IQE at low excitations increases as the Al content increases, whereas the peak IQE reduces from 73% to 56% as the Al content increases. The underlying mechanisms are also discussed in this paper.
氮化铝镓纳米线已成为半导体深紫外发光器件的一种新兴方法。为了进一步提高器件性能,了解AlGaN纳米线的光学质量至关重要。然而,目前对AlGaN纳米线室温内量子效率(IQE)的分析主要采用单一激发功率下的温度依赖光致发光(PL)方法或采用不同激发功率下室温和低温下的PL强度比。在这两种情况下,我们都需要假设低温IQE为100%,这并不总是有效的,特别是当激励功率在低温下发生变化时。在这项工作中,我们通过详细的激发功率相关的PL实验和理论分析来研究AlGaN纳米线的室温IQE。这使我们能够推导出AlGaN纳米线的内在室温IQE作为激励功率的函数。结果表明,在Al含量为22% ~ 54%的范围内,所有样品的IQE都随着激发的增加而增加,然后效率下降。不同样品在低激励下的IQE随Al含量的增加而增加,峰值IQE随Al含量的增加而从73%下降到56%。本文还讨论了其基本机制。
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引用次数: 5
About the robustness of Schottky conjecture when quasi-one-dimensional stages are present 关于准一维阶段存在时肖特基猜想的鲁棒性
Edgar Marcelino de Carvalho Neto
The Schwarz–Christoffel transformation is used to analytically evaluate the field enhancement factor close to the apex of two-stage conducting structures consisting of a vertical line centered on the top of an isosceles trapezoidal protrusion on an infinite line. This way the validity of the Schottky conjecture (SC) is assessed for different ratios involving the dimensions of the system, which is expected to model quasi-one-dimensional structures, such as nanotubes, on the top of multistage structures used in different scientific and technological applications. The results obtained in this work suggest that the SC remains a good approximation beyond the region in which it is usually expected to be valid.
利用Schwarz-Christoffel变换,分析了在无限线上以等腰梯形凸起为中心的垂直线构成的两级导电结构在靠近顶点处的场增强因子。通过这种方式,肖特基猜想(SC)的有效性被评估为涉及系统维度的不同比率,该系统有望模拟准一维结构,如纳米管,在不同的科学和技术应用中使用的多级结构的顶部。在这项工作中获得的结果表明,SC在通常预期有效的区域之外仍然是一个很好的近似。
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引用次数: 1
Formation of ideally ordered porous anodic zirconia by anodization of vacuum deposited Zr on molds 通过在模具上真空沉积锆的阳极氧化形成理想有序多孔阳极氧化锆
T. Kondo, Touko Tamura, T. Yanagishita, H. Masuda
We studied the formation of ideally ordered nanoporous zirconia by anodizing Zr having a texturing pattern. A texturing pattern was formed on a Zr surface by peeling off a sputtered zirconium film from a metal (Ni) mold having an ordered array of convexes. In contrast to texturing by nanoimprinting, the present texturing process never requires the pressing of a mold onto the Zr surface. During the anodization of Zr that has a texturing pattern on its surface, which is an ideally ordered array of concaves, each concave acted as a starting point of the formation of nanoholes. By the present process, porous anodic zirconia having an ideally ordered array of nanoholes was obtained. The interval between nanoholes in the porous anodic zirconia agreed with the texturing pattern.
我们研究了通过阳极氧化具有织构图案的Zr来形成理想有序的纳米多孔氧化锆。通过从具有有序凸阵列的金属(Ni)模具上剥离溅射锆膜,在Zr表面形成了纹理图案。与纳米压印的纹理相比,目前的纹理工艺不需要将模具压在Zr表面上。在氧化Zr的过程中,其表面有一个纹理图案,这是一个理想的有序的凹面阵列,每个凹面作为纳米孔形成的起点。通过本工艺制备了具有理想有序纳米孔排列的多孔氧化锆。多孔氧化锆中纳米孔之间的间隔与织构模式一致。
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引用次数: 1
Information extraction from Murphy–Good plots of tungsten field electron emitters 钨场电子发射体墨菲-古德曲线的信息提取
Mazen A. Madanat, Mohammad Al Share, Mohammad M. Allaham, M. Mousa
This study introduces an easy methodology to test and analyze experimental field electron emission current-voltage data from metallic single-tip emitters; this novel and easy methodology is called the Murphy–Good plots. Tungsten electron emitters were used as an example and were prepared by the electrochemical etching process. The current-voltage characteristics are obtained in high vacuum levels and using a traditional field emission microscope. Murphy–Good plots are used to apply the well-known field electron emission orthodoxy test to the experimental data and then to extract the emitters’ characterization parameters if the test is passed. The novelty in using this type of plots lies in its independency on any correction factors, unlike the traditional Fowler–Nordheim and Millikan–Lauritsen plots, in addition to its simple theoretical form. The results are calculated using a simple web tool that applies the field electron emission orthodoxy test to any type of the current-voltage analysis plots and then to extract the characterization parameters of the emitters.
本文介绍了一种简单的方法来测试和分析来自金属单尖端发射器的实验场电子发射电流-电压数据;这种新颖而简单的方法被称为墨菲-古德图。以钨基电子发射体为例,采用电化学刻蚀法制备了钨基电子发射体。利用传统的场发射显微镜在高真空条件下获得了电流-电压特性。采用Murphy-Good图对实验数据进行著名的场电子发射正统检验,如果检验通过,则提取发射体的表征参数。与传统的Fowler-Nordheim和Millikan-Lauritsen方法不同,这种方法的新颖之处在于它不依赖任何校正因子,而且理论形式简单。使用简单的web工具计算结果,该工具将场电子发射正统性测试应用于任何类型的电流-电压分析图,然后提取发射器的表征参数。
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引用次数: 3
Systematic growth of carbon nanotubes on aluminum substrate for enhanced field emission performance 在铝衬底上系统生长碳纳米管以增强场发射性能
P. Maity, S. Gandhi, Manuj Dixit, I. Lahiri
For more than two decades, carbon nanotubes (CNTs) have shown great potential for a wide range of applications. Several methods are known to synthesize CNTs, though only a few of them are able to produce good quality and economically available CNTs. Chemical vapor deposition (CVD) is one of those methods that produce economically feasible and good quality CNTs onto specific substrates, even with nanopatterning. However, growing CNTs by CVD at temperatures below 700 °C remained a long-time challenge, as this meant keeping a host of low-melting materials out of bounds for direct CNT growth on them. In this work, CNTs have been synthesized directly onto a low-melting, conducting substrate, aluminum, by thermal CVD, at a temperature as low as 550 °C and up to as high as 650 °C (just below the melting point of aluminum). The diameters of the grown CNTs were observed to be influenced by process parameters, e.g., temperature and pressure. The effect of synthesis parameters on CNT diameters was verified by scanning electron microscopy and transmission electron microscopy. The quality of the CNTs was checked by Raman spectroscopy, selected area electron diffraction pattern of transmission electron microscopy, and XPS. It was observed that an increase in temperature and pressure had a significant effect on the diameters of the CNTs. Randomly entangled CNTs were measured to have an average diameter of 28 nm at 550 °C and one atmospheric (760 Torr) pressure, whereas it was observed to be 78 nm at a temperature of 650 °C and pressure of 0.01 Torr. The field emission response, i.e., the turn-on field (2.5 V/μm) and the maximum emission current density (2.17 mA/cm2) of the CNTs synthesized at the temperature of 550 °C and pressure of 1 atm (760 Torr) was found to be excellent.
近二十年来,碳纳米管(CNTs)已显示出广泛的应用潜力。目前已知几种合成碳纳米管的方法,但只有少数几种方法能够制备出高质量且经济可行的碳纳米管。化学气相沉积(CVD)是在特定衬底上生产经济可行且质量良好的碳纳米管的方法之一,即使采用纳米图案。然而,在低于700°C的温度下通过CVD生长碳纳米管仍然是一个长期的挑战,因为这意味着要保持大量低熔点材料在其上直接生长碳纳米管的范围之外。在这项工作中,通过热气相沉积法将碳纳米管直接合成到低熔点的导电衬底铝上,温度低至550℃,高至650℃(刚好低于铝的熔点)。观察到生长的CNTs的直径受工艺参数(如温度和压力)的影响。通过扫描电镜和透射电镜验证了合成参数对碳纳米管直径的影响。通过拉曼光谱、透射电子显微镜的选定区域电子衍射图和XPS检查CNTs的质量。观察到温度和压力的增加对CNTs的直径有显著影响。随机缠绕的碳纳米管在550°C和一个大气压(760 Torr)下的平均直径为28 nm,而在650°C和0.01 Torr压力下的平均直径为78 nm。在550℃、760 Torr (1atm)压力下合成的CNTs具有优异的场发射响应性能,即导通场(2.5 V/μm)和最大发射电流密度(2.17 mA/cm2)。
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引用次数: 2
Development of microfabricated planar slow-wave structures on dielectric substrates for miniaturized millimeter-band traveling-wave tubes 微型化毫米波段行波管介质基板微加工平面慢波结构的研究
N. Ryskin, Roman A. Torgashov, A. Starodubov, A. Rozhnev, A. Serdobintsev, A. Pavlov, V. Galushka, D. Bessonov, G. Ulisse, V. Krozer
We report the results of the design, simulation, fabrication, and cold-test measurements of millimeter-band 2D planar microstrip slow-wave structures (SWSs) on dielectric substrates. Such structures have a high slow-wave factor, which allows for low-voltage operation and reduction in the size and weight of the device. A low-cost and flexible fabrication technology based on magnetron sputtering and subsequent laser ablation has been developed and is reported in the paper. Microstrip meander-line SWS circuits at V-, W-, and D-bands have been fabricated and characterized. The fabrication of ring-bar planar SWSs by the photolithographic method is also discussed. Experimental measurement of S-parameters of the fabricated structures reveals good transmission properties. Return loss (S11) does not exceed −10 dB and attenuation is about 2 dB/cm in the V-band, 10 dB/cm in the W-band, and 8.5 dB/cm in the D-band.
本文报道了介电基片上毫米波段二维平面微带慢波结构(SWSs)的设计、模拟、制造和冷试验测量结果。这种结构具有很高的慢波系数,允许低电压操作并减小设备的尺寸和重量。本文报道了一种基于磁控溅射和后续激光烧蚀的低成本柔性制造技术。制备了V、W、d波段的微带弯曲线SWS电路,并对其进行了表征。本文还讨论了光刻法制备环形棒状平面SWSs的方法。实验结果表明,该结构具有良好的传输性能。回波损耗(S11)不超过−10 dB, v波段衰减约为2db /cm, w波段衰减约为10db /cm, d波段衰减约为8.5 dB/cm。
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引用次数: 13
High signal-to-noise ratio differential conductance spectroscopy 高信噪比差分电导光谱
Hamed Alemansour, S. Moheimani, J. Owen, J. Randall, E. Fuchs
The scanning tunneling microscope (STM) has enabled manipulation and interrogation of surfaces with atomic-scale resolution. Electronic information about a surface is obtained by combining the imaging capability of the STM with scanning tunneling spectroscopy, i.e., measurement of current-voltage (I/V) characteristics of the surface. We propose a change in the STM feedback loop that enables capturing a higher quality dI/dV image. A high frequency dither voltage is added to the bias voltage of the sample, and the fundamental frequency component of the resulting current is demodulated. The in-phase component of this signal is then plotted along with the X and Y position data, constructing the dI/dV image. We show that by incorporating notch filters in the STM feedback loop, we may utilize a high-amplitude dither voltage to significantly improve the quality of the obtained dI/dV image.
扫描隧道显微镜(STM)已经实现了对原子尺度分辨率表面的操纵和探测。通过将STM的成像能力与扫描隧道光谱相结合,即测量表面的电流-电压(I/V)特性,获得表面的电子信息。我们建议改变STM反馈回路,以捕获更高质量的dI/dV图像。将高频抖动电压加到样品的偏置电压上,并解调所产生电流的基频分量。然后将该信号的同相分量与X和Y位置数据一起绘制,构建dI/dV图像。我们表明,通过在STM反馈回路中加入陷波滤波器,我们可以利用高幅度抖动电压来显着提高获得的dI/dV图像的质量。
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引用次数: 1
期刊
Journal of Vacuum Science & Technology. B. Nanotechnology and Microelectronics: Materials, Processing, Measurement, and Phenomena
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