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Pack-boriding of Sleipner steel: microstructure analysis and kinetics modeling 斯莱普纳钢的包硼化:微观结构分析和动力学建模
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-24 DOI: 10.1515/mt-2023-0331
Peter Orihel, Jana Ptačinová, P. Gogola, M. Keddam, P. Jurči
Abstract In this research work, we subjected the Sleipner steel to pack-boronizing within the temperature range of 1173–1323 K, lasting from 1 to 10 h. Our study involved assessing the steel’s microstructure by examining interphase morphology and measuring the layers’ thicknesses through scanning electron microscopy. To determine the phase composition of the boronized layers, we employed X-ray diffraction analysis. Furthermore, we investigated the redistribution of certain elements during the boronizing process using EDS mapping and EDS point analysis. The boride layers were found to consist of FeB and Fe2B phases. We conducted microhardness testing using the Vickers method on the diffusion zone, Fe2B, and FeB. Lastly, we utilized a diffusion model to evaluate the activation energies of boron in FeB and Fe2B, and we presented the results in terms of activation energies.
摘要 在这项研究工作中,我们在 1173-1323 K 的温度范围内对 Sleipner 钢进行了 1 到 10 小时的包硼处理。我们的研究包括通过相间形态检查和扫描电子显微镜测量层厚度来评估钢的微观结构。为了确定硼化层的相组成,我们采用了 X 射线衍射分析法。此外,我们还利用 EDS 图谱和 EDS 点分析法研究了硼化过程中某些元素的重新分布情况。结果发现,硼化物层由 FeB 和 Fe2B 相组成。我们使用维氏方法对扩散区、Fe2B 和 FeB 进行了显微硬度测试。最后,我们利用扩散模型评估了硼在 FeB 和 Fe2B 中的活化能,并以活化能的形式展示了结果。
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引用次数: 0
Identifying stir casting process parameters to maximize strength of LM13 with TiB2 and ZrC hybrid metal matrix composite 确定搅拌铸造工艺参数,最大限度提高含 TiB2 和 ZrC 混合金属基复合材料的 LM13 的强度
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-21 DOI: 10.1515/mt-2023-0193
B. Siddharthan, Kumaravel Arumugam
Abstract In this study, an LM13 metal-matrix composite was fabricated using two reinforcement particles (hard and soft) of titanium diboride and zirconium carbide. An experimental design was used to narrow down the trials. The significance of the model was tested using Student’s t-test and p values. The response surface statistical method was used to obtain the optimum process parameters for the high-strength hybrid metal matrix composite. From the experimental results, a maximum strength of 209 MPa was gained at a stirrer speed of 700 rpm, weight fraction of TiB2 and ZrC of 9 %, and casting temperature of 675 °C. The ANOVA results showed that TiB2 was the main influential process parameter, followed by the stirrer speed, casting temperature, and zirconium boride. The microstructure showed a fine and uniform distribution of reinforcement particles in the LM13 matrix. The fracture surface exhibited a mixed fracture pattern, which was due to the good bonding between the reinforcement and matrix at the interface.
摘要 本研究使用二硼化钛(Titanium diboride)和碳化锆(Zirconium carbide)两种增强颗粒(硬质和软质)制作了 LM13 金属基复合材料。实验设计用于缩小试验范围。使用学生 t 检验和 p 值检验了模型的显著性。采用响应面统计方法获得了高强度混合金属基复合材料的最佳工艺参数。实验结果表明,在搅拌器转速为 700 rpm、TiB2 和 ZrC 的重量分数为 9 %、浇铸温度为 675 °C 的条件下,获得的最大强度为 209 MPa。方差分析结果表明,TiB2 是主要的影响工艺参数,其次是搅拌器速度、浇铸温度和硼化锆。微观结构显示,强化颗粒在 LM13 基体中分布细小均匀。断裂面呈现出混合断裂模式,这是由于在界面处增强体与基体之间的良好结合。
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引用次数: 0
Performance of additively manufactured Ti6Al4V ELI finger joints: biomechanical testing and evaluation for arthritis management 添加式制造的 Ti6Al4V ELI 手指关节的性能:生物力学测试和关节炎管理评估
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-21 DOI: 10.1515/mt-2023-0328
Panaruj Bussayasripatt, Kitti Poungsiri, Chetarpa Yipyintum, Chris Charoenlap, Chindanai Hongsaprabhas, K. Pataradool, Thanawat Tantimethanon, Thanawat Phetrattanarangsi, C. Puncreobutr, B. Lohwongwatana
Abstract Approximately 24 out of every 100 adults in the United States, or 58.5 million people, have arthritis, which refers to a condition that causes pain and inflammation in a joint according to US National Center for Chronic Disease Prevention and Health Promotion. Osteoarthritis is the most common type of arthritis, and it may damage almost any joint but mainly occur in hands, hips and knees. While there are several joint replacement options for hips and knees, there are only limited options for finger joints. In this paper, we report on several aspects of testing of novel finger joints: testing apparatus design, cadaveric performance test and material testing results of titanium joints using 3D-printed Ti6Al4V extra low interstitial (ELI). Soft cadaveric hands with finger joints were surgically replaced by additively manufactured titanium joints following the exact same anatomy of the cadavers. These small joints were engineered to mimic the biological and natural movements of fingers. The apparatus, methodology and results of biomechanical tests were deployed to evaluate and validate the joints particularly those of titanium joints manufactured via laser powder bed fusion methods (PBF-L/M).
摘要 根据美国国家慢性病预防和健康促进中心的数据,在美国,每 100 个成年人中约有 24 人,即 5850 万人患有关节炎。骨关节炎是最常见的关节炎类型,它几乎可以损害任何关节,但主要发生在手、臀部和膝盖。虽然髋关节和膝关节有多种关节置换选择,但手指关节的选择却很有限。在本文中,我们报告了新型手指关节测试的几个方面:测试仪器设计、尸体性能测试和使用 3D 打印 Ti6Al4V 超低间隙(ELI)钛关节的材料测试结果。根据尸体的解剖结构,用添加剂制造的钛关节通过手术替换了带有手指关节的软尸体手。这些小关节的设计模仿了手指的生物和自然运动。生物力学测试的仪器、方法和结果用于评估和验证关节,特别是通过激光粉末床融合方法(PBF-L/M)制造的钛关节。
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引用次数: 0
Design optimization of hybrid material B-pillar under crush loading 破碎载荷下混合材料b柱的设计优化
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-15 DOI: 10.1515/mt-2023-0069
İsmail Öztürk
Abstract B-pillars are vital structural components in rollover-related accidents. In this study, the performances of homogeneous B-pillars designed from B1500HS-T25, AA2024-T351, and AA6061-T6 materials and hybrid B-pillars designed from their combinations under crushing load were compared in energy absorption using simulation results. Optimization studies were conducted utilizing the upper part B1500HS-T25 and lower part AA6061-T6 hybrid B-pillar, which gave the highest energy absorption value. Method of feasible directions was utilized to solve the single-objective optimization, and B-pillar mass decreased by 22.6 % from 2.736 to 2.117 kg compared with the reference B-pillar. Global Response Search Method and Multi-Objective Genetic Algorithm were used to solve the multi-objective optimization problem. B-pillar with min mass decreased mass value by 25 % from 2.736 to 2.052 kg for both methods. This optimum hybrid B-pillar can be utilized in car design.
b柱是侧翻事故中重要的结构部件。本研究通过仿真结果,比较了采用B1500HS-T25、AA2024-T351和AA6061-T6材料设计的均质b柱和采用其组合设计的混合b柱在破碎载荷作用下的吸能性能。利用上部B1500HS-T25和下部AA6061-T6混合型b柱进行了优化研究,两者吸能值最高。采用可行方向法进行单目标优化,b柱质量从2.736 kg降至2.117 kg,比参考b柱质量降低22.6%。采用全局响应搜索法和多目标遗传算法求解多目标优化问题。采用最小质量的b柱,两种方法的质量值均从2.736 kg下降到2.052 kg,降幅达25%。该优化混合动力b柱可用于汽车设计。
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引用次数: 0
Investigation of the effects of halloysite nanoclay on friction and wear behavior of automotive brake pads 高岭土纳米粘土对汽车刹车片摩擦磨损性能的影响研究
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-14 DOI: 10.1515/mt-2023-0027
Hüseyin Bayrakçeken, Hicri Yavuz
Abstract They are produced with the desired performance with friction modifiers, reinforcements, lubricants, binders, and fillers used in various properties in brake pads. This study investigated the effect of the use of halloysite nanoclay material used in different sectors as a filler in brake pads. The hot-pressing method produced brake pad samples containing 10–15 % and 20 % halloysite nanoclay. A full-scale brake pad tester determined the samples’ friction coefficient and wear rates. Scanning electron microscopy (SEM) and 3D profilometer analyses were performed on the worn sample surfaces after the experiment. As a result, it was determined that the halloysite nanoclay samples met the desired brake lining properties.
它们是用摩擦改性剂、增强剂、润滑剂、粘结剂和填料生产的,具有所需的性能,用于各种性能的刹车片。本研究探讨了高岭土纳米粘土材料作为刹车片填料在不同行业的应用效果。采用热压法制备了含10 - 15%和20%高岭土纳米粘土的刹车片样品。一个全尺寸的刹车片测试仪测定了样品的摩擦系数和磨损率。实验结束后,对磨损试样表面进行扫描电镜和三维轮廓仪分析。结果表明,高岭土纳米粘土样品满足制动衬片的性能要求。
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引用次数: 0
Structural comparison of conventional and chiral auxetic morphed aircraft rib 常规与手性变形飞机肋的结构比较
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-14 DOI: 10.1515/mt-2023-0155
Cevher Yusuf Inan, Zafer Evis, Berkan Ozturk
Abstract Tri-chiral structures are auxetic structures that show negative Poisson’s ratio. This effect is due to their microstructure and geometric sequence. They are used in the development of novel products as they show improved damping and energy absorption properties. While traditional manufacturing methods remain dysfunctional, the development of additive manufacturing technology provides opportunities for new studies in various industries such as aviation, textile, and automotive. In this study, passive airfoil morphing application was applied and a comparative study was carried out. A two-stage study was conducted. First, the tri-chiral pattern was fabricated by an FDM 3D printer with PLA+ and subjected to the in-plane compression test. Stress–strain curves of the tri-chiral structure were generated. Then, it was used in airfoil morphing applications. Morphed airfoil was also manufactured and a compression test was applied. Secondly, the aerostatic loads of the aircraft were calculated. Both conventional and chiral morphed ribs’ behaviors under flight loads were examined using the FEM and results were compared. The weight difference was calculated. In addition, eigenfrequency and eigenvectors of traditional and chiral ribs were computed and transverse vibration frequencies were expressed. Despite being more than 50 % lighter, chiral morphed rib was found to be stiffer than conventional rib.
摘要:三手性结构是具有负泊松比的生长型结构。这种效应是由于它们的微观结构和几何顺序。它们被用于新产品的开发,因为它们表现出改善的阻尼和能量吸收特性。虽然传统的制造方法仍然功能失调,但增材制造技术的发展为航空、纺织和汽车等各个行业的新研究提供了机会。在本研究中,采用被动翼型变形应用,并进行了对比研究。进行了两个阶段的研究。首先,在FDM 3D打印机上用PLA+制备了三手性图案,并进行了面内压缩试验。生成了三手性结构的应力-应变曲线。然后,它被用于翼型变形应用。变形翼型也制造和压缩试验应用。其次,对飞机的气动载荷进行了计算。采用有限元方法研究了常规变形肋和手性变形肋在飞行载荷作用下的性能,并对结果进行了比较。计算重量差。此外,计算了传统肋和手性肋的特征频率和特征向量,并表示了横向振动频率。尽管重量轻了50%以上,但研究发现手性变形肋骨比传统肋骨更硬。
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引用次数: 0
Adhesive wear behavior and microstructure of FeCr–FeMn–FeB–C coatings FeCr-FeMn-FeB-C涂层的黏着磨损性能及显微组织
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-03 DOI: 10.1515/mt-2023-0347
Mehmet Yaz
Abstract This study employs a high-energy-density gas tungsten arc welding (GTAW) process to fabricate a surface coating on a substrate of 0.15 percent carbon steel, incorporating powders of FeCr, FeMn, FeB, and graphite. The investigation encompasses a multifaceted approach, utilizing X-ray diffraction (XRD), optical micrograph (OM) analysis, energy-dispersive X-ray analysis (EDS), scanning electron microscopy (SEM) imaging, microhardness testing, and adhesive wear testing, with the aim of examining the composite coating’s microstructural attributes, microhardness, and performance under dry-sliding wear conditions. The research findings reveal the formation of diverse carbides and borides, including Mn 5 C 2 , Fe 3 C, B 8 C, B 4 C, Fe 3 B, Fe 7 C 3 , FeB, and MnB on the coated surfaces. Notably, the graphite particles within the FeB–FeMn–FeCr–C composite TIG welding coatings exhibit a range of morphologies, varying from sheet-like to dendritic structures.
本研究采用高能量密度气体钨极电弧焊(GTAW)工艺,在0.15%碳钢基体上制备了一层表面涂层,并加入了FeCr、FeMn、FeB和石墨粉末。研究包括多方面的方法,利用x射线衍射(XRD)、光学显微照片(OM)分析、能量色散x射线分析(EDS)、扫描电子显微镜(SEM)成像、显微硬度测试和粘着磨损测试,目的是检查复合涂层的微观结构属性、显微硬度和干滑动磨损条件下的性能。研究结果表明,涂层表面形成了多种碳化物和硼化物,包括mn2c、fe3c、b8c、b4c、fe3b、fe7c3、FeB和MnB。值得注意的是,在FeB-FeMn-FeCr-C复合TIG焊接涂层中的石墨颗粒表现出一系列的形态,从片状结构到枝晶结构不等。
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引用次数: 0
Frontmatter 头版头条
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-11-01 DOI: 10.1515/mt-2023-frontmatter11
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引用次数: 0
Tribo-corrosion behavior of electroplating, nitrocarburizing, and QPQ processes on barrel finishing 电镀、氮化碳和QPQ工艺对桶体精加工的摩擦腐蚀行为
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-10-19 DOI: 10.1515/mt-2023-0056
Aysu Hande Yucel, Alpay Yilmaz, Mustafa Bakkal, Ali Taner Kuzu
Abstract In this study, the effects of nitrocarburizing, QPQ, and Cr coating on the surface properties of 32CrMoV12-10 gun barrels are discussed. Hardness measurements, pin-on-disc tests, and anodic polarization tests were performed to examine the hardness values, wear resistance, friction coefficient, and corrosion resistance. The hardness of the specimen treated with QPQ was found to be the highest. Comparing the hardness profiles, it was observed that the casing depth of the nitrocarburized sample was shallower than that of the QPQ-treated sample. The pin-on-disc test revealed that the nitrocarburized sample exhibited a high coefficient of friction, while the Cr-coated sample showed the lowest coefficient of friction. Analyzing the Tafel polarization curve, it was determined that the nitrocarburized and QPQ-treated specimens demonstrated similar levels of corrosion resistance. However, it can be noted that the QPQ-treated specimen had a slightly lower corrosion rate.
摘要本研究探讨了氮碳共渗、QPQ和Cr涂层对32CrMoV12-10枪管表面性能的影响。通过硬度测量、销盘测试和阳极极化测试来检验硬度值、耐磨性、摩擦系数和耐腐蚀性。经QPQ处理后的试样硬度最高。对比硬度分布,发现氮碳处理后的套管深度比qpq处理后的套管深度浅。销盘试验结果表明,氮碳涂层试样的摩擦系数较高,而cr涂层试样的摩擦系数最低。通过对Tafel极化曲线的分析,确定了氮碳处理和qpq处理的试样具有相似的耐蚀性。然而,可以注意到,经过qpq处理的试样具有稍低的腐蚀速率。
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引用次数: 0
Optimum design of a seat bracket using artificial neural networks and dandelion optimization algorithm 基于人工神经网络和蒲公英优化算法的座椅支架优化设计
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-10-13 DOI: 10.1515/mt-2023-0201
Mehmet Umut Erdaş, Mehmet Kopar, Betül Sultan Yildiz, Ali Riza Yildiz
Abstract Nature-inspired metaheuristic algorithms are gaining popularity with their easy applicability and ability to avoid local optimum points, and they are spreading to wide application areas. Meta-heuristic optimization algorithms are used to achieve an optimum design in engineering problems aiming to obtain lightweight designs. In this article, structural optimization methods are used in the process of achieving the optimum design of a seat bracket. As a result of topology optimization, a new concept design of the bracket was created and used in shape optimization. In the shape optimization, the mass and stress values obtained depending on the variables, constraint, and objective functions were created by using artificial neural networks. The optimization problem based on mass minimization is solved by applying the dandelion optimization algorithm and verified by finite element analysis.
自然启发式元启发式算法以其简单的适用性和避免局部最优点的能力而越来越受到人们的欢迎,并得到了广泛的应用。在以轻量化设计为目标的工程问题中,采用元启发式优化算法实现最优设计。本文将结构优化方法应用于实现座椅支架优化设计的过程中。在拓扑优化的基础上,提出了一种新的支架概念设计,并将其应用于支架的形状优化。在形状优化中,利用人工神经网络建立了依赖于变量、约束和目标函数的质量和应力值。应用蒲公英优化算法求解了基于质量最小化的优化问题,并进行了有限元分析验证。
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引用次数: 0
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Materials Testing
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