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Fatigue performance of laser cut carbon fiber-reinforced epoxy and polyamide 6 considering specimen width 考虑试样宽度的激光切割碳纤维增强环氧树脂和聚酰胺6的疲劳性能
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-08 DOI: 10.1515/mt-2023-0170
L. Gerdes, S. Mrzljak, J.-M. Keuntje, V. Wippo, P. Jaeschke, Frank Walther
Abstract Since the development of laser systems technology led to a significantly decreased energy input by pulsing, laser cutting became a noteworthy method for cutting fiber-reinforced polymers. Despite the occurrence of heat introduction and heat-affected zones (HAZ), there are advantages regarding processing speed and maneuverability. Within this work, the influence of two cutting parameters (low (A) and high heat introduction (B)) on the fatigue properties of carbon fiber–reinforced epoxy and polyamide 6 were investigated. At the same time, micro waterjet cut specimens were added as a reference. In doing so, laminates were cut to different specimen widths and orientations. Multiple amplitude tests were performed with strain and temperature measurements. The results show an influence of specimen width on fatigue lifetime for the epoxy system, but not in polyamide 6. The 45° specimens for both CFR-EP and CFR-PA6 showed a decreased lifetime when cut with parameters B. However, these findings do not apply to 0° specimens, since parameters A lead to a smaller lifetime for CFR-EP, and no influence was found for CFR-PA6. Furthermore, no clear HAZ could be identified for A. Since there is a decrease in lifetime for CFR-EP, the necessity of applying further methods for HAZ detection is described.
由于激光系统技术的发展导致脉冲能量输入显著减少,激光切割成为一种值得注意的切割纤维增强聚合物的方法。尽管存在热引入和热影响区(HAZ),但在加工速度和可操作性方面具有优势。在这项工作中,研究了两种切削参数(低(A)和高热引入(B))对碳纤维增强环氧树脂和聚酰胺6疲劳性能的影响。同时,加入微水射流切割试样作为参考。在此过程中,层压板被切割成不同的试样宽度和方向。通过应变和温度测量进行了多次振幅测试。结果表明,试样宽度对环氧树脂体系的疲劳寿命有影响,而对聚酰胺6体系的疲劳寿命没有影响。在45°的CFR-EP和CFR-PA6样品中,当用参数b切割时,CFR-EP和CFR-PA6的寿命都缩短了。然而,这些发现不适用于0°的样品,因为参数a导致CFR-EP的寿命缩短,而对CFR-PA6没有发现影响。此外,由于CFR-EP的寿命减少,因此需要应用进一步的HAZ检测方法。
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引用次数: 0
Tensile, bending, and impact properties of laminated carbon/aramid/glass hybrid fiber composites 层压碳/芳纶/玻璃混杂纤维复合材料的拉伸、弯曲和冲击性能
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-08 DOI: 10.1515/mt-2023-0207
S. Ekşi, Fatih Emir Danyildiz, Neslihan Özsoy, Murat Özsoy
Abstract In this study, hybrid (carbon, glass, and aramid) fabric epoxy composite laminates were fabricated with different layering sequences by hand lay-up. The effects of layering arrangements of laminated composite fibers on the mechanical properties of hybrid composites were investigated. Tensile, bending, and impact tests were performed to obtain the mechanical behaviors of hybrid composites. It was found that the layering sequences significantly affect the tensile, bending strength, and impact energy. As a result of the tensile tests, the highest tensile strength was obtained in the 3C + 3G combination. The highest load-carrying capacity in three-point bending tests was obtained in the 2G + 2A + 2C combination. The combination with the highest impact energy was 2C + 2G + 2A, and the lowest was 3C + 3G. It has been observed that hybrid composites containing aramid fiber absorb higher impact energy than others. The results showed that the layering sequences are essential in hybrid composites with the same fiber and layer number.
摘要本研究采用手工铺层的方法,制备了碳、玻璃、芳纶等杂化环氧复合材料层合板。研究了复合纤维层状排列方式对混杂复合材料力学性能的影响。进行了拉伸、弯曲和冲击试验,获得了混杂复合材料的力学行为。结果表明,分层顺序对材料的拉伸强度、弯曲强度和冲击能有显著影响。拉伸试验结果表明,在3C + 3G组合中拉伸强度最高。在三点弯曲试验中,2G + 2A + 2C组合的承载能力最高。冲击能最高的组合为2C + 2G + 2A,最低的组合为3C + 3G。含有芳纶纤维的杂化复合材料比其他复合材料吸收更高的冲击能。结果表明,在相同纤维数和层数的混杂复合材料中,层序是至关重要的。
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引用次数: 0
Effect of carbon nanotubes on microstructure and mechanical properties of TiZrVMnCu–Er high entropy alloy composites 碳纳米管对TiZrVMnCu-Er高熵合金复合材料组织和力学性能的影响
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-08 DOI: 10.1515/mt-2023-0066
Xing Wang, Xiao-song Jiang, Jinmei Chen, Hongliang Sun
Abstract To improve the ductility and toughness of refractory high entropy alloy (Ti, Zr, V), Mn and Cu were added to form TiZrVMnCu high entropy alloy with soft and hard phases. Carbon nanotubes (CNTs) and Er were introduced to fabricated composites with high strength and ductility. The relative density, microhardness, and compressive strength of TiZrVMnCu–Er–CNTs composites were in direct proportional to CNTs content from 0 to 0.5 wt%. The composite with 0.5 wt% CNTs has the highest hardness (634.4 HV) and strength (1720.7 MPa), and the strain variable is 14.3 %. The fracture toughness of the composites was improved by the crack bridging mechanism and crack deflection mechanism induced by adding CNTs. The fine grain, second phase strengthening mechanism, and the load transfer mechanism induced by CNTs improved the strength and hardness of the composites. Er can achieve solid solution strengthening or play a role in the second phase and fine grain strengthening.
摘要:为了提高难熔高熵合金(Ti, Zr, V)的延展性和韧性,在合金中加入Mn和Cu,形成具有软硬相的TiZrVMnCu高熵合金。将碳纳米管(CNTs)和铒(Er)引入制备高强度、高延展性复合材料。在0 ~ 0.5 wt%范围内,TiZrVMnCu-Er-CNTs复合材料的相对密度、显微硬度和抗压强度与CNTs含量成正比。CNTs含量为0.5 wt%的复合材料具有最高的硬度(634.4 HV)和强度(1720.7 MPa),应变变量为14.3 %。复合材料的断裂韧性通过添加CNTs引起的裂纹桥接机制和裂纹挠曲机制得到提高。CNTs诱导的细晶粒、第二相强化机制和载荷传递机制提高了复合材料的强度和硬度。Er可实现固溶强化或在第二相和细晶强化中起作用。
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引用次数: 0
Experimental investigation of mechanical properties of PLA, ABS, and PETG 3-d printing materials using fused deposition modeling technique 采用熔融沉积建模技术对PLA、ABS和PETG三维打印材料的力学性能进行了实验研究
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-08 DOI: 10.1515/mt-2023-0202
Mehmet Kopar, Ali Riza Yildiz
Abstract In recent years, there has been a logarithmic interest in three-dimensional printing technologies. This technique has made it possible to make more intricately shaped parts of superior quality, allowing for use in a variety of industries, including aircraft, automobiles, and ships. This study characterized the materials and assessed the mechanical features of PLA, PETG, and ABS materials generated at various raster angles. The strength ratios of the various materials have been found to fluctuate when the raster angles change. The PLA parts created at a picture raster angle of 45° had the maximum tensile strength. ABS material created with a picture raster angle of 45° has been shown to have the best energy absorption, and PLA material made with a raster angle of 45° has the best performance compressive strength. When bending strength was evaluated, it was found that samples of ABS made with a raster angle of 0–90° had the greatest value. The SEM micrographs were obtained, and the tensile test was used to examine the fracture behavior of the materials. As a result, it has been found that materials created using various raster angles can have various strength values from one another.
近年来,人们对三维打印技术产生了对对数的兴趣。这种技术使得制造更复杂形状的高质量零件成为可能,允许在各种工业中使用,包括飞机、汽车和船舶。本研究对材料进行了表征,并评估了PLA、PETG和ABS材料在不同光栅角度下的力学特性。各种材料的强度比随着光栅角度的变化而波动。以45°的图像光栅角度创建的PLA部件具有最大的拉伸强度。图像光栅角度为45°的ABS材料具有最佳的吸能性能,而图像光栅角度为45°的PLA材料具有最佳的抗压强度性能。在进行抗弯强度评估时,发现栅格角度为0-90°的ABS样品值最大。获得了SEM显微图像,并通过拉伸试验检测了材料的断裂行为。因此,已经发现使用各种光栅角度创建的材料可以具有彼此不同的强度值。
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引用次数: 0
Electrochemical, mechanical, and antibacterial properties of the AZ91 Mg alloy by hybrid and layered hydroxyapatite and tantalum oxide sol–gel coating 羟基磷灰石和氧化钽混合层状溶胶-凝胶涂层对AZ91镁合金电化学、力学和抗菌性能的影响
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-08 DOI: 10.1515/mt-2023-0138
Sevda Albayrak, Canser Gül, Nuray Emin, U. Gökmen, Halil Karakoç, A. Uzun, H. Çinici
Abstract The corrosion and bacterial behavior of AZ91 magnesium alloy coated with sol–gel-deposited amorphous tantalum oxide and hydroxyapatite have been investigated. The objective was to assess the potential suitability of AZ91 for permanent prosthesis applications. The coatings were applied in layered and hybrid configurations and characterized using various techniques including X-ray diffractometry, Fourier transform infrared spectroscopy, scanning electron microscopy/energy dispersive spectrometry, and drop analyses. The antibacterial properties were evaluated through interactions with Staphylococcus aureus and Escherichia coli strains. Mechanical properties and adhesion were determined via linear scratch tests, and electrochemical corrosion tests were conducted in different media. The release of aluminum ions from the samples in Dulbecco’s Modified Eagle’s Medium was monitored over 28 days. The findings revealed that the amorphous tantalum oxide coating, particularly in combination with hydroxyapatite, improved antibacterial properties and positively influenced corrosion and scratch resistance. The layered and hybrid coatings demonstrated the highest corrosion resistance. The release of aluminum ions remained within acceptable levels in the tested medium. Overall, the study provides valuable insights into the potential of sol–gel coatings on AZ91 for prosthetic applications, considering antibacterial behavior, corrosion resistance, and aluminum release.
摘要研究了溶胶-凝胶沉积无定形氧化钽和羟基磷灰石涂层AZ91镁合金的腐蚀和细菌行为。目的是评估AZ91用于永久性假体应用的潜在适用性。涂层以层状和混合结构应用,并使用各种技术进行表征,包括x射线衍射、傅里叶变换红外光谱、扫描电子显微镜/能量色散光谱和液滴分析。通过与金黄色葡萄球菌和大肠杆菌的相互作用评价其抗菌性能。通过线性划痕试验和电化学腐蚀试验测定了复合材料的力学性能和附着力。在Dulbecco 's Modified Eagle 's Medium中,对样品中铝离子的释放进行了28天的监测。结果表明,非晶态氧化钽涂层,特别是与羟基磷灰石结合,提高了抗菌性能,并对耐腐蚀和抗划伤性能产生了积极影响。层状和杂化涂层具有最高的耐蚀性。在测试介质中,铝离子的释放保持在可接受的水平。总的来说,该研究为AZ91溶胶-凝胶涂层在假肢应用中的潜力提供了有价值的见解,考虑到抗菌行为、耐腐蚀性和铝释放。
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引用次数: 0
Effect of polyurethane matrix and steel fiber in combination with glass fiber or basalt fiber on the properties of hybrid composite laminates 聚氨酯基体和钢纤维与玻璃纤维或玄武岩纤维复合对混杂复合层压板性能的影响
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-09-01 DOI: 10.1515/mt-2023-0026
Bayan Jabbar Fayzulla, Mehmet Eroglu, Ahmet Erkliğ
Abstract Polyurethane is a versatile polymer with a high degree of toughness and ductility used in a wide variety of applications. In this study, two-part thermoset polyurethane was used as a matrix material to prepare hybrid and non-hybrid composites. Hybrid laminates were prepared by combining either glass fiber or basalt fibers with steel fibers. The mechanical properties of prepared composite specimens were characterized and scanning electron microscope (SEM) observation was performed around the fracture region of the tested specimens. The results revealed a significant increment in tensile strength, and flexural strength in BS 1 -PU (8 layers of basalt-1 layer of steel) hybrid laminate by 357.74 % and 64.59 %, respectively, compared to steel fibers reinforced polyurethane composites. Furthermore, GS 4 -PU hybrid composite (5 layers of glass-4 layers of steel) achieved an improvement in tensile strain by 12.07 %, flexural strain by 25.32 %, and absorbed energy by 18.21 %, compared to glass fibers reinforced polyurethane composite. Moreover, the SEM observations revealed that the replacement of some basalt and glass layers with steel layers leads to a positive hybridization effect of the overall produced hybrid composites.
聚氨酯是一种多用途聚合物,具有高度的韧性和延展性,应用广泛。本研究以双组分热固性聚氨酯为基体材料,制备了杂化和非杂化复合材料。将玻璃纤维或玄武岩纤维与钢纤维复合制备了混杂层合板。对制备的复合材料试样进行了力学性能表征,并对试样断口周围进行了扫描电镜(SEM)观察。结果表明,与钢纤维增强聚氨酯复合材料相比,BS 1 -PU(8层玄武岩-1层钢)复合材料的抗拉强度和抗折强度分别提高了357.74%和64.59%。与玻璃纤维增强聚氨酯复合材料相比,gs4 -PU复合材料(5层玻璃-4层钢)的拉伸应变提高12.07%,弯曲应变提高25.32%,吸收能量提高18.21%。此外,SEM观察表明,用钢层取代部分玄武岩层和玻璃层导致了整体杂化复合材料的正杂化效应。
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引用次数: 0
Frontmatter 头版头条
4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-08-31 DOI: 10.1515/mt-2023-frontmatter9
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引用次数: 0
A19-saponin–modified polymethyl methacrylate base denture composites: antimicrobial, mechanical and water absorption potentials a19 -皂苷改性聚甲基丙烯酸甲酯基托复合材料:抗菌、机械和吸水电位
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-08-31 DOI: 10.1515/mt-2023-0017
T. O. Azeez, Grace Onyinyechi Iroh, Daniel Segun Odetunde, Amaka Tessy Egbuonu, P. Agbasi
Abstract The increased growth of Candida albicans (C. albicans) with allergy reaction of MMA remains an issue of concern among denture wearers. C. albicans growth inhibition, mechanical and water absorption potentials of extracted A19-saponin–commingled PMMA denture base composites were investigated. Soxhlet extraction technique for defatting of Dialium guineense (D. guineense) stem powder was used with ethanol to extract A19-saponin. Fungicidal inhibition concentration of A19-saponin extract of D. guineense was determined. PMMA denture base was prepared with incorporation of A19-saponin at different concentrations of obtained 23.2 % yield. The mechanical and water absorption properties were determined. The minimum and maximum fungicidal inhibition concentrations and susceptibility of 25 and 100 % for extracted A19-saponin were obtained, respectively. PMMA, MMA and extracted A19-saponin of ratio of 30 g: 5 ml: 5 ml denture was optimally fabricated. A19-saponin increased the impact strength and hardness by 352.94 and 11.54 % with reduced water absorption by 82.85 %. Thus, A19-saponin as an additive improved quality of denture.
白色念珠菌(C. albicans)与MMA过敏反应的增加一直是义齿佩戴者关注的问题。研究了提取的a19皂苷复合PMMA义齿基托复合材料对白色念珠菌生长的抑制作用、机械电位和吸水电位。采用索氏提取法,用乙醇提取豚草茎粉中的a19皂苷。测定了豚草a19皂苷提取物的抑菌浓度。加入不同浓度的a19皂苷制备PMMA义齿基托,收率为23.2% %。测定了材料的力学性能和吸水性能。提取的a19皂苷的最小抑菌浓度为25%,最大抑菌敏感性为100% %。优选PMMA、MMA与提取的a19皂苷配比为30 g: 5 ml: 5 ml制作义齿。a19皂苷提高了冲击强度和硬度分别为352.94和11.54 %,降低了吸水率82.85 %。因此,a19 -皂苷作为添加剂可以改善义齿的质量。
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引用次数: 0
Effect of bonding conditions on mechanical performance of DP600 steels at different ambient temperatures 不同环境温度下粘接条件对DP600钢力学性能的影响
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-08-28 DOI: 10.1515/mt-2023-0020
Oktay Çavuşoğlu, Işıl Bolova, Hakan Berk Aydın, A. Kara, Berna Güzeldağ, Haluk Dinkçi
Abstract Adhesive bonding is used to join materials that are difficult to join with other joining methods. In this study, the effects of adhesive bonding curing conditions and different ambient conditions on the tensile shear loading process were investigated for dual-phase 600 steel materials that are widely preferred in the automotive industry. Steel sheets used in the automotive industry are exposed to environmental conditions at different temperatures. For this purpose, uniaxial tensile tests at different ambient temperatures were carried out to determine the mechanical properties of the adhesive bonded materials. The curing conditions affect adhesive mechanical properties. The lap shear strength decreased as the ambient temperature increased.
摘要:胶粘剂粘接是用于其它连接方法难以连接的材料的连接。在本研究中,研究了粘结固化条件和不同环境条件对汽车工业中广泛使用的双相600钢材料拉伸剪切加载过程的影响。汽车工业中使用的钢板暴露在不同温度的环境条件下。为此,进行了不同环境温度下的单轴拉伸试验,以确定胶粘剂粘合材料的力学性能。固化条件影响胶粘剂的力学性能。搭接抗剪强度随环境温度升高而降低。
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引用次数: 0
Bulge test technique and digital image correlation for the determination of the biaxial behavior of polymeric films 用膨胀试验技术和数字图像相关法测定聚合物薄膜的双轴性能
IF 2.5 4区 材料科学 Q2 MATERIALS SCIENCE, CHARACTERIZATION & TESTING Pub Date : 2023-08-24 DOI: 10.1515/mt-2023-0139
F. Kharrat, Rania Chaari, M. Khlif, L. Hilliou, J. Covas, M. Haboussi, C. Bradai
Abstract Materials can display multiple mechanical behaviors when they are biaxially stressed. In this research work, films obtained through the blowing process were investigated in order to compare the mechanical properties and behavior of the film under uniaxial and biaxial stress conditions. Bulge test coupled with a continuous full-field strain measurement was undertaken in order to characterize polymeric film in a biaxial stress state. As far as this study is concerned, a laboratory-made pneumatic bulge test machine was used for the determination of the biaxial behavior of a 50 μm thickness PLSF (modified PLA) film. 3D-digital image correlation (3D-DIC) technique was used in order to compute the strain field continuously during the test. Tensile test was equally performed on the film along its machine direction (MD) and transverse direction (TD). Strain field distribution in the film sample was analyzed and compared in both tests. The tensile test results displayed an isotropic behavior of the film in both directions. However, a difference in the strain at break was noticed because of the thickness instability along the TD. The comparison between uniaxial and biaxial properties resulted in almost the same properties with respect to the Young Modulus as well as the tensile strength.
摘要材料在双轴应力作用下可以表现出多种力学行为。在本研究中,研究了通过吹制工艺获得的薄膜,以比较薄膜在单轴和双轴应力条件下的力学性能和行为。为了表征聚合物薄膜在双轴应力状态下的特性,进行了膨胀试验和连续的全场应变测量。在本研究中,我们使用自制的充气充气试验机对50 μm厚度的PLSF(改性PLA)薄膜的双轴性能进行了测试。采用三维数字图像相关(3D-DIC)技术连续计算试验过程中的应变场。薄膜沿机械方向(MD)和横向(TD)进行拉伸试验。对两种试验中薄膜试样的应变场分布进行了分析和比较。拉伸试验结果显示薄膜在两个方向上都具有各向同性。然而,由于沿TD的厚度不稳定,注意到断裂时应变的差异。单轴和双轴性能的比较导致杨氏模量和抗拉强度几乎相同的性能。
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引用次数: 0
期刊
Materials Testing
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